CN1563932A - Method of sampling greenhouse gas by utilizing gas balance bag - Google Patents

Method of sampling greenhouse gas by utilizing gas balance bag Download PDF

Info

Publication number
CN1563932A
CN1563932A CN 200410017545 CN200410017545A CN1563932A CN 1563932 A CN1563932 A CN 1563932A CN 200410017545 CN200410017545 CN 200410017545 CN 200410017545 A CN200410017545 A CN 200410017545A CN 1563932 A CN1563932 A CN 1563932A
Authority
CN
China
Prior art keywords
gas
case
soil
bag
sampling
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN 200410017545
Other languages
Chinese (zh)
Other versions
CN1258079C (en
Inventor
胡湛波
严立
孔海南
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Jiaotong University
Original Assignee
Shanghai Jiaotong University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shanghai Jiaotong University filed Critical Shanghai Jiaotong University
Priority to CN 200410017545 priority Critical patent/CN1258079C/en
Publication of CN1563932A publication Critical patent/CN1563932A/en
Application granted granted Critical
Publication of CN1258079C publication Critical patent/CN1258079C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Landscapes

  • Sampling And Sample Adjustment (AREA)

Abstract

A gas balance bag is put into a closed box in use for measuring gas flux discharged by soil or plants. An amount of air is filled into the gas balance bag from small hole in the closed box, making the gas balance bag expand so as to take up certain volume in the closed box. Then, extracting gas measuring and calculating processed result are carried out according to traditional method suitable to closed box. The gas balance bag adjusts consistent air pressure between inside box and outside box. Comparing with measuring in site or in lab, the invention measures gas flux discharged by soil or plants accurately and reduces error.

Description

Utilize the gas equilibrium bag to carry out the method for greenhouse gases sampling
Technical field
The present invention relates to a kind of method of utilizing the gas equilibrium bag to carry out the greenhouse gases sampling, be specifically related to a kind of method of measuring soil or plant discharging greenhouse gases flux.Belong to the gas sampling technical field.
Background technology
It is one of research focus of current whole world concern that terrestrial climate warms, the N that mankind's activity produces 2O, CH 4Isothermal chamber gas is ascendant trend year by year, is the key factor that causes global greenhouse effect.According to Intergovernmental Panel on Climate Change (IPCC), in mankind's activity, the N that agricultural production and sewage disposal process produce 2O, CH 4Isothermal chamber gas comprises 19%.In more than 10 year, the flux mensuration that produces greenhouse gases about agricultural tillage, grassland, wetland, sewage disposal process is the focus of research greenhouse gases, and a large amount of relevant reports are arranged in the past.At the research process of greenhouse gases, measure emission flux of gas accurately whether, bring significant impact can for the emission flux and the decision-making reduction of discharging measure of assessment greenhouse gases.
About measuring the method for soil or plant emission flux of gas, what be widely used at present is traditional fully sheathed case method.The Chinese patent of applying for disclosed mensuration soil gas emission flux has: " a kind of method of measuring discharging quantity of gas from farmland greenhouse " (application number: 97111901.5), its principle mainly is to manage target soil or the plant casing with a sealing is covered, the gas that target soil or plant are produced is collected in the casing of certain volume fully, regularly, calculate the flux of greenhouse gases again with the gas concentration in the sampling thief sampling determination casing.
Traditional assay method of plant discharging greenhouse gases is by relatively soil---the object gas emission flux of botanical system and bare area soil is studied the gaseous emission contribution of plant in system.Apply for Chinese patent " dry crop directly discharges the field in-situ determination method of nitrous oxide the flux " (application number: 01127917.6) of disclosed mensuration plant emission flux of gas, change the traditional plant emission gases and measure thinking, be that the material of plant base stem portion with emissions object gas not coated and with film the soil around the basic stem covered, make the gas of the soil discharging under the target plant can not enter the casing that covers plant, adopt conventional fully sheathed case method to measure gas flux then.
Yet more than existing method all exists error bigger, can not accurately measure target soil, plant emission flux of gas.Cause a bigger common cause of resultant error to be: the gas sampling process has been ignored sampling loading pressure and the outer inconsistent problem of atmospheric pressure of case, makes sampling process can not truly reflect target soil or the plant gaseous emission rule under state of nature.To measure CH 4Be example, in traditional fully sheathed case method of sampling, each about 1 hour of sampling time.The CH that in fully sheathed case, discharges with soil 4Gas flow increases, and makes CH in the case 4Concentration (CH 4Dividing potential drop) rises gradually, cause total air pressure (CH in the case 4Dividing potential drop and atmospheric pressure sum) greater than the outer atmospheric pressure of case.This pressure reduction is particularly evident at the later stage and the big sampled point of greenhouse gas emission flux of sampling, the soil discharging CH that consequently fully sheathed case covered 4Be suppressed, the speed of emission gases reduces in case, is not the true reflection of original-state soil to airborne release greenhouse gases speed.Another error is to occur in the moment of sampling.With the moment of special-purpose gas production bottle or the about 200ml gas of syringe extraction, because the air pressure outside the case, impels soil unusual discharging CH in case greater than the case internal gas pressure 4Gas can not truly reflect the gaseous emission speed of soil.
The basic reason that produces above error is the inside and outside gaseous tension imbalance of sampling box, makes the drainage rate of soil or plant acceleration (or slowing down) greenhouse gases, causes the error at measurment of soil or plant greenhouse emission flux of gas.
Summary of the invention
The objective of the invention is at the deficiencies in the prior art, provide a kind of gas equilibrium bag that utilizes to carry out the greenhouse gases method of sampling, can automatic control stuff box inside and outside gas equilibrium reduces the gas sampling error.
For realizing such purpose, the present invention is provided with a gas equilibrium bag in the fully sheathed case of measuring soil or plant discharging gas flux, fill an amount of air for the gas equilibrium bag with special-purpose air pump by the aperture of opening on the fully sheathed case, make the expansion of gas equilibrium bag and occupy certain volume in the fully sheathed case, then by traditional fully sheathed case conventional method extracting gases, mensuration, computing result.The gas equilibrium bag can be consistent by the regulating box inner and outer air pressure, thereby realizes accurately measuring the greenhouse gas emission flux of soil or plant.
Method of the present invention is specific as follows:
1, is manufactured with the sampling box of gas equilibrium bag: the aperture of on the common closed box of gathering gas, opening an about 5-10mm, with the openend of gas equilibrium bag by stretching out in the case outside case, and be fixed on the tank wall of fully sheathed case tapping, keep the gas in the polybag to communicate with atmosphere by perforate.The gas equilibrium bag can adopt common plastic film to make, and size is: 50 * 100mm, film thickness is: 0.5~1.5mm.
2, before fully sheathed case covers target soil or plant, with hand air pump or blow up a balloon and fill an amount of air in the case gas equilibrium bag, make the gas equilibrium bag be expanded to about 2/3rds volumes and get final product by the perforate on the fully sheathed case.
3, extracting gases, analysis, calculating obtain the result of the greenhouse gas emission flux of target soil or plant.
In gas production mensuration process, when in the fully sheathed case since the greenhouse gases of soil or plant discharging cause the case internal gas pressure greater than case outside during atmospheric pressure, the gas equilibrium bag is extruded and dwindles, get rid of air in a certain amount of bag by the aperture of opening on the fully sheathed case, promptly be consistent by the air pressure inside and outside the gas equilibrium bag regulating box in the case.And in the moment with the sampling needle sampling, when the sealing loading pressure reduces, the outer air of fully sheathed case can enter the gas equilibrium bag in the case by the aperture on the fully sheathed case, and the case inner and outer air pressure is consistent, and avoids the speed moment increasing of soil or plant emission gases in case.
The present invention realizes easily, simple to operate, can measure the flux of soil or plant discharging greenhouse gases truly, exactly, reduce the error at measurment of in-site detecting and laboratory study, can be used for assessing the flux that physical environment, agricultural, industry and sewage treatment project produce greenhouse gases, instruct and produce and research.
Description of drawings
Fig. 1 is the sampling box structural representation of the band gas equilibrium bag of the present invention's employing.
Among the figure, 1 is gas sample tube, and 2 is the sampling box casing, and 3 is aperture, and 4 is the gas equilibrium bag.
Embodiment
Below in conjunction with drawings and Examples technical scheme of the present invention is further described.
The sampling box of the band gas equilibrium bag that the present invention adopts as shown in Figure 1, sampling box is made up of gas sample tube 1, the sampling box casing 2 that has aperture 3, gas equilibrium bag 4.
Embodiment: polluted water land processing procedure soil produces the flux of greenhouse gases and measures
1, is manufactured with the sampling box of gas equilibrium bag
Be made into the body structure of 300 * 300 * 400mm with the thick organic glass of 5mm, the top is provided with the tracheae of gas production, open the aperture of an about 8mm at tank wall, (size is: 50 * 100mm with a polybag, film thickness is: openend 1.0mm) is by stretching out in the case outside case, stick with glue agent then the film of the openend of polybag is fixed on the tank wall of fully sheathed case tapping, keep the gas in the polybag to communicate with atmosphere by perforate;
2, before fully sheathed case covers the soil of disposing of sewage, fill air for the case inner plastic bag with blowing up a balloon by the perforate on the fully sheathed case, make polybag be expanded to about 2/3rds volumes and get final product;
3, with above sealing case lid on the soil that needs are measured, base inserts soil 50mm;
4, press designing requirement with sampling needle, every 15 minutes extracting gases samples once, with the N in the chromatography of gases analytic sample 2O, CH 4, obtain the flux of sewage disposal system soil emission greenhouse gas.
In gas production mensuration process, when in the fully sheathed case since the greenhouse gases of soil or plant discharging cause the case internal gas pressure greater than case outside during atmospheric pressure, the gas equilibrium bag is extruded and dwindles, and gets rid of air in a certain amount of bag by the aperture of opening on the fully sheathed case, and the inside and outside air pressure of regulating box is consistent.And in the moment with the sampling needle sampling, when the sealing loading pressure reduced, the outer air of fully sheathed case can enter the gas equilibrium bag in the case by the aperture on the fully sheathed case, and the case inner and outer air pressure is consistent.The present invention can measure the flux of soil or plant discharging greenhouse gases truly, exactly, reduces the error at measurment of in-site detecting and laboratory study.

Claims (1)

1, a kind of method of utilizing the gas equilibrium bag to carry out the greenhouse gases sampling, it is characterized in that on the closed box of gathering gas, opening the aperture of a 5-10mm, with size is 50 * 100mm, film thickness is that the openend of gas equilibrium bag of 0.5~1.5mm is by stretching out in the case outside case, and be fixed on the tank wall of fully sheathed case tapping, keep the gas in the gas equilibrium bag to communicate with atmosphere by perforate, before fully sheathed case covers target soil or plant, give gas equilibrium bag filling air in the case by the perforate on the fully sheathed case, make the gas equilibrium bag be expanded to 2/3rds volumes, extracting gases according to a conventional method then, analyze, calculate, obtain the result of the greenhouse gas emission flux of target soil or plant.
CN 200410017545 2004-04-08 2004-04-08 Method of sampling greenhouse gas by utilizing gas balance bag Expired - Fee Related CN1258079C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 200410017545 CN1258079C (en) 2004-04-08 2004-04-08 Method of sampling greenhouse gas by utilizing gas balance bag

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 200410017545 CN1258079C (en) 2004-04-08 2004-04-08 Method of sampling greenhouse gas by utilizing gas balance bag

Publications (2)

Publication Number Publication Date
CN1563932A true CN1563932A (en) 2005-01-12
CN1258079C CN1258079C (en) 2006-05-31

Family

ID=34479030

Family Applications (1)

Application Number Title Priority Date Filing Date
CN 200410017545 Expired - Fee Related CN1258079C (en) 2004-04-08 2004-04-08 Method of sampling greenhouse gas by utilizing gas balance bag

Country Status (1)

Country Link
CN (1) CN1258079C (en)

Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101839840A (en) * 2010-04-09 2010-09-22 南京化工职业技术学院 Plant monitor for indoor air
CN102252876A (en) * 2011-06-13 2011-11-23 浙江省农业科学院 Buffer type soil gas sampling device
CN105258982A (en) * 2015-09-21 2016-01-20 浙江省农业科学院 Dry land gas collector
CN105866275A (en) * 2016-04-05 2016-08-17 济宁神农画圆生态系统模式推广有限公司 Method and device for quantitative analysis on nitrogen-oxygen absorption capacity of nitrogen-fixing bacteria in sealed container
CN105973652A (en) * 2016-06-30 2016-09-28 东莞市升微机电设备科技有限公司 Closed-cabin sampling system
CN106093312A (en) * 2016-08-08 2016-11-09 东莞市升微机电设备科技有限公司 There is the abnormal smells from the patient of illumination test function, VOC and floating harmful substance detection cabin
CN106093311A (en) * 2016-08-08 2016-11-09 北京市产品质量监督检验院 Abnormal smells from the patient, VOC and floating harmful substance test device
CN106248880A (en) * 2016-08-08 2016-12-21 东莞市升微机电设备科技有限公司 There is the abnormal smells from the patient of External Circulation Filtration Apparatus, VOC and floating harmful substance detection cabin
CN106525135A (en) * 2016-11-30 2017-03-22 中国科学院大气物理研究所 Enclosed type automatic observation box for substance flux
CN106770933A (en) * 2016-11-30 2017-05-31 中国科学院大气物理研究所 The system and method for box method species flux automatic Observation
CN107328633A (en) * 2017-07-27 2017-11-07 防灾科技学院 A kind of degasser and its application
CN108489845A (en) * 2018-03-01 2018-09-04 四川大学 By packing the method for weighing and measuring dam flood-discharge atomizing concentration
CN108594915A (en) * 2018-06-27 2018-09-28 东莞市升微机电设备科技有限公司 A kind of confined chamber and control method of volume adjustable
CN109374366A (en) * 2018-11-07 2019-02-22 中国科学院东北地理与农业生态研究所 A kind of the soil gas acquisition device and its application method of variable volume
CN110501192A (en) * 2019-08-21 2019-11-26 中国水利水电科学研究院 A kind of constant temperature, closed soil respiration collection device
CN114441242A (en) * 2020-11-02 2022-05-06 中国石油化工股份有限公司 Gas collecting bottle and using method and application thereof

Cited By (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101839840A (en) * 2010-04-09 2010-09-22 南京化工职业技术学院 Plant monitor for indoor air
CN102252876A (en) * 2011-06-13 2011-11-23 浙江省农业科学院 Buffer type soil gas sampling device
CN105258982B (en) * 2015-09-21 2017-11-24 浙江省农业科学院 Nonirrigated farmland gas collector
CN105258982A (en) * 2015-09-21 2016-01-20 浙江省农业科学院 Dry land gas collector
CN105866275A (en) * 2016-04-05 2016-08-17 济宁神农画圆生态系统模式推广有限公司 Method and device for quantitative analysis on nitrogen-oxygen absorption capacity of nitrogen-fixing bacteria in sealed container
CN105973652A (en) * 2016-06-30 2016-09-28 东莞市升微机电设备科技有限公司 Closed-cabin sampling system
CN112903374A (en) * 2016-06-30 2021-06-04 东莞市升微机电设备科技有限公司 Closed cabin sampling system
CN106093311A (en) * 2016-08-08 2016-11-09 北京市产品质量监督检验院 Abnormal smells from the patient, VOC and floating harmful substance test device
CN106248880A (en) * 2016-08-08 2016-12-21 东莞市升微机电设备科技有限公司 There is the abnormal smells from the patient of External Circulation Filtration Apparatus, VOC and floating harmful substance detection cabin
CN106093312A (en) * 2016-08-08 2016-11-09 东莞市升微机电设备科技有限公司 There is the abnormal smells from the patient of illumination test function, VOC and floating harmful substance detection cabin
CN106248880B (en) * 2016-08-08 2018-09-28 东莞市升微机电设备科技有限公司 Smell, VOC and floating harmful substance with External Circulation Filtration Apparatus detect cabin
CN106093311B (en) * 2016-08-08 2019-03-19 北京市产品质量监督检验院 Smell, VOC and floating harmful substance test device
CN106525135A (en) * 2016-11-30 2017-03-22 中国科学院大气物理研究所 Enclosed type automatic observation box for substance flux
CN106770933A (en) * 2016-11-30 2017-05-31 中国科学院大气物理研究所 The system and method for box method species flux automatic Observation
CN106770933B (en) * 2016-11-30 2019-04-23 中国科学院大气物理研究所 The system and method for box method species flux automatic Observation
CN107328633A (en) * 2017-07-27 2017-11-07 防灾科技学院 A kind of degasser and its application
CN107328633B (en) * 2017-07-27 2024-04-02 防灾科技学院 Degassing device and application thereof
CN108489845A (en) * 2018-03-01 2018-09-04 四川大学 By packing the method for weighing and measuring dam flood-discharge atomizing concentration
CN108594915B (en) * 2018-06-27 2023-08-29 东莞市升微机电设备科技有限公司 Volume-adjustable closed chamber and control method
CN108594915A (en) * 2018-06-27 2018-09-28 东莞市升微机电设备科技有限公司 A kind of confined chamber and control method of volume adjustable
CN109374366A (en) * 2018-11-07 2019-02-22 中国科学院东北地理与农业生态研究所 A kind of the soil gas acquisition device and its application method of variable volume
CN109374366B (en) * 2018-11-07 2022-02-15 中国科学院东北地理与农业生态研究所 Volume-variable soil gas collection device and using method thereof
CN110501192A (en) * 2019-08-21 2019-11-26 中国水利水电科学研究院 A kind of constant temperature, closed soil respiration collection device
CN110501192B (en) * 2019-08-21 2020-09-25 中国水利水电科学研究院 Constant-temperature and airtight soil respiration collection device
CN114441242A (en) * 2020-11-02 2022-05-06 中国石油化工股份有限公司 Gas collecting bottle and using method and application thereof
CN114441242B (en) * 2020-11-02 2024-05-07 中国石油化工股份有限公司 Gas collecting bottle and use method and application thereof

Also Published As

Publication number Publication date
CN1258079C (en) 2006-05-31

Similar Documents

Publication Publication Date Title
CN1258079C (en) Method of sampling greenhouse gas by utilizing gas balance bag
Soderberg et al. Stable isotopes of water vapor in the vadose zone: A review of measurement and modeling techniques
CN102053145B (en) In-situ automatic measurement method of CO2 of root system
CN106018182B (en) The root system analog acquisition system monitored for PAHs diffusion flux in soil
CN103424341A (en) Simulator for transport of soil pollutant
CN102879290B (en) Coal rock desorption testing method
AU2010290994A1 (en) In-borehole gas monitor apparatus and method comprising a VOC concentration analyser and a VOC collector
CN205103245U (en) Soil heavy metal migration conversion analogue means
CN105486552B (en) The lasting active in-situ acquisition system of class organic pollution in a kind of gaseous phase of soil
CN106940365A (en) A kind of indoor soil incubation device for integrating ventilation culture with gas collecting and application
CN105116130B (en) Soil column device for simulating leaching, greenhouse gas collection and ammonia volatilization
CN203324268U (en) Earth pillar infiltration and leaching simulator
CN102440153A (en) Pulse type device for conducting quantitative marking on plant with <13>CO2, and method for marking plant by utilizing same
CN205449758U (en) Outlet pressure adjustable coal petrography seepage flow experimental system
CN110220988A (en) A kind of simulation soil column N2O dissolves the method and device of process nitrogen acquisition
RU2394220C2 (en) Device for collecting gas samples from soil
CN107478468A (en) Microcell sampling instrument annex
CN103698476A (en) Isotopic tracer method for determining carbon sources and carbon sinks of perennial vegetation in situ
CN203764632U (en) Constant-temperature garbage soil anaerobic degradation device
CN216377642U (en) Denitrification test device
CN205580913U (en) Rising strength measurement appearance of test tube seedling
CN102478467A (en) Physical absorption gas degassing cylinder, degasser and degassing method
CN108444536A (en) The measurement device and method of portable refuse landfill sulfurous gas discharge capacity
CN209803134U (en) Simulation measuring device for litter decomposition-soil nutrient return quantity
CN210923201U (en) Vegetation source volatile organic compounds developments sampling device

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20060531