CN1482209A - Production method of vinegar powder from bamboo or timber vinegar material - Google Patents
Production method of vinegar powder from bamboo or timber vinegar material Download PDFInfo
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- CN1482209A CN1482209A CNA021295344A CN02129534A CN1482209A CN 1482209 A CN1482209 A CN 1482209A CN A021295344 A CNA021295344 A CN A021295344A CN 02129534 A CN02129534 A CN 02129534A CN 1482209 A CN1482209 A CN 1482209A
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- jealous woman
- bamboo
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
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Abstract
The present invention relates to charcoal production with bamboo and wood material and is especially the preparation process of high quality vinegar powder with the vinegar liquid collected during producing charcoal with bamboo and arbor material. The preparation process includes collecting vinegar liquid from charcoal kiln with smoke exhaust temperature of 80-150 deg.c and inside temperature of 350-800 deg.c; processing the vinegar liquid with separating column comprising active carbon, quartz sand and cationic exchange resin and subsequent quiescence and filtering or direct distillation to obtain pure vinegar liquid; quiescence to separate and decompressing concentration; and high speed centrifugal spray drying in drying chamber or ion exchange to obtain pure vinegar powder.
Description
Technical field
The invention belongs to bamboo or tall this plant of wooden class is the charcoal processing field of raw material, and the jealous woman liquid of being gathered when particularly being the raw material charcoal processing with bamboo or tall this plant of wooden class is raw material, prepares the method for high-quality bamboo or wooden class jealous woman powder.
Background technology
It is two overall situation problems of puzzlement social development that topsoil and water pollute always; in today that environment constantly worsens; environment protection will become Eternal Theme; under this background; a kind of is raw material with bamboo or tall this plant of wooden class; especially be the bamboo leachate that the raw material charcoal processing is extracted with the bamboo, arise at the historic moment as emerging function and the required high-tech bamboo of environment protection matter product.In the past, the tail gas when making charcoal was directly to emit, and did not collect; Afterwards, it is found that formed jealous woman liquid but had very high utility value after the tail gas of heat is met freezing air, as can be used as plant-growth promotion and mediator agent, industrial raw material, sanitas raw material, coal stain, a filial piety agent, deodorizing composition, wastewater purificant etc.For this reason, in the charcoal processing process, people have begun development and use and the research to wooden, ature of coal etc. being the jealous woman liquid of raw material extraction.The development and use of jealous woman liquid and research is the history in existing more than 100 year abroad, and obtained positive effect; As all being to be major product in countries such as Japan, Korea S to produce jealous woman liquid; Development and use at China's bamboo leachate then just begin, and all kinds of jealous woman liquid is difficult to obtain high-quality all kinds of jealous woman liquid owing to the byproduct as charcoal processing.
China is that the world produces bamboo big country, " bamboo culture " is the important component part of Chinese 5,000 years of civilization, bamboo is described as the sunrise industry of 21st century, but bamboo make charcoal and the Application and Development and scientific research of bamboo leachate aspect, the situation that its work lags behind is very outstanding, and the development space of bamboo industry and potentiality are huge.
Bamboo or pyroligneous liquor belong to acid, in high-quality bamboo or pyroligneous liquor, contain moisture content 85-90wt%, organism 10-15wt% (kind surplus in the of 280), wherein, acids such as formic acid Butyrecacid account for about 50%, secondly are multiple organic compound such as amino acid, alcohol, phenol, hexanoyl, flavones, aldehydes and ring-type fat.
Summary of the invention
The purpose of this invention is to provide a kind of is the method for feedstock production jealous woman powder with bamboo or timber vinegar material, makes all kinds of jealous woman liquid such as bamboo or wood become solid, reduces production costs when transportation is stored and be easy to use, improves the effective component content and the product quality of jealous woman powder,
Of the present invention is the method for feedstock production jealous woman powder with bamboo or timber vinegar material, and this method steps comprises:
(1). the collection of bamboo or pyroligneous liquor
When gathering bamboo or pyroligneous liquor, the smoke outlet temperature of the kiln in the sintering is 80 ℃～150 ℃, and kiln temperature is 350 ℃～800 ℃;
(2). prepare pure jealous woman liquid
The jealous woman liquid that step (1) is gathered leaves standstill, leaches behind the separator column that gac, quartz sand, Zeo-karb are formed, obtain pure jealous woman liquid, wherein quartz sand can account for that 75～85wt%, gac can account for 3～5wt%, Zeo-karb can account for 10～20wt%;
Or the jealous woman liquid that step (1) is gathered directly distilled obtain pure jealous woman liquid;
Or the jealous woman liquid that step (1) is gathered is directly by Zeo-karb, the pure jealous woman liquid of the various compositions of extraction separation;
The jealous woman liquid that gained is pure is that proportion is 1.02～1.05, and the pH value is 2～3 maroon transparent liquid;
(3). carry out concentrating under reduced pressure after the pure jealous woman liquid that step (2) is obtained leaves standstill, the temperature in the thickener is 40 ℃～90 ℃; The proportion that obtains concentrated solution is 1.0～1.2;
(4). the spissated jealous woman liquid that step (3) obtains is put into kiln, and inlet temperature is 80 ℃～95 ℃, and dry room temp is 120 ℃～140 ℃, carries out hig h-speed centrifugal spray drying, the various consummate jealous woman powder that extraction separation is required;
Or with the required various consummate jealous woman powder of cationic exchange extraction separation.
(5). the consummate jealous woman powder that can further step (4) be obtained does not add any bonding agent, and granulation on tablets press can be prepared required particle.
Described gac is acid gac, as have the 303 type indefinite form granulated active carbons that limit company produces with Huzhou, Zhejiang Province San Shan charcoal.
Described Zeo-karb is acidic resins, as the 732 type Zeo-karbs that can use Deqing, Zhejiang Province county environment-friendly materials factory to produce.
Jealous woman powder of the present invention promotes various organic content, the purity quality increases substantially, use pure water, or high-quality bamboo or pyroligneous liquor are with bamboo of the present invention or wooden jealous woman powder, at different use objects, dilute according to certain ratio, can be used as plant-growth promotion and mediator agent, industrial raw material, sanitas raw material, coal stain, send out the antioxidant of filial piety agent, deodorizing composition, wastewater purificant, medical material (it is medicine that bamboo juice is just arranged), fodder additives and grease production etc. in Compendium of Materia Medica.For example: add in the farm manure, play and remove stench and promote the microbial reproduction effect, raise pigs, the deodorizing in poulty house, be used for the soil prevention and control of plant diseases, pest control; Soil improvement, building up fertility to promote that nursery stock germinates, growth, drives away weeds and sewage disposal, pharmaceutically can fungi-proofing sterilization, itch stopping and diminish inflammation also has certain curative effect to allergic dermatitis, hepatopathy, diabetes; As fodder additives, improve domestic animal, the meat of fish improves the quality of egg and improves nutrition.
The present invention will fire the flue gas that produces in all kinds of bamboos or the charcoal process and be made full use of, and deep processing makes product like this, both solve some problems that exist in the environmental protection, play active effect for environment protection again.
The present invention not only solves and obtains high-quality jealous woman liquid, initiated jealous woman liquid is become the jealous woman powder, and solve storage, transportation and easy to use in reduced production cost significantly, be to achieve many things at one stroke.The more important thing is and saved timber, effectively protected continuous utilization and the comprehensive exploitation of the forest reserves and bamboo grove.
Embodiment
Embodiment 1.
80 ℃～90 ℃ of the smoke outlet temperature of the native stove that burns bamboo charcoal, during 350 ℃～400 ℃ of kiln temperatures, collect bamboo jealous woman stoste 1000kg at the smoke outlet place of kiln, through gac, quartz sand, Zeo-karb blended separator column, obtain pure jealous woman liquid, wherein, the separator column material consists of quartz sand 75%, gac 5% (Huzhou, Zhejiang Province San Shan charcoal have the 303 type indefinite form granulated active carbons that limit company produces), Zeo-karb 20% (the 732 type Zeo-karbs that Deqing, Zhejiang Province county environment-friendly materials factory produces); Enter the concentrating under reduced pressure device after pure bamboo leachate left standstill and concentrate, the concentrating under reduced pressure temperature is 40 ℃～90 ℃, the proportion of concentrated solution be 1.12, pH2.8, enter spray-dryer then and carry out spraying drying, obtaining dry powder is 39.2 kilograms.By analysis: acetate type content is 75wt%, and flavonoid content is 15wt%, and other organic compound content is 10wt%.Can be used as plant-growth promotion and mediator agent etc.Embodiment 2.
140 ℃～150 ℃ of the smoke outlet temperature of the native stove that burns bamboo charcoal, during 750 ℃～800 ℃ of kiln temperatures, collect bamboo jealous woman stoste 1000kg at the smoke outlet place of kiln, through gac, quartz sand, Zeo-karb blended separator column, obtain pure jealous woman liquid, wherein, the separator column material consists of quartz sand 80%, gac 3% (Huzhou, Zhejiang Province San Shan charcoal have the 303 type indefinite form granulated active carbons that limit company produces), Zeo-karb 17% (the 732 type Zeo-karbs that Deqing, Zhejiang Province county environment-friendly materials factory produces); Enter the concentrating under reduced pressure device after pure bamboo leachate left standstill and concentrate, the concentrating under reduced pressure temperature is 60 ℃～85 ℃, the proportion of concentrated solution be 1, pH is 3, enters spray-dryer then and carries out spraying drying, obtaining dry powder is 37.5 kilograms.By analysis: acetate type content is 60wt%, and flavonoid content is 11wt%, and other organic compound content is 28wt%, impurity 1wt%.Can be used as industrial raw material.
Embodiment 3.
100 ℃～110 ℃ of the smoke outlet temperature of the native stove that burns bamboo charcoal, during 500 ℃～550 ℃ of kiln temperatures, collect bamboo jealous woman stoste 1000kg at the smoke outlet place of kiln, the jealous woman liquid of gathering is directly distilled obtain pure jealous woman liquid; Entering the concentrating under reduced pressure device after pure bamboo leachate left standstill concentrates, the concentrating under reduced pressure temperature is 40 ℃～50 ℃, the proportion of concentrated solution be 1, pH is 2.2, with cationic exchange (the 732 type Zeo-karbs that Deqing, Zhejiang Province county environment-friendly materials factory produces) the required various consummate jealous woman powder of extraction separation, obtaining dry powder is 38.5 kilograms.By analysis: acetate type content is 80wt%, and flavonoid content is 12wt%, and other organic compound content is 8wt%.Can be used as industrial raw material.
Embodiment 4.
140 ℃～150 ℃ of the smoke outlet temperature of the native stove that burns charcoal, during 700 ℃～750 ℃ of kiln temperatures, collect wooden jealous woman stoste 1000kg at the smoke outlet place of kiln, the jealous woman liquid of gathering is passed through Zeo-karb, the pure jealous woman liquid of the various compositions of extraction separation, described Zeo-karb are the 732 type Zeo-karbs that Deqing, Zhejiang Province county environment-friendly materials factory produces; Enter the concentrating under reduced pressure device after pure pyroligneous liquor left standstill and concentrate, the concentrating under reduced pressure temperature is 85 ℃～90 ℃, the proportion of concentrated solution be 1.2, pH is 2, enters spray-dryer then and carries out spraying drying, obtaining dry powder is 40 kilograms.By analysis: acetate type content is 75wt%, and flavonoid content is 8wt%, and other organic compound content is 15%, impurity 2wt%.Can be used as industrial raw material.
Claims (7)
1. one kind is the method for feedstock production jealous woman powder with bamboo or timber vinegar material, it is characterized in that: this method steps comprises:
(1). the collection of bamboo or pyroligneous liquor
When gathering bamboo or pyroligneous liquor, the smoke outlet temperature of the kiln in the sintering is 80 ℃～150 ℃, and kiln temperature is 350 ℃～800 ℃;
(2). prepare pure jealous woman liquid
The jealous woman liquid that step (1) is gathered leaves standstill, leaches behind the separator column that gac, quartz sand, Zeo-karb are formed, obtain pure jealous woman liquid, wherein the composition quartz sand of material accounts for that 75～85wt%, gac account for 3～5wt%, Zeo-karb accounts for 10～20wt% in the separator column;
Or the jealous woman liquid that step (1) is gathered directly distilled obtain pure jealous woman liquid;
Or the jealous woman liquid that step (1) is gathered is directly by Zeo-karb, the jealous woman liquid of the various compositions of extraction separation;
(3). carry out concentrating under reduced pressure after the pure jealous woman liquid that step (2) is obtained leaves standstill, the temperature in the thickener is 40 ℃～90 ℃;
(4). the spissated jealous woman liquid that step (3) obtains is put into kiln, and dry room temp is 120 ℃～140 ℃, carries out hig h-speed centrifugal spray drying, the various consummate jealous woman powder that extraction separation is required;
Or with the required various consummate jealous woman powder of cationic exchange extraction separation;
Described gac is acid gac; Described Zeo-karb is acidic resins.
2. the method for claim 1 is characterized in that: the directly granulation on tablets press of consummate jealous woman powder that described step (4) obtains.
3. the method for claim 1, it is characterized in that: the inlet temperature of described step (4) kiln is 80 ℃～95 ℃.
4. the method for claim 1, it is characterized in that: described acid gac is 303 type indefinite form granulated active carbons.
5. the method for claim 1, it is characterized in that: described acidic resins are 732 type Zeo-karbs.
6. the method for claim 1, it is characterized in that: the jealous woman liquid that gained is pure is that proportion is 1.02～1.05, and the pH value is 2～3 maroon transparent liquid.
7. the method for claim 1, it is characterized in that: the proportion of the concentrated solution that described step (3) obtains is 1.0～1.2.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB021295344A CN1221634C (en) | 2002-09-12 | 2002-09-12 | Production method of vinegar powder from bamboo or timber vinegar material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB021295344A CN1221634C (en) | 2002-09-12 | 2002-09-12 | Production method of vinegar powder from bamboo or timber vinegar material |
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| Publication Number | Publication Date |
|---|---|
| CN1482209A true CN1482209A (en) | 2004-03-17 |
| CN1221634C CN1221634C (en) | 2005-10-05 |
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| Application Number | Title | Priority Date | Filing Date |
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| CNB021295344A Expired - Fee Related CN1221634C (en) | 2002-09-12 | 2002-09-12 | Production method of vinegar powder from bamboo or timber vinegar material |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1326973C (en) * | 2005-11-01 | 2007-07-18 | 韦勇 | Technique for producing bamboo vinegar powder |
| CN102008071A (en) * | 2010-10-07 | 2011-04-13 | 吴子平 | Fresh bamboo juice extraction process |
| CN108207530A (en) * | 2018-02-11 | 2018-06-29 | 广西宜州天源绿佳农业科技有限公司 | A kind of implantation methods of Selenium-enriched radish |
| CN115959887A (en) * | 2022-12-14 | 2023-04-14 | 吉林省德乾堂弓形虫研究所 | Preparation method of pyroligneous ceramic product for external patch |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100374040C (en) * | 2006-04-28 | 2008-03-12 | 郑兴福 | Bamboo salt preparation method |
-
2002
- 2002-09-12 CN CNB021295344A patent/CN1221634C/en not_active Expired - Fee Related
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1326973C (en) * | 2005-11-01 | 2007-07-18 | 韦勇 | Technique for producing bamboo vinegar powder |
| CN102008071A (en) * | 2010-10-07 | 2011-04-13 | 吴子平 | Fresh bamboo juice extraction process |
| CN102008071B (en) * | 2010-10-07 | 2013-03-20 | 吴子平 | Fresh bamboo juice extraction process |
| CN108207530A (en) * | 2018-02-11 | 2018-06-29 | 广西宜州天源绿佳农业科技有限公司 | A kind of implantation methods of Selenium-enriched radish |
| CN108207530B (en) * | 2018-02-11 | 2021-04-16 | 浙江窝里宅农业发展有限公司 | Planting method of selenium-rich radishes |
| CN115959887A (en) * | 2022-12-14 | 2023-04-14 | 吉林省德乾堂弓形虫研究所 | Preparation method of pyroligneous ceramic product for external patch |
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| CN1221634C (en) | 2005-10-05 |
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Granted publication date: 20051005 Termination date: 20130912 |