CN1412543A - Optical parameter measurement device of fluorescent powder for vacuum UV - Google Patents
Optical parameter measurement device of fluorescent powder for vacuum UV Download PDFInfo
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- CN1412543A CN1412543A CN 01131964 CN01131964A CN1412543A CN 1412543 A CN1412543 A CN 1412543A CN 01131964 CN01131964 CN 01131964 CN 01131964 A CN01131964 A CN 01131964A CN 1412543 A CN1412543 A CN 1412543A
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Abstract
The optical parameter measuring equipment of fluorescent powder for vacuum UV light includes vacuum box with vacuum pump, carriage mounted in the vacuum box and connected with driving device, several sample disks for holding fluorescent powder which are distributed on the carriage, coding device which is mounted on the end of driving device extented from vacuum box and used for detecting sample disk number, at least an exciting light source mounted in the vacuum box and used for irradiating sample disk and a photoelectric measuring instrument for receiving emissive light of sample. Said invention can measure several optical parameters of spectrum distribution, relative brightness, chroma coordinate, colour purity, colour temperature, peak emissive wavelength and radiation degree and band width, etc. of the fluorescent powder.
Description
Technical field
The present invention relates to the optical parameter measurement device of fluorescent powder for vacuum UV.
Background technology
The high-definition large-screen flat pannel display has become the focus and the trend of current information technical development, adopt high-octane vacuum ultraviolet-excited color plasma flat pannel display (being called for short PDP), become the outstanding person of giant-screen flat pannel display, the wall built-up colour TV is become a reality.One of critical material that PDP is used is a fluorescent powder, because the swift and violent projection of PDP technology, and used fluorescent powder and test anxious To be improved accordingly.
Because PDP fluorescent powder adopts the stronger excited by vacuum ultraviolet of photon energy, and used spectrum and optical parameter measuring instrument device is in ultraviolet one visible range usually, therefore, can't use.At present, can be used to measure the method for fluorescent powder for vacuum UV optical parametric, mainly contain three kinds in the document.The one, on the high energy synchronous radiation accelerator, utilize the vacuum-ultraviolet light excitated fluorescent powder of a certain node output luminous, again through the emission spectrum of spectrometer measurement fluorescent powder.This method not only needs to use synchrotron, and will add a whole set of optics extraction system, so complex structure, and is bulky, and price is extremely expensive, is difficult to obtain to use in actual production; The 2nd, can utilize the high-temperature plasma radiation source, constantly inject required inert gas and making it be in ionization under the high-temperature plasma state, and launching required vacuum-ultraviolet light, excitated fluorescent powder is luminous, again through spectrometer measurement fluorescent powder spectroscopic data.The system of this method is also huger, and needs continuous inert gas injecting and form high-temperature plasma, and many inconvenience are also arranged in actual applications; The third method is the vacuum ultraviolet continuous discharge spectrum that adopts deuterium lamp to produce, and through the vacuum ultraviolet monochromator beam split, obtains the vacuum ultraviolet spectroscopy of single wavelength, excitated fluorescent powder.Signal is very weak after the vacuum-ultraviolet light process vacuum ultraviolet monochromator beam split in the method, measures signal to noise ratio (S/N ratio) and poor stability.In addition, the measurement optical path length of this method, vacuum tightness requires high.And above-mentioned these measuring methods can only obtain the part optical parametric of vacuum uv phosphor, have many problems in actual applications.
Summary of the invention
Purpose of the present invention aims to provide a kind of optical parameter measurement device of simple in structure, price is low, volume is little, measurement parameter is complete, precision is high, easy to use fluorescent powder for vacuum UV.
The optical parameter measurement device of the fluorescent powder for vacuum UV of invention comprises the vacuum tank of being with vacuum pump, be provided with the carriage that connects with drive unit in the vacuum tank, be distributed with the sample disc that several put fluorescent powder on the carriage, stretch out the code device that the vacuum tank end is equipped with test sample dish numbering at drive unit, at least one excitation source and radiative photoelectric measuring instrument of at least one reception sample to the sample disc irradiates light is installed on vacuum tank.
Above-mentioned vacuum tank is vacuum state or is filled with inert gas, as helium, xenon, neon, nitrogen etc.
Said photoelectric measuring instrument can be device in vacuum tank and the brightness detector that is connected with measurement instrument outside the case, or be plugged on the nitometer of vacuum tank eyelet, or the spectral radiometer that links to each other with vacuum tank by condenser or optical fiber.
Said excitation source can be vacuum UV lamp or electron-beam excitation source or ion beam excitaton source or laser beam excitaton source.
Drive unit can be worm and gear transmission or gear drive, also can be that stepper motor directly drives.This drive unit driven bracket is made rotation or moving linearly.
For preventing direct reflection, usually, make the sample in the excitation source vertical irradiation sample disc, photoelectric measuring instrument receives sample emission light from the direction with sample normal angle at 45, perhaps excitation source is from shining sample with the direction at sample normal angle at 45, and photoelectric measuring instrument receives sample emission light perpendicular to the sample disc direction.
The effect that compared with the prior art the present invention obtains is: the present invention is turned round by the drive unit driven bracket; make the sample in the corresponding numbered samples dish of excitation source direct irradiation; utilize photoelectric measuring instrument; reception is in the emission light of the fluorescent powder sample of vacuum or inert gas shielding; can record the spectral distribution of vacuum uv phosphor, many optical parametrics such as relative brightness, chromaticity coordinates, excitation, colour temperature, peak emission wavelength and radiancy, bandwidth.It is simple in structure, price is low, and measurement parameter is more complete, the precision height, and signal is strong, and is easy to use.
Description of drawings
Fig. 1 is a kind of concrete structure synoptic diagram of the present invention.
Embodiment
With reference to Fig. 1, the optical parameter measurement device of fluorescent powder for vacuum UV of the present invention comprises the vacuum tank 5 of being with vacuum pump 10,19 is case lid among the figure, be provided with the carriage 7 that connects with drive unit 8 in the vacuum tank, this example, drive unit adopts Worm and worm-wheel gearing, and it links to each other with the rotating disc type carriage by vacuum seal axle 8-1, the driven bracket rotation.On carriage, be distributed with the sample disc 6 that several are used to put fluorescent powder, vacuum seal axle 8-1 is in the code device 9 that the outer end of vacuum tank is equipped with test sample dish numbering, here, code device is to be made of the photoelectricity interrupter 9-2 that code-wheel 9-1 with pilot hole and notch and detection are encoded, and perhaps also can adopt optical electric axial angle encoder.Excitation source 1 to the sample disc irradiates light is installed on vacuum tank, in the illustrated example, what excitation source adopted is the vacuum UV lamp that volume is little, exposure intensity is big, it comprises the lamp chamber 21 with magnesium fluoride front window 20, two sparking electrodes 22 that link to each other with power supply 2 through lead-in wire are arranged in the lamp chamber, be filled with the inert gas of one or more mixing in the cavity, as fill helium, xenon or other inert gas, when discharge, produce stronger 147nm, the vacuum ultraviolet of 172nm or other wavelength.Usually, several vacuum UV lamp devices of being filled with different inert gas respectively on vacuum tank, are convenient to as required, are selected the vacuum ultraviolet irradiation sample of required wavelength, bring convenience to use.Two sparking electrodes in the vacuum UV lamp lamp chamber can be two plate electrodes, or two rod-shaped electrodes or the center is shaft-like, and the outer ring is an electrode cylindraceous, or two concentric type drum electrodes.In this example, receive the radiative photoelectric measuring instrument of sample and have two, one be device in vacuum tank and the brightness detector 4 that is connected with measurement instrument 3 outside the case, another is the spectral radiometer 11 that links to each other with vacuum tank by the optical fiber 13 that is plugged on vacuum tank eyelet 12.The diagram contrive equipment adopts the sample of vacuum UV lamp vertical irradiation sample disc, and brightness detector, optical fiber receive the sample reflected light from the direction with sample normal angle at 45.Wherein spectral radiometer 11 is connected with computing machine 18, in order to receive measurement data and control survey process with computing machine, measurement data is handled.Apparatus of the present invention can accurately obtain the spectral distribution of fluorescent powder for vacuum UV, many optical parametrics such as relative brightness, chromaticity coordinates, excitation, colour temperature, peak emission wavelength and radiancy, bandwidth.
Claims (10)
1. the optical parameter measurement device of fluorescent powder for vacuum UV, it is characterized in that it comprises the vacuum tank [5] of band vacuum pump [10], be provided with in the vacuum tank and carriage [7] that drive unit [8] connects, be distributed with several sample disc of putting fluorescent powder [6] on the carriage [7], stretch out the code device [9] that vacuum tank [5] end is equipped with test sample dish numbering at drive unit, at least one excitation source to the sample disc irradiates light [1] and the radiative photoelectric measuring instrument of at least one reception sample are installed on vacuum tank.
2. by the optical parameter measurement device of the described fluorescent powder for vacuum UV of claim 1, it is characterized in that being filled with inert gas or being vacuum state in the vacuum tank [5].
3. press the optical parameter measurement device of the described fluorescent powder for vacuum UV of claim 1, it is characterized in that said photoelectric measuring instrument is that device is in vacuum tank and the brightness detector [4] that is connected with measurement instrument [3] outside the case, or be plugged on the nitometer of vacuum tank eyelet [12], or the spectral radiometer [11] that links to each other with vacuum tank [5] by condenser or optical fiber [13].
4. by the optical parameter measurement device of the described fluorescent powder for vacuum UV of claim 3, it is characterized in that said spectral radiometer [11] is connected with computing machine [18].
5. press the optical parameter measurement device of the described fluorescent powder for vacuum UV of claim 1, it is characterized in that said excitation source [1] is a vacuum UV lamp, it comprises the lamp chamber [21] with magnesium fluoride front window [20], two sparking electrodes [22] that link to each other with power supply through lead-in wire are arranged in the lamp chamber, be filled with the inert gas of one or more mixing in the cavity.
6. press the optical parameter measurement device of the described fluorescent powder for vacuum UV of claim 5, it is characterized in that said sparking electrode [22] is two plate electrodes, or two rod-shaped electrodes or the center is shaft-like, the outer ring is an electrode cylindraceous, or two concentric type drum electrodes.
7. by the optical parameter measurement device of the described fluorescent powder for vacuum UV of claim 1, it is characterized in that said excitation source [1] is the electron-beam excitation source, or the ion beam excitaton source, or the laser beam excitaton source.
8. press the optical parameter measurement device of the described fluorescent powder for vacuum UV of claim 1, it is characterized in that the sample in excitation source [1] the vertical irradiation sample disc [6], photoelectric measuring instrument receives sample emission light from the direction with sample normal angle at 45, perhaps excitation source [1] is from shining sample with the direction at sample normal angle at 45, and photoelectric measuring instrument receives sample emission light perpendicular to the sample disc direction.
9. by the optical parameter measurement device of the described fluorescent powder for vacuum UV of claim 1, it is characterized in that said drive unit [8] is worm and gear transmission or gear drive or stepper motor directly drives.
10. press the optical parameter measurement device of the described fluorescent powder for vacuum UV of claim 1, it is characterized in that said code device [9] is by the code-wheel with pilot hole and notch [9-1] and detects photoelectricity interrupter [9-2] formation of encoding, or optical electric axial angle encoder.
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CNB01131964XA CN1171085C (en) | 2001-10-18 | 2001-10-18 | Optical parameter measurement device of fluorescent powder for vacuum UV |
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CNB01131964XA CN1171085C (en) | 2001-10-18 | 2001-10-18 | Optical parameter measurement device of fluorescent powder for vacuum UV |
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CN1412543A true CN1412543A (en) | 2003-04-23 |
CN1171085C CN1171085C (en) | 2004-10-13 |
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Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101498657B (en) * | 2008-01-31 | 2012-07-18 | 中国科学院福建物质结构研究所 | Optical spectrometer sample stand used for loading powder sample |
CN102728507A (en) * | 2011-04-15 | 2012-10-17 | 长庚大学 | Fluorescent powder coating equipment and method for detecting white light color temperature in real time in manufacturing process |
CN103604789A (en) * | 2013-11-25 | 2014-02-26 | 南京信息职业技术学院 | System and method for testing performance of fluorescent powder |
CN103811242A (en) * | 2013-10-21 | 2014-05-21 | 浙江开元光电照明科技有限公司 | Electrodeless fluorescent lamp simulation lamp making device |
CN106950191A (en) * | 2017-02-28 | 2017-07-14 | 电子科技大学 | Supporting detection sample produces the experimental system of spectral characteristic in the case where electronics notes excitation |
CN108169406A (en) * | 2017-12-15 | 2018-06-15 | 大连理工大学 | A kind of high temperature and pressure lubricating oil list drop evaporation and catch fire device and its application method |
CN108827892A (en) * | 2018-06-21 | 2018-11-16 | 芜湖市金马电子信息有限责任公司 | A kind of dry analysis device for food safety detection |
CN109540862A (en) * | 2018-12-28 | 2019-03-29 | 暨南大学 | A kind of phosphorescence performance testing device |
CN113092374A (en) * | 2021-04-12 | 2021-07-09 | 青岛科技大学 | Small-sized vacuum photoelectric test system |
-
2001
- 2001-10-18 CN CNB01131964XA patent/CN1171085C/en not_active Expired - Fee Related
Cited By (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101498657B (en) * | 2008-01-31 | 2012-07-18 | 中国科学院福建物质结构研究所 | Optical spectrometer sample stand used for loading powder sample |
CN102728507B (en) * | 2011-04-15 | 2014-08-13 | 长庚大学 | Fluorescent powder coating equipment and method for detecting white light color temperature in real time in manufacturing process |
CN102728507A (en) * | 2011-04-15 | 2012-10-17 | 长庚大学 | Fluorescent powder coating equipment and method for detecting white light color temperature in real time in manufacturing process |
CN103811242B (en) * | 2013-10-21 | 2016-08-17 | 浙江开元光电照明科技有限公司 | Electrodeless florescent lamp simulates lamp device processed |
CN103811242A (en) * | 2013-10-21 | 2014-05-21 | 浙江开元光电照明科技有限公司 | Electrodeless fluorescent lamp simulation lamp making device |
CN103604789B (en) * | 2013-11-25 | 2016-04-06 | 南京信息职业技术学院 | A kind of fluorescent powder Performance Test System and method of testing |
CN103604789A (en) * | 2013-11-25 | 2014-02-26 | 南京信息职业技术学院 | System and method for testing performance of fluorescent powder |
CN106950191A (en) * | 2017-02-28 | 2017-07-14 | 电子科技大学 | Supporting detection sample produces the experimental system of spectral characteristic in the case where electronics notes excitation |
CN106950191B (en) * | 2017-02-28 | 2019-11-05 | 电子科技大学 | Mating test sample generates the experimental system of spectral characteristic under electronics note excitation |
CN108169406A (en) * | 2017-12-15 | 2018-06-15 | 大连理工大学 | A kind of high temperature and pressure lubricating oil list drop evaporation and catch fire device and its application method |
CN108827892A (en) * | 2018-06-21 | 2018-11-16 | 芜湖市金马电子信息有限责任公司 | A kind of dry analysis device for food safety detection |
CN109540862A (en) * | 2018-12-28 | 2019-03-29 | 暨南大学 | A kind of phosphorescence performance testing device |
CN113092374A (en) * | 2021-04-12 | 2021-07-09 | 青岛科技大学 | Small-sized vacuum photoelectric test system |
CN113092374B (en) * | 2021-04-12 | 2022-11-15 | 青岛科技大学 | Small vacuum photoelectric test system |
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