CN1615698A - Compound antiseptic agent - Google Patents
Compound antiseptic agent Download PDFInfo
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- CN1615698A CN1615698A CN 200310113356 CN200310113356A CN1615698A CN 1615698 A CN1615698 A CN 1615698A CN 200310113356 CN200310113356 CN 200310113356 CN 200310113356 A CN200310113356 A CN 200310113356A CN 1615698 A CN1615698 A CN 1615698A
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- zinc oxide
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Abstract
The compound antiseptic consists of silver carbonate 48-76-50 wt%, zinc oxide 38-75-41.32 wt%, and silicon dioxide 9.92-11.25 wt%. The preparation process includes mixing silver carbonate, zinc oxide and silicon dioxide in certain proportion inside a ball mill, calcining the mixture in electric furnace, grinding in vibrating and stirring grinder into fine powder, drying in intermittent dryer, making powder in screen powder making machine and light-proof packing. The product has stable antiseptic effect, wide application range and no environmental pollution.
Description
Technical field:
The present invention relates to a kind of antibacterial agent, particularly a kind of complex antimicrobials.
Background technology:
Along with the raising of people's living standard and the enhancing of health care consciousness, people are to work and family assanation pay attention to day by day, reduce the infringement of bacterium that surrounding environment grows to human body as far as possible, enter the nineties later stage, countries in the world begin actively to develop antibacterial agent and antibacterial product, make anti-bacteria ceramic, antibiotic cloth, antibiotic paint, articles for daily use such as antibiotic tableware are arisen at the historic moment, and relate to papermaking, household electrical appliances, automobile, paint, coating, pottery, all conglomeraties such as articles for daily use, but the prescription of existing various antibacterial agents and preparation method, the processing technology complexity, investment is big, the production cost height, accommodation is little, easily cause environmental pollution, and antibacterial effect is all undesirable.
Summary of the invention:
Purpose of the present invention just is to overcome weak point of the prior art, provides a kind of prescription and preparation method, processing technology simple, invests for a short time, and production cost is low, wide accommodation, non-environmental-pollution, and the desirable complex antimicrobials of antibacterial effect.
The object of the present invention is achieved like this, and it is made up of following raw materials by weight percent, silver carbonate 48.76-50, zinc oxide 38.75-41.32, silica 9.92-11.25.Its preparation method comprises following processing step: with electronic scale with silver carbonate, zinc oxide, silica is combined together by weight percentage, the material for preparing is put into the ball mill homogenizing to be mixed, the mixed material of homogenizing sent in the high temperature frit electric furnace calcine, calcining heat is controlled at 1000 ℃-1200 ℃, time was controlled at 10 hours-14 hours, with the calcining after material send into vibrations mixer grinder in processing levigate, granular material after process is levigate enters and carries out bake drying in the periodic dryer, make its moisture below 3%, dried material is sent into powder process in the screen mesh type flour mill again, granularity is controlled at 5um-45um, the granular material lucifuge of preparation is packed get final product.
The purpose of this utility model can realize that also its finished product oxide content is by following technical measures: silver oxide 42%-46%, zinc oxide 36%-44%, silica 8%-10%.
Compared to existing technology, the present invention has prescription and preparation method, processing technology is simple, rationally advanced, and material is easily purchased, and invests for a short time, and production cost is low, wide accommodation, non-environmental-pollution, advantages such as antibacterial bacteriostatic effect stability, long action time.
Description of drawings:
Accompanying drawing is a process chart of the present invention
Embodiment:
Below in conjunction with drawings and Examples in detail the present invention is described in detail, it is made up of following raw materials by weight percent, silver carbonate 48.76-50, zinc oxide 38.75-41.32, silica 9.92-11.25.Its preparation method comprises following processing step: with electronic scale with silver carbonate, zinc oxide, silica is combined together by weight percentage, the material for preparing is put into the ball mill homogenizing to be mixed, the mixed material of homogenizing sent in the high temperature frit electric furnace calcine, calcining heat is controlled at 1000 ℃-1200 ℃, time was controlled at 10 hours-14 hours, with the calcining after material send into vibrations mixer grinder in processing levigate, granular material after process is levigate enters and carries out bake drying in the periodic dryer, make its moisture below 3%, dried material is sent into powder process in the screen mesh type flour mill again, granularity is controlled at 5um-45um, the granular material lucifuge of preparation is packed get final product.Its finished product oxide content is: silver oxide 42%-46%, zinc oxide 36%-44%, silica 8%-10%.
Be the specific embodiment of 1000g of the present invention below: (table one)
Table one:
| Component | Embodiment 1 | Embodiment 2 | Embodiment 3 | |||
| Percentage by weight % | Weight g | Percentage by weight % | Weight g | Percentage by weight % | Weight g | |
| Silver carbonate | 50 | ?500 | ?50 | 500 | 48.76 | ?487.6 |
| Zinc oxide | 38.75 | ?387.5 | ?40 | 400 | 41.32 | ?413.2 |
| Silica | 11.25 | ?112.5 | ?10 | 100 | 9.92 | ?99.2 |
| Add up to | 100 | ?1000 | ?100 | 1000 | 100 | ?1000 |
With each component in the table one with electronic scale with silver carbonate, zinc oxide, silica is combined together by weight percentage, then the material for preparing being put into the ball mill homogenizing mixes, the mixed material of homogenizing sent in the high temperature frit electric furnace calcine, calcining heat is controlled at 1100 ℃, time was controlled at 12 hours, take out then, cooling, with the calcining after material send into vibrations mixer grinder in processing levigate, granular material after process is levigate enters and carries out bake drying in the periodic dryer, make its moisture below 3%, dried material is sent into powder process in the screen mesh type flour mill again, granularity is controlled at 5um-45um, the granular material lucifuge of preparation is packed get final product.Its finished product oxide content is: silver oxide 42%-46%, zinc oxide 36%-44%, silica 8%-10%.Satisfy the demand of different industries, the present invention can be widely used in papermaking, household electrical appliances, automobile, paint, coating, pottery, all conglomeraties such as articles for daily use, make various antibacterial products, effectively guarantee health of human body, the present invention is used in the self-cleaning function that ceramic industry had both been given ceramic articles for use, have antibiotic, bacteriostasis also can effectively improve the quality of Ceramic glaze, increases glaze glossiness and flatness, prescription of the present invention and preparation method, processing technology is simple, rationally advanced, material is easily purchased, and invests for a short time, and production cost is low, wide accommodation, non-environmental-pollution, the antibacterial bacteriostatic effect stability, long action time is the ideal substitute of existing antibacterial agent.
Claims (3)
1. complex antimicrobials, it is characterized in that: it is made up of following raw materials by weight percent, silver carbonate 48.76-50, zinc oxide 38.75-41.32, silica 9.92-11.25.
2. according to the preparation method of the described complex antimicrobials of claim 1, it is characterized in that: it comprises following processing step:
A. prepare burden: silver carbonate, zinc oxide, silica are combined together by weight percentage with electronic scale;
B. homogenizing is mixed: the material for preparing is put into the ball mill homogenizing mix;
C. calcine: the mixed material of homogenizing is sent in the high temperature frit electric furnace calcined, calcining heat is controlled at 1000 ℃-1200 ℃, and the time was controlled at 10 hours-14 hours;
D. grind: it is levigate that the material after will calcining is sent into the interior processing of vibrations mixer grinder;
E. dry: the granular material after process is levigate enters and carries out bake drying in the periodic dryer, makes its moisture below 3%;
F. powder process: dried material is sent into powder process in the screen mesh type flour mill, and granularity is controlled at 5um-45um;
G. pack: the granular material lucifuge packing of preparation is got final product;
3. according to the described complex antimicrobials of claim 1, it is characterized in that: its finished product oxide content is: silver oxide 42%-46%, zinc oxide 36%-44%, silica 8%-10%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200310113356 CN1615698A (en) | 2003-11-12 | 2003-11-12 | Compound antiseptic agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200310113356 CN1615698A (en) | 2003-11-12 | 2003-11-12 | Compound antiseptic agent |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1615698A true CN1615698A (en) | 2005-05-18 |
Family
ID=34759910
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200310113356 Pending CN1615698A (en) | 2003-11-12 | 2003-11-12 | Compound antiseptic agent |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1615698A (en) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2008103621A1 (en) | 2007-02-20 | 2008-08-28 | Microban Products Company | Ceramic glaze having antimicrobial property |
| CN101912638A (en) * | 2010-07-26 | 2010-12-15 | 郭云童 | Nano silver-carrying-silicon dioxide catheter and production method thereof |
| CN102210325A (en) * | 2011-01-27 | 2011-10-12 | 深圳市源兴纳米医药科技有限公司 | Composite antibacterial powder and preparation method thereof |
| CN101606537B (en) * | 2009-06-23 | 2011-12-21 | 哈尔滨工业大学 | Preparation method of SiO2-AgCl composite antibacterial thin films |
| CN101731271B (en) * | 2009-12-29 | 2012-05-30 | 浙江理工大学 | Inorganic nanometer-sized mesoporous antibacterial agent and preparation method thereof |
| US9974310B2 (en) | 2016-03-09 | 2018-05-22 | Microban Products Company | Ceramic additive formulation and method of making |
| US10159255B2 (en) | 2008-02-16 | 2018-12-25 | Microban Products Company | Biocidal glazing composition, method, and article |
| US10899657B1 (en) | 2016-03-09 | 2021-01-26 | Microban Products Company | Ceramic additive formulation and method of making |
| US11844351B2 (en) | 2016-10-31 | 2023-12-19 | Microban Products Company | Method of treating a glazed ceramic article |
-
2003
- 2003-11-12 CN CN 200310113356 patent/CN1615698A/en active Pending
Cited By (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10045538B2 (en) | 2007-02-20 | 2018-08-14 | Microban Products Company | Ceramic glaze having antimicrobial property |
| US10045539B2 (en) | 2007-02-20 | 2018-08-14 | Microban Products Company | Ceramic glaze having antimicrobial property |
| US9446980B2 (en) | 2007-02-20 | 2016-09-20 | Microban Products Company | Ceramic glaze having antimicrobial property |
| US9446981B2 (en) | 2007-02-20 | 2016-09-20 | Microban Products Company | Ceramic glaze having antimicrobial property |
| US10856549B2 (en) | 2007-02-20 | 2020-12-08 | Microban Products Company | Ceramic glaze having antimicrobial property |
| EP2118038A4 (en) * | 2007-02-20 | 2015-11-04 | Microban Products | Ceramic glaze having antimicrobial property |
| WO2008103621A1 (en) | 2007-02-20 | 2008-08-28 | Microban Products Company | Ceramic glaze having antimicrobial property |
| US10863745B2 (en) | 2007-02-20 | 2020-12-15 | Microban Products Company | Ceramic glaze having antimicrobial property |
| US9434638B2 (en) | 2007-02-20 | 2016-09-06 | Microban Products Company | Ceramic glaze having antimicrobial property |
| US10045537B2 (en) | 2007-02-20 | 2018-08-14 | Microban Products Company | Ceramic glaze having antimicrobial property |
| US10856550B2 (en) | 2007-02-20 | 2020-12-08 | Microban Products Company | Ceramic glaze having antimicrobial property |
| US10159255B2 (en) | 2008-02-16 | 2018-12-25 | Microban Products Company | Biocidal glazing composition, method, and article |
| CN101606537B (en) * | 2009-06-23 | 2011-12-21 | 哈尔滨工业大学 | Preparation method of SiO2-AgCl composite antibacterial thin films |
| CN101731271B (en) * | 2009-12-29 | 2012-05-30 | 浙江理工大学 | Inorganic nanometer-sized mesoporous antibacterial agent and preparation method thereof |
| CN101912638A (en) * | 2010-07-26 | 2010-12-15 | 郭云童 | Nano silver-carrying-silicon dioxide catheter and production method thereof |
| CN102210325A (en) * | 2011-01-27 | 2011-10-12 | 深圳市源兴纳米医药科技有限公司 | Composite antibacterial powder and preparation method thereof |
| CN102210325B (en) * | 2011-01-27 | 2013-11-06 | 深圳市源兴纳米医药科技有限公司 | Composite antibacterial powder and preparation method thereof |
| US9974310B2 (en) | 2016-03-09 | 2018-05-22 | Microban Products Company | Ceramic additive formulation and method of making |
| US10299483B2 (en) | 2016-03-09 | 2019-05-28 | Microban Products Company | Ceramic additive formulation and method of making |
| US10899657B1 (en) | 2016-03-09 | 2021-01-26 | Microban Products Company | Ceramic additive formulation and method of making |
| US11767256B1 (en) | 2016-03-09 | 2023-09-26 | Microban Products Company | Ceramic additive formulation and method of making |
| US11844351B2 (en) | 2016-10-31 | 2023-12-19 | Microban Products Company | Method of treating a glazed ceramic article |
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