CN1561792A - Method for preparing common origanum herb oil micro capsule powder for natural fodder germicide - Google Patents
Method for preparing common origanum herb oil micro capsule powder for natural fodder germicide Download PDFInfo
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- CN1561792A CN1561792A CNA2004100337793A CN200410033779A CN1561792A CN 1561792 A CN1561792 A CN 1561792A CN A2004100337793 A CNA2004100337793 A CN A2004100337793A CN 200410033779 A CN200410033779 A CN 200410033779A CN 1561792 A CN1561792 A CN 1561792A
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Abstract
An origanum herb oil softgel as antibacterial agent for feed is prepared from origanum herb oil extracted from origanum herb, stearic acid as well material and SiO2 particles as adsorbent through fusing and cooling.
Description
The present invention relates to the preparation technology of a kind of animal with natural antibacterial agent origanum oil micro-capsule powder.
The natural anti-bacteria agent for feeding origanum oil is the active material with antibacterial action that extracts from the Chinese herbal medicine wild marjoram, is mainly used in treatment as diseases such as diarrhea, enteritis, diarrhoea.Extracorporeal disinfecting and bacteriostatic test show that the wild marjoram extract causes the enteritis bacterium and 100 strain shigella dysenteriaes such as shigella flexneri, sonne bacillus all have significant sterilization and bacteriostasis to 31 kinds of gram-positive bacteria and Gram-negative bacteria, salmonella, Escherichia coli, proteus vulgaris etc. are common.Because its antibiotic property wide spectrum, safety, residual quantity is extremely low in the animal body, is applied to promoting in diarrhea such as chicken, pig growth, prevention and treatment chicken, piglet and the control fowl body aspects such as coccidia.
Origanum oil is a kind of volatile fragrant oily liquids that has, and it is bigger directly to add in the feed difficulty to, and smell is dense, and the heat loss leads height, and uses and transport also extremely inconvenient.In order to improve bioavailability and absorption efficiency, reduce heat loss rate, be convenient to packing, transportation, sale and feeding again, the origanum oil micro-capsule powder product that exploitation is fit to feed industry and livestock breeding industry demand has become one of developing direction of this product.
U.S. patent of invention US 59950860 has introduced a kind of method for preparing the origanum oil micro-capsule, is origanum oil is distributed in the Arabic gum aqueous solution, forms oil-in-water shape drop, then with carrier calcium bicarbonate mixing, makes through oven drying again.The shortcoming of its technology is low with origanum oil micro-capsule coating rate, and is thermally-stabilised poor.
The preparation method who the objective of the invention is to avoid the deficiency in the existing origanum oil micro-capsule powder technology and a kind of origanum oil micro-capsule powder of high-load origanum oil is provided.
A kind of preparation method of anti-bacteria agent for feeding origanum oil micro-capsule powder is to realize preparing origanum oil micro-capsule powder by adopting fusion to cool off cladding process, and has certain slow release effect concurrently.Adopt the origanum oil micro-capsule powder origanum oil content of the present invention's preparation can reach more than 25%, it is low to have a content height, good fluidity, heat loss rate, has good feeding effect.
Purpose of the present invention can reach by following measure: adopt the wall material of stearic acid material as feeding origanum oil micro-capsule powder; The oily liquids that is coated is an origanum oil, and the micro-capsule center is the flour that has adsorbed origanum oil; The particle diameter of origanum oil micro-capsule is at 40 orders～80 orders.But the stearic acid biological absorptive material that the wall material of micro-capsule powder is used.For origanum oil is the micro-capsule of capsule core material, adopt the fusion cooling method, earlier origanum oil be adsorbed onto on a kind of powder carrier material of efficient oil suction, evenly be blended in then in the wall material of heating and melting after, cool to room temperature is pulverized and is made the origanum oil micro-capsule powder with certain particle diameter that meets demand.
The present invention specifically describes:
Adopt the fusion cooling method to produce the micro-capsule that origanum oil is a capsule core material, promptly earlier origanum oil is adsorbed onto a kind of powder carrier material such as silicon dioxide powder of efficient oil suction, diatomite, kaolin, on the calcium silicates etc. (weight ratio is 1: 1), in common mixer, make its evenly mix jacket type bag that (capsule core material accounts for micro-capsule 50%～30%) be added to it band agitating device then by pot in the monostearate that has been heated to 70 ℃ of fusions, after but the wall material of stearic acid such as calcium stearate or tallow biological absorptive material (the wall material accounts for micro-capsule 50%～70%) evenly mixes, cool to room temperature is pulverized and is made the origanum oil micro-capsule powder that meets the certain particle diameter of having of demand (particle diameter of origanum oil micro-capsule is at 40 orders～80 orders).
Accompanying drawing: process chart of the present invention.
Advantage of the present invention: adopt the origanum oil microcapsule powder origanum oil content of the present invention's preparation can reach more than 25%, have content Height, good fluidity, heat loss rate are low, have good feeding effect.
Embodiment 1 adds 134kg in the jacket type bag of 300L band agitating device in by pot, start stirring, being heated to 70 ℃ melts monostearate, slowly add the heartwood 66kg that makes at the uniform origanum oil of common stirrer for mixing and silicon dioxide powder (120 orders～130 orders) by 1: 1 (weight ratio), mix 5～8min, pour a cooling room temperature in the cooler pan into.The solid matter that makes is ground into 40～80 purpose powdery origanum oil micro-capsule products in pulverizer.Product yield 〉=98%, origanum oil content is 16.5% in the product.
Embodiment 2 adds the 99kg calcium stearate in the jacket type bag of 300L band agitating device in by pot, start stirring, being heated to 70 ℃ melts calcium stearate, slowly add the heartwood 66kg that makes at the uniform origanum oil of common stirrer for mixing and silicon dioxide powder (120 orders～130 orders) by 1: 1 (weight ratio), mix 5～8min, pour a cooling room temperature in the cooler pan into.The solid matter that makes is ground into 40～80 purpose powdery origanum oil micro-capsule products in pulverizer.Product yield 〉=98%, origanum oil content is 20.8% in the product.
Embodiment 3 adds the 66kg tallow in the jacket type bag of 300L band agitating device in by pot, start stirring, being heated to 70 ℃ melts tallow, slowly add the heartwood 66kg that makes at the uniform origanum oil of common stirrer for mixing and silicon dioxide powder (120 orders～130 orders) by 1: 1 (weight ratio), mix 5～8min, pour a cooling room temperature in the cooler pan into.The solid matter that makes is ground into 40～80 purpose powdery origanum oil micro-capsule products in pulverizer.Product yield 〉=98%, origanum oil content is 24.6% in the product.
Embodiment 4 can replace silicon dioxide powder among the embodiment 1,2,3 with diatomite.
Embodiment 5 can replace silicon dioxide powder among the embodiment 1,2,3 with kaolin.
Embodiment 6 can replace silicon dioxide powder among the embodiment 1,2,3 with calcium silicates.
Claims (6)
1 one kinds of animals are used the preparation technology of natural antibacterial agent origanum oil micro-capsule powder, it is characterized in that adopting the fusion cooling method, being about to origanum oil is adsorbed onto on a kind of powder carrier material such as silicon dioxide powder of efficient oil suction by 1: 1 weight ratio, adopt common mixer to make its even mixing, the jacket type bag that then it is added to the band agitating device is heated in the monostearate wall material of 70 ℃ of fusions in the pot Yu, capsule core material accounts for micro-capsule 50%～30%, the wall material accounts for micro-capsule 50%～70%, after evenly mixing, cool to room temperature is pulverized and is made the origanum oil micro-capsule powder that meets the certain particle diameter of having of demand (particle diameter of origanum oil micro-capsule is at 40 orders～80 orders).
The preparation technology of 2 natural antibacterial agent origanum oil micro-capsule powder according to claim 1 is characterized in that available calcium stearate replaces the wall material of monostearate as micro-capsule.
The preparation technology of 3 natural antibacterial agent origanum oil micro-capsule powder according to claim 1 is characterized in that available tallow replaces the wall material of monostearate as micro-capsule.
The preparation technology of 4 natural antibacterial agent origanum oil micro-capsule powder according to claim 1 is characterized in that available diatomite replaces silicon dioxide powder absorption origanum oil to make capsule core material.
The preparation technology of 5 natural antibacterial agent origanum oil micro-capsule powder according to claim 1 is characterized in that available kaolin replaces silicon dioxide powder absorption origanum oil to make capsule core material.
The preparation technology of 6 natural antibacterial agent origanum oil micro-capsule powder according to claim 1 is characterized in that available calcium silicates replaces silicon dioxide powder absorption origanum oil to make capsule core material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2004100337793A CN1224331C (en) | 2004-04-16 | 2004-04-16 | Method for preparing common origanum herb oil micro capsule powder for natural fodder germicide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CNB2004100337793A CN1224331C (en) | 2004-04-16 | 2004-04-16 | Method for preparing common origanum herb oil micro capsule powder for natural fodder germicide |
Publications (2)
| Publication Number | Publication Date |
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| CN1561792A true CN1561792A (en) | 2005-01-12 |
| CN1224331C CN1224331C (en) | 2005-10-26 |
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| CNB2004100337793A Expired - Fee Related CN1224331C (en) | 2004-04-16 | 2004-04-16 | Method for preparing common origanum herb oil micro capsule powder for natural fodder germicide |
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Cited By (15)
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| EP1991052A2 (en) * | 2006-02-15 | 2008-11-19 | Botanocap Ltd. | Applications of microencapsulated essential oils |
| CN102090506A (en) * | 2009-12-11 | 2011-06-15 | 哈尔滨青禾科技有限公司 | Compound Chinese medicinal herbal additive for promoting growth of cadpigs and preparation method thereof |
| CN102090518A (en) * | 2011-01-12 | 2011-06-15 | 乐山市瑞和祥畜牧药业有限公司 | Origanum oil premix and preparation method thereof |
| CN101530466B (en) * | 2009-04-03 | 2012-05-09 | 西北农林科技大学 | Nano medicament containing oregano oil and vitamins |
| CN101953882B (en) * | 2010-10-15 | 2012-05-23 | 郑州后羿制药有限公司 | Compound microcapsule for treating bacterial disease of livestock and poultry and preparation method thereof |
| CN102511666A (en) * | 2011-12-29 | 2012-06-27 | 王广玉 | Oregano oil premix for livestock and poultry and preparation method |
| CN103082093A (en) * | 2013-01-31 | 2013-05-08 | 武汉工业学院 | Coated natural plant essential oil feed additive and application thereof |
| CN103583922A (en) * | 2013-11-25 | 2014-02-19 | 广州美瑞泰科生物工程技术有限公司 | Poultry used disease-resistant growth promotion green feed additive and preparing method thereof |
| US8753676B2 (en) | 2006-02-15 | 2014-06-17 | Botanocap Ltd. | Applications of microencapsulated essential oils |
| CN105248445A (en) * | 2015-11-16 | 2016-01-20 | 河北德瑞化工有限公司 | Slow-release thiamethoxam water dispersible granule and preparing method thereof |
| CN105661042A (en) * | 2016-03-22 | 2016-06-15 | 江西天佳动物药业有限公司 | Micro-capsule-coated compound plant essential oil feed additive and preparation method thereof |
| CN106070202A (en) * | 2006-02-15 | 2016-11-09 | 博塔诺凯普有限公司 | The application of microencapsulated essential oils |
| CN108094680A (en) * | 2017-12-18 | 2018-06-01 | 广州美瑞泰科生物工程技术有限公司 | A kind of feed detoxifying agent and preparation method and application |
| CN109549021A (en) * | 2019-01-25 | 2019-04-02 | 刘锐 | A kind of bird feed additive and preparation method thereof and its application |
| CN113712116A (en) * | 2021-08-20 | 2021-11-30 | 江苏康雅生物科技有限公司 | Origanum oil-coated premixed preparation for livestock and poultry and preparation method thereof |
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| CN106942472B (en) * | 2016-11-14 | 2018-03-13 | 江苏隆达生物科技有限公司 | A kind of feed addictive and production method containing coating wild marjoram perfume (or spice) phenol plants essential oil |
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- 2004-04-16 CN CNB2004100337793A patent/CN1224331C/en not_active Expired - Fee Related
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| US9210926B2 (en) | 2006-02-15 | 2015-12-15 | Botanocap Ltd. | Applications of microencapsulated essential oils |
| EP1991052A2 (en) * | 2006-02-15 | 2008-11-19 | Botanocap Ltd. | Applications of microencapsulated essential oils |
| EP1991052B1 (en) * | 2006-02-15 | 2017-09-06 | Botanocap Ltd. | Applications of microencapsulated essential oils |
| US9717240B2 (en) | 2006-02-15 | 2017-08-01 | Botanocap Ltd. | Applications of microencapsulated essential oils |
| US8753676B2 (en) | 2006-02-15 | 2014-06-17 | Botanocap Ltd. | Applications of microencapsulated essential oils |
| CN106070202A (en) * | 2006-02-15 | 2016-11-09 | 博塔诺凯普有限公司 | The application of microencapsulated essential oils |
| CN101530466B (en) * | 2009-04-03 | 2012-05-09 | 西北农林科技大学 | Nano medicament containing oregano oil and vitamins |
| CN102090506A (en) * | 2009-12-11 | 2011-06-15 | 哈尔滨青禾科技有限公司 | Compound Chinese medicinal herbal additive for promoting growth of cadpigs and preparation method thereof |
| CN102090506B (en) * | 2009-12-11 | 2013-03-13 | 哈尔滨青禾科技有限公司 | Compound Chinese medicinal herbal additive for promoting growth of cadpigs and preparation method thereof |
| CN101953882B (en) * | 2010-10-15 | 2012-05-23 | 郑州后羿制药有限公司 | Compound microcapsule for treating bacterial disease of livestock and poultry and preparation method thereof |
| CN102090518A (en) * | 2011-01-12 | 2011-06-15 | 乐山市瑞和祥畜牧药业有限公司 | Origanum oil premix and preparation method thereof |
| CN102511666A (en) * | 2011-12-29 | 2012-06-27 | 王广玉 | Oregano oil premix for livestock and poultry and preparation method |
| CN103082093B (en) * | 2013-01-31 | 2014-10-29 | 武汉工业学院 | Coated natural plant essential oil feed additive and application thereof |
| CN103082093A (en) * | 2013-01-31 | 2013-05-08 | 武汉工业学院 | Coated natural plant essential oil feed additive and application thereof |
| CN103583922B (en) * | 2013-11-25 | 2015-04-22 | 广州美瑞泰科生物工程技术有限公司 | Poultry used disease-resistant growth promotion green feed additive and preparing method thereof |
| CN103583922A (en) * | 2013-11-25 | 2014-02-19 | 广州美瑞泰科生物工程技术有限公司 | Poultry used disease-resistant growth promotion green feed additive and preparing method thereof |
| CN105248445A (en) * | 2015-11-16 | 2016-01-20 | 河北德瑞化工有限公司 | Slow-release thiamethoxam water dispersible granule and preparing method thereof |
| CN105661042A (en) * | 2016-03-22 | 2016-06-15 | 江西天佳动物药业有限公司 | Micro-capsule-coated compound plant essential oil feed additive and preparation method thereof |
| CN108094680A (en) * | 2017-12-18 | 2018-06-01 | 广州美瑞泰科生物工程技术有限公司 | A kind of feed detoxifying agent and preparation method and application |
| CN109549021A (en) * | 2019-01-25 | 2019-04-02 | 刘锐 | A kind of bird feed additive and preparation method thereof and its application |
| CN113712116A (en) * | 2021-08-20 | 2021-11-30 | 江苏康雅生物科技有限公司 | Origanum oil-coated premixed preparation for livestock and poultry and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN1224331C (en) | 2005-10-26 |
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Legal Events
| Date | Code | Title | Description |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| EE01 | Entry into force of recordation of patent licensing contract |
Assignee: Feed Research Institute Chinese Academy of Agricultural Sciences Assignor: Longhai Haixin feed premix Co., Ltd. Contract record no.: 2010350000292 Denomination of invention: Method for preparing common origanum herb oil micro capsule powder for natural fodder germicide Granted publication date: 20051026 License type: Exclusive License Open date: 20050112 Record date: 20101103 |
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| EE01 | Entry into force of recordation of patent licensing contract |
Assignee: Longhai Haixin feed premix Co., Ltd. Assignor: Feed Research Institute Chinese Academy of Agricultural Sciences Contract record no.: 2010350000292 Denomination of invention: Method for preparing common origanum herb oil micro capsule powder for natural fodder germicide Granted publication date: 20051026 License type: Exclusive License Open date: 20050112 Record date: 20101103 |
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| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20051026 Termination date: 20130416 |