CN1673400A - Vacuum double-stirring device for producing carborundum particle reinforced aluminium-based composite material - Google Patents

Vacuum double-stirring device for producing carborundum particle reinforced aluminium-based composite material Download PDF

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Publication number
CN1673400A
CN1673400A CNA2005100111607A CN200510011160A CN1673400A CN 1673400 A CN1673400 A CN 1673400A CN A2005100111607 A CNA2005100111607 A CN A2005100111607A CN 200510011160 A CN200510011160 A CN 200510011160A CN 1673400 A CN1673400 A CN 1673400A
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agitator
interior
shaft
stirring
bearing
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CNA2005100111607A
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CN1327015C (en
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韩建民
沙镇嵩
李卫京
陈怀君
李荣华
崔世海
徐向阳
刘元富
王金华
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Beijing Jiaotong University
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Beijing Jiaotong University
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/10Greenhouse gas [GHG] capture, material saving, heat recovery or other energy efficient measures, e.g. motor control, characterised by manufacturing processes, e.g. for rolling metal or metal working

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  • Mixers Of The Rotary Stirring Type (AREA)

Abstract

The vacuum double-stirrer apparatus for preparing SiC grain reinforced aluminum base material includes inner stirrer, outer stirrer, shaft coupler, frequency varying motor, frequency variator, bearing, bearing seat, bearing housing, observing hole, supporting frame, supporting table and sealing ring. The outer stirrer is located on the supporting table and connected to the frequency varying motor via triangular belt; the inner stirrer is located with the hollow shaft and supporting centripedal ball bearing and connected to the frequency varying motor via the shaft coupler; and the frequency varying motor driven with the frequency variator controls the rotation direction and speed of both the inner stirrer and the outer stirrer. The present invention performs the complex inner and outer stirring, and can raise the grain mixing efficiency, the grain dispersing homogeneity and the deairing capacity and lower the reinforcing grain loss and fault inside the material.

Description

The vacuum double-stirring device of preparation enhancing aluminum-base composite material by silicon carbide particles
Technical field
The present invention relates to a kind of whipping appts, in especially a kind of preparation enhancing aluminum-base composite material by silicon carbide particles process, under vacuum environment, Composite Melt is carried out the inside and outside pair of whipping device that composite machine stirs.
Background technology
In the preparation method of numerous silicon carbide reinforced aluminum matrix composites, stirring casting method has that technology is simple, equipment less investment, techno-economic effect are good, be easy to the characteristics that realize that industrialization is produced.So-called mechanical stirring casting, be to add silicon-carbide particle in sensing liquid state or the melt that is in the two-phase region, by the mixture of mechanical stirring molten metal and silicon carbide, silicon-carbide particle is entered and be evenly distributed in the molten metal, be cast into the matrix material ingot casting then.Document " the granule enhancement type aluminum matrix composite stirs process of smelting research " and " SiC pThe preparation method of/Al matrix material and research direction " in reported that liquid stirring casting method prepares the equipment of enhancing aluminum-base composite material by silicon carbide particles, its whipping appts all adopts stepless speed-change motor to drive the agitator rotation and forms eddy current, the negative pressure that eddy current produces is brought particle in the melt into, and by the high speed rotating of agitator blades the particles dispersed of reuniting is come; In the melt of two-phase region, the blade of rotation also can be smashed the solid-state dendrite of the part in the matrix alloy liquation, strengthens the chance of enhanced granule and interdendritic friction, collision, thus acquisition even particle distribution, matrix material that crystal grain is tiny.There are 3 limitation in the whipping appts of this form.At first, agitator blades is parallel vertical row's formula of vertical rotation axis or propeller type, the blade of parallel vertical row's form only produces stronger radially whipping force, the negative pressure that the power that particle enters melt relies on eddy current to produce fully, make particle enter melt smoothly, must improve the rotating speed of agitator, it is too big that too high stirring velocity can cause the silicon-carbide particle on the liquid level to fly upward, easily taken away by vacuum system, cause in the matrix material silicon-carbide particle content inaccurate, and stirring velocity is too high, and melt splashes, wraps up in gas easily, influences the density of matrix material; Though the propeller type blade has axial whipping force, but whipping force a little less than, if the mixing effect that will obtain, need higher stirring velocity, too high stirring velocity can make bath surface produce than great fluctuation process equally and roll, the scum silica frost of bath surface, oxide compound are involved in melt easily, form defectives such as slag inclusion, pore.Secondly, whipping appts adopts the unidirectional rotation mode of single shaft, and enhanced granule is under eddy effect, and part enters melt, also has the part enhanced granule under action of centrifugal force, be deposited in gradually on the sidewall of crucible, can't enter melt, greatly reduce the precise control of carborundum content in the matrix material, and the unidirectional alr mode of single shaft of employing high speed rotating, owing to force to stir and inertia effect, make the enhanced granule group of reuniting in the melt little with the speed of rotation difference of melt, the efficient of crushed particles group is low.At last, because enhancing aluminum-base composite material by silicon carbide particles viscosity is big, the gas of gas that whipping process is involved in and silicon-carbide particle surface attachment is formed bubble in melt, particularly the bubble of melt bottom is subjected to the eddy current suction function to be difficult to rising, emersion bath surface, causes existing in the matrix material more pore.
Summary of the invention
The objective of the invention is to overcome the defective of above-mentioned prior art, the inside and outside double-stirring device of preparation enhancing aluminum-base composite material by silicon carbide particles under a kind of vacuum condition is provided.
Technical scheme of the present invention:
The double-stirring device for preparing enhancing aluminum-base composite material by silicon carbide particles under vacuum condition provided by the invention comprises: interior agitator, external agitator, shaft coupling, variable-frequency motor, frequency transformer, bearing, bearing support, vision slit, bracing frame, brace table, sealing-ring.Brace table is provided with an oblique through hole, and the main body of vision slit is passed oblique through hole, and is welded on the brace table; The middle part of external agitator is installed on the brace table by taper roller bearing and bearing support, the upper end of external agitator is by taper roller bearing and the bearing housing location that is fixed on the bracing frame, and the belt pulley on the external agitator tubular shaft connects by the belt pulley of wire belt and variable-frequency motor; The interior stirring shaft of interior agitator passes the cavity of external agitator tubular shaft, support by the radial ball bearing on the step that is installed in the external agitator tubular shaft, and locate by the radial ball bearing in the bearing housing that is fixed on the bracing frame, interior stirring shaft and interior stirring shaft coupling adopt key joint, the shaft coupling bolted-on connection of interior stirring shaft coupling and variable-frequency motor; Two variable-frequency motors are driven by separately frequency transformer respectively, and turning to and rotating speed of control external agitator and interior agitator stirred by the agitator arm of external agitator and the screw-blade and the stirring wing of interior agitator.
The present invention's beneficial effect compared to existing technology:
1. the screw-blade of interior agitator arm and stirring wing provide axially and stirring action power radially simultaneously.Under vacuum condition, the high temperature slow forward of interior agitator arm stirs, and has guaranteed the stationarity of bath surface, and produces vortex formation negative pressure in melt heart portion, and silicon-carbide particle is involved in the melt; In the high-speed forward of two-phase region stirred, the solution of having avoided violent stirring to cause flew upward with gas and is involved in, and had intensive broken silicon-carbide particle group and made enhanced granule homodisperse effect in melt; The low-speed reverse of interior agitator stirs and can strengthen compound dynamics with the bottom melt Conveying to bath surface, can take out of melting intravital bubble simultaneously, and the reverse stirring of interior agitator also can reduce the static pressure that melt is overflowed to bubble in addition.
2. the agitator arm forward stirring at low speed scraped of external agitator is repelled by eddy current and is deposited in enhanced granule on the sidewall of crucible, it is pushed the eddy current center, reduced the loss of enhanced granule, in addition, the reverse stirring at low speed of the agitator arm of external agitator also can broken float over the bubble and the crust layer of bath surface, at a slow speed under the cooperation of high-temperature stirring and vacuum condition in the other direction, make the bubble effusion melt in the melt at interior agitator arm, reduce the gas in the matrix material.
3. external agitator turned round simultaneously in this whipping appts can make, realization in the same way, oppositely speed change is rotated, under suitable inside and outside stirring velocity, direction and whipping temp cooperate, strengthened being involved in and homodisperse efficient and effect of enhanced granule greatly, and melt degasifying effect, in addition because high temperature adopts down stirring at low speed, reduced high-temperature fusant to the washing away and corrode of agitator, reduced the foreign matter content of matrix material.
4. this device good airproof performance can carry out liquid state and stir compoundly in vacuum environment or under the protection of inert gas, reduce the oxidation chance, is beneficial to and obtains good comprehensive mechanical performance.
Description of drawings
Fig. 1 vacuum double-stirring device structural representation.
Fig. 2 external agitator structural representation.
Fig. 3 external agitator structure vertical view.
The outer stirring shaft structural representation of Fig. 4.
Agitator structure synoptic diagram in Fig. 5.
Stirring shaft structural representation in Fig. 6.
Fig. 7 vision slit structural representation.
Among the figure: mixing component in 1,2 crucibles, 3 bodies of heater, 4 outer mixing components, stirring shaft in 5,6 radial ball bearings, 7 body of heater cover plates, 8 brace tables, 9 lock plungers, 10 bearing supports, 11 belt pulleys, 12 tubular shafts, 13 variable-frequency motors, 14 end caps, 15 bracing frames, 16 sealing sockets, 17 frequency transformers, 18 variable-frequency motors, 19 frequency transformers, 20 motor couplers, stir shaft coupling in 21,22 end caps, 23 vision slits, 24 spring sealed circles, 25 radial ball bearings, 26 bearing housings, 27 taper roller bearings, 28 rubber seal, 29 rubber seal, 30 asbestos rings, 31 wire belts, 32 end caps, 33 taper roller bearings, 34 spring sealed circles, 35 rectangular slots, 36 outer agitator arm hanger brackets, 37 tapped through holes, 38 outer agitator arms, 39 threaded holes, 40 steps, 41 sealing grooves, 42 threaded holes, 43 bearing supports, 44 belt pulleys, 45 shaft shoulders, agitator arm in 46,47 screw-blades, 48 stirring wings, 49 threaded holes, 50 shaft shoulders, 51 shaft shoulders, 52 keyways, 53 vision slit main bodys, 54 rubber cradles, 55 sheet glass
Embodiment
With the accompanying drawing is embodiment, and the invention will be further described:
The vacuum double-stirring device of preparation enhancing aluminum-base composite material by silicon carbide particles, it comprises agitator, shaft coupling, variable-frequency motor, frequency transformer, bearing, bearing support, vision slit, bracing frame, brace table, sealing-ring, the shaft coupling of agitator and variable-frequency motor connects, and drives variable-frequency motor by frequency transformer and drives the agitator rotation.
Described agitator comprises external agitator and interior agitator.
The middle part of external agitator is installed on the brace table 8 by taper roller bearing 33 and bearing support 10, the upper end of external agitator is by taper roller bearing 27 and bearing housing 26 location that are fixed on the bracing frame 15, and the belt pulley 44 on the external agitator tubular shaft 12 connects by the belt pulley 11 of wire belt 31 with variable-frequency motor 13.
The interior stirring shaft 5 of interior agitator passes the cavity of external agitator tubular shaft 12, by 6 supportings of the radial ball bearing on the step 40 that is installed in the external agitator tubular shaft 12, and by 25 location of the radial ball bearing in the bearing housing 26 that is fixed on the bracing frame 15, interior stirring shaft 5 and interior stirring shaft coupling 21 key connecting, interior stirring shaft coupling 21 is used bolted-on connection with the motor coupler 20 of variable-frequency motor 18.
Variable- frequency motor 13,18 is fixed by bolts on the bracing frame 15, and bracing frame 15 is fixed by bolts on the brace table 8.Variable- frequency motor 13,18 is driven by frequency transformer 17,19 respectively, and turning to and rotating speed of control external agitator and interior agitator stirred by the outer agitator arm 38 of external agitator and the stirring wing 48 and the screw-blade 47 of interior agitator.
External agitator is made up of outer mixing component 4 and tubular shaft 12, and tubular shaft 12 adopts screw to connect with outer mixing component 4, and passes the taper roller bearing 33 in the bearing support 10, connects with the belt pulley 11 of wire belt 31 with variable-frequency motor 13.Spring sealed circle 34 in the bearing support 10 is finished between tubular shaft 12 and the brace table 8, and the sealing between tubular shaft 12 and the bearing support 10.26 of the bearing support 43 of tubular shaft 12 upper ends and bearing housings connect with taper roller bearing 27, and be fixing with end cap 14.Taper roller bearing 33 usefulness end caps 32 are pressed in the bearing support 10, and 10 of end cap 32 and bearing supports adopt screw to connect.
Interior agitator is made up of interior mixing component 1 and interior stirring shaft 5, interior mixing component 1 is used spiral marking connection with interior stirring shaft 5, rubber seal 28 and spring sealed circle 24 are finished between interior stirring shaft 5 and the tubular shaft 12, and the sealing between interior stirring shaft 5 and the sealing socket 16, end cap 22 is used for holddown spring sealing-ring 24.
Vision slit 23 is made up of vision slit main body 53, rubber cradle 54 and sheet glass 55, and vision slit 23 is welded on the oblique through hole on the brace table 8, and the angle of inclination should guarantee to observe the melt liquid level in the crucible 2.Vision slit 23 is used for adding silicon-carbide particle in crucible and whipping process is observed the bath surface state.
Outer mixing component 4 is made up of the outer agitator arm 38 of outer agitator arm hanger bracket 36 and two " Z " shapes, tapped through hole 37 is arranged at outer agitator arm hanger bracket 36 bottoms, top is provided with slot 35, outer agitator arm 38 1 ends are screw thread, be fixed on two nuts on the slot 35 of outer agitator arm hanger bracket 36, outer mixing component 4 is by the tapped through hole 37 of outer agitator arm hanger bracket 36 bottoms, and is fixing with screw and tubular shaft 12.
The inner chamber of tubular shaft 12 is provided with step 40 and sealing groove 41, and its lower end is provided with threaded hole 39, and the middle part is provided with vee-pulley 44, and top is bearing support 43, and the bearing support end face is provided with threaded hole 42.
Interior mixing component 1 is welded by interior agitator arm 46, screw-blade 47, stirring wing 48, interior agitator arm 46 1 ends are screw thread, cooperate with the threaded hole 49 of interior stirring shaft 5 bottoms, stirring wing 48 is vertical with interior agitator arm 46, and be welded on screw-blade 47 edges, along on the screw, per 270 spend one at angles from screw-blade 47 bottoms.
Interior stirring shaft 5 one ends are provided with threaded hole 49, and the other end is provided with keyway 52, with interior stirring shaft coupling 21 key joints, the rotating shaft middle part is provided with two place's shaft shoulders 50,51, the shaft shoulder 50 is pressed on the radial ball bearing 6, and with stirring shaft 5 in supporting, the shaft shoulder 51 cooperates with rubber seal 28 and plays sealing function.
During the preparation enhancing aluminum-base composite material by silicon carbide particles, aluminium ingot is put into crucible 2, it is melted fully, after the removal of impurities of skimming, vacuum double-stirring device is pressed on the body of heater cover plate 7, the stirring wing 48 of mixing component 1 enters in the melt fully in making, regulate the nut on the outer agitator arm 38, make outer agitator arm 38 enter the melt suitable length, and the sidewall of crucible of trying one's best, 7 of brace table 8 and body of heater cover plates are provided with heat insulation asbestos ring 30 and rubber seal 29, and by lock plunger 9 brace table 8 and body of heater 3 are locked.Take off the sheet glass 55 in the vision slit 23, after by vision slit main body 53 silicon-carbide particle being joined bath surface, sheet glass 55 is pressed on the rubber cradle 54, starting vacuum system vacuumizes the crucible inner chamber, handle frequency transformer 17,19 drive variable-frequency motor 13, the rotating speed of external agitator carries out compound stirring with turning to melt in 18 controls, inside and outside agitator arm forward is stirred at a slow speed, keep bath surface more stably, silicon-carbide particle is brought melt into by swirling action power, and the silicon-carbide particle that constantly will be deposited on the sidewall of crucible by external agitator pushes the eddy current center, make silicon-carbide particle be involved in melt very soon, finish to melt adding silicon carbide process; Stop outer the stirring subsequently, cooling makes melt be in the two-phase region, carries out high speed and stirs in powerful, makes to have simultaneously in the melt axially and whipping force radially, expeditiously the silicon-carbide particle group fragmentation of reuniting also is distributed in the melt equably, finishes the blending process of silicon carbide and melt; Heat up at last and carry out opposite direction and stir at a slow speed, constantly with the melt Conveying of bottom to bath surface, stir bath surface crust layer brokenly by positive dirction is outer at a slow speed, make foaming in the melt melt of under vacuum action, overflowing, finish degasification process.When material is compound finish after, shed vacuum, open lock plunger 9, vacuum double-stirring device is shifted out, can be with the matrix material casting ingot-forming.

Claims (7)

1. vacuum double-stirring device for preparing enhancing aluminum-base composite material by silicon carbide particles, it comprises agitator, shaft coupling, variable-frequency motor, frequency transformer, bearing, bearing support, vision slit, bracing frame, brace table, sealing-ring, the shaft coupling of agitator and variable-frequency motor connects, drive variable-frequency motor by frequency transformer and drive the agitator rotation, it is characterized in that:
Described agitator comprises external agitator and interior agitator;
The middle part of external agitator is installed on the brace table (8) by taper roller bearing (33) and bearing support (10), the upper end of external agitator is by taper roller bearing (27) and be fixed on bearing housing (26) location on the bracing frame (15), and the belt pulley (44) on the external agitator tubular shaft (12) connects by the belt pulley (11) of wire belt (31) with variable-frequency motor (13);
The interior stirring shaft (5) of interior agitator passes the cavity of external agitator tubular shaft (12), by the supporting of the radial ball bearing (6) on the step (40) that is installed in the external agitator tubular shaft (12), and by the location of the radial ball bearing (25) in the bearing housing (26) that is fixed on the bracing frame (15), interior stirring shaft (5) and interior stirring shaft coupling (21) key connecting;
Variable-frequency motor (13,18) is driven by frequency transformer (17,19) respectively, and turning to and rotating speed of control external agitator and interior agitator stirred by the outer agitator arm (38) of external agitator and the stirring wing (48) and the screw-blade (47) of interior agitator.
2. the vacuum double-stirring device of preparation enhancing aluminum-base composite material by silicon carbide particles according to claim 1, it is characterized in that: external agitator is made up of outer mixing component (4) and tubular shaft (12), outer mixing component (4) connects with screw with tubular shaft (12), spring sealed circle (34) in the bearing support (10) is finished between tubular shaft (12) and the brace table (8), and the sealing between tubular shaft (12) and the bearing support (10).
Interior agitator is made up of interior mixing component (1) and interior stirring shaft (5), interior mixing component (1) is used spiral marking connection with interior stirring shaft (5), rubber seal (28) and spring sealed circle (24) are finished between interior stirring shaft (5) and the tubular shaft (12), and the sealing between interior stirring shaft (5) and the sealing socket (16).
3. the vacuum double-stirring device of preparation enhancing aluminum-base composite material by silicon carbide particles according to claim 1, it is characterized in that: vision slit (23) is made up of vision slit main body (53), rubber cradle (54) and sheet glass (55), and the angle of inclination that vision slit (23) is welded on the brace table (8) should guarantee to observe the interior melt liquid level of crucible (2).
4. the vacuum double-stirring device of preparation enhancing aluminum-base composite material by silicon carbide particles according to claim 2, it is characterized in that: outer mixing component (4) is made up of the outer agitator arm (38) of outer agitator arm hanger bracket (36) and two " Z " shapes, tapped through hole (37) is arranged at outer agitator arm hanger bracket (36) bottom, top is provided with slot (35), outer agitator arm (38) one ends are screw thread, be fixed on two nuts on the slot (35) of outer agitator arm hanger bracket (36), outer mixing component (4) is by the tapped through hole (37) of outer agitator arm hanger bracket (36) bottom, and is fixing with screw and tubular shaft (12).
5. the vacuum double-stirring device of preparation enhancing aluminum-base composite material by silicon carbide particles according to claim 2, it is characterized in that: the inner chamber of tubular shaft (12) is provided with step (40) and sealing groove (41), its lower end is provided with threaded hole (39), the middle part is provided with vee-pulley (44), top is bearing support (43), and the bearing support end face is provided with threaded hole (42).
6. the vacuum double-stirring device of preparation enhancing aluminum-base composite material by silicon carbide particles according to claim 2, it is characterized in that: interior mixing component (1) is welded by interior agitator arm (46), screw-blade (47), stirring wing (48), interior agitator arm (46) one ends are screw thread, cooperate with the threaded hole (49) of interior stirring shaft (5) bottom, stirring wing (48) is vertical with interior agitator arm (46), and be welded on screw-blade (47) edge, along on the screw, per 270 spend one at angles from screw-blade (47) bottom.
7. the vacuum double-stirring device of preparation enhancing aluminum-base composite material by silicon carbide particles according to claim 2, it is characterized in that: interior stirring shaft (5) one ends are provided with threaded hole (49), the other end is provided with keyway (52), with interior stirring shaft coupling (21) key joint, the rotating shaft middle part is provided with two place's shaft shoulders (50,51), the shaft shoulder (50) is pressed on the radial ball bearing (6), and supporting interior stirring shaft (5), the shaft shoulder (51) cooperates with rubber seal (28) and plays sealing function.
CNB2005100111607A 2005-01-13 2005-01-13 Vacuum double-stirring device for producing carborundum particle reinforced aluminium-based composite material Expired - Fee Related CN1327015C (en)

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CN102925723A (en) * 2012-10-24 2013-02-13 河南理工大学 Method for preparing particle-reinforced aluminum-based composite
CN103862005A (en) * 2014-04-08 2014-06-18 哈尔滨工业大学 Device for manufacturing metal matrix composite or semisolid slurry and using method thereof
CN104653151A (en) * 2015-02-16 2015-05-27 中国石油集团渤海钻探工程有限公司 Gas drilling solid injection machine
CN105833785A (en) * 2015-03-20 2016-08-10 共慧冶金设备科技(苏州)有限公司 Spiral stirring device and application equipment thereof
CN106756191A (en) * 2016-11-28 2017-05-31 北京有色金属研究总院 It is a kind of to rotate the device and method that method of impregnation prepares particle enhanced aluminum-based composite material
CN108093792A (en) * 2018-01-15 2018-06-01 吉林大学 Solid fertilizer compounding in real time and conveying combination device

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CN102925723A (en) * 2012-10-24 2013-02-13 河南理工大学 Method for preparing particle-reinforced aluminum-based composite
CN103862005A (en) * 2014-04-08 2014-06-18 哈尔滨工业大学 Device for manufacturing metal matrix composite or semisolid slurry and using method thereof
CN103862005B (en) * 2014-04-08 2016-05-04 哈尔滨工业大学 A kind of device and using method thereof of preparing metal-base composites or semi solid slurry
CN104653151A (en) * 2015-02-16 2015-05-27 中国石油集团渤海钻探工程有限公司 Gas drilling solid injection machine
CN105833785A (en) * 2015-03-20 2016-08-10 共慧冶金设备科技(苏州)有限公司 Spiral stirring device and application equipment thereof
CN106756191A (en) * 2016-11-28 2017-05-31 北京有色金属研究总院 It is a kind of to rotate the device and method that method of impregnation prepares particle enhanced aluminum-based composite material
CN106756191B (en) * 2016-11-28 2018-07-17 北京有色金属研究总院 A kind of rotation method of impregnation prepares the device and method of particle enhanced aluminum-based composite material
CN108093792A (en) * 2018-01-15 2018-06-01 吉林大学 Solid fertilizer compounding in real time and conveying combination device

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