CN1560292A - Porous composite materical with inorganic phase magnesium base and preparation process thereof - Google Patents

Porous composite materical with inorganic phase magnesium base and preparation process thereof Download PDF

Info

Publication number
CN1560292A
CN1560292A CNA2004100121661A CN200410012166A CN1560292A CN 1560292 A CN1560292 A CN 1560292A CN A2004100121661 A CNA2004100121661 A CN A2004100121661A CN 200410012166 A CN200410012166 A CN 200410012166A CN 1560292 A CN1560292 A CN 1560292A
Authority
CN
China
Prior art keywords
inorganic phase
inorganic
magnesium
alloy
base porous
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CNA2004100121661A
Other languages
Chinese (zh)
Inventor
赵浩峰
刘燕萍
王玲
刘红梅
蔚晓嘉
卫爱丽
范晋平
郝兴明
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Taiyuan University of Technology
Original Assignee
Taiyuan University of Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Taiyuan University of Technology filed Critical Taiyuan University of Technology
Priority to CNA2004100121661A priority Critical patent/CN1560292A/en
Publication of CN1560292A publication Critical patent/CN1560292A/en
Pending legal-status Critical Current

Links

Landscapes

  • Manufacture Of Alloys Or Alloy Compounds (AREA)

Abstract

The invention is an inorganic-phase Mg-based multiporous composite and its preparing method, concretely an inorganic phase-containing multiporous Mg-based composite and its preparing method, and its characteristic: it is a composite prepared by melting process, where a 100 mum-1 mm sized organic phase (Mg, Fe, Al)3[(Si, Al)4O10](OH)2.4H2O distributed in the Mg alloy base, the bulk percent of the organic phase is 20-50% and the total bulk percent of the pores is 10-30%, and its advantages: are no-environmental pollution, its weight is lighter than that of the foamed aluminum with the same porosity, and it can act as vibration absorbing parts in rapid machineries like automobiles, etc, and also be used in the fields of sound insulating, noise preventing, etc.

Description

Inorganic phase magnesium-base porous compound material and preparation method
Technical field
The invention belongs to metal material field, relating to a kind of is the material that contains equally distributed inorganic phase and hole of base with the magnesium alloy.
Technical background
At present, magnesium alloy is used aborning with specific tenacity and the high superperformance of specific rigidity.Its reason is the in light weight of material, if in the weight with the low material of volume decline, can only form many holes in matrix alloy, promptly forms composite material of foamed metal.See that at present foamed metal mainly is aluminum foam material, nickel foam material etc., has prepared the aluminum foam material as patent 01106207 usefulness direct foaming of melt mass method.But the density of aluminium is compared the density height of magnesium.If magnesium and basic alloy can be made porous material, can further enlarge the purposes of foamed metal.
Summary of the invention
The objective of the invention is at the problems referred to above, propose a kind of have an even hole contain magnesium base composite material of inorganic phase and preparation method thereof.
The inorganic phase magnesium-base porous compound material of the present invention is a kind of matrix material of being made up of inorganic phase, pore and metallic matrix, it is characterized in that be a kind of in magnesium alloy substrate, be distributed be of a size of 100 μ m-1mm (Mg, Fe, Al) 3[(Si, Al) 4O 10] (OH) 24H 2The inorganic phase of O, inorganic mutually shared volume percent is 20-50%, and the pore volume accounts for the matrix material of 10-30%, and the metallic matrix component content is: (2~15wt%), (2~10wt%), (0.5~3wt%), Re (0.3~2wt%) for Mn for Zn for Al.The preparation of inorganic phase magnesium-base porous compound material be characterised in that will be of a size of earlier 100 μ m-1mm (Mg, Fe, Al) 3[(Si, Al) 4O 10] (OH) 24H 2In the steel-molded mould that links to each other with vacuum system bottom the inorganic phase powder of O is packed into, compress, then steel-molded mould being put into the cabinet-type electric furnace that is filled with argon gas heats up, temperature rise is to 590-630 ℃, thereafter will melt good component content is: Al (2~15wt%), Zn (2~10wt%), Mn (0.5~3wt%), (0.3~2wt%) magnesium alloy pours in the sprue cup on forming mould top Re, the volume of casting metal is 8-5: 2-5 with the ratio of the volume of inorganic powder mutually, start vacuum system simultaneously, alloy infiltrates under the effect of vacuum pressure in the gap between the inorganic phase powder, vacuum pressure is 0.1-0.7MPa, treats just can open mould behind the alloy graining, obtains inorganic phase magnesium-base porous compound material.
One of advantage of the present invention is, inorganic phase magnesium-base porous compound material preparation is simple, and cost is low, non-environmental-pollution; Another advantage of the present invention is: the weight ratio of inorganic phase magnesium-base porous compound material is low with the foamed aluminium of hole ratio, has alleviated the weight of structural part.
The inorganic phase magnesium-base porous compound material of the present invention can be used for quick absorbing parts mechanically such as automobile, is used for fields such as sound insulation, noise control.
Embodiment
Embodiment 1:
Inorganic phase magnesium-base porous compound material is a kind of matrix material of being made up of inorganic phase, pore and metallic matrix, it is characterized in that a kind of in metallic matrix, be distributed with 500 μ m (Mg, Fe, Al) 3[(Si, Al) 4O 10] (OH) 24H 2The inorganic phase of O, inorganic mutually shared volume percent are 20%, and the pore volume accounts for 10% matrix material, and the metallic matrix component content is: Al2wt%, Zn2wt%, Mn0.5wt%, Re0.3wt%.The preparation method of magnesium-base porous compound material be will be of a size of earlier 500 μ m (Mg, Fe, Al) 3[(Si, Al) 4O 10] (OH) 24H 2In the steel-molded mould that links to each other with vacuum system bottom the inorganic phase powder of O is packed into, compress, then steel-molded mould being put into the cabinet-type electric furnace that is filled with argon gas heats up, temperature rise to 590 ℃, thereafter will melt good component content is: Al2wt%, Zn2wt%, Mn0.5wt%, the magnesium alloy of Re0.3wt% pours in the sprue cup on forming mould top, and the volume of casting metal is 8: 2 with the ratio of the volume of inorganic powder mutually, starts vacuum system simultaneously, alloy infiltrates under the effect of vacuum pressure in the gap between the inorganic phase powder, vacuum pressure is 0.4MPa, treats just can open mould behind the alloy graining, obtains inorganic phase magnesium-base porous compound material.
Embodiment 2:
Inorganic phase magnesium-base porous compound material is a kind of matrix material of being made up of inorganic phase, pore and metallic matrix, it is characterized in that a kind of in metallic matrix, be distributed with 100 μ m (Mg, Fe, Al) 3[(Si, Al) 4O 10] (OH) 24H 2The inorganic phase of O, inorganic mutually shared volume percent are 50%, and the pore volume accounts for 30% matrix material, and the metallic matrix component content is: Al 15wt%, Zn10wt%, Mn3wt%, Re2wt%.The preparation method of magnesium-base porous compound material be will be of a size of earlier 100 μ m (Mg, Fe, Al) 3[(Si, Al) 4O 10] (OH) 24H 2In the steel-molded mould that links to each other with vacuum system bottom the inorganic phase powder of O is packed into, compress, then steel-molded mould being put into the cabinet-type electric furnace that is filled with argon gas heats up, temperature rise to 610 ℃, thereafter will melt good component content is: Al15wt%, Zn10wt%, Mn3wt%, the magnesium alloy of Re2wt% pours in the sprue cup on forming mould top, and the volume of casting metal is 5: 5 with the ratio of the volume of inorganic powder mutually, starts vacuum system simultaneously, alloy infiltrates under the effect of vacuum pressure in the gap between the inorganic phase powder, vacuum pressure is 0.1MPa, treats just can open mould behind the alloy graining, obtains inorganic phase magnesium-base porous compound material.
Embodiment 3:
Inorganic phase magnesium-base porous compound material is a kind of matrix material of being made up of inorganic phase, pore and metallic matrix, it is characterized in that a kind of in metallic matrix, be distributed with 1mm (Mg, Fe, Al) 3[(Si, Al) 4O 10] (OH) 24H 2The inorganic phase of O, inorganic mutually shared volume percent are 30%, and the pore volume accounts for 25% matrix material, and the metallic matrix component content is: Al8wt%, Zn6wt%, Mn1wt%, Re1wt%.The preparation method of magnesium-base porous compound material be earlier earlier with size 1mm (Mg, Fe, Al) 3[(Si, Al) 4O 10] (OH) 24H 2In the steel-molded mould that links to each other with vacuum system bottom the inorganic phase powder of O is packed into, compress, then steel-molded mould being put into the cabinet-type electric furnace that is filled with argon gas heats up, temperature rise to 630 ℃, thereafter will melt good component content is: Al8wt%, Zn6wt%, Mn1wt%, the magnesium alloy of Re1wt% pours in the sprue cup on forming mould top, and the volume of casting metal is 7: 3 with the ratio of the volume of inorganic powder mutually, starts vacuum system simultaneously, alloy infiltrates under the effect of vacuum pressure in the gap between the inorganic phase powder, vacuum pressure is 0.7MPa, treats just can open mould behind the alloy graining, obtains inorganic phase magnesium-base porous compound material.

Claims (2)

1. inorganic mutually magnesium-base porous metallic substance, it is characterized in that be a kind of in magnesium alloy substrate, be distributed be of a size of 100 μ m-1mm (Mg, Fe, Al) 3[(Si, Al) 4O 10] (OH) 24H 2The inorganic phase of O, inorganic mutually shared volume percent is 20-50%, and the pore volume accounts for the matrix material of 10-30%, and the metallic matrix component content is: (2~15wt%), (2~10wt%), (0.5~3wt%), Re (0.3~2wt%) for Mn for Zn for Al.
2. the method for preparing right 1 described inorganic phase magnesium-base porous compound material, it is characterized in that will being of a size of earlier 100 μ m-1mm (Mg, Fe, Al) 3[(Si, Al) 4O 10] (OH) 24H 2In the steel-molded mould that links to each other with vacuum system bottom the inorganic phase powder of O is packed into, compress, then steel-molded mould being put into the cabinet-type electric furnace that is filled with argon gas heats up, temperature rise is to 590-630 ℃, thereafter will melt good component content is: Al (2~15wt%), Zn (2~10wt%), Mn (0.5~3wt%), (0.3~2wt%) magnesium alloy pours in the sprue cup on forming mould top Re, the volume of casting metal is 8-5: 2-5 with the ratio of the volume of inorganic powder mutually, start vacuum system simultaneously, alloy infiltrates under the effect of vacuum pressure in the gap between the inorganic phase powder, vacuum pressure is 0.1-0.7MPa, treats just can open mould behind the alloy graining, obtains inorganic phase magnesium-base porous compound material.
CNA2004100121661A 2004-02-28 2004-02-28 Porous composite materical with inorganic phase magnesium base and preparation process thereof Pending CN1560292A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNA2004100121661A CN1560292A (en) 2004-02-28 2004-02-28 Porous composite materical with inorganic phase magnesium base and preparation process thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNA2004100121661A CN1560292A (en) 2004-02-28 2004-02-28 Porous composite materical with inorganic phase magnesium base and preparation process thereof

Publications (1)

Publication Number Publication Date
CN1560292A true CN1560292A (en) 2005-01-05

Family

ID=34440033

Family Applications (1)

Application Number Title Priority Date Filing Date
CNA2004100121661A Pending CN1560292A (en) 2004-02-28 2004-02-28 Porous composite materical with inorganic phase magnesium base and preparation process thereof

Country Status (1)

Country Link
CN (1) CN1560292A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100357479C (en) * 2006-05-30 2007-12-26 南京信息工程大学 Magnesium-base nano pore composite material and preparation
CN107699723A (en) * 2017-09-29 2018-02-16 重庆理工大学 The preparation method of magnesium-base porous compound material containing ceramic hollow ball

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100357479C (en) * 2006-05-30 2007-12-26 南京信息工程大学 Magnesium-base nano pore composite material and preparation
CN107699723A (en) * 2017-09-29 2018-02-16 重庆理工大学 The preparation method of magnesium-base porous compound material containing ceramic hollow ball

Similar Documents

Publication Publication Date Title
EP1755809B1 (en) Method of production of porous metallic materials
JP4322665B2 (en) Manufacturing method of metal / foam metal composite parts
CN105624451B (en) A kind of high-strength and high ductility closed-cell aluminum foam and preparation method thereof
CN100560763C (en) A kind of aperture is porous Al alloy of micro-meter scale and preparation method thereof
Rivero et al. Compressive properties of Al-A206/SiC and Mg-AZ91/SiC syntactic foams
CN110052613B (en) Aluminum/magnesium/aluminum alloy composite plate and preparation method and application thereof
CN105903969A (en) Porous copper material with directional layered pores and preparation method of porous copper material
CN107695318B (en) A kind of foam magnesium sandwich plate and its Semi-Solid Thixoforming Seepage Foundry method
CN1274856C (en) Process for preparing foam magnesium
Banhart et al. Light-metal foams: Some recent developments
CN100497695C (en) Magnesium-base porous compound material and method of producing the same
CN1256452C (en) Tapping zinc alloy and preparation method
CN1560292A (en) Porous composite materical with inorganic phase magnesium base and preparation process thereof
CN113042735A (en) Preparation method of hollow silicon carbide aluminum-based composite material
CN112899513A (en) Foamed aluminum with open-close hole coexisting structure and preparation method thereof
CN1252298C (en) Foam composite material with magnesium base and its preparation process
CA3077575A1 (en) Method for foaming metal in a liquid bath
CN107552797A (en) A kind of method that foam metal is prepared using freezing drawing process
KR100253710B1 (en) Multi-layer, porous aluminium powder sintered material with a wire-net shaped reinforcing member therein and a manufacturing method thereof
CN114226692A (en) Preparation method of porous metal-based composite material with double-wall core-shell structure hollow glass beads
CN1252299C (en) Process for cold pressing-solving-vacuum sintering preparation of foamed aluminum
JP3237115B2 (en) Method and product for producing foam of Ti-Al intermetallic compound
US20030110882A1 (en) Vehicle steering wheel
US20090165981A1 (en) Process For Recycling Light Metal Parts
CN112746193B (en) Preparation method of foam magnesium or magnesium alloy

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C02 Deemed withdrawal of patent application after publication (patent law 2001)
WD01 Invention patent application deemed withdrawn after publication