CN1594478A - Vinyl ester resin building steel-bar-planting glue and preparation method thereof - Google Patents
Vinyl ester resin building steel-bar-planting glue and preparation method thereof Download PDFInfo
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- CN1594478A CN1594478A CN 200410013427 CN200410013427A CN1594478A CN 1594478 A CN1594478 A CN 1594478A CN 200410013427 CN200410013427 CN 200410013427 CN 200410013427 A CN200410013427 A CN 200410013427A CN 1594478 A CN1594478 A CN 1594478A
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Abstract
The invention discloses a vinyl ester resin building steel-bar-planting glue and preparation method thereof, wherein the glue comprises component A and component B by the weight ratio of 100 : 1-3, the component A comprises vinyl ester resin 30-45%, thickening agent 4-10%, filling material 40-55%, toughening agent 5-10%, defoaming agent 0.05-0.5%, coupling agent 0.05-0.5%, polymerization inhibitor 0.05-0.3%, accelerating agent 0.05-0.5%, and the component B comprises curing agent 50-70%, thinning agent 10-30%, filling material 10-30%, pigment 1-2%.
Description
Technical field
The present invention relates to the chemical raw material field, particularly vinyl ester resin building bar planting glue and preparation method thereof.
Background technology
Along with construction industry greatly develop and construction structure glue is given birth to the widespread usage of muscle technology, the consumption of tackiness agent is increasing.Original adhesive technology and tackiness agent have many weak points.With thermally melting glue or polystyrene glue, the low molecular solvent more than 40% is wherein arranged, be unfavorable for that the decoration construction personnel's is healthy; Domesticly now mainly be mixed with glue with the Resins, epoxy scene, construction is inconvenient; Also useful epoxy or vinylformic acid preparation two component adhesive, but have that fragility is big, the volatilization deal is big, polluted air, gelatin viscosity are low, shortcomings such as trickling phenomenon and preservation period be short occur.
Summary of the invention
Problem to be solved by this invention is: at above-mentioned prior art, propose quick solidifying under a kind of normal temperature, pollution-free, bonding firmly and long vinyl ester resin building bar planting glue of good toughness, retention period and preparation method thereof.
The present invention for the technical scheme that problem adopted of the above-mentioned proposition of solution is: it is formed by first component and second component mixed preparing, the mixing match of first component and second component is 100: 1～3 by weight, the component concentration of described first component is vinyl ester resin 30～45% by weight, thickening material 4～10%, filler 40～55%, toughner 5～10%, defoamer 0.05～0.5%, coupling agent 0.05～0.5%, stopper 0.05～0.3%, promotor 0.05～0.5%, the component weight percentage sum is 100%
The component concentration of described second component is solidifying agent 50～70%, thinner 10～30%, filler 10～30%, pigment 1～2% by weight, and each component weight percentage sum is 100%.
Press such scheme, the mixing match of described first component and second component is 100: 1.5～2.5 by weight, the component concentration of described first component is vinyl ester resin 35～40%, thickening material 4～6%, filler 50～55%, toughner 5～7%, defoamer 0.1～0.3%, coupling agent 0.05～0.2%, stopper 0.2～0.3%, promotor 0.2～0.5% by weight, the component weight percentage sum is 100%
The component concentration of described second component is solidifying agent 50～55%, thinner 16～24%, filler 25～30%, pigment 1～2% by weight, and each component weight percentage sum is 100%.
Press such scheme, the thickening material in the described first component is one or more the mixing in crystallinity unsaturated polyester resin, aerosil, staybelite, WE polyethylene wax, the organobentonite.
Press such scheme, the solidifying agent in the described second component is one or more the mixing in benzoyl peroxide, peroxidation 2,4 dichloro benzene formyl, dicumyl peroxide, the peroxidation tert-butyl ester, cyclohexanone peroxide, the methylethyl ketone peroxide.
Press such scheme, the promotor in the described first component is NN-xylidine, NN-Diethyl Aniline, NN-diformazan to one or more the mixing in aniline, cobalt naphthenate, the cobalt iso-octoate.
Press such scheme, the toughner in the described first component is one or more the mixing in liquid polysulfide rubber, liquid acrylonitrile butadiene rubber, polysulfones, the urethane.
Press such scheme, the stopper in the described first component is one or more the mixing in benzoquinones, naphthoquinones, Resorcinol, oil of mirbane, t-butyl catechol, the hydroquinone monomethyl ether.
Press such scheme, the filler in described first component and the second component is one or more the mixing in aluminium powder, copper powder, iron powder, aluminum oxide, pure aluminium silicate, zirconium silicate, titanium dioxide, talcum powder, ground dolomite, the silica powder.
Press such scheme, the pigment in the described second component is to get any one in carbon black, red iron oxide, medium chrome yellow medium yellow, the iron oxide green.
Press such scheme, the defoamer in the described first component is one or both the mixing among methyl-silicone oil, the BYKA-555.
Press such scheme, the coupling agent in the described first component is one or both the mixing in γ-An Bingjisanyiyangjiguiwan, γ-(2,3 glycidoxy) propyl-triethoxysilicane.
Press such scheme, the thinner in the described second component is a dibutyl phthalate (DBP).
Described vinyl ester resin building bar planting glue preparation method's technical scheme is characterized in that may further comprise the steps and makes:
(1) preparation of first component: Vinylite 30～45%, thickening material 4～10%, promotor 0.05～0.5%, defoamer 0.05～0.5%, coupling agent 0.05～0.5%, stopper 0.05～0.3%, the toughner 5～10% of first component are poured in the stirring tank successively, poured into while stirring when pouring into; Again filler 40～55% is added in the stirring tank after stirring, pour into while stirring, mix thoroughly, stirring tank is warming up to 60～80 ℃ then, vacuumize, stir 1.5～2.5h, it is mixed promptly get the first component;
(2) preparation of second component: the solidifying agent 50～70% of second component mixed with thinner 10～30% mix thoroughly, again filler 10～30% and pigment 1～2% are added in the mixed solution, add and fashionablely add while stirring, mix thoroughly and can promptly get the second component,
(3) mixed preparing: the second component that first component that step (1) is made and step (2) make is that 100: 1～3 mixed preparing promptly get vinyl ester resin building bar planting glue by weight.
The using method of vinyl ester resin building bar planting glue: normal use can be in the first component: the ratio of second component=100: 1～3 is transferred and is mixed even use, preferred first component: in second component=100: 1.5～2.5 or the two-tube packing bottle that makes in this ratio of packing into, the extruding back is mixed by the bottleneck mixing device.Initial set about 6 minutes, completely solidified after 45 minutes if wish that set time, the longer or shorter consumption that increases solidifying agent that subtracts was regulated, can not influence solidified intensity and other effect, and is simple and convenient.
Tackiness agent of the present invention adopts Vinylite to make the main raw of tackiness agent, selects suitable curing and accelerating system for use, and the resistance aggressiveness system of no-float divides two components packing.Make this kind tackiness agent that many advantages be arranged: can solidify under the quick solidifying under the normal temperature, low temperature; Be convenient to operation; Smell is little, solidifies the back odorlessness, and is pollution-free; Solidification intensity is higher, and bonding firmly; Good toughness; Preserve and long service life.
Specific embodiments
Embodiment 1
With the MFE-3 vinyl vibrin of first component (magnificent prosperous polymkeric substance company limited produce) 35%, crystallinity unsaturated polyester resin Crystic Impreg (ScottBacler company) 5%, NN-Diethyl Aniline 0.3%, BYKA-555 (German Bi Ke chemical company produce) 0.2%, KH-560 (γ-(2, propyl-triethoxysilicane) 0.1% 3 glycidoxies), t-butyl catechol 0.1%, benzoquinones 0.2%, liquid polysulfide rubber 6% pour in the stirring tank successively, pour into while stirring when pouring into; After stirring again with silica powder (150 order) 50%, aluminium powder: 3% (325 order) adds in the stirring tank, pours into while stirring, mixes thoroughly, stirring tank is warming up to 70 ℃ then, vacuumizes, and stirs 2h and promptly gets the first component;
The benzoyl peroxide 50% of second component mixed with dibutyl phthalate (DBP) 20% mix thoroughly, again silica powder (150 order) 28% and carbon black 2% are added in the mixed solution, add and fashionablely add while stirring, mix thoroughly and promptly get the second component.
During use with the first component: the ratio of second component=100: 2.5 transfer mix evenly vinyl ester resin building bar planting glue.
Embodiment 2
The MFE-3 vinyl vibrin of first component (magnificent prosperous polymkeric substance company limited produce) 36%, crystallinity unsaturated polyester resin Crystic Impreg 5%, cobalt naphthenate 0.3%, NN-Diethyl Aniline 0.05%, BYKA-555 (German Bi Ke chemical company produce) 0.2%, KH-560 0.05%, t-butyl catechol 0.1%, naphthoquinones 0.2%, liquid polysulfide rubber 5% are poured in the stirring tank successively, poured into while stirring when pouring into; Again silica powder (150 order) 50%, aluminium powder 3% (325 order) are added in the stirring tank after stirring, pour into while stirring, mix thoroughly, stirring tank is warming up to 70 ℃ then, vacuumize, stir 2h and promptly get the first component;
The cyclohexanone peroxide 50% of second component mixed with dibutyl phthalate (DBP) 20% mix thoroughly, again silica powder (150 order) 28% and red iron oxide 2% are added in the mixed solution, add and fashionablely add while stirring, mix thoroughly and promptly get the second component.
During use with the first component: the ratio of second component=100: 1.5 transfer mix evenly vinyl ester resin building bar planting glue.
Embodiment 3
The MFE-3 vinyl vibrin of first component (magnificent prosperous polymkeric substance company limited produce) 38%, organobentonite 2%, aerosil 2%, NN-Diethyl Aniline 0.3%, methyl-silicone oil 0.2%, KH-550 (γ-An Bingjisanyiyangjiguiwan) 0.1%, t-butyl catechol 0.1%, Resorcinol 0.2%, liquid acrylonitrile butadiene rubber 6% are poured in the stirring tank successively, poured into while stirring when pouring into; Again silica powder (150 order) 48%, iron powder 3% are added in the stirring tank after stirring, pour into while stirring, mix thoroughly, stirring tank is warming up to 70 ℃ then, vacuumize, stir 2h and promptly get the first component;
The benzoyl peroxide 50% of second component mixed with dibutyl phthalate (DBP) 20% mix thoroughly, again silica powder (150 order) 25% and iron oxide green 2% are added in the mixed solution, add and fashionablely add while stirring, mix thoroughly and promptly get the second component.
During use with the first component: the ratio of second component=100: 1.5 transfer mix evenly vinyl ester resin building bar planting glue.
Claims (13)
1. vinyl ester resin is built bar planting glue, it is characterized in that forming by first component and second component mixed preparing, the mixing match of first component and second component is 100: 1～3 by weight, the component concentration of described first component is vinyl ester resin 30～45% by weight, thickening material 4～10%, filler 40～55%, toughner 5～10%, defoamer 0.05～0.5%, coupling agent 0.05～0.5%, stopper 0.05～0.3%, promotor 0.05～0.5%, the component weight percentage sum is 100%
The component concentration of described second component is solidifying agent 50～70%, thinner 10～30%, filler 10～30%, pigment 1～2% by weight, and each component weight percentage sum is 100%.
2. by the described vinyl ester resin building of claim 1 bar planting glue, the mixing match that it is characterized in that first component and second component is 100: 1.5～2.5 by weight, the component concentration of described first component is vinyl ester resin 35～40%, thickening material 4～6%, filler 50～55%, toughner 5～7%, defoamer 0.1～0.3%, coupling agent 0.05～0.2%, stopper 0.2～0.3%, promotor 0.2～0.5% by weight, the component weight percentage sum is 100%
The component concentration of described second component is solidifying agent 50～55%, thinner 16～24%, filler 25～30%, pigment 1～2% by weight, and each component weight percentage sum is 100%.
3. by claim 1 or 2 described vinyl ester resins building bar planting glue, it is characterized in that thickening material in the described first component is one or more the mixing in crystallinity unsaturated polyester resin, aerosil, staybelite, WE polyethylene wax, the organobentonite.
4. by claim 1 or 2 described vinyl ester resin building bar planting glue, it is characterized in that solidifying agent in the described second component is one or more the mixing in benzoyl peroxide, peroxidation 2,4 dichloro benzene formyl, dicumyl peroxide, the peroxidation tert-butyl ester, cyclohexanone peroxide, the methylethyl ketone peroxide.
5. by claim 1 or 2 described vinyl ester resins building bar planting glue, the promotor in the described first component is NN-xylidine, NN-Diethyl Aniline, NN-diformazan to one or more the mixing in aniline, cobalt naphthenate, the cobalt iso-octoate.
6. by claim 1 or 2 described vinyl ester resins building bar planting glue, the toughner in the described first component is one or more the mixing in liquid polysulfide rubber, liquid acrylonitrile butadiene rubber, polysulfones, the urethane.
7. by claim 1 or 2 described vinyl ester resins building bar planting glue, the stopper in the described first component is one or more the mixing in benzoquinones, naphthoquinones, Resorcinol, oil of mirbane, t-butyl catechol, the hydroquinone monomethyl ether.
8. by claim 1 or 2 described vinyl ester resins building bar planting glue, the filler in described first component and the second component is one or more the mixing in aluminium powder, copper powder, iron powder, aluminum oxide, pure aluminium silicate, zirconium silicate, titanium dioxide, talcum powder, ground dolomite, the silica powder.
9. by claim 1 or 2 described vinyl ester resin building bar planting glue, the pigment in the described second component is to get any one in carbon black, red iron oxide, medium chrome yellow medium yellow, the iron oxide green.
10. by claim 1 or 2 described vinyl ester resins building bar planting glue, the defoamer in the described first component is one or both the mixing among methyl-silicone oil, the BYKA-555.
11. by claim 1 or 2 described vinyl ester resins building bar planting glue, the coupling agent in the described first component is one or both the mixing in γ-An Bingjisanyiyangjiguiwan, γ-(2,3 glycidoxy) propyl-triethoxysilicane.
12. by claim 1 or 2 described vinyl ester resin building bar planting glue, the thinner in the described second component is a dibutyl phthalate (DBP).
13, a kind of method for preparing claim 1 vinyl ester resin building bar planting glue is characterized in that may further comprise the steps and makes:
(1) preparation of first component: Vinylite 30～45%, thickening material 4～10%, promotor 0.05～0.5%, defoamer 0.05～0.5%, coupling agent 0.05～0.5%, stopper 0.05～0.3%, the toughner 5～10% of first component are poured in the stirring tank successively, poured into while stirring when pouring into; Again filler 40～55% is added in the stirring tank after stirring, pour into while stirring, mix thoroughly, stirring tank is warming up to 60～80 ℃ then, vacuumize, stir 1.5～2.5h, it is mixed promptly get the first component;
(2) preparation of second component: the solidifying agent 50～70% of second component mixed with thinner 10～30% mix thoroughly, again filler 10～30% and pigment 1～2% are added in the mixed solution, add and fashionablely add while stirring, mix thoroughly and can promptly get the second component,
(3) mixed preparing: the second component that first component that step (1) is made and step (2) make is that 100: 1～3 mixed preparing promptly get vinyl ester resin building bar planting glue by weight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN 200410013427 CN1235999C (en) | 2004-07-07 | 2004-07-07 | Vinyl ester resin building steel-bar-planting glue and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN 200410013427 CN1235999C (en) | 2004-07-07 | 2004-07-07 | Vinyl ester resin building steel-bar-planting glue and preparation method thereof |
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| CN1235999C CN1235999C (en) | 2006-01-11 |
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Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101974304A (en) * | 2010-11-08 | 2011-02-16 | 武汉理工大学 | Vinylester resin stone adhesive and preparation method thereof |
| CN102559120A (en) * | 2011-12-30 | 2012-07-11 | 浙江天和树脂有限公司 | Temperature-resistant, corrosion-resistant and high-adhesion adhesive and preparation method thereof |
| CN102604590A (en) * | 2012-03-01 | 2012-07-25 | 环球石材（福建）有限公司 | Silica glue, preparation technology thereof, and technology for reinforcing rough stone material by using silica glue |
| CN102807715A (en) * | 2012-07-27 | 2012-12-05 | 苏州市兴吴工程塑胶有限公司 | Formula of toughened polystyrene plastic |
| CN102994033A (en) * | 2012-10-31 | 2013-03-27 | 安徽东方金河精密机械制造有限公司 | Polyester adhesive |
| CN104830241A (en) * | 2015-05-26 | 2015-08-12 | 李亮军 | High-strength binder composition |
| CN105441004A (en) * | 2015-12-01 | 2016-03-30 | 武汉市科达云石护理材料有限公司 | Flame-retardant vinyl type anchor adhesive |
| CN106367004A (en) * | 2016-08-27 | 2017-02-01 | 安徽天瞳智能科技有限公司 | Resin adhesive with good toughness and high bonding strength |
| CN107324717A (en) * | 2017-06-28 | 2017-11-07 | 常州市尚泽纺织品有限公司 | A kind of inorganic anchoring adhesive and preparation method thereof |
| CN107603159A (en) * | 2017-09-18 | 2018-01-19 | 张家港九力新材料科技有限公司 | A kind of flame retardant type compounding vinyl alkyd and preparation method thereof |
| CN109337299A (en) * | 2018-09-11 | 2019-02-15 | 法施达(大连)工程材料有限公司 | A kind of modified vinyl anchoring adhesive and preparation method thereof |
| CN110003835A (en) * | 2019-04-22 | 2019-07-12 | 湖北坤能科技有限公司 | Anchor Agent and its preparation and application for railway maintenance |
| CN110105932A (en) * | 2019-04-19 | 2019-08-09 | 中国石油天然气股份有限公司 | A kind of oil/gas well sleeve plugging resin material and preparation method thereof |
| CN110218025A (en) * | 2019-04-18 | 2019-09-10 | 广东家康新材料有限公司 | A kind of high durable environmentally friendly granite sink and preparation method thereof |
| CN116218150A (en) * | 2023-03-31 | 2023-06-06 | 武汉联影医疗科技有限公司 | Matching material and application and preparation method thereof |
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2004
- 2004-07-07 CN CN 200410013427 patent/CN1235999C/en active Active
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101974304A (en) * | 2010-11-08 | 2011-02-16 | 武汉理工大学 | Vinylester resin stone adhesive and preparation method thereof |
| CN102559120A (en) * | 2011-12-30 | 2012-07-11 | 浙江天和树脂有限公司 | Temperature-resistant, corrosion-resistant and high-adhesion adhesive and preparation method thereof |
| CN102559120B (en) * | 2011-12-30 | 2013-11-06 | 浙江天和树脂有限公司 | Temperature-resistant, corrosion-resistant and high-adhesion adhesive and preparation method thereof |
| CN102604590A (en) * | 2012-03-01 | 2012-07-25 | 环球石材（福建）有限公司 | Silica glue, preparation technology thereof, and technology for reinforcing rough stone material by using silica glue |
| CN102807715A (en) * | 2012-07-27 | 2012-12-05 | 苏州市兴吴工程塑胶有限公司 | Formula of toughened polystyrene plastic |
| CN102994033A (en) * | 2012-10-31 | 2013-03-27 | 安徽东方金河精密机械制造有限公司 | Polyester adhesive |
| CN102994033B (en) * | 2012-10-31 | 2014-01-08 | 安徽东方金河精密机械制造有限公司 | Polyester adhesive |
| CN104830241A (en) * | 2015-05-26 | 2015-08-12 | 李亮军 | High-strength binder composition |
| CN105441004A (en) * | 2015-12-01 | 2016-03-30 | 武汉市科达云石护理材料有限公司 | Flame-retardant vinyl type anchor adhesive |
| CN106367004A (en) * | 2016-08-27 | 2017-02-01 | 安徽天瞳智能科技有限公司 | Resin adhesive with good toughness and high bonding strength |
| CN107324717A (en) * | 2017-06-28 | 2017-11-07 | 常州市尚泽纺织品有限公司 | A kind of inorganic anchoring adhesive and preparation method thereof |
| CN107603159A (en) * | 2017-09-18 | 2018-01-19 | 张家港九力新材料科技有限公司 | A kind of flame retardant type compounding vinyl alkyd and preparation method thereof |
| CN107603159B (en) * | 2017-09-18 | 2020-02-04 | 张家港九力新材料科技有限公司 | Flame-retardant compound vinyl alkyd resin and preparation method thereof |
| CN109337299A (en) * | 2018-09-11 | 2019-02-15 | 法施达(大连)工程材料有限公司 | A kind of modified vinyl anchoring adhesive and preparation method thereof |
| CN109337299B (en) * | 2018-09-11 | 2021-02-02 | 法施达(大连)实业集团有限公司 | Modified vinyl bar-planting adhesive and preparation method thereof |
| CN110218025A (en) * | 2019-04-18 | 2019-09-10 | 广东家康新材料有限公司 | A kind of high durable environmentally friendly granite sink and preparation method thereof |
| CN110105932A (en) * | 2019-04-19 | 2019-08-09 | 中国石油天然气股份有限公司 | A kind of oil/gas well sleeve plugging resin material and preparation method thereof |
| CN110105932B (en) * | 2019-04-19 | 2021-03-09 | 中国石油天然气股份有限公司 | Resin material for plugging oil-gas well casing and preparation method thereof |
| CN110003835A (en) * | 2019-04-22 | 2019-07-12 | 湖北坤能科技有限公司 | Anchor Agent and its preparation and application for railway maintenance |
| CN110003835B (en) * | 2019-04-22 | 2021-06-08 | 湖北坤能科技有限公司 | Anchoring agent for railway maintenance and preparation and application methods thereof |
| CN116218150A (en) * | 2023-03-31 | 2023-06-06 | 武汉联影医疗科技有限公司 | Matching material and application and preparation method thereof |
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