CN1594537A - Wine absorption clarificant and method for preparing same - Google Patents
Wine absorption clarificant and method for preparing same Download PDFInfo
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- CN1594537A CN1594537A CN 200410041077 CN200410041077A CN1594537A CN 1594537 A CN1594537 A CN 1594537A CN 200410041077 CN200410041077 CN 200410041077 CN 200410041077 A CN200410041077 A CN 200410041077A CN 1594537 A CN1594537 A CN 1594537A
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- attapulgite clay
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- absorptive clarificant
- clarificant
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Abstract
The invention discloses a wine absorption clarificant and method for preparing same, which consists of using concave-convex rod stone clay as raw material, sulfuric acid processing, naturally activating, carrying out hydrolytic decomposition, screening, purifying, airing, and granulating.
Description
Technical field
The present invention relates to the drinks working method, be specifically related to a kind of drinks absorptive clarificant and production method thereof.
Background technology
Various alcohol products in process of production, turbid phenomenon in various degree appears in the capital, need adsorb and clarify, this is most important during brewery produces, it also is one of difficult production technique, be a difficult problem on this technology of solution of promptly economizing again soon, many scientific payoffss are used for actual production, have obtained effect preferably.From the production technique of present brewery, common method is still and adopts activated carbon as drinks adsorption clarification material, the starch of employing, diatomite, wilkinite and attapulgite clay (claiming polygorskite again) is also arranged, as the adsorption clarification material.
The adsorption clarification effect of activated carbon is better, but the production cost height, the loss of wine body note gas is bigger, and particularly after handling low alcohol white spirit, the wine body is light tasteless, and mouthfeel is relatively poor; The adsorption clarification effect of starch, diatomite, wilkinite and attapulgite clay is lower than activated carbon, though production cost is relatively low, the loss of wine body note gas is less, and the production cycle is long, and technology is comparatively complicated.
Chinese patent notification number CN1044124, the day for announcing is 07 month 25 days nineteen ninety, name is called " a kind of purifying method for wine ", discloses a kind of purifying method for wine.This invention is to adopt polygorskite after treatment to make sorbent material, is seated in the container that glass, plastics, pottery or aluminium make, and wine is promptly clarified by this container.
Attapulgite clay is a kind of moisture magnesium alumino metasilicate salt mine, and it has performances such as good adsorption, decolouring, pulping.Attapulgite clay pH value=8.5 ± 1.0 that simple process clear water is moistening, processing is torn, dried, and be entrained with in various degree impurity, the adsorption clarification material that can not be used for drinks, because the pH value of alcohol product is less than 7.0, contain multiple acid, flavor compound that lipid is useful, directly with the adsorption clarification material of attapulgite clay as drinks, though also can play the effect of adsorption clarification, but can bring different assorted flavor into to alcohol product, and can reduce useful flavor compound, destroy the total quality of wine.
Summary of the invention
The objective of the invention is to overcome weak point in the prior art, a kind of drinks absorptive clarificant and production method thereof are provided.
Production method of the present invention be with attapulgite clay as raw material, through vitriolization with after activating naturally, be hydrolyzed, sieve, purification, airing, granulation, finished product is the drinks absorptive clarificant.The pH value of surplus water=6.0～7.5 after the hydrolysis, utilization once more capable of circulation does not have environmental pollution.
Owing to take vitriolization and natural activating process, and utilize hydrolysis to reach the purpose of purification attapulgite clay, the pH value of attapulgite clay can be dropped to 5.5～7.0 from 〉=7.5.Measure according to Sheng Chan Shi Practice, attapulgite clay is in pulverizing and abrasive dust two procedures, adsorption rate will decay 5～15%, in order to improve the adsorption rate of attapulgite clay, save this two procedures in process of production, in conjunction with attapulgite clay hydrolysis, sub-sieve, purification, particle fineness also can reach 100 μ m, and adsorption rate has risen 3～10%.Greatly reduce production cost, this is a significant advantage of the present invention.
Drinks absorptive clarificant of the present invention adds and needs in the wine pond (or wine jar) of adsorption clarification, because the effect of water in the wine, the rapid disintegration of absorptive clarificant is reduced to the mud state of fineness≤100 μ m, dash with air pump and to turn over for several times, to promote wine liquid and absorptive clarificant thorough mixing, natural sedimentation is 8～72 hours then, different assorted flavor in the sorbing liquor effectively just, and reach the purpose of the muddy wine of clarification.
Use drinks absorptive clarificant of the present invention, the various drinks of producing, can adsorb preferably and produce muddy material, and seldom adsorb other useful composition, and not influencing the local flavor of wine, the loss of wine body note gas is small, clarifying effect is obvious, vinosity is as clear as crystal, and prolonged storage and be refrigerated to-15 ℃ turbid phenomenon can not occur again.The required equipment less investment, production technique is simple, and cost is very cheap, only accounts for 10～20% of drinks special active carbon cost.
Drinks absorptive clarificant of the present invention is after use, and available distillatory method is extracted Disabled and stayed alcohol in the absorptive clarificant, takes out the absorptive clarificant after the distillation, can also continue to use 2～5 times, greatly reduces production cost, improves the business economic benefit.
Drinks absorptive clarificant of the present invention is applicable to the absorption and the clarifying production technique of various liquor, beer, grape wine, yellow rice wine, fruit wine, alcohol, also is applicable to the sewage disposal of industries such as papermaking, printing and dyeing, pharmacy, sugaring, monosodium glutamate, food.
The present invention is achieved by following technical proposals:
1, select materials: attapulgite clay dries after 20～60 days through natural weathering, and moisture answers≤13%.
2, batching (weight percent): attapulgite clay 48～65%, water 33～50%, sulfuric acid (concentration is 98%) 0.5～2%, each component summation=100% (weight).
3, activation: be sprayed at behind the Dilution of sulphuric acid on the attapulgite clay, reaching the activatory purpose, and under normal temperature condition, activate 24～72 hours naturally.
4, hydrolysis: the water adding is deposited in the cement pit of attapulgite clay, and being hydrolyzed is that attapulgite clay mud, the weight of water are 3～4 times of attapulgite clay weight, begins after 8～24 hours with high-pressure pump towards turning over 3～5 times.
5, screening: the attapulgite clay slurry transportation is sieved purification, fineness≤100 μ m in stainless steel drum sieve.
6, airing: attapulgite clay mud through 48～72 hours natural sedimentation after, emit unnecessary water, attapulgite clay mud is forwarded to the airing of cement threshing ground.
7, granulation: attapulgite clay mud when moisture reaches 18～22%, is squeezed into the cylindrical pellet of length≤5mm with forcing machine, and is transported to the airing of cement threshing ground once more after airing, when moisture≤10%, can be packaged as finished product.
8, using method: with the ratio of actual weight * (0.3～1.5) % of drinks absorptive clarificant meat dishes to go with liquor, adding needs in the wine pond (or wine jar) of adsorption clarification, dash in 1 hour with air pump and to turn over 2～3 times, natural sedimentation is 8～72 hours then, different assorted flavor in the sorbing liquor effectively just, and reach the purpose of the muddy wine of clarification.
Embodiment:
The invention will be further described below in conjunction with embodiment.
1, select materials, weathering and drying: the kind of attapulgite clay is a lot, should choose the relatively good attapulgite clay of absorption property, picks up except that the assorted stone of visible and other foreign matter, allow its natural weathering 45 days, constantly disintegration is less irregular block thing, and is dried, and moisture answers≤13%.
2, batching (weight percent): attapulgite clay 60%, water 38.2%, sulfuric acid (concentration is 98%) 1.8%.
3, activate: after sulfuric acid is slowly added entry, be sprayed on the attapulgite clay, stir in the input stirrer, and be transported in the cement pit, various material react withs in sulfuric acid and the attapulgite clay, to reach the activatory purpose, activation is 48 hours naturally.
4, hydrolysis: water is slowly added in the attapulgite clay cement pit of depositing after the activation, the weight of water is 3 times of attapulgite clay weight, attapulgite clay disintegration constantly in water is tiny particulate mud, begins after 24 hours with high-pressure pump towards turning over 4 times.
5, screening: with slush pump the attapulgite clay slurry transportation is sieved in stainless steel drum sieve, the attapulgite clay slurry transportation of fineness≤100 μ m is precipitated in another cement pit; The coarse particles of fineness 〉=100 μ m is that impurity such as quartz sand, opal are passed into disuse mostly, reaches the purpose of purification with this.
6, airing: attapulgite clay mud through after 48～72 hours the natural sedimentation, is emitted unnecessary water in precipitation, and Yu Shui changes over to next time and uses, and attapulgite clay mud forwards the airing of cement threshing ground to.
7, granulation: attapulgite clay mud is after airing, and when moisture reached 18～22%, promptly available forcing machine was squeezed into the cylindrical pellet of length≤5mm, and is transported to the airing of cement threshing ground once more, when moisture≤10%, can be packaged as finished product.
8, using method: with the ratio of actual weight * 0.5% of drinks absorptive clarificant meat dishes to go with liquor, adding needs in the wine pond (or wine jar) of adsorption clarification, because the effect of water in the wine, the rapid disintegration of absorptive clarificant is reduced to the mud state of fineness≤100 μ m, at this moment dash in 1 hour with air pump and turn over 3 times, to promote wine liquid and absorptive clarificant thorough mixing, natural sedimentation is 24 hours then, different assorted flavor in the sorbing liquor effectively just, and reach the purpose of the muddy wine of clarification.
Claims (8)
1, a kind of drinks absorptive clarificant and production method thereof is characterized in that: adopt attapulgite clay as raw material, through vitriolization with after activating naturally, be hydrolyzed, sieve, purification, airing, granulation, finished product is the drinks absorptive clarificant.
2, a kind of drinks absorptive clarificant according to claim 1 and production method thereof is characterized in that, attapulgite clay dries after 20～60 days through natural weathering, and moisture answers≤13%.
3, a kind of drinks absorptive clarificant according to claim 1 and production method thereof, it is characterized in that, batching (weight ratio): attapulgite clay 48～65%, water 33～50%, sulfuric acid (concentration is 98%) 0.5～2%, each component summation 100% (weight).
4, a kind of drinks absorptive clarificant according to claim 1 and production method thereof is characterized in that, are sprayed at behind the Dilution of sulphuric acid on the attapulgite clay, to reach the activatory purpose, need nature activation 24～72 hours.
5, a kind of drinks absorptive clarificant according to claim 1 and production method thereof, it is characterized in that, the water adding is deposited in the cement pit of attapulgite clay, be hydrolyzed and be attapulgite clay mud, the weight of water is 3～4 times of attapulgite clay weight, begins after 8～24 hours with high-pressure pump towards turning over 3～5 times.
6, a kind of drinks absorptive clarificant according to claim 1 and production method thereof is characterized in that, the attapulgite clay slurry transportation is sieved purification, fineness≤100 μ m in stainless steel drum sieve.
7, a kind of drinks absorptive clarificant according to claim 1 and production method thereof is characterized in that, attapulgite clay mud through 48～72 hours natural sedimentation after, emit unnecessary water, attapulgite clay mud is forwarded to the airing of cement threshing ground.
8, a kind of drinks absorptive clarificant according to claim 1 and production method thereof, it is characterized in that, attapulgite clay mud is after airing, moisture was at 18～22% o'clock, be squeezed into the cylindrical pellet of length≤5mm with forcing machine, and be transported to the airing of cement threshing ground, when moisture≤10%, can be packaged as finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410041077 CN1594537A (en) | 2004-06-25 | 2004-06-25 | Wine absorption clarificant and method for preparing same |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410041077 CN1594537A (en) | 2004-06-25 | 2004-06-25 | Wine absorption clarificant and method for preparing same |
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| CN1594537A true CN1594537A (en) | 2005-03-16 |
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| CN 200410041077 Pending CN1594537A (en) | 2004-06-25 | 2004-06-25 | Wine absorption clarificant and method for preparing same |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101787340A (en) * | 2010-03-18 | 2010-07-28 | 淮阴工学院 | Method for purifying and ageing wine |
| CN101787339A (en) * | 2010-03-18 | 2010-07-28 | 淮阴工学院 | Attapulgite clay-based purifying and aging agent used for wine and preparation method thereof |
| CN106554896A (en) * | 2016-10-31 | 2017-04-05 | 山东鸿兴源食品有限公司 | A kind of cooking wine clarifier and preparation method thereof |
| CN114988987A (en) * | 2022-06-29 | 2022-09-02 | 陕西华泰生物精细化工有限公司 | Extraction method of peach carin phenol |
-
2004
- 2004-06-25 CN CN 200410041077 patent/CN1594537A/en active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101787340A (en) * | 2010-03-18 | 2010-07-28 | 淮阴工学院 | Method for purifying and ageing wine |
| CN101787339A (en) * | 2010-03-18 | 2010-07-28 | 淮阴工学院 | Attapulgite clay-based purifying and aging agent used for wine and preparation method thereof |
| CN101787340B (en) * | 2010-03-18 | 2012-04-04 | 淮阴工学院 | Method for purifying and ageing wine |
| CN101787339B (en) * | 2010-03-18 | 2012-07-18 | 淮阴工学院 | Attapulgite clay-based purifying and aging agent used for wine and preparation method thereof |
| CN106554896A (en) * | 2016-10-31 | 2017-04-05 | 山东鸿兴源食品有限公司 | A kind of cooking wine clarifier and preparation method thereof |
| CN114988987A (en) * | 2022-06-29 | 2022-09-02 | 陕西华泰生物精细化工有限公司 | Extraction method of peach carin phenol |
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