CN1558210A - Coupled type polarization preserving fiber fadeout wave sensor - Google Patents
Coupled type polarization preserving fiber fadeout wave sensor Download PDFInfo
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- CN1558210A CN1558210A CNA2004100162591A CN200410016259A CN1558210A CN 1558210 A CN1558210 A CN 1558210A CN A2004100162591 A CNA2004100162591 A CN A2004100162591A CN 200410016259 A CN200410016259 A CN 200410016259A CN 1558210 A CN1558210 A CN 1558210A
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Abstract
The present invention is one coupled high-sensitivity polarization maintaining fiber evanescent wave sensor, and belongs to the field of optical fiber and sensor technology. The sensor consists of mainly light source, monochromator, sensing fiber coupler probe or sensing element, detector, signal processing unit and container holding measured medium. The sensing fiber coupler probe or sensing element is one melting cone type polarization maintaining fiber coupler probe and packed inside basal body with sensing polarization maintaining fiber cone area, polarization maintaining fiber lead-in ends and fixing glue to fix the fiber; and near the fiber cone area, there is hollow channel for the tested gas or liquid to pass through and surround the fiber cone area; and the sensing fiber coupler probe or sensing element is held inside the container with the measured medium and surrounded by the measured medium. The present invention has simple structure, high sensitivity, high selectivity and other advantages.
Description
Technical field:
The present invention addresses a kind of novel manifold type high-sensitivity polarization maintaining fiber evanescent wave sensor, belongs to optical fiber and sensor technical field.
Background technology:
In order to discern content of elements, obtain intermolecular interrelated information, extract, separate and identify required material, the micro substance that carries out high sensitivity, high resolving power, high selectivity detects, application in fields such as environmental monitoring, biomedicine, chemical industry, material analysiss is very important, and development prospect is widely arranged.Traditional surveying instrument and method, as spectrophotometer, absorption spectroscopy, they need be sampled, add reagent and measure to measured matter, few, the complicated operation of detecting information amount so not only, and also real-time is poor, sensitivity is low, waste of human resource is big.In recent years, the fast development of optical fiber evanescent wave sensing technology is expected to solve the problem that the traditional measurement mode exists.
At present, in the world a plurality of countries etc. to based on absorbing and the evanescent wave sensor of the multi-form and structure of fluorescence principle has carried out more deep research.The most general based on the research of principle of absorption optical fiber evanescent wave sensor, it is unmarked measurement, simple in structure, convenient test, but sensitivity is lower, as, the content of zellon in the patina halogen test optical fiber water such as Austria Jakusch, minimum survey is limited to 300 μ g/L; Germany Buerck etc. measures phreatic aromatic hydrocarbon content, the minimum 200 μ g/L that are limited to.Optical fiber evanescent wave sensor based on the fluorescence principle steps on a new stage for the raising measurement sensitivity steps, its sensitivity will exceed absorption 1～4 order of magnitude, pollute content as the explosive TNT in the usefulness fluorescence measurement water gagings of mark such as U.S. Shriver-Lake, measurement sensitivity has reached 8 μ g/L.Carrying out fluorescence measurement with mark is because 20～30% measured object mass-energy autofluorescence is only arranged, and most of fluorescence formula test macros need add some indicator (as the orange fluorescein of pyridine etc.) just can carry out assay determination.Fluorescence method is because a little less than the fluorescence signal, so need the high-sensitivity detection instrument, simultaneously underlined indicator adds also can disturb measured object molecule absorption ability and accuracy of measurement, causes test to pollute.By contrast, the correlative study of China relatively lags behind.The domestic research that also has some scholars to be engaged in this aspect utilized SO in the twin-beam compensation principle of absorption test water as University Of Tianjin but in recent years,
3 2-, minimum survey limit reaches 1600 μ g/L; Xiamen University utilizes the dissolved oxygen DO in the quench method measurement water, and minimum survey is limited to 30 μ g/L.
Up to the present, the emphasis of research mainly is placed on the evanescent wave sensor of principle of absorption, fluorescence principle both at home and abroad.But it is the difficult point problem of its application of restriction and development that unmarked high sensitivity and high selectivity are measured always.Therefore, study a kind of new sensor mechanism and method for sensing, solve the general character difficult problem of sensing technology in using, the Fibre Optical Sensor that achieves have good reliability, highly sensitive, selectivity strong, do not have sampling, characteristics that no reagent is measured be necessary, also be urgent need.
Summary of the invention
At above problem, the present invention starts with from the sensor mechanism of test, has proposed a kind of novel manifold type high-sensitivity polarization maintaining fiber evanescent wave sensor.It utilizes the melting cone type polarization-maintaining fiber coupler as optical fiber evanescent wave sensing element based on the evanescent wave theory of light wave coupled wave theory and optical fiber, thus the evanescent wave that obtains having coupling effect.
The object of the present invention is to provide a kind of highly sensitive, manifold type polarization maintaining optical fibre evanescent wave sensor that selectivity is strong.
A kind of manifold type polarization maintaining optical fibre evanescent wave sensor of the present invention, mainly by light source, monochromator, sensing with fiber coupler probe or sensing element, detector, signal processing unit and fill by the container of side medium and form; It is characterized in that sensing is an a kind of melting cone type polarization-maintaining fiber coupler probe with fiber coupler probe or sensing element, and as the sensing element of optical fiber evanescent wave; This polarization-maintaining fiber coupler probe or sensing element are packaged in the matrix, and the polarization maintaining optical fibre awl district of a sensing is arranged in the matrix, and respectively there is the polarization maintaining optical fibre leading-in end of a sensing with polarization-maintaining fiber coupler at two ends, and it is fixed on the matrix optical fiber by fixing glue; Near the optical taper district, also leave the hollow turnover groove that tested gas or liquid is passed through and surround the optical taper district; Fiber coupler probe or sensing element are positioned in the container that fills measured medium, and are surrounded by measured medium.
The minimum diameter in the sensing polarization maintaining optical fibre awl district in the above-mentioned matrix is 5-9 a times of fibre core.
The principle of work of manifold type polarization maintaining optical fibre evanescent wave sensor of the present invention is as described below: when surrounding the media variations in polarization-maintaining coupler sensing nose cone district, the evanescent wave in coupling mechanism awl district will with medium interaction, different medium (or the different concentration of same medium) will change the coupling effect of polarization-maintaining fiber coupler, thereby the splitting ratio of coupling mechanism is changed, detect the parameter that splitting ratio just can obtain measured matter like this.Owing to utilize coupling principle, the output signal of test is the splitting ratio of coupling mechanism, has nothing to do so it changes with the light intensity of light path, and very strong antijamming capability is arranged; Because what measured matter changed is the coupling effect rather than the light intensity of polarization-maintaining coupler, so very high measurement sensitivity is arranged; Owing to adopt polarization-maintaining fiber coupler, eliminated the influence of polarization interference to sensor as sensing element.
If will distinguish materials different in the tested potpourri, promptly solve optionally problem, then can on light path, utilize light wave scanning, obtain the all-wave spectrogram of compounding substances, and then in signal processing, analyze the all-wave spectrogram, extract measured matter.
Manifold type polarization maintaining optical fibre evanescent wave sensor of the present invention has advantages such as simple in structure, highly sensitive, that selectivity is good, antijamming capability is strong, and it can be applicable to the high precision, high resolving power measurement, extraction, discriminating of liquid, gas in the fields such as biology, chemistry, medicine, environment, material etc.
Description of drawings
Fig. 1 is a gradually formula wave sensor schematic diagram of manifold type polarization maintaining optical fibre of the present invention
Among the figure: 1-light source; 2-monochromator, 3-sensing are popped one's head in or sensing element with polarization-maintaining fiber coupler; 4,5---detector, 6-signal processing unit; 7-container; 8-measured medium
Fig. 2 is the encapsulation synoptic diagram of fiber coupler probe or sensing element
Among the figure: the thin slice optical fiber leading-in end of 31-polarization-maintaining fiber coupler; 32-matrix; 33-fixing glue; The polarization maintaining optical fibre awl district of 34-sensing; The hollow turnover groove of 35-tested gas or liquid.
Embodiment
Now in conjunction with the accompanying drawings and embodiments, the present invention further is described in after
Embodiment one: referring to Fig. 1 and Fig. 2, a kind of manifold type polarization maintaining optical fibre evanescent wave sensor of the present invention, mainly by light source 1, monochromator 2, sensing with fiber coupler probe or sensing element 3, detector 4,5, signal processing unit 6 and fill by the container 7 of side medium 8 and form; Sensing is a kind of melting cone type polarization-maintaining fiber coupler probes with fiber coupler probe or sensing element 3, and as the sensing element of optical fiber evanescent wave; This polarization-maintaining fiber coupler probe or sensing element 3 are packaged in the matrix 32, the polarization maintaining optical fibre awl district 34 that one sensing is arranged in the matrix 32, respectively there is the polarization maintaining optical fibre leading-in end 31 of a sensing with polarization-maintaining fiber coupler at two ends, and it is fixed on the matrix 32 optical fiber 31 by fixing glue 33; Near optical taper district 34, also leave the hollow turnover groove 35 that tested gas or liquid is passed through and surround optical taper district 34; Fiber coupler probe or sensing element 3 are positioned in the container 7 that fills measured medium 8, and are surrounded by measured medium.
The minimum diameter in the sensing polarization maintaining optical fibre awl district 34 in the above-mentioned matrix 32 is 5-9 times of fibre core.
Concrete operations principle and process prescription are as follows: the light that light source 1 sends enters monochromator 2 and sends a branch of monochromatic light, entering sensing pops one's head in or sensing element 3 with polarization-maintaining fiber coupler, the mixing measured medium 8 that this probe or sensing unit 3 have container 7 to contain surrounds, the evanescent wave of measured medium and sensing element 3 interacts, changed the light intensity that is transferred to detector 4 and 5, both change the splitting ratio of polarization-maintaining coupler, become electric signal entering signal processing unit 6 through opto-electronic conversion then.The analysis of spectrum of the synchronous two-way output signal of length scanning of signal processing unit 6 and monochromator 2, and with wavelet analysis (WT) and partial least square method (PLS) wave spectrogram that methods analyst mixes that combines, resolve into the wave spectrogram of each component, and the irrelevant information of filtering, useful signal extracted.The different content information that like this will highly selective obtains mixing measured medium.
Polarization-maintaining fiber coupler sensing element of the present invention is in manufacturing process, and adopting the oxyhydrogen flame lamp is the low baking temperature torch, in order to reduce stress and to keep high polarization state to need long preheating time; It is relatively slow that optical fiber draws the speed of awl in addition; Draw the length of awl to want the sensitivity of view sensor and decide, the awl long more sensitivity in district is high more, but anti-jamming capacity is poor more, and the general minimum diameter of selecting the awl district is that 5～9 times of fibre core get final product.
In order to reduce the influence of temperature to sensor, the sensing probe fit on adopts the material close with the fiber optic materials temperature characterisitic, as quartz.In addition, the material of negative temperature coefficient also can compensate temperature variation in the practical application as the substrate of sensor head.Two non-awl ends that adopt the little glue of temperature effect to be stained with to connect coupling mechanism and substrate solidify glue as secondary UV.
Measure for blending agent, in order to improve Selectivity of Sensor, to tell single material, selected light source must cover all wave bands of measured matter, so this light source should be the light source of broad band, or the combination of several light sources;
The monochromator that is adopted also should cover all wave bands of measured matter, the resolution of monochromator will be decided on the center wavelength profile of tested various one matters, if centre wavelength is just selected high-resolution monochromator for use at a distance of nearer, otherwise adopts the low monochromator of resolution to get final product;
Claims (2)
1. manifold type polarization maintaining optical fibre evanescent wave sensor, mainly by light source (1), monochromator (2), sensing with fiber coupler probe or sensing element (3), detector (4,5), signal processing unit (6) and fill by the container of side medium (8) (7) and form; It is characterized in that sensing is an a kind of melting cone type polarization-maintaining fiber coupler probe with fiber coupler probe or sensing element (3), and as the sensing element of optical fiber evanescent wave; This polarization-maintaining fiber coupler probe or sensing element (3) are packaged in the matrix (32), the polarization maintaining optical fibre awl district (34) that one sensing is arranged in the matrix (32), respectively there is the polarization maintaining optical fibre leading-in end (31) of a sensing with polarization-maintaining fiber coupler at two ends, and it is fixed on the matrix (32) optical fiber (31) by fixing glue (33); Near optical taper district (34), also leave the hollow turnover groove (35) that tested gas or liquid is passed through and surround optical taper district (34); Fiber coupler probe or sensing element (3) are positioned in the container (7) that fills measured medium (8), and are surrounded by measured medium.
2. a kind of manifold type polarization maintaining optical fibre evanescent wave sensor according to claim 1, the minimum diameter that it is characterized in that the sensing polarization maintaining optical fibre awl district (34) in the described matrix (32) are 5-9 times of fibre core.
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| Application Number | Priority Date | Filing Date | Title |
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| CN 200410016259 CN1260562C (en) | 2004-02-12 | 2004-02-12 | Coupled type polarization preserving fiber fadeout wave sensor |
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| CN 200410016259 CN1260562C (en) | 2004-02-12 | 2004-02-12 | Coupled type polarization preserving fiber fadeout wave sensor |
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| CN1558210A true CN1558210A (en) | 2004-12-29 |
| CN1260562C CN1260562C (en) | 2006-06-21 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108072620A (en) * | 2018-02-05 | 2018-05-25 | 西南石油大学 | It is a kind of using optical fiber evanescent field sensor research dyestuff solid-liquid interface adsorption dynamics adsorption kinetics method |
| CN108168767A (en) * | 2018-01-02 | 2018-06-15 | 河北大学 | A kind of production method of hydraulic pressure optical fiber sensing system and its interior sensing base band |
| CN110186656A (en) * | 2019-07-02 | 2019-08-30 | 德州可视激光科技有限公司 | Laser-projector coupler splitting ratio real-time detection apparatus |
-
2004
- 2004-02-12 CN CN 200410016259 patent/CN1260562C/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108168767A (en) * | 2018-01-02 | 2018-06-15 | 河北大学 | A kind of production method of hydraulic pressure optical fiber sensing system and its interior sensing base band |
| CN108072620A (en) * | 2018-02-05 | 2018-05-25 | 西南石油大学 | It is a kind of using optical fiber evanescent field sensor research dyestuff solid-liquid interface adsorption dynamics adsorption kinetics method |
| CN110186656A (en) * | 2019-07-02 | 2019-08-30 | 德州可视激光科技有限公司 | Laser-projector coupler splitting ratio real-time detection apparatus |
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| CN1260562C (en) | 2006-06-21 |
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