CN1487033A - Ultraviolet ray cured paint for surface treatment or alumium ou aluminium sections - Google Patents
Ultraviolet ray cured paint for surface treatment or alumium ou aluminium sections Download PDFInfo
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- CN1487033A CN1487033A CNA031502555A CN03150255A CN1487033A CN 1487033 A CN1487033 A CN 1487033A CN A031502555 A CNA031502555 A CN A031502555A CN 03150255 A CN03150255 A CN 03150255A CN 1487033 A CN1487033 A CN 1487033A
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Abstract
The present invention belongs to the field of paint technology, and is especially ultraviolet ray cured paint for the protection and decoration of aluminum surface. Modifying methyl acrylic acid prepolymer in 20-50 wt%, reactive acrylate monomer in 10-50 wt% and light initiator in 2-6 wt% are mixed, heted to 50-60deg.c while stirring and added with assistant in 0-5 wt% while stirring for complete dissolution. Then, glazing powder in 0-20 wt% and solvent in 0-30 wt% are added through stirring, and the mixture is cooled and filtered to obtain the said paint. The paint may be sprayed, showered, roller applied or brushed onto the surface of aluminum sections, pure alminum, antirust aluminum and other aluminum material, and has the advantages of normal temperature curing, high production efficiency, being green and power saving, free adjustment of brightness and color of the coating, etc.
Description
Technical field
The invention belongs to paint field, the ultraviolet-curing paint that particularly is used for the protection of aluminium or aluminium shape surface and decorates.
Background technology
At present, two kinds of coating are adopted in the surface treatment of aluminium or aluminium section bar: the one, electrocoating paint, electrocoating paint in aqueous dispersion the effect of electric field deposit in aluminium or aluminium shape surface, again through high bake and film-forming; The 2nd, powder coating, powder coating is adsorbed onto aluminium or aluminium shape surface by the mode of electrostatic spraying, then fusion at high temperature and crosslinked film forming.No matter above any treatment technology all exist the equipment investment cost height, time of drying is long, energy consumption is high, can not freely adjust defectives such as gloss of film degree and color, and wherein also there are shortcomings such as curing rear surface weak effect in powder coating.
Summary of the invention
The purpose of this invention is to provide a kind of ultraviolet-curing paint that is used for aluminium or aluminium shape surface processing, after spraying, roller coat, showering or brushing the film surface, use uviolizing, making films solidified in the utmost point short period of time (a few second).With reach reduce facility investment, coating time of drying long, energy consumption is high, can not freely adjust defectives such as gloss of film degree and color.
Technical scheme of the present invention is: by the reaction system of (methyl) acrylic acid modified prepolymer, reactive acrylate monomer, light trigger, auxiliary agent, mute light powder or pigment and an amount of solvent composition, press the certainweight percentage mix evenly after, just can obtain being used for the ultraviolet-curing paint of aluminium or aluminium shape surface processing.
The ultraviolet-curing paint that is used for aluminium or aluminium shape surface processing of the present invention forms and content is:
(methyl) acrylic acid modified prepolymer 20-50wt%
Reactive acrylate monomer 10-55wt%
Light trigger 2-6wt%
Auxiliary agent 0-5wt%
Mute light powder (flatting silica) or pigment 0-30wt%
Solvent 0-30wt%
In the above-mentioned coating component, described (methyl) acrylic acid modified prepolymer makes with ordinary method, prepolymer be epoxy (methyl) acrylate, urethane (methyl) acrylate, polyester (methyl) acrylate, amino (methyl) acrylate, acrylic copolymer wherein one or more etc.
Described reactive acrylate monomer is contained in the acrylate of 1-6 acryl one or more: 1. simple function group monomer, as butyl acrylate, cyclohexyl acrylate, Isooctyl acrylate monomer (EHA) or (methyl) Hydroxyethyl acrylate (MHEA) etc.; 2. two monomers, as tri (propylene glycol) diacrylate (TPGDA), dipropylene glycol diacrylate (DPGDA), neopentylglycol diacrylate (NPGDA), the third oxidation neopentylglycol diacrylate (PO-NPGDA), ethoxyquin neopentylglycol diacrylate (EO-NPGDA), two (Diethylene Glycol) diacrylates (PDDA) of phthalic acid or 1,6 hexanediyl ester (HDDA) etc.; 3. polyfunctional monomer is as Viscoat 295 (TMPTA), ethoxyquin Viscoat 295 (EO-TMPTA), the third oxidation Viscoat 295 (PO-TMPTA), pentaerythritol triacrylate (PETA), double pentaerythritol C5 methacrylate (DPPA) or double pentaerythritol methacrylate (DPHA) etc.Usually use with above-mentioned acrylate one or more mixtures wherein.
Described light trigger is that benzoin ethers (st-yrax ethers), benzil ketals class, acetophenones, acyl group oxidation are Phosphorus, one or more mixtures in benzophenone or the aminated compounds; Perhaps one or more mixtures among the Darocur 1173 of Ciba-Geigy company, Irgacure 184, Irgacure 369, Irgacure 149, Irgacure 651, Irgacure 819, Irgacure 907 or the Darocur 4265; Perhaps TPO, ITX or their mixture; The perhaps mixture of above-mentioned light trigger
Described auxiliary agent comprises flow agent, defoamer, Ricinate and anti-wear agent.Wherein the flow agent add-on is the 0.2-1wt% of coating total amount, and the defoamer add-on is the 0.1-0.5wt% of coating total amount, and the wetting dispersing agent add-on is the 0.5-2wt% of coating total amount, and the anti-wear agent add-on is the 0.5-3wt% of coating total amount.Described flow agent, defoamer, Ricinate and anti-wear agent use together or use separately.
Described flow agent is BYK306, BYK307, BYK333, BYK358, EFKA3277, EFKA3777, EFKA3883, DEUCHEM432, DEUCHEM836 one or more mixtures wherein etc.
Described defoamer is BYK052, BYK055, DEUCHEM2700, DEUCHEM3100, Tego920 one or more mixtures wherein etc.
Described wetting dispersing agent is Disperbyk103, Disperbyk104S, BYK-P104S, Disperbyk161, Disperbyk2000, EFKA4010, DEUCHEM904S one or more mixtures wherein etc.
Described anti-wear agent is BYK920 etc.
Described mute light powder is OK500, OK520, TS100, HP340, SP4-9705, Grace C 1006, Grace RAD2005 one or more mixtures wherein etc.
Described pigment is mineral dyes such as titanium dioxide or carbon black; Phthalocyanine blue, green, the brown chrome yellow of the phthalein mountain valley with clumps of trees and bamboo or pigment dyestuff such as bright red; Special effect pigments such as bronze (copper powder), silver powder (aluminium powder), pearlescence, fluorescent material, illusion-colour pigment or reflective pigment.Inorganic or pigment dyestuff all in advance with the polyurethane acrylate prepolymer mixing and be ground to the fineness of diameter＜20 μ m, is made various pigment slurrys, obtains required color by allotment again.
Described solvent is butanone, vinyl acetic monomer, N-BUTYL ACETATE, Virahol, ethylene glycol monoethyl ether or ethylene glycol ether acetate one or more mixtures wherein etc.
Preparation method's step that the present invention is used for the ultraviolet-curing paint of aluminium or aluminium shape surface protection and decoration is:
(1) will account for (methyl) acrylic acid modified prepolymer, the 10-50wt% of total system 20-50wt%
The light trigger of reactive acrylate monomer and 2-6wt% mixes, and is warming up to
50-60 ℃, stir;
(2) in step (1), add the auxiliary agent that accounts for total system 0.5-5wt% then, stir fully
Until dissolving fully.
(3) will account for the mute light powder (or pigment) of total system 0-20wt% and the solvent of 0-30wt% again
Join in the system of step (2), stir, disperse, cooling is filtered, and obtains
The ultraviolet-curing paint that is used for the protection of aluminium or aluminium shape surface and decorates.
The ultraviolet-curing paint that is used for aluminium or aluminium shape surface protection and decoration of the present invention can be widely used in aluminium alloy extrusions, fine aluminium, corrosion-resisting aluminium and other alumina etc., has good sticking power, ambient cure, production efficiency height, environmental protection and energy saving and can freely adjust advantages such as gloss of film degree and color.Characteristics such as its cured coating film has that surface effect is good, hardness is high, wear-resisting, corrosion-resistant, good endurance.
Embodiment
Embodiment 1.
Epoxy (methyl) acrylate 30wt%
Aliphatic urethane acrylate 10wt%
Cyclohexyl acrylate 45wt%
Butyl acrylate 10wt%
Darocur?1173??????????????????????????2wt％
Irgacure?184??????????????????????????2wt％
BYK?055???????????????????????????????0.5wt％
BYK?333???????????????????????????????0.5wt％
The preparation method of the ultraviolet-curing paint of mentioning according to above-mentioned specification sheets that is used for the protection of aluminium or aluminium shape surface and decorates prepares the ultraviolet-curing paint that is used for aluminium or aluminium shape surface protection and decorates.
Embodiment 2.
Amino (methyl) acrylate 10wt%
Aliphatic urethane acrylate 20wt%
Two (Diethylene Glycol) diacrylate 40wt% of phthalic acid
The third oxidation neopentylglycol diacrylate 10wt%
TS?100????????????????????????????????4wt％
Irgacure?184??????????????????????????3wt％
Irgacure?149??????????????????????????1wt％
BYK?306???????????????????????????????0.5wt％
BYK?055???????????????????????????????0.5wt％
EFKA?4010?????????????????????????????1wt％
Butanone 10wt%
The preparation method of the ultraviolet-curing paint of mentioning according to above-mentioned specification sheets that is used for the protection of aluminium or aluminium shape surface and decorates prepares the ultraviolet-curing paint that is used for aluminium or aluminium shape surface protection and decorates.
Embodiment 3.
Epoxy (methyl) acrylate 20wt%
Aliphatic urethane acrylate 10wt%
Amino (methyl) acrylate 10wt%
1,6 hexanediyl ester 10wt%
PDDA????????????????????????????????????????20wt％
EHA?????????????????????????????????????????5wt％
Irgacure?149????????????????????????????????2wt％
TPO (PVG China spoke chemical company limited) 2wt%
Titanium dioxide 2wt%
Phthalocyanine blue 0.5wt%
Disperbyk161????????????????????????????????1wt％
BYK?306?????????????????????????????????????0.5wt％
BYK?920?????????????????????????????????????2wt％
N-BUTYL ACETATE 10wt%
Ethylene glycol ether acetate 5wt%
The preparation method of the ultraviolet-curing paint of mentioning according to above-mentioned specification sheets that is used for the protection of aluminium or aluminium shape surface and decorates prepares the ultraviolet-curing paint that is used for aluminium or aluminium shape surface protection and decorates.
Embodiment 4.
Aliphatic urethane acrylate 24wt%
Amino (methyl) acrylate 20wt%
PO-NPGDA?????????????????????????????????????20wt％
PDDA?????????????????????????????????????????30wt％
Irgacure?184?????????????????????????????????4wt％
Silver powder 0.5wt%
Pearlescence 0.5wt%
BYK?358?????????????????????????????????????0.5wt％
EFKA3277????????????????????????????????????0.5wt％
The preparation method of the ultraviolet-curing paint of mentioning according to above-mentioned specification sheets that is used for the protection of aluminium or aluminium shape surface and decorates prepares the ultraviolet-curing paint that is used for aluminium or aluminium shape surface protection and decorates.
Embodiment 5.
Acrylic copolymer 45wt%
TPGDA?????????????????????????????????????????20wt％
EO-TMPTA??????????????????????????????????????10wt％
Irgacure?4265?????????????????????????????????3wt％
Irgacure?369??????????????????????????????????2wt％
Fluorescent material 8wt%
Disperbyk2000?????????????????????????????????1wt％
Tego?920??????????????????????????????????????0.5wt％
DEUCHEM432????????????????????????????????????0.5wt％
N-BUTYL ACETATE 5wt%
Virahol 5wt%
The preparation method of the ultraviolet-curing paint of mentioning according to above-mentioned specification sheets that is used for the protection of aluminium or aluminium shape surface and decorates prepares the ultraviolet-curing paint that is used for aluminium or aluminium shape surface protection and decorates.
The embodiment effect
Adopt mode applications such as spraying, roller coat, showering or brushing, the excessive useable solvents of viscosity during construction (butanone: dilution N-BUTYL ACETATE=1: 1), coating thickness is 20-40 μ m, effect is as follows behind ultraviolet light polymerization:
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Testing method | |
| Set time (S) | 5 | 3.5 | 3 | 6 | 5.5 | Company standard |
| Hardness (H) | 3 | 3 | 3 | 2 | 3 | GB6739-86 |
| Gloss or color | Gao Guang | Mute light | Blue | Flash effect | Fluorescent effect | Company standard |
| Sticking power (level) | 1 | 1 | 1 | 1 | 1 | GB9286-88 |
| Wear resistance (mg) | 0.008 | 0.005 | 0.004 | 0.006 | 0.007 | GB1768-79 |
| Water tolerance (240h) | No change | No change | No change | No change | No change | GB1733-79 |
| Acid resistance (72h) | No change | No change | No change | No change | No change | GB1763-79 |
| Alkali resistance (72h) | No change | No change | No change | No change | No change | GB1763-79 |
Claims (10)
1. ultraviolet-curing paint that is used for the protection of aluminium or aluminium shape surface and decorates, it is characterized in that: described system component and content are:
(methyl) acrylic acid modified prepolymer 20-50wt%
Reactive acrylate monomer 10-55wt%
Light trigger 2-6wt%
Auxiliary agent 0-5wt%
Mute light powder or pigment 0-30wt%
Solvent 0-30wt%.
2. coating as claimed in claim 1, it is characterized in that: described (methyl) acrylic acid modified prepolymer makes with ordinary method, and prepolymer is epoxy (methyl) acrylate, urethane (methyl) acrylate, polyester (methyl) acrylate, amino (methyl) acrylate, acrylic copolymer one or more mixtures wherein.
3. coating as claimed in claim 1 is characterized in that: olefin(e) acid ester monomer is in the described reactivity:
(1). the simple function group monomer has butyl acrylate, cyclohexyl acrylate, Isooctyl acrylate monomer or (methyl) Hydroxyethyl acrylate;
Perhaps (2). two monomers are tri (propylene glycol) diacrylate, dipropylene glycol diacrylate, neopentylglycol diacrylate, the third oxidation neopentylglycol diacrylate, ethoxyquin neopentylglycol diacrylate, two (Diethylene Glycol) diacrylates of phthalic acid or 1,6 hexanediyl ester;
Perhaps (3). polyfunctional monomer is Viscoat 295, ethoxyquin Viscoat 295, the third oxidation Viscoat 295, pentaerythritol triacrylate, double pentaerythritol C5 methacrylate or double pentaerythritol methacrylate;
The perhaps mixture of aforesaid propylene acid esters.
4. coating as claimed in claim 1 is characterized in that: described light trigger is that benzoin ethers, benzil ketals class, acetophenones, acyl group oxidation are Phosphorus, one or more mixtures in benzophenone or the aminated compounds; Perhaps one or more mixtures among the Darocur 1173 of Ciba-Geigy company, Irgacure 184, Irgacure 369, Irgacure 149, Irgacure 651, Irgacure 819, Irgacure 907 or the Darocur 4265; Perhaps TPO, ITX or their mixture; The perhaps mixture of above-mentioned light trigger.
5. coating as claimed in claim 1 is characterized in that: described auxiliary agent comprises flow agent, defoamer, Ricinate and anti-wear agent; Wherein the flow agent add-on is the 0.2-1wt% of coating total amount, and the defoamer add-on is the 0.1-0.5wt% of coating total amount, and the wetting dispersing agent add-on is the 0.5-2wt% of coating total amount, and the anti-wear agent add-on is the 0.5-3wt% of coating total amount; Described flow agent, defoamer, Ricinate and anti-wear agent use together or use separately.
6. coating as claimed in claim 5 is characterized in that:
Described flow agent is BYK 306, BYK 307, BYK 333, BYK 358, EFKA 3277, EFKA 3777, EFKA 3883, DEUCHEM 432, DEUCHEM 836 one or more mixtures wherein;
Described defoamer is BYK 052, BYK 055, DEUCHEM 2700, DEUCHDM 3100, Tego 920 one or more mixtures wherein;
Described wetting dispersing agent is Disperbyk 103, Disperbyk 104S, BYK-P104S, Disperbyk 161, Disperbyk 2000, EFKA 4010, DEUCHDM 904S one or more mixtures wherein;
Described anti-wear agent is BYK 920.
7. coating as claimed in claim 1 is characterized in that: described mute light powder is OK 500, OK 520, Grace C 1006, Hp 340, TS 100, Grace RAD 2005, SP4-9705 one or more mixtures wherein.
8. coating as claimed in claim 1 is characterized in that: described pigment comprises titanium dioxide or carbon black mineral dye; Phthalocyanine blue, green, the brown chrome yellow of the phthalein mountain valley with clumps of trees and bamboo or bright red pigment dyestuff; Bronze, silver powder, pearlescence, fluorescent material, illusion-colour pigment or reflective pigment.
9. coating as claimed in claim 8 is characterized in that: described mineral dye or pigment dyestuff are all in advance with the polyurethane acrylate prepolymer mixing and be ground to the fineness of diameter＜20 μ m.
10. coating as claimed in claim 1 is characterized in that: described solvent is butanone, vinyl acetic monomer, N-BUTYL ACETATE, Virahol, ethylene glycol monoethyl ether or ethylene glycol ether acetate one or more mixtures wherein.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA031502555A CN1487033A (en) | 2002-08-07 | 2003-07-23 | Ultraviolet ray cured paint for surface treatment or alumium ou aluminium sections |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN02126002 | 2002-08-07 | ||
| CN02126002.8 | 2002-08-07 | ||
| CNA031502555A CN1487033A (en) | 2002-08-07 | 2003-07-23 | Ultraviolet ray cured paint for surface treatment or alumium ou aluminium sections |
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| Publication Number | Publication Date |
|---|---|
| CN1487033A true CN1487033A (en) | 2004-04-07 |
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|---|---|---|---|
| CNA031502555A Pending CN1487033A (en) | 2002-08-07 | 2003-07-23 | Ultraviolet ray cured paint for surface treatment or alumium ou aluminium sections |
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| CN100343344C (en) * | 2005-12-26 | 2007-10-17 | 中国化工建设总公司常州涂料化工研究院 | Ultraviolet curing coating for metal plating surface protection |
| CN100415841C (en) * | 2004-11-25 | 2008-09-03 | 比亚迪股份有限公司 | Ultraviolet light curing yaguang coating and its production thereof |
| CN100465671C (en) * | 2005-02-02 | 2009-03-04 | 东洋油墨制造株式会社 | Coloring composition,Color filter within this and its producing method |
| WO2009146589A1 (en) * | 2008-06-06 | 2009-12-10 | Ding Naijin | A flakeboard surfaced with aluminium foil coated with uv-cured paint |
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| CN100415841C (en) * | 2004-11-25 | 2008-09-03 | 比亚迪股份有限公司 | Ultraviolet light curing yaguang coating and its production thereof |
| CN100465671C (en) * | 2005-02-02 | 2009-03-04 | 东洋油墨制造株式会社 | Coloring composition,Color filter within this and its producing method |
| CN100343344C (en) * | 2005-12-26 | 2007-10-17 | 中国化工建设总公司常州涂料化工研究院 | Ultraviolet curing coating for metal plating surface protection |
| EP2035794B1 (en) * | 2006-06-27 | 2020-05-06 | 3M Innovative Properties Company | Colorimetric sensors, array of sensors, sensor device and method of detecting radiation or thermal energy |
| WO2009146589A1 (en) * | 2008-06-06 | 2009-12-10 | Ding Naijin | A flakeboard surfaced with aluminium foil coated with uv-cured paint |
| WO2010078799A1 (en) * | 2009-01-06 | 2010-07-15 | 深圳桑菲消费通信有限公司 | Uv coating for magnesium-aluminum alloy surface spraying |
| CN101880503A (en) * | 2010-07-23 | 2010-11-10 | 佛山市顺德区鸿昌涂料实业有限公司 | UV surface paint applied to electrostatic coating |
| CN101880503B (en) * | 2010-07-23 | 2012-12-05 | 佛山市顺德区鸿昌涂料实业有限公司 | UV surface paint applied to electrostatic coating |
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