CN1513436A - Dandruff eliminating ginger type shampoo - Google Patents
Dandruff eliminating ginger type shampoo Download PDFInfo
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- CN1513436A CN1513436A CNA031142508A CN03114250A CN1513436A CN 1513436 A CN1513436 A CN 1513436A CN A031142508 A CNA031142508 A CN A031142508A CN 03114250 A CN03114250 A CN 03114250A CN 1513436 A CN1513436 A CN 1513436A
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Abstract
A ginger shampoo able to control dandruff is prepared from ordinary shampoo (97.5-99.5 wt.%) and ginger oil resin extracted by supercritical CO2 extraction through proportional mixing. Its advantages are high effect and no toxic by-effect.
Description
Technical field
The present invention relates to a kind of dandruff removing shampoo, relating to specifically with the Rhizoma Zingiberis Recens extract is the dandruff removing shampoo of effective ingredient.
Background technology
The dandruff is meant the macroscopic squama granule that head produces, be because the metabolism of skin of head superficial cell is accelerated mostly, cause cell to move to skin surface, under the situation of full maturity (keratinization) not with fast speeds, cell promptly comes off in flakes, forms to invite the scalp of people's worry.The reason that causes the dandruff is a lot, and is relevant with individual's body constitution, dysbolismus and heredity etc., because steatocryptosis causes that hypersteatosis also can produce the dandruff.The medical research in modern age finds that pityrosporum furfur is the main cause that causes the dandruff and seborrheic dermatitis.World's Dermatology in 1987 can on determined that the origin cause of formation of the dandruff and the fungus of a kind of " pityrosporum furfur " by name have substantial connection, the quantity of " pityrosporum furfur " is higher by 40% than ordinary person on the people's that the dandruff the is many skin, and this achievement in research has been opened up new way for the treatment dandruff.
The physician is used to dispel the dandruff to the antifungal synthetic drug and obtains certain achievement.Many on the market at present dandruff removing shampoos contain antibacterials mostly, as two Zinc Pyrithione (ZPT), ketoconazole (ketoconazol) etc., wherein the inhibition effect of ketoconazole dandruff that seborrheic dermatitis is caused is best, but it has certain side effect [two ones of Pharmacopoeias of People's Republic of China, 1989], belong to forbidding raw material [cosmetics health standard version in 2002, P21] at home in the cosmetics; ZPT brings the use difficulty for the prescription teacher because the difficulty that suspends is prone to quality problems such as precipitation in finished product.Do not find as yet to extract the dandruff removing shampoo of ginger oil resin entirely as the effective Chinese medicine ingredients of dandruff removing with the Rhizoma Zingiberis Recens extract of Nantural non-toxic side effect.
Rhizoma Zingiberis Recens (Zingiber officinale Rosc) is the Zingiberaceae perennial plant, throughout the country widely plantation.The effective ingredient of Rhizoma Zingiberis Recens mainly comprises Rhizoma Zingiberis Recens quintessence oil and gingerol (mainly containing zingiberol, zingiberone, shogaol etc.).Rhizoma Zingiberis Recens has warming spleen and stomach for dispelling cold as Chinese herbal medicine, effects such as recuperating depleted YANG is promoted blood circulation, pathogenic wind expelling and blood circulation promoting.External various pathogens there is the obvious suppression effect according to data record Rhizoma Zingiberis Recens preserved material, and (4-hydroxy-3-methoxyphenyl)ethyl methyl ketone and ginger ketenes have intensive sterilizing power, and experimental study in vitro shows that the extract of Rhizoma Zingiberis Recens also has inhibitory action [Chinese medicine modern study and application 1441] to the part fungus.
Send out, take a shower in order to pathogenic wind expelling and blood circulation promoting with the washing of Rhizoma Zingiberis Recens pot, popular long at folks of china.The extracting method difference of Rhizoma Zingiberis Recens, the composition and the content of the extract that obtains have than big-difference, and influence the shelf stability of extract, thereby cause the different or unstable of its effect.
The method of existing extraction and separating effective components of ginger mostly is steam distillation, milling process and organic solvent extractionprocess.What steam distillation extracted is the volatile oil component of Rhizoma Zingiberis Recens, and effective ingredient such as gingerol can not be extracted out, also contain a lot of Rhizoma Zingiberis Recens effective ingredient in the leftover bits and pieces after the processing; Though milling process can obtain more comprehensive effective components of ginger, treatment step is loaded down with trivial details, and unstable product quality, and yield is very low; The oil of ginger that organic solvent method extracts has pungent and fragrance is not obvious, main cause be Rhizoma Zingiberis Recens volatile oil extract and the process of post processing in lost problems such as the quantity of solvent that also exists consumption simultaneously is big, inflammable, dissolvent residual; The method that also has employing that steam distillation is combined with organic solvent method is promptly carried volatile oil earlier and is carried gingerol again, but its process complexity, the quality of extract is not good, and loss of effective components is big.Said method all exists some common shortcomings, higher as temperature in the leaching process, the effective ingredient of Rhizoma Zingiberis Recens in leaching process owing to condition too " badly " destroy, lose the former flavoursome and medical value of Rhizoma Zingiberis Recens, the product yield of producing is low, poor quality [ZL99117040.7].
Supercritical carbon dioxide extraction method is a kind of novel green isolation technics, the temperature of its extraction is not high, isolated with oxygen, be specially adapted to extract the determination system of thermal unstable material that is subjected to resemble the gingerol, this is that other extracting method is incomparable, and productivity ratio height, simple to operate, safe and reliable, non-environmental-pollution, thereby can produce the high-quality full extraction ginger oil resin that comprises Rhizoma Zingiberis Recens quintessence oil and gingerol with this extracting method.
Some scholar's research have prepared the shampoo of the effective ingredient that contains Rhizoma Zingiberis Recens in recent years; As Chinese patent application number be: CN90105701.0, name is called the application of " efficient natural plant shampoo prescription and technology thereof ", disclosing a kind of is shampoo and the preparation method that raw material is made with multiple Chinese herbal medicine, has wherein comprised 5% Rhizoma Zingiberis, and its main pharmacodynamics is to educate to send out function.Chinese patent application number is: the CN93100488.8 name is called: the application of " a kind of ginger shampoo and production method thereof ", disclose with water vapour and organic solvent extraction Rhizoma Zingiberis Recens volatile oil and Rhizoma Zingiberis Recens extractum, and, have pathogenic wind expelling and blood circulation promoting, allaying tiredness, alleviation headache effect in order to the preparation shampoo.The above-mentioned Rhizoma Zingiberis Recens hair shampoo article that contains is mainly used in to educate and sends out and the pathogenic wind expelling and blood circulation promoting effect, does not find and utilizes Rhizoma Zingiberis Recens extract to reach the dandruff removing effect.
The purpose of this invention is to provide a kind of dandruff eliminating ginger shampoo, it is to adopt to contain Rhizoma Zingiberis Recens extract and extract ginger oil resin entirely as effective Chinese medicine ingredients, reaches to have Nantural non-toxic side effect and dandruff dispelling effect.
In technical scheme design of the present invention, consider that the content of full extraction ginger oil resin is too light as too low fragrance; Too high as content, increase cost on the one hand, heating felt strong on the one hand in addition, and some consumers have sense of discomfort, simultaneously eyes are caused stimulation; In addition, also can influence the stability of finished product.
Therefore technical scheme of the present invention is:
A kind of dandruff eliminating ginger shampoo is made up of full extraction ginger oil resin and common shampoo.Wherein extract ginger oil resin entirely and account for 0.5～2.5% of dandruff eliminating ginger shampoo gross weight, all the other are shampoo; The main component of full extraction ginger oil resin and account for that the ginger oil resin total weight percent is that zingiberene accounts for 29.81%, zingiberone accounts for 5.61%, shogaol accounts for 3.71%, zingiberol accounts for 10.69%, is weight ratio.
Preferred version of the present invention is to extract 0.8～1.5% (weight ratio) that ginger oil resin accounts for dandruff eliminating ginger shampoo gross weight entirely.
More preferably scheme of the present invention is to extract 1% (weight ratio) that ginger oil resin accounts for dandruff eliminating ginger shampoo gross weight entirely.
Above-mentioned full extraction ginger oil resin is to adopt supercritical carbon dioxide extraction method patented method [ZL99117040.7] to extract gained.Can dewater simultaneously, take off when separating Rhizoma Zingiberis Recens with this patented method assorted, the extract water content that obtains few (moisture content is less than 1.0%), easier preservation, and each batch steady quality.The full extraction ginger oil resin that this method is extracted also comprises phellandrene, ar-curcumene, farnesene, bisabolene and sesquiphellandrene etc. except that mentioned component, account for 33.6% (weight ratio).
In the technical solution of the present invention, shampoo is made up of common substrate, comprises cleansing, conditioning ingredients, functional component etc.
The characteristics of dandruff eliminating ginger shampoo of the present invention are to comprise following prescription: anion surfactant is 13～16 parts, amphoteric surfactant is that 3～1 0 parts, pearlescent flake are that 0～3 part, glycerol are 3 parts, 1.2 parts of cation guar gums, 0.1 part of antiseptic, 0.5～2.5 part of full extraction ginger oil resin, alkyl polyglucoside is 0～4 part, and Oleum Cocois monoalkyl amide is 0～4 part etc.
Described dandruff eliminating ginger shampoo specifically is to comprise following prescription: laurilsulfate ether sodium salt (AES) is 16 parts, the alkyl CAB is that 3 parts, pearlescent flake are that 3 parts, glycerol are that 3 parts, 1.2 parts of cation guar gums, albumen Copeptin are 0.1 part of 1 part, Kazon, extracts 1 part of ginger oil resin etc. entirely.
Described dandruff eliminating ginger shampoo specifically can also comprise following prescription: laurilsulfate ether sodium salt (AES) is 13 parts, the alkyl CAB is that 10 parts, glycerol are that 3 parts, 1.2 parts of cation guar gums, albumen Copeptin are 1 part, 0.1 part of Kazon, extract 1 part of ginger oil resin entirely, alkyl polyglucoside is 4 parts, and Oleum Cocois monoalkyl amide is 4 parts etc.
The preparation method of dandruff eliminating ginger shampoo of the present invention is to adopt common method will extract ginger oil resin entirely to form with common shampoo mix homogeneously.
The present invention's preparation has the shampoo of dandruff removing effect and the dandruff removing effect of product has been carried out quantitative assay.Belong to the improvement of daily hair shampoo article.
Experimentation proves: the ginger shampoo of preparation has better bacteriostasis to pityrosporum furfur, 20 minutes bacteriostasis rate of pityrosporum furfur is reached more than 25%, and the bacteriostasis rate that adds full extraction ginger oil resin shampoo approximately is not add 5 times of full extraction ginger oil resin shampoo.
Description of drawings
Fig. 1 the present invention adds the shampoo and the shampoo (being blank sample) that does not add full extraction ginger oil resin, 20 minutes test result figure to the pityrosporum furfur bacteriostasis of full extraction ginger oil resin;
The dandruff of Fig. 2 crowd's trial edition invention product reduces design sketch.
Beneficial effect of the present invention is to have washing cleaning and debris removing effect, and is non-stimulated to skin through the evidence no side effects, safe and reliable. After the hair washing of this shampoo, has good debris removing effect.
Specific embodiment
Embodiment: below be specific embodiments of the invention, example 1 is not for adding the blank experiment of full extraction ginger oil resin, 2～7 are fixing other prescription of shampoo, change the addition that extracts ginger oil resin entirely; Example 8-9 changes other prescription of shampoo for the addition of fixing full extraction ginger oil resin is 1%.The used shampoo prescription of above-mentioned test is as follows:
| The raw material name | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | Example 6 | Example 7 | Example 8 | Example 9 |
| Laurilsulfate ether sodium salt (AES) | 16.00 | ?16.0 ?0 | ?16.00 | ?16.00 | ?16.00 | ?16.0 ?0 | ?16.00 | ?15.0 ?0 | ?13.0 ?0 |
| The alkyl CAB | 3.0 | ?3.0 | ?3.0 | ?3.0 | ?3.0 | ?3.0 | ?3.0 | ?7 | ?10 |
| Pearlescent flake | 3.0 | ?3.0 | ?3.0 | ?3.0 | ?3.0 | ?3.0 | ?3.0 | ?0 | ?0 |
| Deionized water | 72.6 | ?72.1 | ?71.8 | ?71.6 | ?71.1 | ?70.6 | ?70.1 | ?67.6 | ?62.6 |
| Kazon | 0.1 | ?0.1 | ?0.1 | ?0.1 | ?0.1 | ?0.1 | ?0.1 | ?0.1 | ?0.1 |
| Glycerol | 3.00 | ?3.00 | ?3.00 | ?3.00 | ?3.00 | ?3.00 | ?3.00 | ?3.00 | ?3.00 |
| The E-14S cation guar gum | 1.2 | ?1.2 | ?1.2 | ?1.2 | ?1.2 | ?1.2 | ?1.2 | ?1.2 | ?1.2 |
| Citric acid | 0.1 | ?0.1 | ?0.1 | ?0.1 | ?0.1 | ?0.1 | ?0.1 | ?0.1 | ?0.1 |
| The albumen Copeptin | 1 | ?1 | ?1 | ?1 | ?1 | ?1 | ?1 | ?1 | ?1 |
| Full extraction ginger oil resin | 0 | ?0.5 | ?0.8 | ?1.0 | ?1.5 | ?2.0 | ?2.5 | ?1.0 | ?1.0 |
| Alkyl polyglucoside | 0 | ?0 | ?0 | ?0 | ?0 | ?0 | ?0 | ?2.0 | ?4 |
| Oleum Cocois monoalkyl amide | 0 | ??0 | ??0 | ??0 | ??0 | 0 | 0 | ??2.0 | ??4 |
| High-temperature stability | + | ??+ | ??+ | ??+ | ??+ | The high temperature light discolouration | The high temperature light discolouration | ??+ | ??+ |
| Fragrance | ------ | Too light | Good | Fine | Fine | Fine | Fine | Fine | Fine |
| Hotness | ------ | ??------ | Moderate | Moderate | Moderate | Moderate | Steady heat | Moderate | Moderate |
| Bacteriostasis rate * | 6 | ??25 | ??------ | ??29.1 | ??45 | ------ | 61.5 | ??------ | ??35.6 |
| Overall merit | ------ | Generally | Good | Good | Good | Can accept | Can accept | Good | Good |
"+": expression is stable
" * ": represent 20 minutes test results to the pityrosporum furfur bacteriostasis:
In shampoo, the addition of full extraction ginger oil resin is respectively 0.5%, 0.8%, 1.0%, 1.5%, 2.0%, 2.5%, the results showed that the warmth sensation of skin and dandruff removing effect grow from weak to strong, the addition that wherein extracts ginger oil resin entirely is when 0.8～1.5% scope, be thought of as goodly from composite factors such as the ratio of performance to price, quality stability, fragrance, skin sense and dandruff removing effects, addition is 1% o'clock, takes all factors into consideration best.It is lighter that addition is less than 0.5% o'clock fragrance, and addition is greater than 2.5%, and groups of people can feel that hotness is strong excessively, and influence the product shelf stability.
Crowd's trial state:
We take the finished product of example 3 preparation, have the volunteer of dandruff to carry out testing research on probation to 32, statistical result as follows: using has behind the product personnel's dandruff of 65.63% to reduce.
Claims (7)
1, a kind of dandruff eliminating ginger shampoo is characterized in that the natural Rhizoma Zingiberis Recens extract that contains the extraction of 0.5～2.5% (weight ratio) supercritical carbon dioxide extraction method in the dandruff eliminating ginger shampoo extracts ginger oil resin entirely, and all the other are shampoo; In the full extraction ginger oil resin main component and account for that the ginger oil resin total weight percent is that zingiberene accounts for 29.81%, zingiberone accounts for 5.61%, shogaol accounts for 3.71%, zingiberol accounts for 10.69%.
2, the described dandruff eliminating ginger shampoo of claim 1 is characterized in that extracting full ginger oil resin and accounts for 0.8～1.5% of dandruff eliminating ginger shampoo gross weight.
3, the described dandruff eliminating ginger shampoo of claim 1 is characterized in that extracting full ginger oil resin and accounts for 1% of dandruff eliminating ginger shampoo gross weight.
4, the described dandruff eliminating ginger shampoo of claim 1 is characterized in that shampoo is made up of common substrate, comprises cleansing, conditioning ingredients, functional component etc.
5, claim 1 or 4 described dandruff eliminating ginger shampoos, it is characterized in that shampoo comprises following prescription: anion surfactant is 13～16 parts, amphoteric surfactant is that 3～10 parts, pearlescent flake are that 0～3 part, glycerol are 3 parts, 1.2 parts of cation guar gums, 0.1 part of antiseptic, 0.5～2.5 part of full extraction ginger oil resin, alkyl polyglucoside is 0～4 part, and Oleum Cocois monoalkyl amide is 0～4 part etc.
6, the described dandruff eliminating ginger shampoo of claim 5, it is characterized in that comprising following prescription: laurilsulfate ether sodium salt (AES) is 16 parts, the alkyl CAB is that 3 parts, pearlescent flake are that 3 parts, glycerol are that 3 parts, 1.2 parts of cation guar gums, albumen Copeptin are 0.1 part of 1 part, Kazon, extracts 1 part of ginger oil resin etc. entirely.
7, the described dandruff eliminating ginger shampoo of claim 5, it is characterized in that comprising following prescription: laurilsulfate ether sodium salt (AES) is 13 parts, the alkyl CAB is that 10 parts, glycerol are that 3 parts, 1.2 parts of cation guar gums, albumen Copeptin are 1 part, 0.1 part of Kazon, extract 1 part of ginger oil resin entirely, alkyl polyglucoside is 4 parts, and Oleum Cocois monoalkyl amide is 4 parts etc.
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| Application Number | Priority Date | Filing Date | Title |
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| CNB031142508A CN100355413C (en) | 2003-04-18 | 2003-04-18 | Dandruff eliminating ginger type shampoo |
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| Application Number | Priority Date | Filing Date | Title |
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| CNB031142508A CN100355413C (en) | 2003-04-18 | 2003-04-18 | Dandruff eliminating ginger type shampoo |
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| CN1513436A true CN1513436A (en) | 2004-07-21 |
| CN100355413C CN100355413C (en) | 2007-12-19 |
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| CNB031142508A Expired - Fee Related CN100355413C (en) | 2003-04-18 | 2003-04-18 | Dandruff eliminating ginger type shampoo |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101015515B (en) * | 2007-03-05 | 2010-04-14 | 于崇万 | Scurf dispelling liquid |
| CN103405356A (en) * | 2013-08-23 | 2013-11-27 | 吴江市利达上光制品有限公司 | Preparation method of fresh ginger liquid shampoo |
| CN103690387A (en) * | 2013-12-25 | 2014-04-02 | 丘少荣 | Shampoo with pearl-radiation |
| JP2014512350A (en) * | 2011-04-01 | 2014-05-22 | ロレアル | Use of (ethoxyhydroxyphenyl) alkyl ketones or ethoxyhydroxyalkylphenol compounds as antidandruff agents |
| CN104023701A (en) * | 2011-04-01 | 2014-09-03 | 莱雅公司 | Cosmetic Composition Comprising 4-(3-Ethoxy-4-Hydroxyphenyl)-2-Butanone |
| CN105147593A (en) * | 2015-10-23 | 2015-12-16 | 河南省商业科学研究所有限责任公司 | Dandruff-removing hair-protecting composition containing probiotics and herbal extract, as well as shampoo and preparation method thereof |
| CN107184514A (en) * | 2017-05-22 | 2017-09-22 | 韩仙国 | A kind of ginger shampoo |
| CN107384594A (en) * | 2017-08-23 | 2017-11-24 | 佛山市三水区嘉华化学研究院（普通合伙） | A kind of Zingiber corallinum Hance essential oil with dandruff dispelling activity and its preparation method and application |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01299208A (en) * | 1988-05-27 | 1989-12-04 | Sansho Seiyaku Co Ltd | Dandruff-preventive agent |
| CN1090749A (en) * | 1993-01-30 | 1994-08-17 | 广州市医药工业研究所 | A kind of ginger shampoo and production method thereof |
| CN1098859C (en) * | 1999-08-20 | 2003-01-15 | 广州市轻工研究所 | Process for supercritical carbon dioxide extracting and separating effective components of ginger |
-
2003
- 2003-04-18 CN CNB031142508A patent/CN100355413C/en not_active Expired - Fee Related
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101015515B (en) * | 2007-03-05 | 2010-04-14 | 于崇万 | Scurf dispelling liquid |
| JP2014512350A (en) * | 2011-04-01 | 2014-05-22 | ロレアル | Use of (ethoxyhydroxyphenyl) alkyl ketones or ethoxyhydroxyalkylphenol compounds as antidandruff agents |
| CN104023701A (en) * | 2011-04-01 | 2014-09-03 | 莱雅公司 | Cosmetic Composition Comprising 4-(3-Ethoxy-4-Hydroxyphenyl)-2-Butanone |
| CN104023701B (en) * | 2011-04-01 | 2017-04-26 | 莱雅公司 | Cosmetic Composition Comprising 4-(3-Ethoxy-4-Hydroxyphenyl)-2-Butanone |
| CN103405356A (en) * | 2013-08-23 | 2013-11-27 | 吴江市利达上光制品有限公司 | Preparation method of fresh ginger liquid shampoo |
| CN103405356B (en) * | 2013-08-23 | 2016-02-24 | 苏州靖羽新材料有限公司 | A kind of preparation method of ginger shampoo |
| CN103690387A (en) * | 2013-12-25 | 2014-04-02 | 丘少荣 | Shampoo with pearl-radiation |
| CN105147593A (en) * | 2015-10-23 | 2015-12-16 | 河南省商业科学研究所有限责任公司 | Dandruff-removing hair-protecting composition containing probiotics and herbal extract, as well as shampoo and preparation method thereof |
| CN107184514A (en) * | 2017-05-22 | 2017-09-22 | 韩仙国 | A kind of ginger shampoo |
| CN107384594A (en) * | 2017-08-23 | 2017-11-24 | 佛山市三水区嘉华化学研究院（普通合伙） | A kind of Zingiber corallinum Hance essential oil with dandruff dispelling activity and its preparation method and application |
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|---|---|
| CN100355413C (en) | 2007-12-19 |
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