CN1596649A - Herbicide composition containing methyl sulcotrione - Google Patents
Herbicide composition containing methyl sulcotrione Download PDFInfo
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- CN1596649A CN1596649A CN 200410056840 CN200410056840A CN1596649A CN 1596649 A CN1596649 A CN 1596649A CN 200410056840 CN200410056840 CN 200410056840 CN 200410056840 A CN200410056840 A CN 200410056840A CN 1596649 A CN1596649 A CN 1596649A
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Abstract
A composite herbicide contains sulcotrine-methyl and one of 18 herbicide including propisochlor, acetochlor, atrazine, etc.
Description
Technical field:
The present invention relates to contain the binary built Herbicidal combinations of mesotrione, be mainly used in cornfield weeding.
Background technology:
At present China's corn field herbicide mainly contains the A Yi mixture of using before the seedling (atrazine+Acetochlor), use behind the seedling 2,4-D butyl ester, dicamba, Brominal, beautiful farming are happy etc.Because the longevity of residure of atrazine in soil is longer, be unfavorable for crop rotation, not only influence back stubble is planted brassicaceous vegetable, and to afterwards stubble is planted wheat, soybean also can produce poisoning, and it is bigger that the herbicidal effect of the weed killer herbicide of soil treatment is influenced by soil moisture, drug effect is relatively poor when arid, even invalid; And cauline leaf handles in the weed killer herbicide 2, and 4-D butyl ester, dicamba, Brominal etc. only have preventive effect preferably to broad leaved weed, and are invalid to grassy weed; Cauline leaf inorganic agent nicosulfuron all has preventive effect preferably to broad leaved weed and grassy weed, but higher because of its cost, and influences its large-area applying.
Mesotrione is a kind of novel three ketones weed killer herbicide, but both native list processings before the seedling, but also cauline leaf spraying behind the seedling, instant effect simultaneously, simultaneously mesotrione residual life in soil short, so to succession crop safety.Simultaneously, its biologically active surpasses the sulphur humulone more than 10 times, has more potentiality to be exploited with competitive, because it is environmentally friendly, calendar year 2001 sells in the EU countries and the U.S. in 2002 by the approval of Environmental Protection Agency USA.But its control efficiency to broad leaved weed common in the corn field such as Siberian cocklebur, Tong fiber crops, japanese bearbind, acalypha copperleaf etc. is not very good.In addition, the domestic and international composition of also not mentioned it and other specific compounds of patent.Therefore it is unforeseen with the effect of other compound use.
Summary of the invention:
The stack that effectiveness that Herbicidal combinations was showed that mesotrione and compound that some is specific are formed with certain proportion among the present invention and activity level have exceeded individual composition activity, this exercising result is called synergistic effect.The invention provides the one group of compound that has synergistic effect with mesotrione, in the hope of a kind of efficient, low-residual of further invention, low cost and grassy weed and broad leaved weed all there are the disposable herbicide composition of better preventive effect, they can enlarge kills the grass spectrum, improves herbicidal effect, reduces residual activity, reduces poisoning to crop, delays the drug-fast generation of weeds and the succession of community, reduction dosage, reduces environmental pollution, laborsaving simultaneously, economical, reduce farmer's burdens.
The binary mixture preparation of preventing and kill off corn field weed that mesotrione and weed killer herbicide M form is mainly used in corn field, is pesticidal preparations.The active ingredient weed killer herbicide M that the present invention relates to is respectively:
Propisochlor Propisochlor
Prosulfuron Prosulfuron (C
15H
16F
3N
5O
4S) 419.4
Carfentrazoneethyl Carfentrazone-ethyl (C
15H
14CL
2F
3N
3O
3) 412.2
Fluthiacetmethyl Fluthiacet-ethyl (C
15H
15CLFN
3O
3S
2) 403.9
Diflufenzopyr Diflufenzopyr (C
15H
12F
2N
4O
3) 394.3
Metobenzuron Metobenzuron (C
22H
28N
2O
5) 400.5
Flumicloracpentryl Flumiclorac-pentyl (C
21H
23CLFNO
5) 423.9
Acetochlor Acetochlor (C
14H
20ClNO
2)
Atrazine Atrazine (C
8H
14ClN
5) 215.69
Dimethenamid Dimethenamid (C
12H
18ClNO
2S) 275.8
Flumetsulam Flumetsulam (C
12H
9F
2N
5O
2S) 325.3
Rimsulfuron 25 Rimsulfuron (C
14H
17N
5O
7S
2) 431.4
Halosulfuronmethyl Halosulfuron-methyl (C
13H
15ClN
6O
7S) 434.8
Isoxaflutole Isoxaflutole (C
15H
12F
3NO
4S) 359.4
Sulphonyl azoles humulone Sulfentrazone (C
11H
10C
12F
2N
4O
3S) 387.2
Flufenacet Flufenacet (C
14H
13F
4N
3O
2S) 363.3
Amicarbazone Amicarbazone (C
10H
19N
5O
2) 241.29
Metosulam Metosulam (C
14H
13C
12N
5O
4S) 418.3
The purpose of this invention is to provide and a kind ofly be applicable to that single broadleaf weed prevents and kill off, to the binary mixture preparation that contains the methyl yellow humulone when stubble corn and succession crop safety.
Herbicide formulations of the present invention is to be the binary mixture of active ingredient by mesotrione and weed killer herbicide M, be mainly used in the disposable single broadleaf weed that corn field takes place of preventing and kill off, the active ingredient that contains in this mixture is respectively sulphur humulone: M=1: 30-50: 1, add an amount of auxiliary agent or carrier, can be processed into the dispersibility granula, do outstanding agent, aqua, suspending agent, wetting powder, missible oil, sustained release agent, granule.
The present invention is to be the binary mixture and the application thereof of active ingredient by mesotrione and weed killer herbicide M, and advantage is
1, easy to use.Composition proposed by the invention can seedling pre-treatment (closed soil treatment) but also behind the seedling cauline leaf spraying handle, use optimum period long, the user can freely select spraying time according to environmental condition.
2, broad weed-killing spectrum.One of the composition that the present invention proposes mesotrione list is used most of lists dicotyledonous all effective, after using with other weed killer herbicides M, not only can effectively kill the weeds after being unearthed, and also the weeds of not being unearthed in the controlled soil are improved herbicidal effect.
3, save drug cost.The composition that the present invention proposes, can disposablely prevent and kill off the single broadleaf weed after great majority are emerged in the corn field, and the weeds that do not sprout as yet in the soil, the weeds of dispenser controlled corn field in most of breeding times, saved half farming season of user, relatively happy with the beautiful farming of corn field herbicide after seedling simultaneously, the mu cost is from 15-20 unit/mu, drop to 3-8 unit/mu, saved drug cost greatly.
4, to working as stubble corn and succession crop safety.The composition that the present invention proposes is through verification experimental verification, not only to when the safety of stubble crop corn fine, and after the medication 3 months, to the equal safety of crops such as the soybean of back stubble plantation, paddy rice, rape, Chinese sorghum, wheat.Illustrate that the said composition lasting period can reach three months, just in time control weeds harm in the corn growth stage, also can not influence succession crop simultaneously, solved heterocycle herbicides such as use atrazine, change the problem of stubble difficulty.
Part embodiment of the present invention:
Embodiment:
Embodiment 1:
The compound method of 25% mesotrione propisochlor granule
Mesotrione 10% (weight)
Propisochlor 15% (weight)
Farming breast 500
#5% (weight)
Farming breast 1600
#5% (weight)
Draw back powder 5% (weight)
JFC 3% (weight)
Diatomite 57% (weight)
Said mixture is evenly mixed, grinds, mix suitable quantity of water and mediate, the mixture pelleting of gained, be drying to obtain granule.
Embodiment 2:
The compound method of 26% mesotrione prosulfuron aqueous suspension agent
Mesotrione 5% (weight)
Prosulfuron 21% (weight)
Farming breast 500
#3% (weight)
Farming breast 600
#5% (weight)
Calcium lignosulfonate 10% (weight)
K
124% (weight)
Water 52% (weight)
Various compositions are mixed, in sand mill, be ground to the active ingredient particle diameter less than 3 μ m.
Embodiment 3:
The compound method of 51% mesotrione carfentrazoneethyl wetting powder
Mesotrione 6% (weight)
Carfentrazoneethyl 45% (weight)
Methylcellulose 8% (weight)
JFC 4% (weight)
Kaolin 37% (weight)
Various materials are added in the reactor successively, under stirring condition, it is fully mixed, be crushed to certain fineness.
Embodiment 4:
The compound method of 51% mesotrione fluthiacetmethyl dispersibility granula
Mesotrione 3% (weight)
Carfentrazoneethyl 48% (weight)
Methylcellulose 10% (weight)
Saponin 6% (weight)
Kaolin 23% (weight)
Disintegrant 10% (weight)
Said mixture is evenly mixed, grinds, mix suitable quantity of water and granulation, be drying to obtain the dispersibility granula.
Embodiment 5:
The compound method of 25% mesotrione diflufenzopyr sustained release agent
Mesotrione 5% (weight)
Diflufenzopyr 20% (weight)
Neopelex 8% (weight)
SOPA 15% (weight)
Water 32% (weight)
Active carbon 20% (weight)
Various active ingredients are mixed, in sand mill, be ground to the active ingredient particle diameter, be loaded on and make sustained release agent in the active carbon less than 3 μ m.
Embodiment 6:
The compound method of 31% mesotrione metobenzuron aqueous suspension agent
Mesotrione 12% (weight)
Diflufenzopyr 19% (weight)
Neopelex 6% (weight)
NNO 3% (weight)
Water 60% (weight)
Various compositions are mixed, in sand mill, be ground to the active ingredient particle diameter less than 3 μ m.
Embodiment 7:
41% mesotrione flumicloracpentryl is done the compound method of outstanding agent
Mesotrione 3% (weight)
Flumicloracpentryl 38% (weight)
Sodium lignin sulfonate 5% (weight)
Saponin 3% (weight)
Kaolin 41% (weight)
Disintegrant 10% (weight)
Said mixture is evenly mixed, grinds, mix suitable quantity of water and mist projection granulating, be drying to obtain outstanding agent.
Embodiment 8:
The compound method of 51% mesotrione Acetochlor wetting powder
Mesotrione 2% (weight)
Acetochlor 49% (weight)
Methyl naphthalene sulfonate formaldehyde condensate 10% (weight)
Lauryl sodium sulfate 3% (weight)
Bentonite 36% (weight)
Various materials are added in the reactor successively, under stirring condition, it is fully mixed, be crushed to certain fineness.
Embodiment 9:
The compound method of 51% mesotrione atrazine missible oil
Mesotrione 2% (weight)
Atrazine 49% (weight)
Methanonaphthalene sodium sulfonate 6% (weight)
Emulsifier 600 # 10% (weight)
Dimethylbenzene 33% (weight)
Various materials are added in the reactor successively, under stirring condition, it is fully mixed.
Embodiment 10:
The compound method of 51% mesotrione dimethenamid wetting powder
Mesotrione 26% (weight)
Dimethenamid 25% (weight)
Methylcellulose 8% (weight)
JFC 5% (weight)
Kaolin 36% (weight)
Various materials are added in the reactor successively, under stirring condition, it is fully mixed, be crushed to certain fineness.
Embodiment 11:
The compound method of 31% mesotrione Flumetsulam aqua
Mesotrione 6% (weight)
Flumetsulam 25% (weight)
Farming newborn 500# 8% (weight)
Farming newborn OX-635# 3% (weight)
Water 58% (weight)
Various materials are added in the reactor successively, stir, it is fully mixed.
Embodiment 12:
The compound method of 41% mesotrione rimsulfuron 25 aqueous suspension agent
Mesotrione 16% (weight)
Rimsulfuron 25 25% (weight)
Farming breast 600
#5% (weight)
Sodium lignin sulfonate 5% (weight)
Neopelex 5% (weight)
Water 44% (weight)
Various compositions are mixed, in sand mill, be ground to the active ingredient particle diameter less than 3 μ m.
Embodiment 13:
The compound method of 51% mesotrione halosulfuronmethyl wetting powder
Mesotrione 10% (weight)
Halosulfuronmethyl 41% (weight)
Methylcellulose 8% (weight)
Lauryl sodium sulfate 5% (weight)
Kaolin 36% (weight)
Various materials are added in the reactor successively, under stirring condition, it is fully mixed, be crushed to certain fineness.
Embodiment 14:
The compound method of 15% mesotrione isoxaflutole aqueous suspension agent
Mesotrione 10% (weight)
Isoxaflutole 5% (weight)
Naphtholsulfonic acid formaldehyde condensation products sodium salt 5% (weight)
Sldium lauryl sulfate 6% (weight)
Water 74% (weight)
Various compositions are mixed, in sand mill, be ground to the active ingredient particle diameter less than 3 μ m.
Embodiment 15:
The compound method of 25% mesotrione sulphonyl azoles humulone aqueous suspension agent
Mesotrione 20% (weight)
Sulphonyl azoles humulone 5% (weight)
Calcium lignosulfonate 5% (weight)
Neopelex 8% (weight)
Water 72% (weight)
Various compositions are mixed, in sand mill, be ground to the active ingredient particle diameter less than 3 μ m.
Embodiment 16:
The compound method of 51% mesotrione flufenacet wetting powder
Mesotrione 16% (weight)
Flufenacet 35% (weight)
Methylcellulose 8% (weight)
JFC 5% (weight)
Kaolin 36% (weight)
Various materials are added in the reactor successively, under stirring condition, it is fully mixed, be crushed to certain fineness.
Embodiment 17:
The compound method of 51% mesotrione amicarbazone wetting powder
Mesotrione 21% (weight)
Amicarbazone 30% (weight)
Methylcellulose 8% (weight)
Saponin 4% (weight)
Kaolin 37% (weight)
Various materials are added in the reactor successively, under stirring condition, it is fully mixed, be crushed to certain fineness.
Embodiment 18:
The compound method of 15% mesotrione metosulam aqueous suspension agent
Mesotrione 10% (weight)
Metosulam 5% (weight)
Draw back powder 5% (weight)
Neopelex 6% (weight)
Water 74% (weight)
Various compositions are mixed, in sand mill, be ground to the active ingredient particle diameter less than 3 μ m.
Embodiment 19:
The drug effect report (embodiment 1 preparation) of 25% mesotrione propisochlor granule
The corn 5-6 leaf phase, weeds 2-5 leaf phase dispenser, 45 days investigation strain preventive effect results are as follows behind the medicine
| The medicament title | Consumption effective content (gram/mu) | Lady's-grass | Siberian cocklebur | The barnyard grass grass | Kitchen garden | Acalypha copperleaf | |||||
| Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | ||
| 25% mesotrione SC | ??100 | ???8.0 | ???89.6 | ???4.2 | ???92.5 | ???7.6 | ???88.7 | ???2.2 | ??79.3 | ????1.8 | ??80.6 |
| 72% propisochlor EC | ??30 | ???7.3 | ???90.5 | ????- | ????- | ???4.8 | ???92.9 | ????- | ???- | ?????- | ???- |
| 25% first propisochlor granule | ??200 | ???5.6 | ???92.7 | ???4.0 | ???92.9 | ???4.1 | ???93.9 | ???1.0 | ??90.7 | ????1.4 | ??85.3 |
| Blank | ???- | ???76.8 | ????- | ???56.1 | ????- | ???67.3 | ????- | ???10.8 | ???- | ????9.3 | ???- |
Test shows: propisochlor and mesotrione are used with to enlarge and are killed the grass spectrum, and increase preventive effect, no antagonism.
Embodiment 20:
The drug effect report (embodiment 2 preparations) of 26% mesotrione prosulfuron aqueous suspension agent
The corn 5-6 leaf phase, weeds 2-5 leaf phase dispenser, 45 days investigation strain preventive effect results are as follows behind the medicine
| The medicament title | Consumption effective content (gram/mu) | Lady's-grass | Siberian cocklebur | Bermuda grass | Kitchen garden | Acalypha copperleaf | |||||
| Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | ||
| 25% mesotrione SC | ??100 | ????5.8 | ???91.5 | ????3.2 | ???94.2 | ????8.1 | ????87.0 | ????1.6 | ????86.2 | ????1.8 | ???79.8 |
| 20% prosulfuron WDG | ??50 | ????7.6 | ???88.9 | ????5.7 | ???89.7 | ????5.4 | ????91.3 | ????2.1 | ????81.9 | ????1.5 | ???83.1 |
| 26% first trifluoropropyl SC | ??120 | ????5.0 | ???92.7 | ????3.0 | ???94.6 | ????5.2 | ????91.6 | ????1.6 | ????86.2 | ????1.5 | ???83.1 |
| Blank | ???- | ????68.3 | ?????- | ????55.6 | ?????- | ????62.1 | ?????- | ????11.6 | ?????- | ????8.9 | ????- |
Test shows: prosulfuron and mesotrione are used the preventive effect a little more than each single agent with, and no antagonism is to crop safety.
Embodiment 21:
But the drug effect of 51% mesotrione carfentrazoneethyl wet-milling report (embodiment 3 preparations)
The corn 3-5 leaf phase, weeds 2-4 leaf phase dispenser, 30 days investigation strain preventive effect results are as follows behind the medicine
| The medicament title | Consumption effective content (gram/mu) | Lady's-grass | Clearvers | Piemarker | Lamb's-quarters | Acalypha copperleaf | |||||
| Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | ||
| 25% mesotrione SC | ??100 | ????4 | ??94.3 | ????9.0 | ???83.1 | ???6.7 | ???89.0 | ????2.1 | ???78.8 | ???1.4 | ???83.1 |
| 50% carfentrazoneethyl WP | ??20 | ????- | ???- | ????4.1 | ???92.3 | ???4.9 | ???91.9 | ????1.0 | ???89.9 | ???1.4 | ???83.1 |
| 51% first carfentrazoneethyl WP | ??100 | ???3.7 | ??94.8 | ????4 | ???92.5 | ???4.6 | ???92.4 | ????0.8 | ???91.9 | ???1.1 | ???86.7 |
| Blank | ???- | ???70.6 | ???- | ????53.2 | ????- | ???60.7 | ????- | ????9.9 | ????- | ???8.3 | ????- |
Test shows: carfentrazoneethyl and mesotrione are used the back herbicidal effect with a little more than single agent, help increasing mutually drug effect, and do not have antagonism.
Embodiment 22:
The drug effect report (embodiment 4 preparations) of 51% mesotrione fluthiacetmethyl dispersibility granula
The corn 5-6 leaf phase, weeds 2-5 leaf phase dispenser, 45 days investigation strain preventive effect results are as follows behind the medicine
| The medicament title | Consumption effective content (gram/mu) | Lady's-grass | Siberian cocklebur | The barnyard grass grass | Lamb's-quarters | Acalypha copperleaf | |||||
| Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | ||
| 25% mesotrione SC | ??100 | ????4.4 | ??94.0 | ???3.2 | ???94.3 | ???4.5 | ???92.8 | ???2.2 | ???81.0 | ????1.7 | ???82.5 |
| 20% fluthiacetmethyl WP | ??20 | ????- | ???- | ???3.6 | ???93.6 | ????- | ????- | ???1.6 | ???86.2 | ????1.2 | ???87.6 |
| 51% first fluorine thiophene WDG | ??100 | ????3.4 | ??95.3 | ???3.0 | ???94.7 | ???4.4 | ???93.0 | ???1.2 | ???89.7 | ????1.0 | ???89.7 |
| Blank | ???- | ????72.9 | ???- | ???56.5 | ????- | ???62.8 | ?????- | ???11.6 | ????- | ????9.7 | ?????- |
Test shows: fluthiacetmethyl and mesotrione are used with to enlarge and are killed the grass spectrum, and to crop safety.
Embodiment 23:
The drug effect report (embodiment 5 preparations) of 25% mesotrione diflufenzopyr sustained release agent
The corn 3-4 leaf phase, weeds 2-4 leaf phase dispenser, 45 days investigation strain preventive effect results are as follows behind the medicine
| The medicament title | Consumption effective content (gram/mu) | Lady's-grass | Eleusine indica | The barnyard grass grass | Kitchen garden | Acalypha copperleaf | |||||
| Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | ||
| 25% mesotrione SC | ??100 | ??4.8 | ??93.8 | ??4.6 | ??91.1 | ??4.1 | ??93.9 | ???1.2 | ???89.4 | ???1.2 | ???87.8 |
| 75% diflufenzopyr WDG | ??120 | ??8.3 | ??89.4 | ??9.6 | ??81.4 | ??8.4 | ??87.6 | ???1.4 | ???87.6 | ???1.8 | ???81.6 |
| 25% first diflufenzopyr sustained release agent | ??200 | ??4.5 | ??94.2 | ??4.5 | ??91.3 | ??4.2 | ??93.8 | ???1.2 | ???89.4 | ???1.0 | ???89.8 |
| Blank | ???- | ??78.0 | ???- | ??51.6 | ???- | ??67.6 | ???- | ???11.3 | ????- | ???9.8 | ????- |
Test shows: mesotrione and diflufenzopyr are used with suitable with each single agent preventive effect, and do not have antagonism.
Embodiment 24:
The drug effect report (embodiment 6 preparations) of 31% mesotrione metobenzuron suspending agent
The corn 3-4 leaf phase, weeds 2-4 leaf phase dispenser, 30 days investigation strain preventive effect results are as follows behind the medicine
| The medicament title | Consumption effective content (gram/mu) | Lady's-grass | The barnyard grass grass | Siberian cocklebur | Black nightshade | Lamb's-quarters | |||||
| Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | ||
| 25% mesotrione SC | ??100 | ??4.6 | ??93.8 | ??5.0 | ??90.6 | ??4.8 | ??92.7 | ???1.7 | ??85.5 | ???1.2 | ???88.9 |
| 75% metobenzuron WP | ??100 | ??8.1 | ??89.0 | ??9.8 | ??81.5 | ??4.4 | ??93.4 | ???1.1 | ??90.6 | ???1.0 | ???90.7 |
| 31% first methoxy benzene WP | ??200 | ??4.1 | ??94.4 | ??4.5 | ??91.5 | ??4.0 | ??94.0 | ???1.1 | ??90.6 | ???0.9 | ???91.7 |
| Blank | ???- | ??73.8 | ???- | ??53.1 | ???- | ??66.2 | ???- | ???11.7 | ???- | ???10.8 | ????- |
Test shows: mesotrione and metobenzuron mix weeding effect be a little more than each single agent, and do not have antagonism, methyl sulphur
Humulone and metobenzuron have been used mutual synergistic effect with.
Embodiment 25:
41% mesotrione flumicloracpentryl is done the drug effect report (embodiment 7 preparations) of outstanding agent
The corn 3-6 leaf phase, weeds 2-4 leaf phase dispenser, 40 days investigation strain preventive effect results are as follows behind the medicine
| The medicament title | Consumption effective content (gram/mu) | Lady's-grass | Siberian cocklebur | Lamb's-quarters | Kitchen garden | Black nightshade | |||||
| Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | ||
| 25% mesotrione SC | ???100 | ???3.3 | ????95.6 | ????1.8 | ????92.4 | ???2.8 | ???77.8 | ???1.7 | ????85.7 | ???2.8 | ????70.5 |
| 18% flumicloracpentryl EC | ???100 | ???13.2 | ????82.2 | ????2.0 | ????91.6 | ???1.2 | ???90.3 | ???1.5 | ????87.3 | ???2.3 | ????75.4 |
| 41% first flumicloracpentryl is done outstanding agent | ???100 | ???3.0 | ????96.0 | ????1.5 | ????93.7 | ???1.3 | ???89.7 | ???1.6 | ????86.2 | ???2.5 | ????74.1 |
| Blank | ????- | ???74.1 | ?????- | ????23.8 | ?????- | ???12.6 | ????- | ???11.6 | ?????- | ???9.5 | ?????- |
Test shows: mesotrione and flumicloracpentryl mix weeding effect be a little more than each single agent, and do not have antagonism, methyl sulphur grass
Ketone and flumicloracpentryl have been used mutual synergistic effect with.
Embodiment 26:
The drug effect report (embodiment 8 preparations) of 51% mesotrione Acetochlor wetting powder
The corn 3-5 leaf phase, weeds 2-4 leaf phase dispenser, 45 days investigation strain preventive effect results are as follows behind the medicine
| The medicament title | Consumption effective content (gram/mu) | Lady's-grass | Green foxtail | The barnyard grass grass | Kitchen garden | Acalypha copperleaf | |||||
| Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | ||
| 25% mesotrione SC | ??100 | ???4.0 | ??95.8 | ???2.8 | ??92.2 | ???3.2 | ??94.7 | ???1.9 | ???84.2 | ????1.6 | ????84.8 |
| 50% acetochlor ec | ??500 | ???4.8 | ??95.0 | ???1.2 | ??96.6 | ???3.6 | ??94.1 | ???- | ????- | ?????- | ?????- |
| 51% first Acetochlor WP | ??500 | ???3.0 | ??96.9 | ???1.4 | ??96.1 | ???3.9 | ??93.6 | ???1.6 | ???87.0 | ????1.1 | ????89.1 |
| Blank | ???- | ???95.6 | ???- | ???35.7 | ???- | ???60.9 | ????- | ???12.3 | ????- | ????10.5 | ?????- |
Test shows: mesotrione and Acetochlor are used with to enlarge and are killed the grass spectrum, to crop safety.
Embodiment 27:
The drug effect report (embodiment 9 preparations) of 51% mesotrione atrazine missible oil
The corn 5-6 leaf phase, weeds 2-5 leaf phase dispenser, 45 days investigation strain preventive effect results are as follows behind the medicine
| The medicament title | Consumption effective content (gram/mu) | Lady's-grass | Eleusine indica | The barnyard grass grass | Kitchen garden | Acalypha copperleaf | |||||
| Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | ||
| 25% mesotrione SC | ??100 | ???5.2 | ??93.7 | ???3.8 | ??92.0 | ???3.1 | ??93.6 | ???1.3 | ??89.1 | ????1.9 | ????82.2 |
| 80% atrazine SC | ??200 | ???4.1 | ??95.0 | ???3.5 | ??92.6 | ???3.2 | ??93.4 | ????- | ???- | ?????- | ?????- |
| 51% first atrazine EC | ??240 | ???4.0 | ??95.2 | ???3.6 | ??92.4 | ???3 | ??93.8 | ???1.3 | ??89.1 | ????1.4 | ????86.9 |
| Blank | ???- | ???82.5 | ???- | ???47.3 | ????- | ???48.6 | ???- | ???11.9 | ???- | ????10.7 | ?????- |
Test shows: mesotrione and atrazine are used with to enlarge and are killed the grass spectrum, to crop safety.
Embodiment 28:
The drug effect report (embodiment 10 preparations) of 51% mesotrione dimethenamid wetting powder
The corn 5-6 leaf phase, weeds 2-5 leaf phase dispenser, 45 days investigation strain preventive effect results are as follows behind the medicine
| The medicament title | Consumption effective content (gram/mu) | Lady's-grass | Siberian cocklebur | The barnyard grass grass | Green foxtail | Acalypha copperleaf | |||||
| Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | ||
| 25% mesotrione SC | ??100 | ??6.0 | ??92.2 | ??4.2 | ??92.5 | ??7.6 | ??88.7 | ???2.2 | ??79.3 | ???1.8 | ??80.6 |
| 75% dimethenamid EC | ??400 | ??6.3 | ??91.8 | ??7.4 | ??86.8 | ??4.8 | ??92.9 | ???1.0 | ??90.7 | ???3.5 | ??62.4 |
| 51% first diformazan fen WP | ??400 | ??5.6 | ??92.7 | ??4.0 | ??92.9 | ??4.1 | ??93.9 | ???1.0 | ??90.7 | ???1.4 | ??85.3 |
| Blank | ???- | ??76.8 | ????- | ??56.1 | ????- | ??67.3 | ???- | ???10.8 | ???- | ???9.3 | ???- |
Test shows: dimethenamid and mesotrione mix weeding effect be a little more than each single agent, and do not have antagonism.
Embodiment 29:
The drug effect report (embodiment 11 preparations) of 31% mesotrione Flumetsulam aqua
The corn 5-6 leaf phase, weeds 2-5 leaf phase dispenser, 45 days investigation strain preventive effect results are as follows behind the medicine
| The medicament title | Consumption effective content (gram/mu) | Lady's-grass | Siberian cocklebur | Piemarker | Black nightshade | Acalypha copperleaf | |||||
| Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | ||
| 25% mesotrione SC | ???100 | ????5.8 | ????91.5 | ????3.2 | ????94.2 | ????4.1 | ????81.4 | ????1.6 | ??86.2 | ????1.8 | ???79.8 |
| 40% Flumetsulam WDG | ???100 | ????9.6 | ????85.9 | ????5.7 | ????89.7 | ????2.4 | ????89.1 | ????2.1 | ??81.9 | ????1.5 | ???83.1 |
| The phonetic sulphur aqua of 31% first azoles | ???150 | ????5.0 | ????92.7 | ????3.0 | ????94.6 | ????2.2 | ????90.0 | ????1.6 | ??86.2 | ????1.5 | ???83.1 |
| Blank | ????- | ????68.3 | ?????- | ????55.6 | ?????- | ????22.1 | ????- | ????11.6 | ????- | ????8.9 | ?????- |
Test shows: Flumetsulam and mesotrione are used the preventive effect a little more than each single agent with, and no antagonism is to crop safety.
Embodiment 30:
The drug effect report (embodiment 12 preparations) of 41% mesotrione rimsulfuron 25 aqueous suspension agent
The corn 3-5 leaf phase, weeds 2-4 leaf phase dispenser, 30 days investigation strain preventive effect results are as follows behind the medicine
| The medicament title | Consumption effective content (gram/mu) | Lady's-grass | Clearvers | The barnyard grass grass | Lamb's-quarters | Acalypha copperleaf | |||||
| Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | ||
| 25% mesotrione SC | ??100 | ???4.0 | ??94.3 | ???9.0 | ???83.1 | ???6.7 | ???89.0 | ???2.1 | ???78.8 | ????1.4 | ????83.1 |
| 5% rimsulfuron 25 EC | ??100 | ???4.6 | ??93.5 | ???4.1 | ???92.3 | ???4.9 | ???91.9 | ???1.0 | ???89.9 | ????1.4 | ????83.1 |
| 41% first rimsulfuron 25 WP | ??80 | ???3.7 | ??94.8 | ???4.0 | ???92.5 | ???4.6 | ???92.4 | ???0.8 | ???91.9 | ????1.1 | ????86.7 |
| Blank | ???- | ???70.6 | ????- | ???53.2 | ?????- | ???60.7 | ????- | ???9.9 | ????- | ????8.3 | ?????- |
Test shows: rimsulfuron 25 and mesotrione are used the back herbicidal effect with a little more than single agent, help increasing mutually drug effect, and
No antagonism.
Embodiment 31:
The drug effect report (embodiment 13 preparations) of 51% mesotrione halosulfuronmethyl wetting powder
The corn 5-6 leaf phase, weeds 2-5 leaf phase dispenser, 45 days investigation strain preventive effect results are as follows behind the medicine
| The medicament title | Consumption effective content (gram/mu) | Lady's-grass | Siberian cocklebur | The barnyard grass grass | Lamb's-quarters | Kitchen garden | |||||
| Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | ||
| 25% mesotrione SC | ??100 | ??4.4 | ??94.0 | ??3.2 | ??94.3 | ??4.5 | ??92.8 | ???2.2 | ??81.0 | ????1.7 | ??82.5 |
| 30% fluthiacetmethyl WP | ??100 | ???- | ???- | ??7.6 | ??86.5 | ???- | ???- | ???1.6 | ??86.2 | ????1.2 | ??87.6 |
| The phonetic WP of 51% first chlorine pyrrole | ??100 | ??3.4 | ??95.3 | ??3.0 | ??94.7 | ??4.4 | ??93.0 | ???1.2 | ??89.7 | ????1.0 | ??89.7 |
| Blank | ???- | ??72.9 | ???- | ??56.5 | ????- | ??62.8 | ???- | ???11.6 | ????- | ????9.7 | ???- |
Test shows: halosulfuronmethyl and mesotrione are used with to enlarge and are killed the grass spectrum, and to crop safety.
Embodiment 32:
The drug effect report (embodiment 14 preparations) of 15% mesotrione isoxaflutole aqueous suspension agent
The corn 3-4 leaf phase, weeds 2-4 leaf phase dispenser, 45 days investigation strain preventive effect results are as follows behind the medicine
| The medicament title | Consumption effective content (gram/mu) | Lady's-grass | Green foxtail | The barnyard grass grass | Kitchen garden | Acalypha copperleaf | |||||
| Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | ||
| 25% mesotrione SC | ??100 | ??4.8 | ??93.8 | ???9.6 | ??81.4 | ???8.4 | ??87.6 | ????1.2 | ???89.4 | ????1.2 | ????87.8 |
| 35% isoxaflutole SC | ??100 | ??4.3 | ??94.5 | ???4.6 | ??91.1 | ???4.1 | ??93.9 | ????- | ????- | ?????- | ?????- |
| 15% first isoxazole SC | ??300 | ??4.5 | ??94.2 | ???4.5 | ??91.3 | ???4.2 | ??93.8 | ????1.2 | ???89.4 | ????1.0 | ????89.8 |
| Blank | ???- | ??78.0 | ???- | ???51.6 | ???- | ???67.6 | ????- | ????11.3 | ????- | ????9.8 | ?????- |
Test shows: mesotrione and isoxaflutole are used with to enlarge and are killed the grass spectrum, and to crop safety.
Embodiment 33:
The drug effect report (embodiment 15 preparations) of 25% mesotrione sulphonyl azoles humulone aqueous suspension agent
The corn 3-4 leaf phase, weeds 2-4 leaf phase dispenser, 30 days investigation strain preventive effect results are as follows behind the medicine
| The medicament title | Consumption effective content (gram/mu) | Lady's-grass | The barnyard grass grass | Siberian cocklebur | Black nightshade | Lamb's-quarters | |||||
| Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | ||
| 25% mesotrione SC | ??100 | ?4.8 | ??93.5 | ??5.0 | ??90.6 | ??4.5 | ??93.2 | ??1.7 | ??85.5 | ??1.4 | ??87.0 |
| 68% sulphonyl azoles humulone WP | ??200 | ?4.1 | ??94.4 | ??9.8 | ??81.5 | ??4.4 | ??93.4 | ??1.2 | ??89.7 | ??1.0 | ??90.7 |
| 25% methylsulfonyl azoles SC | ??500 | ?4.1 | ??94.4 | ??4.5 | ??91.5 | ??4.2 | ??93.7 | ??1.1 | ??90.6 | ??0.9 | ??91.7 |
| Blank | ???- | ?73.8 | ???- | ??53.1 | ????- | ??66.2 | ???- | ??11.7 | ????- | ??10.8 | ????- |
Test shows: mesotrione and sulphonyl azoles humulone mix weeding effect be a little more than each single agent, and do not have antagonism.
Embodiment 34:
The drug effect report (embodiment 16 preparations) of 51% mesotrione flufenacet wetting powder
The corn 3-6 leaf phase, weeds 2-4 leaf phase dispenser, 40 days investigation strain preventive effect results are as follows behind the medicine
| The medicament title | Consumption effective content (gram/mu) | Lady's-grass | Green foxtail | The barnyard grass grass | Kitchen garden | Black nightshade | |||||
| Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | ||
| 25% mesotrione SC | ??100 | ??3.8 | ??94.9 | ???6.8 | ??71.4 | ??1.8 | ??77.8 | ????1.7 | ???85.7 | ???2.8 | ???70.5 |
| 20% flufenacet SC | ??100 | ??3.8 | ??94.9 | ???2.0 | ??91.6 | ??1.3 | ??89.7 | ?????- | ????- | ????- | ????- |
| 51% first flufenacet WP | ??100 | ??3.4 | ??95.4 | ???1.5 | ??93.7 | ??1.2 | ??90.3 | ????1.6 | ???86.2 | ???2.5 | ???74.1 |
| Blank | ???- | ??74.1 | ???- | ???23.8 | ???- | ??12.6 | ???- | ???11.6 | ????- | ???9.5 | ????- |
Test shows: mesotrione and flufenacet are used with to enlarge and are killed the grass spectrum, and do not have antagonism, mesotrione and fluorine thiophene
Grass amine has been used mutual synergistic effect with.
Embodiment 35:
The drug effect report (embodiment 17 preparations) of 51% mesotrione amicarbazone wetting powder
The corn 3-5 leaf phase, weeds 2-4 leaf phase dispenser, 45 days investigation strain preventive effect results are as follows behind the medicine
| The medicament title | Consumption effective content (gram/mu) | Lady's-grass | Green foxtail | The barnyard grass grass | Kitchen garden | Acalypha copperleaf | |||||
| Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | ||
| 25% mesotrione SC | ??100 | ???6.0 | ??93.0 | ???6.8 | ??81.0 | ??4.2 | ??94.7 | ???1.9 | ??84.2 | ???1.6 | ???84.8 |
| 50% amicarbazone WP | ??200 | ???5.8 | ??93.2 | ???1.2 | ??96.6 | ??3.6 | ??94.1 | ????- | ???- | ?????- | ????- |
| 51% first amicarbazone WP | ??200 | ???5.0 | ??94.2 | ???1.4 | ??96.1 | ??3.9 | ??93.6 | ???1.6 | ??87.0 | ????1.1 | ???89.1 |
| Blank | ???- | ???85.6 | ???- | ???35.7 | ???- | ??60.9 | ???- | ???12.3 | ???- | ????10.5 | ????- |
Test shows: mesotrione and amicarbazone are used with to enlarge and are killed the grass spectrum, to crop safety.
Embodiment 36:
The drug effect report (embodiment 18 preparations) of 15% mesotrione metosulam aqueous suspension agent
The corn 5-6 leaf phase, weeds 2-5 leaf phase dispenser, 45 days investigation strain preventive effect results are as follows behind the medicine
| The medicament title | Consumption effective content (gram/mu) | Lady's-grass | Clearvers | The barnyard grass grass | Black nightshade | Acalypha copperleaf | |||||
| Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | Strain/m 2 | Preventive effect (%) | ||
| 25% mesotrione SC | ??100 | ??5.2 | ??91.9 | ??8.6 | ??81.8 | ??4.1 | ??91.6 | ??2.8 | ??76.5 | ???1.9 | ??82.2 |
| 60% metosulam WDG | ??50 | ??4.1 | ??93.6 | ??3.5 | ??92.6 | ??4.5 | ??90.7 | ??1.3 | ??89.1 | ???2.7 | ??74.8 |
| 15% first metosulam SC | ??300 | ??4.0 | ??93.8 | ??3.2 | ??93.2 | ??4.0 | ??91.8 | ??1.3 | ??89.1 | ???1.4 | ??86.9 |
| Blank | ???- | ??64.5 | ???- | ??47.3 | ???- | ??48.6 | ???- | ??11.9 | ???- | ???10.7 | ????- |
Test shows: mesotrione and metosulam are used with to enlarge and are killed the grass spectrum, to crop safety.
Claims (3)
1, a kind of Herbicidal combinations is characterized in that, it is that active ingredient is formed the binary Herbicidal compositions by mesotrione and weed killer herbicide M, and the weight proportion of active ingredient is in this mixture: mesotrione: M=1: 30-50: 1.
2, according to the Herbicidal combinations of claim 1, it is characterized in that weed killer herbicide M is a kind of in propisochlor, prosulfuron, carfentrazoneethyl, fluthiacetmethyl, diflufenzopyr, metobenzuron, flumicloracpentryl, Acetochlor, atrazine, dimethenamid, Flumetsulam, rimsulfuron 25, halosulfuronmethyl, isoxaflutole, sulphonyl azoles humulone, flufenacet, amicarbazone, the metosulam.
According to the Herbicidal combinations of claim 1, it is characterized in that 3, mixture can be processed into the dispersibility granula, do outstanding agent, aqua, suspending agent, wetting powder, missible oil, sustained release agent, granule.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410056840 CN1596649A (en) | 2004-08-25 | 2004-08-25 | Herbicide composition containing methyl sulcotrione |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410056840 CN1596649A (en) | 2004-08-25 | 2004-08-25 | Herbicide composition containing methyl sulcotrione |
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| CN1596649A true CN1596649A (en) | 2005-03-23 |
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| CN 200410056840 Pending CN1596649A (en) | 2004-08-25 | 2004-08-25 | Herbicide composition containing methyl sulcotrione |
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