CN1730570A - High temperature energy-saving corrosion-resisting paint , preparation and usage - Google Patents

High temperature energy-saving corrosion-resisting paint , preparation and usage Download PDF

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Publication number
CN1730570A
CN1730570A CN 200510088840 CN200510088840A CN1730570A CN 1730570 A CN1730570 A CN 1730570A CN 200510088840 CN200510088840 CN 200510088840 CN 200510088840 A CN200510088840 A CN 200510088840A CN 1730570 A CN1730570 A CN 1730570A
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China
Prior art keywords
high temperature
temperature energy
resisting paint
additive
filler
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Pending
Application number
CN 200510088840
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Chinese (zh)
Inventor
陈国军
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陈国军
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Priority to CN 200510088840 priority Critical patent/CN1730570A/en
Publication of CN1730570A publication Critical patent/CN1730570A/en
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Abstract

The invention discloses a high temperature energy conservation corrosion resistant coating material, which comprises filling material, addition agent and adhesive by the weight ratio of 1-5:1:1-10. The invention also discloses the process for preparing the coating material, which comprises the steps of mixing filling material powder with addition agent proportionally, grinding to 600 mesh in a wet grinder, finally stirring and mixing with adhesive.

Description

A kind of high temperature energy-saving corrosion-resisting paint and preparation thereof and using method
[technical field]
The present invention relates to a kind of high temperature energy-saving corrosion-resisting paint and preparation thereof and using method.
[background technology]
The antirust problem of metallic surface is a global difficult problem always.Traditional metal surface treatment technology is mainly based on plating, but along with the expansion of electroplating Application Areas, and also increasing by negative impacts such as the high energy consumption of its generation, high pollutions, Chinese government's explicit order stops to handle examining newly-built Electroplate Factory.Electroplate Factory investment is big in addition, and technical stability is poor, and converted products costs an arm and a leg, and the ordinary investor also can only hang back, and the metal surface treatment technology of developing a kind of advanced person substitutes the traditional electrical depositing process and is not only people's expectations and expects it also is trend of the times.
[summary of the invention]
The problem that the present invention need solve just is to overcome the defective of existing metal surface treating method, and a kind of high temperature energy-saving corrosion-resisting paint and preparation thereof and using method are provided.
For addressing the above problem, the present invention adopts following technical scheme:
High temperature energy-saving corrosion-resisting paint of the present invention, it is made up of filler, additive and binding agent, and the weight ratio between them is a filler: additive: binding agent equals 1-5: 1: 1-10.
Preferably, the weight ratio between filler of the present invention, additive and the binding agent is a filler: additive: binding agent equals 3: 1: 6.
Filler of the present invention is that blackening agent and raw material are formed by grog, and the weight ratio between them is a grog: raw material equal 1: 1-8.
Preferably, the weight ratio of grog of the present invention and raw material is a grog: raw material equal 1: 4.
The preparation method of grog of the present invention is: with 300 purpose MnO 2, Fe 2O 3, Co 2O 3, CuO is 1: 6: 2 by weight: 1 mixed is evenly carried out sintering reaction under 1250 ℃, sintering process is for being rapidly heated in 2 hours 600 ℃ earlier, and the back slowly was warmed up to 1200 ℃ in 2 hours, be incubated 2 hours then, used SiO again 2It is 325 purpose powder that the stone ball is pulverized;
Described raw material are by the Al more than 300 orders 2O 3, TiO 2, Cr 2O 3And SiO 2Uniform mixing is formed, and the ratio between them is 1: 1: 1: 1, and SiO wherein 2Amount comprises SiO in the grog preparation process 2The loss amount of stone ball.
Additive of the present invention is formed as the anti-sinking agent of thickening as toughner and carboxymethyl cellulose as water-resisting agent and dibutyl phthalate (DBP) as coupling agent and silica-gel powder as dispersion agent, vinyltriethoxysilane by sodium silicate is water-soluble, and their weight ratio is 5: 22.5: 20: 1: 1.5.
Binding agent of the present invention is made up of at third latex of the silicon more than 20%, silicon sol and water glass organosilane monomer content, and their weight ratio is 5: 1: 2.
The present invention provides a kind of method for preparing described high temperature energy-saving corrosion-resisting paint simultaneously, it with filler powder and additive be mixed in proportion the back behind grinding to 600 order under the wet wheeling machine with binding agent mix viscous liquid, its pH value is 9.
The present invention also provides a kind of using method of described high temperature energy-saving corrosion-resisting paint, and it comprises the steps:
The cleaning of A construction surface: remove rust staining and oil stain on the metal covering of constructing;
B spraying: directly spray described coating to construction surface;
C dried: with the metal covering airing of sprayed coating 4 hours;
D sintering: the metal covering of spraying is warmed to 200 ℃, is incubated 1 hour, and then is warming up to 600 ℃, be incubated 1 hour, and then be warming up to 1200 ℃, be incubated 1 hour.
When sintering described in the using method of the present invention also can be worked as construction surface and do not reached working order more than 600 ℃, can adopt temperature was that baking hot body more than 1200 ℃ is to the baking that is rapidly heated of the metal covering of spraying.
Coating of the present invention is the high temperature protection energy-saving coatings of metal, and coating of the present invention forms the protection ceramic membrane in the metal outside behind sintering, and ceramic membrane has high-temperature thermodynamics performance and the corrosion resistance nature close with metal.By strengthened coat and metallic matrix interface interaction, they are bonded together securely, and make the protection ceramic membrane behind the sintering have corrosion-resistant and function high radiant rate.
Coating antistripping mechanism of the present invention is as follows:
Coating of the present invention is made up of binding agent, additive and filler.Binding agent is that mineral binder bond and organic binder bond are composited under additive helps, and binding agent is partial to weakly alkaline, and hydroxyl is provided, and (OH), metallic matrix can provide positive ion, just in time forms chemical bond with hydroxyl and combines.Under coupling agent helps, realize the combination of covalent linkage, in coating, can provide Cr 3+, Si 4+, Co 3+, Al 3+Ion, these ionic ionic radius are respectively 0.064nm, 0.041nm, 0.063nm, 0.051nm, these metal ion radiuses and Fe base, interstitial void between the metallic molecule of Al base or Cu base is similar, they infilter the metallic matrix interface easily in the coating sintering, with the Fe base, the excessive layer of Al base or Cu base solid solution formation interface, so produce " pinning " effect with basal plane, the binding agent of coating soaks into metal and filler, maintain down at the space of O-Si-O key reticulated structure, form a densification and hard integral body, its comprehensive thermodynamic property and matrix are complementary, thereby are difficult for peeling off from basal plane.
Coating erosion resistance mechanism of the present invention is as follows:
The filler of coating of the present invention is so that net agent SiO 2With corrosion-resistant agglutinant Cr 2O 3, Al 2O 3And TiO 2Form, cause the net agent and form tridimensional network under the help of binding agent, no matter the O-Si-O key remains the unordered noncrystalline state of macroscopic view in low temperature still is hot environment, and structure interval is about 0.158nm, and under the help of binding agent, make gap smaller, corrosive ion O 2-, Cl -, S 4+Radius be followed successively by 0.18nm, 0.14nm and 0.053nm, O like this 2-, Cl -, S 4+Be difficult for infiltrate O-Si-O network and the corroding metal matrix Deng corrosive ion, thereby play corrosion resistant effect.Organic binder bond compensates the mineral binder bond network again in sintering process in addition, improves the density of coating, and under coupling agent helped, the wetted and organic composition dispersed combination of inorganic components after the sintering reaction, formed the film of hard and compact.
Coating Energy saving mechanism of the present invention is as follows:
Coating of the present invention is added a certain proportion of blackening agent in the filler formulation of coating, can bring up to the radiation coefficient of coating more than 0.9, and this blackening agent is by Fe 2O 3, MnO 2, Co 2O 3, CuO is mixed in proportion to pulverize behind the sintering and makes, this is because Fe 3+, Mn 4+, Co 3+, Cu 2+Ionic radius is approaching, substitute doping each other during high temperature sintering, thereby increased impurity level, improve the radiant ratio of infrared band.Sintered product is Fe 3O 4, CoFe 2O 4, CuFeMnO 4Etc. the radiant ratio height corrosive sinter of the also low temperature resistant soda acid salt of high temperature oxidation resisting corrosion again, thereby improve heat energy utilization, play energy-saving effect.
The present invention is energy-conservation about 10%, prolongs the metallic matrix life-span more than 1 times.
The advantage of coating of the present invention is:
1, heatproof degree height: can reach more than 1200 ℃, satisfy large-scale Thermal Equipment substantially, as the job requirement of boiler superheater, economizer, condenser, heat exchanger and petroleum cracking stove.
2, construction requirement is low: during construction, be not subjected to the restriction of space, environment and condition, and simple as exterior wall latex paint in the spary.
3, cost is low: can make production promote enterprise has enough profit margins.
4, produce simply: no complex process, raw material sources are abundant, non-environmental-pollution.
The coating technology index is as follows behind the metallizing of the present invention surface:
1, coating in infrared band average radiation rate greater than 0.9.
2, the coating working temperature is less than 1200 ℃.
3, coating can be born 800 ℃ of high temperature oxidation and corrosions and the corruption of low temperature soda acid salt atmosphere for a long time
Erosion, work-ing life is more than 1 year.
4, coating can be born 800 ℃ to room temperature air cooling, thermal shocking more than 5 times repeatedly.
5, coating is applicable to various metallic matrixes.
6, coating can be born the mechanical shock of concrete floor face under 1 meter high freely falling body and do not come off and lacerated wound
7, the color tunable of coating.
[embodiment]
The preparation of embodiment 1 grog
With 300 purpose MnO 2, Fe 2O 3, Co 2O 3, CuO is 1: 6: 2 by weight: 1 mixed is evenly carried out sintering reaction under 1250 ℃, sintering process is for being rapidly heated in 2 hours 600 ℃ earlier, and the back slowly was warmed up to 1200 ℃ in 2 hours, be incubated 2 hours then, used SiO again 2It is 325 purpose powder that the stone ball is pulverized.
The preparation of embodiment 2 coating
With filler powder and additive be mixed in proportion the back behind grinding to 600 order under the wet wheeling machine with binding agent mix viscous liquid, concrete proportioning raw materials such as following table:
Title material Specification Weight
Filler Grog Embodiment 1 preparation; 325 orders 6kg
Raw material Al 2O 3 Technical grade, 400 orders 6kg
TiO 2 Technical grade, 400 orders 6kg
Cr 2O 3 Technical grade, 400 orders 6kg
SiO 2 Technical grade, 400 orders 6kg
Additive Sodium silicate Technical grade 1kg
Vinyl 3 Ethoxysilanes 4.5kg
Silica-gel powder 4kg
Dibutyl phthalate (DBP) 0.2kg
Carboxymethyl cellulose 0.3kg
Binding agent Silicon third latex The monomer silicon content is more than 20%, admittedly contain thing 45% 10kg
Silicon sol Technical grade 2kg
Water glass Technical grade 4kg
Water 34kg
The spraying of embodiment 3 coating
The cleaning of A construction surface: remove rust staining and oil stain on the metal covering of constructing;
B spraying: directly spray described coating to construction surface;
C dried: with the metal covering airing of sprayed coating 4 hours;
D sintering: the metal covering of spraying is warmed to 200 ℃, is incubated 1 hour, and then is warming up to 600 ℃, be incubated 1 hour, and then be warming up to 1200 ℃, be incubated 1 hour.
The spraying of embodiment 4 coating
When construction surface did not reach working order more than 600 ℃, can adopt temperature was that baking hot body more than 1200 ℃ is to the baking that is rapidly heated of the metal covering of spraying.

Claims (10)

1, a kind of high temperature energy-saving corrosion-resisting paint, it is made up of filler, additive and binding agent, and the weight ratio between them is a filler: additive: binding agent equals 1-5: 1: 1-10.
2, high temperature energy-saving corrosion-resisting paint as claimed in claim 1 is characterized in that: the weight ratio between described filler, additive and the binding agent is a filler: additive: binding agent equals 3: 1: 6.
3, high temperature energy-saving corrosion-resisting paint as claimed in claim 2 is characterized in that: described filler is that blackening agent and raw material are formed by grog, and the weight ratio between them is a grog: raw material equal 1: 1-8.
4, high temperature energy-saving corrosion-resisting paint as claimed in claim 3 is characterized in that: the weight ratio of described grog and raw material is a grog: raw material equal 1: 4.
5, high temperature energy-saving corrosion-resisting paint as claimed in claim 4 is characterized in that: the preparation method of described grog is: with 300 purpose MnO 2, Fe 2O 3, Co 2O 3, CuO is 1: 6: 2 by weight: 1 mixed is evenly carried out sintering reaction under 1250 ℃, sintering process is for being rapidly heated in 2 hours 600 ℃ earlier, and the back slowly was warmed up to 1200 ℃ in 2 hours, be incubated 2 hours then, used SiO again 2It is 325 purpose powder that the stone ball is pulverized;
Described raw material are by the Al more than 300 orders 2O 3, TiO 2, Cr 2O 3And SiO 2Uniform mixing is formed, and the ratio between them is 1: 1: 1: 1, and SiO wherein 2Amount comprises SiO in the grog preparation process 2The loss amount of stone ball.
6, high temperature energy-saving corrosion-resisting paint as claimed in claim 5, it is characterized in that: described additive is formed as the anti-sinking agent of thickening as toughner and carboxymethyl cellulose as water-resisting agent and dibutyl phthalate (DBP) as coupling agent and silica-gel powder as dispersion agent, vinyltriethoxysilane by sodium silicate is water-soluble, and their weight ratio is 5: 22.5: 20: 1: 1.5.
7, high temperature energy-saving corrosion-resisting paint as claimed in claim 6 is characterized in that: described binding agent is made up of at third latex of the silicon more than 20%, silicon sol and water glass organosilane monomer content, and their weight ratio is 5: 1: 2.
8, a kind of preparation is as the method for arbitrary described high temperature energy-saving corrosion-resisting paint of claim 1-7, it is characterized in that: it with filler powder and additive be mixed in proportion the back behind grinding to 600 order under the wet wheeling machine with binding agent mix viscous liquid, its pH value is 9.
9, a kind of using method of the arbitrary described high temperature energy-saving corrosion-resisting paint as claim 1-7 is characterized in that it comprises the steps:
The cleaning of A construction surface: remove rust staining and oil stain on the metal covering of constructing;
B spraying: directly spray described coating to construction surface;
C dried: with the metal covering airing of sprayed coating 4 hours;
D sintering: the metal covering of spraying is warmed to 200 ℃, is incubated 1 hour, and then is warming up to 600 ℃, be incubated 1 hour, and then be warming up to 1200 ℃, be incubated 1 hour.
10, using method as claimed in claim 9 is characterized in that: describedly be sintered to that to adopt temperature be that baking hot body more than 1200 ℃ is to the baking that is rapidly heated of the metal covering of spraying.
CN 200510088840 2005-08-02 2005-08-02 High temperature energy-saving corrosion-resisting paint , preparation and usage Pending CN1730570A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
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Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 200510088840 CN1730570A (en) 2005-08-02 2005-08-02 High temperature energy-saving corrosion-resisting paint , preparation and usage

Publications (1)

Publication Number Publication Date
CN1730570A true CN1730570A (en) 2006-02-08

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Country Status (1)

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