CN1323591C - Technique for antisepsis and producinhg of cosmetics contg. fresh milk - Google Patents

Abstract

The present invention relates to the orrosion protection technique of fresh milk materials applied to cosmetics. The present invention comprises pasteurization to raw fresh milk and addition of a composite anticorrosion agent. When active ingredients in the fresh milk are reserved furthest, the present invention assures that the microbial indicator of the fresh milk materials conforms to the requirement for the production of the cosmetics. The present invention also provides a production process for the fresh milk containing cosmetics. After a cosmetic system is primarily emulsified, the fresh milk materials are added in the system when the temperature of the system is reduced to lower than 60 DEG C. After the fresh milk materials are stirred and are homogeneous, the temperature is continuously reduced, and then, operation is carried out according to a convention production method. The content of the fresh milk in the cosmetics is more than 5%. The present invention also further provides an emulsifier and an excipient which are optimized and applicable in the production of emulsion-shaped cosmetics which comprise the fresh milk.

Description

Anticorrosion and the production method that contains the fresh milk cosmetics

Technical field

The present invention relates to add the aseptic technic of the cosmetics of fresh milk, specifically relate to a kind of fresh-milk material be carried out preservative treatment, thereby realize containing effective corrosion-resistant technology of fresh milk cosmetics; The present invention also relates to the production technology that contains the fresh milk cosmetics simultaneously.

Background technology

The broad definition of cosmetics is meant to smear, to spray or other similar approach, impose on human body surface (as epidermis, hair, nail, lip etc.), play cleaning, maintain, beautify or eliminate the product of bad smell effect, this series products can have abirritation to using the position.From application point, cosmetics mainly comprise several big classes such as skin type, hair care category, hair washing class, cleaning class, beauty treatment class.

Along with growth in the living standard; the consumer also has more demand to the effect of all kinds of cosmetics; developing and produce the cosmetics with various nutrition or protection effect and strive for consumer's approval, improve the popularity of product, is the pursuit direction of numerous manufacturing enterprises.For reaching such effect, various nutritive and health protection components are all managed to add in the cosmetics, for example all kinds of plant extract compositions, and bioactie agent etc., and then indicate that product for example has effects such as whitening spot-removing, anti-ageing, skin nutrition or hair.

Utilize the fresh milk face and skin beautifying to have a long history, Ancient Chinese is put down in writing for this agrostology document " Japan hanako materia medica ": " cow's milk, profit skin, the lung that nourishes heart, analgesic poison "; Supplement to the Herbal carries again: " ox breast, the profit insertion tendon is thirsty ".According to relevant bibliographical information, Tang Dynasty in China name prince wife poplar Yuhuan once used " fresh milk shower " to maintain skin, made that skin is moist, appearance is gorgeous, left a good name through the years; The ancient egypt queen consort restrains Lou Bate and draws (Kleopatra) to come her ice flesh of maintenance to wash milk bath.

Fresh milk and dairy produce are nutritious, contain senior fat, range protein, vitamin and mineral matter, and the more B family vitamin that particularly wherein contains helps the reparative regeneration of Skin Cell, aging that can delaying skin; Contained iron, copper and vitamin A can make skin keep smooth and moisten; Whey in the milk has the elimination effect to facial wrinkles; Simultaneously, fresh milk and dairy produce can also provide the closure grease for skin, form film in case the moisture of skin evaporation; In addition, fresh milk can also temporarily provide moisture, Glycerin, and the protection epidermis, and have removing beverage, anticracking, wrinkle resistant, the anti-ageing effect of waiting for a long time, and can make the skin smooth softness delicate, skin there is significant whitening effect; The pitch-black minimizing of hair is come off ....Along with deepening continuously of development of science and technology and fresh milk skin care research, the beauty and skin care effect of fresh milk is familiar with by people gradually and is accepted, even has the people to propose the saying of " fresh milk is the most natural cosmetics ".

Though fresh milk beauty treatment has had long history, and fresh milk can play good cosmetology effect, clear and definite theoretical foundation arranged as foundation again.But, but seldom can see in the market and real contain the fresh milk cosmetics (promptly, with the product of fresh milk) as main nutritional activities composition, a chief reason is exactly, the abundant nutrients environment of fresh milk is fit to the breeding of bacterium very much, cause raw milk itself very easily putrid and deteriorated,, also be difficult to preserve more than 24 hours even take conventional sterilization treatment.Add in the cosmetics as primary raw material, how to accomplish can be effectively anticorrosion, can save the beneficiating ingredient of fresh milk again from damage, becomes the key that restriction contains the fresh milk Cosmetic Manufacture.So, though have some to add dairy products on the cosmetics market at present, all indicate and wherein added milk protein, milk elite or milk powder, no matter but be to add quantity, still (dairy produce that is added in fact present most of cosmetics all belongs to the recombined milk type to add the dairy produce kind, be not pure fresh-milk truly), these products all are difficult to be called the real fresh milk cosmetics that contain.

On the other hand, owing to contain a large amount of electrolyte in the complicated ingredient of fresh milk,, might destroy the stability of cosmetic emulsions system as it is added in the cosmetics; Simultaneously, because fresh milk self contains the functional components that can produce emulsifying effectiveness, also have higher requirement for the stable of some cosmetic emulsions systems.

Therefore; how can both guarantee effective addition of fresh milk in the cosmetics; product appearance, inherent quality are maintained a long-term stability; make us being easy to accepting; can also keep simultaneously the multivitamin that contains in the fresh milk, to human body beneficial's trace element and can moisten, protect the fatty composition of skin; and can further alleviate skin-balance imbalance and the skin irritatin that produces because of cleaning, be really to realize the fresh milk key point that extensive use also can utilize modernized industrial means to produce in cosmetics.

Summary of the invention

Main purpose of the present invention at first is to provide the aseptic technic that contains the fresh milk cosmetics, that is, the anticorrosion preconditioning technique of fresh milk makes fresh-milk material be fit to add in the cosmetics, and also making suitability for industrialized production contain the fresh milk cosmetics becomes possibility.

Another main purpose of the present invention is to provide a kind of production to contain the technical process of fresh milk cosmetics, reach production technology targetedly by preservative treatment to fresh-milk material, be implemented in and add fresh milk in the cosmetics and produce stable in properties, have the purpose that contains the fresh milk cosmetics of good beauty functions.

The front is mentioned, contain a large amount of nutrition and active component in the fresh milk (fresh breast), also comprise a large amount of bacteriums, country should be smaller or equal to 500,000 CFU/g to total number of bacteria in the one-level milk of regulation in the fresh cow's milk acquisition criteria (GB6914-86), the fresh-milk material that reaches this standard can satisfy the hygienic requirements of processing diet product, and national standard is smaller or equal to 1000CFU/g to the requirement of bacterial population in the cosmetics, and the fresh-milk material that as seen meets processing diet product industry GB can't be directly used in the production of cosmetics.If fresh milk is used for daily cosmetics, what at first will solve promptly is the further sterilization and the preservative treatment problem of fresh milk.

In present Cosmetic Manufacture to the sterilization and the anti-corrosion method of raw material, high-temperature sterilization, pasteurization and the interpolation anticorrisive agent bacteria growing inhibiting of comprising commonly used.The applicant discovers, for fresh dairy milk starting material, though high temperature sterilization can kill most of bacterium, effectively prevents production and the breeding of bacterium, has destroyed the self-contained various bioactive ingredients of fresh breast, and nutritive effect will be had a greatly reduced quality; Though the most of various effective bioactive ingredients that keeps fresh breast of traditional pasteurization energy, wherein active microorganism content also is higher than the regulation in the national standard far away, can not satisfy the Cosmetic Manufacture needs.At this situation, the present invention finds pasteurization is combined with aseptic technic, and raw material fresh milk is implemented preservative treatment, and the fresh milk after the processing can be used as the raw material of fresh milk cosmetics, the cosmetics of producing had both kept the beneficiating ingredient of fresh milk, and can satisfy the quality requirements of product.

The method according to this invention is implemented to add selected anticorrisive agent again behind the pasteurization to fresh milk, and the fresh milk after handling like this can be used as the raw material of fresh milk cosmetics.Through the anticorrisive agent experiment screening to using always in the Cosmetic Manufacture, the applicant finds to adopt selected anticorrisive agent to carry out composite becoming in the fresh milk of composite anti-corrosive preparation adding behind pasteurization, and this fresh milk can be used as the raw material of Cosmetic Manufacture.The method for anticorrosion treatment of fresh milk described in the present invention comprises:

Raw milk is carried out pasteurization;

Add compound preservative in the fresh milk behind the pasteurization, described anticorrisive agent is selected from least two kinds in the following group: 2-methyl-4-isothiazoline-3-ketone (MIT), 2-bromo-2-nitro-1, ammediol (6685), 1,3-dihydroxymethyl-5,5-dimethyl hydantoin (DMDM), 3-iodo-2-propynyl butyl carbamate (IPBC) and [N-methylol-N-(1,3-dihydroxymethyl-2,5-diketone-4-imidazolidinyl)-the N-methylolurea] (extremely beautiful).

Aseptic technic of the present invention proposes at the characteristic of fresh milk, and the fresh milk after preservative treatment should be able to keep the distinctive active nutrient component of fresh milk, requires simultaneously in subsequent production and shelf life of products, and the character of product and bacterium index are all up to specification.Specifically, the anticorrisive agent that is fit to the inventive method not only should effectively suppress bacterial reproduction in the fresh milk, also should be able to stablize compatiblely with fresh milk, so the present invention has finally determined above-mentioned compound preservative, thereby reaches the antiseptic effect of high-efficiency broad spectrum.

Preferably, described anticorrisive agent is for being selected from 2-bromo-2-nitro-1, ammediol (6685), 3-iodo-2-propynyl butyl carbamate (IPBC) and [N-methylol-N-(1,3-dihydroxymethyl-2,5-diketone-4-imidazolidinyl)-and the N-methylolurea] at least two kinds compound preservative in (extremely beautiful).

More preferably, take all factors into consideration factors such as excitant, cost performance, can in the process fresh milk of pasteurized process, add the composite product of forming by following three kinds of anticorrisive agents: 2-bromo-2-nitro-1, ammediol (6685), [N-methylol-N-(1,3-dihydroxymethyl-2,5-diketone-4-imidazolidinyl)-and the N-methylolurea] (extremely beautiful) be 1-2: 3-5 with the compound proportion of 3-iodo-2-propynyl butyl carbamate (IPBC): 1.

The addition of described anticorrisive agent is preferably about the 0.1-1.5% of fresh milk quality, more preferably about 0.2-1%.

The applicant handles in different ways to raw material fresh milk (according to the fresh breast of GB purchase), and the microorganism that detects 48 hours changes, and significantly reduces (seeing also shown in the table 1) through bacterial content in the fresh milk after pasteurization+preservative treatment as can be seen.

Table 1

Milk products	Immediately (enter factory)	24 hours (0-5 ℃)	48 hours (0-5 ℃)
				Purchase fresh breast	300,000-400,000 CFU/g	Not count enable	Not count enable
Fresh breast behind the pasteurization	0.5 ten thousand-0.8 ten thousand CFU/g	1.5 ten thousand-20,000 CFU/g	30,000-40,000 CFU/g
				Fresh breast after pasteurization+preservative treatment	0.5 ten thousand-0.8 ten thousand CFU/g	300-500CFU/g	≤10CFU/g

Be appreciated that, raw material as Cosmetic Manufacture, even through preservative treatment, fresh milk also must be preserved in the environment of strict health before entering subsequent handling, for example, should be kept at and be equipped with in stainless steel circle (the not having the dead angle) refrigerant tank have temperature control and to stir, guarantee that raw milk can preserve more than 24 hours, but because the characteristic of fresh milk, suggestion is no more than 48 hours as far as possible at low temperature and steady temperature (0-5 ℃) following holding time.

The present invention has provided a kind of production on the other hand and has contained the fresh milk cosmetic technology, and this method comprises:

Make the oil phase and the water of cosmetic material carry out preliminary emulsification earlier, when the temperature of this emulsification system is reduced to below 60 ℃, preferred 50-60 ℃ of adding implemented anticorrosion pretreated fresh-milk material according to the method for the invention and added mutually with other, homogeneous makes the interpolation phased soln not have bubble fully and in the system to system through stirring also, further requires to finish follow-up routine operation according to product and prescription after the cooling.

The fresh milk cosmetics that contain involved in the present invention are meant that fresh milk content is at the cosmetics more than 5% in the final products, the cosmetics that the inventive method is produced comprise skin type, cleaning class, hair care category, hair washing class and beauty treatment class etc., for example, skin lotion (frost or honey), mildy wash or bath oil, hair care breast, hair washing breast etc.

The method according to this invention, be the forfeiture of avoiding active component in the fresh milk and the Over emulsfication phenomenon of fresh milk, guarantee the beauty functions of fresh milk in cosmetics, in the oil-in-water type production, fresh milk should be added to as interpolation after oil phase and the preliminary emulsification of water mixed system, the temperature that should control emulsification system when adding fresh milk simultaneously can not be too high, after adding, fresh milk should make reactor keep maximum vacuum, start quick stirring homogeneous, make and add phased soln fully and can lower the temperature when not having bubble and finish the later stage operation according to routine production.

According to preferred version of the present invention, the addition of described fresh milk is the 5-80% of this cosmetics gross weight, and for the cream kind product of oil-in-water type, wherein the preferred addition of fresh milk is 5-50%.

As front by the agency of, one of key of the present invention has provided the preservative treatment technology to fresh-milk material, for the various productions that contain the fresh milk cosmetics are laid a good foundation.After finishing the interpolation of fresh-milk material according to the method described above, can finish final operation, for example additive of the nutritional agents that interpolation is relevant, necessity and anticorrisive agent etc. according to the prescription and the technological requirement of specific product.When containing the fresh milk cosmetics according to explained hereafter oil-in-water type of the present invention, fresh milk has passed through pasteurization and preservative treatment before the adding system, simultaneously, for avoiding fresh milk high temperature to add and excessively emulsification, cause the forfeiture of Over emulsfication phenomenon and active component, reduce the beauty functions of fresh milk in cosmetics, fresh milk requires after lotion oil, the preliminary emulsification of water mixed system, adds as adding when temperature is lower than 60 ℃, through further homogeneous, guarantee that each composition emulsification of cosmetics is complete; In reactor, keep starting quick stirring and homogeneous 1-2 minute under the maximum vacuum, so that the interpolation phased soln is complete and make material not have bubble fully; Simultaneously can start the refrigeration system fast cooling, product operation then, check can be produced routinely and be carried out.

According to preferred version of the present invention, consider and self contain emulsifying agent and several mineral materials composition in the fresh milk, especially wherein contain a large amount of electrolyte, influence the stability of emulsification system when being used for emulsion class (oil-in-water type) cosmetics series easily, so in the production that contains the fresh milk cosmetics of oil-in-water type, the emulsifying agent of selecting for use is preferably anionic emulsifier, the mixture of nonionic emulsifier or nonionic and anion emulsifier, promptly, emulsifying agent in the emulsion production (primary emulsion) is at least a anion emulsifier, or at least a nonionic emulsifier, or the combination of anion emulsifier and nonionic emulsifier.The emulsifying agent example that is suitable for has: lauryl sodium sulfate, potassium cetyl phosphate, laruyl alcohol sulfuric ester triethanolamine salt, stearate, Polyoxyethylene Sorbitol Fatty Acid Esters (Tween-20, Tween-60, Tween-80), polyoxyethylene (20) aliphatic acid ether, olein, polyoxyethylene (25) aliphatic acid ether, polyethylene glycol (20) lanolin, acetylation polyethylene glycol (10) lanolin etc.The consumption of this emulsifying agent is generally 0.5-5.0% (W/W) in final products, and the selection of concrete emulsifying agent is all determined according to the routine techniques of relevant Cosmetic Manufacture.

Optionally; for guaranteeing the final emulsifying effectiveness of product; also can select some coemulsifiers for use; for example glycerin monostearate, two stearic acid sorb alcohol fatty acid ester (Arlacel-20, Arlacel-60, Arlacel-80 etc.), polyethylene glycol (6) glycerin monostearate, stearic acid, acetylation glycerin monostearate etc.; the consumption of these coemulsifiers is generally 0.5-10% (W/W); equally, the concrete selection of this class emulsifying agent all can be determined according to the routine techniques of relevant cosmetics.

Simultaneously, because the adding of fresh-milk material, make the character of emulsion system that change take place, correspondingly, can select being used in combination of one or more excipients, for example: one or more combinations of 18 alcohol, hydroxyethylcellulose, polyacrylic acid, ceresine, beeswax, paraffin, microwax etc., especially select the combination of 18 alcohol or 18 alcohol and other excipients.The consumption of excipient (thickening) agent is generally 0.5-10% (W/W).

Certainly, except that above-mentioned selected emulsifying agent and excipient thickener, also can add basic material and the necessary additive that cosmetics contain usually of the present invention containing in the fresh milk cosmetics, emollient (for example vegetable oil, white oil, animal fat and derivative thereof etc.), NMF (for example glycerine, propane diols, 1 for example, 3-butanediol etc.), essence, deionized water, antioxidant etc., also can add determined nutritional labeling in the prescription.The application of these concrete compositions and consumption can be selected according to the concrete kind (skin type, hair care category, hair washing class, cleaning class, beauty treatment class etc.) of described cosmetics, perhaps add according to convention amount, this is easy to grasp for a person skilled in the art.Owing to added a certain amount of anticorrisive agent in advance in the fresh milk, it also helps simultaneously anticorrosion to final cosmetics, so the addition of anticorrisive agent should be considered (whether the concrete condition decision according to system is added and addition again) to some extent when producing relevant cosmetics in the later stage, and should make that the total amount of anticorrisive agent is no more than hygienic standards for cosmetics regulation (total mass content is controlled at 0.05-0.5%) in the cosmetics.The anticorrisive agent that adds in the described Cosmetic Manufacture can be identical or different with the anticorrisive agent that uses in the fresh milk, is appreciated that the same anticorrisive agent of interpolation is preferred in the cosmetics.

For example, oil-in-water type contains the possible prescription of fresh milk cosmetics (skin moisten honey or cream, mildy wash, hair care breast etc.) and is:

Fresh milk (through preservative treatment): 5-80% (w/w)

(master) emulsifying agent: 0.5-5.0% (w/w)

Coemulsifier: 0.5-10% (w/w)

Emollient (or profit is sent out agent): 5-40% (w/w)

Excipient thickener: 0.5-10% (w/w)

NMF: 5-30% (w/w)

Nutritional labeling: optionally, formula ratio

Functional components: optionally, formula ratio

Anticorrisive agent: convention amount (hygienic standards for cosmetics regulation)

Antioxidant: convention amount

Essence: selectivity is added or convention amount

Deionized water: add to 100%.

More specifically, a representative formula that contains the fresh milk emulsified make-up of the present invention can be:

Glycerin monostearate: 1-5% (w/w)

18 alcohol: 1-6% (w/w)

Glycerine: 20% (w/w)

Polyoxyethylene (25) fatty alcohol ether (A25): 0.5-2% (w/w)

Lauryl sodium sulfate (K12): 0.2-0.8% (w/w)

Fresh milk (after preservative treatment): 5-50% (w/w)

Hydroxyethylcellulose: 0.2-1% (w/w)

Nutritional labeling 1-10% (w/w)

Functional components 0.05-5% (w/w)

(6685+ is U.S.+IPBC) extremely: formula ratio (meeting the hygienic standards for cosmetics regulation) for anticorrisive agent

Essence: an amount of

Deionized water: surplus.

As non-limiting example, all kinds of basic components that contain the fresh milk cosmetics can also be (% (w/w)):

1, skin type (for example skin moisten honey)

Emollient: 5-40

NMF (glycerin/propylene glycol/1,3 butanediol): 5-30

Fresh milk (after preservative treatment): 5-50

Anticorrisive agent: 0.05-0.5 (concrete addition needs to decide according to the anticorrosion dosage that has added in the fresh milk)

Primary emulsion (anion/anion+anion/anion+nonionic/nonionic+nonionic/nonionic): 0.5-3.0

Coemulsifier: 0.5-5.0

Excipient thickener (18 alcohol, or 18 alcohol+hydroxyethylcellulose): 1.0-8

Essence: 0.2

Antioxidant: 0.01-0.5

Deionized water: to 100.

2, hair care category (for example hair care breast)

Profit is sent out agent: 5-50

Hair conditioner: 0.1-3.0

NMF (glycerin/propylene glycol/1,3-butanediol): 5-30

Fresh milk (after preservative treatment): 5-50

Anticorrisive agent: 0.05-0.5 (concrete addition needs to decide according to the anticorrosion dosage that has added in the fresh milk)

Primary emulsion (anion/anion+anion/anion+nonionic/nonionic+nonionic/nonionic): 0.5-3.0

Coemulsifier: 0.5-5.0

Excipient thickener: 18 pure 1.0-8+ wax class 0.1-2

Essence: 0.2

Antioxidant: 0.01-0.5

Water: to 100.

3, cleaning class (for example mildy wash)

Emollient: 5-40

Skin detergents: 0.1-5

NMF (glycerin/propylene glycol/1,3-butanediol): 5-30

Fresh milk (after preservative treatment): 5-50

Anticorrisive agent: 0.05-0.5 (concrete addition needs to decide according to the anticorrosion dosage that has added in the fresh milk)

Primary emulsion (anion/anion+anion/anion+nonionic/nonionic+nonionic/nonionic): 0.5-3.0

Coemulsifier: 0.5-5.0

Excipient thickener (18 alcohol+hydroxyethylcellulose): 1.0-8

Essence: 0.2

Antioxidant: 0.01-0.5

Water: to 100.

The fresh milk cosmetics that contain with oil-in-water type are example, and its production technology can comprise the following steps:

Oil phase in the cosmetics, water are carrying out preliminary emulsification more than 85 ℃, temperature drops to when being lower than 60 ℃ (for example 50-60 ℃), the fresh milk and other interpolation phase that add the process pasteurization and add anticorrisive agent, quick stirring, homogeneous; Cooling is then carried out product operation according to routine production, promptly obtains finished product.

In sum, the aseptic technic of fresh milk provided by the invention, after fresh milk being carried out pasteurization and special preservative treatment, the active component that can keep fresh breast to greatest extent, become the fresh-milk material that can be used for Cosmetic Manufacture, guarantee that bacterial population wherein reaches the requirement of Cosmetic Manufacture, and in a long time can be not putrid and deteriorated, thereby make the addition of fresh milk in cosmetics can reach higher proportion (becoming fresh milk cosmetics truly).On the basis of above-mentioned aseptic technic, by the fresh milk of interpolation after preservative treatment, and, can produce the cosmetic product that contains fresh milk in conjunction with emulsifying agent and the excipient thickener optimized, its outward appearance, inherent quality maintain a long-term stability, and make us being easy to accepting.Enforcement of the present invention will make fresh milk be used widely in cosmetics.

Annotate: the application's scheme describe and prescription in, " through the preservative treatment " or " anticorrosion preliminary treatment " that the fresh milk that adds cosmetics to is indicated all is through pasteurization and added the fresh milk of compound preservative.

The specific embodiment

Below describe the beneficial effect of implementation process of the present invention and generation in detail by specific embodiment, be intended to help the reader to understand essence of the present invention and characteristics better, but not as qualification to this case practical range.

The preservative treatment of embodiment 1, raw milk

According to the fresh milk (the detection index that meets GB6914-86) of the clean professional cattle farm supply of the Yu Mei on production schedule same day, transport to workshop with special-purpose accumulating car, portion is up to the standards through quality inspection, with fresh breast through pasteurization equipment enforcement pasteurization.

Be flexible coupling through delivery pump to the circular storage tank of the stainless steel that has temperature control and stir by detachable pipeline, add composite anticorrisive agent (compound preservative) immediately in proportion and stir.

The aseptic preservation under low temperature and steady temperature of fresh milk after the above-mentioned after-treatment is standby, and this storage temperature can be 0-5 ℃.Suggestion was used in 48 hours.

Among this embodiment, compound preservative is 6685, the compound of U.S. and IPBC extremely, and three's compound proportion is 2: 5: 1, and the interpolation total amount of compound preservative is the 0.4-0.5% of fresh milk quality.The mixed solution and the stirring of U.S., IPBC and an amount of propane diols are fully dissolved it to the addition manner of anticorrisive agent for elder generation adds extremely, add 6685 then.

This fresh milk is preserved through low temperature sealing in 48 hours, and the bacterial detection number is below 10CFU/g, and the proterties quality of fresh milk is good.

Embodiment 2, the different compound preservative of employing carry out preservative treatment to raw milk

The charging of raw milk and processing procedure are identical with embodiment 1, adopt different compound preservatives, and the microorganism detection result who handles the back raw milk is as shown in table 2 below:

Table 2

Anticorrisive agent	Fresh breast behind the pasteurization	24 hours (0-5 ℃)	48 hours (0-5 ℃)	Conclusion
					6685+ is beautiful (2: 5) extremely	0.5 ten thousand-0.8 ten thousand CFU/g	800-1000CFU/g	300-500CFU/g	Well
U.S.+IPBC (5: 1) extremely	0.5 ten thousand-0.8 ten thousand CFU/g	2000-3000CFU/g	1000-1500CFU/g	Better
					6685+IPBC(2∶1)	0.5 ten thousand-0.8 ten thousand CFU/g	500-800CFU/g	100-200CFU/g	Well
6685+ is U.S.+IPBC (2: 5: 1) extremely	0.5 ten thousand-0.8 ten thousand CFU/g	300-500CFU/g	≤10CFU/g	Good

Annotate: bacterium≤100CFU/g is good; ≤ 500CFU/g is good; ≤ 1500CFU/g is better.

Embodiment 3, contain the production of fresh milk skin moisten honey

1, prescription (each component all by weight percentage)

Potassium cetyl phosphate: 2.5

Glycerin monostearate: 2.5

18 alcohol: 6.0, hydroxyethylcellulose: 1.0

Glycerine: 15

1,3-butanediol: 5

Propane diols: 5

Fresh milk (after preservative treatment): 20

Anticorrisive agent: methyl hydroxybenzoate+propylben=0.1+0.05

Essence: an amount of

Deionized water: surplus.

2, production technology

Fresh milk carries out pasteurization and preservative treatment according to the method for embodiment 1 in advance, and (extremely U.S.+IPBC) back is standby in 0-5 ℃ of preservation to add anticorrisive agent 6685+.

Take by weighing each component according to said ratio, and oil phase and water are melted in operation respectively routinely, treat oil, the fusion temperature of water two-phase mixes in reactor when reaching 85 ℃ of left and right sides respectively carries out preliminary emulsification, again temperature is reduced to rapidly about 55 ℃, the fresh milk of interpolation after preservative treatment adds mutually with other, reactor keeps maximum vacuum, started quick stirring and homogeneous 1-2 minute, with guarantee to add phased soln fully and lotion not have bubble be control criterion, start the refrigeration system fast cooling simultaneously, then produce routinely to operate and (for example add necessary nutritional agents, additives such as essence) and the check complete until lotion.

The fresh milk skin moisten honey that contains through above-mentioned explained hereafter is rich in the fresh milk composition, reach heat-resisting repeatedly (40 ± 1 ℃ through long-term shelf storage test (following 3 years of normal temperature), after recovering room temperature in 24 hours, lotion is normal, not muddy), cold-resistant (15 ± 1 ℃, recovered room temperatures in 24 hours after, lotion is normal, do not have muddy water outlet phenomenon) destructive testing, the every sense index of product, physical and chemical index, sanitary index all meet corresponding national standards.

Embodiment 4, contain the fresh milk facial treatment milk

1, prescription (each component all by weight percentage)

Potassium cetyl phosphate: 2.5

Glycerin monostearate: 2.5

18 alcohol: 1.0

Hydroxyethylcellulose: 0.2

White oil: 4

Silicone oil: 3

The sour glyceryl ester of sad, certain herbaceous plants with big flowers (GTCC): 5 (being the skin moisten grease)

Saualane: 4

Glycerine: 15

1,3-butanediol: 5

Propane diols: 5

Fresh milk (after preservative treatment): 30

NMF: 0.05-0.1

Vitamin: 0.1-1

Plant extract: 0.1-2

Essence: 0.2

Anticorrisive agent: methyl hydroxybenzoate+propylben=0.1+0.05

BHT：0.05

Water: to 100.

2, production technology

Concrete production technology is identical with embodiment 3, through experiment similarly to Example 3, proves that its quality is good.

Embodiment 5, contain the fresh milk mildy wash

1, prescription (each component all by weight percentage)

Lauryl sodium sulfate: 1.0

Laruyl alcohol sulfuric ester triethanolamine salt: 0.5

Glycerin monostearate: 2.5

18 alcohol: 4.5

Hydroxyethylcellulose: 0.8

White oil: 10

Silicone oil: 1.5

Saualane: 2

Glycerine: 10

1,3-butanediol: 2

Propane diols: 2

Cocoamidopropyl betaine: 0.5

Fresh milk (after preservative treatment): 20

Essence: 0.2

Anticorrisive agent: MIT+ propylben=0.02+0.05

BHT：0.05

Water: to 100.

2, production technology

Earlier fresh milk is implemented preservative treatment, compound preservative is 6685, the compound of U.S. and IPBC extremely, three's compound proportion is 2: 4: 1, the about 0.35-0.4% of addition in the fresh milk, fresh milk concrete production technology anticorrosion and this mildy wash is identical with embodiment 3, through experiment similarly to Example 3, prove that its quality is good.

Embodiment 6, contain fresh milk hair care breast

1, prescription (each component all by weight percentage)

Lauryl sodium sulfate: 0.7

Polyoxyethylene (20) aliphatic acid ether: 0.5

Glycerin monostearate: 3.5

18 alcohol: 6

Beeswax: 2.0

White oil: 40

Amido silicon oil: 2

Olive oil: 4

Glycerine: 10

1,3-butanediol: 2

Propane diols: 2

Fresh milk (after preservative treatment): 15

Vitamin: 0.1-1

Essence: 0.2

Anticorrisive agent: benzyl carbinol+propylben=0.2+0.05

BHT：0.1

Water: to 100.

2, production technology

Earlier fresh milk is implemented preservative treatment, compound preservative is 6685, the compound of U.S. and IPBC extremely, three's compound proportion is 2: 3: 1, the about 0.30-0.35% of addition in the fresh milk, fresh milk concrete production technology anticorrosion and this mildy wash is identical with embodiment 3, through experiment similarly to Example 3, prove that its quality is good.

Embodiment 7-10

Below list the concrete prescription that some contain the fresh milk cosmetics, its production technology and product quality inspection result are identical with front embodiment.Each component in the prescription all by weight percentage.

Fresh milk moisturizer: lauryl sodium sulfate: 1.0

Glycerin monostearate: 2.5

18 alcohol: 8

White oil, vegetable oil and ester class: 20

Glycerine, propane diols, 1,3-butanediol: 25

Fresh milk (after preservative treatment, identical): 30 with embodiment 4

NMF: 0.1

Algal polysaccharides: 0.5

Anticorrisive agent: methyl hydroxybenzoate+propylben=0.1+0.05

Essence: an amount of

Water: complement to 100.

Fresh milk skin care cream: polyoxyethylene (25) aliphatic acid ether: 2.5

Polyoxyethylene (20) aliphatic acid ether: 0.5

Glycerin monostearate: 2.5

18 alcohol: 6

Hydroxyethylcellulose: 1

White oil, vegetable oil, ester class: 25

Glycerine, propane diols, 1,3-butanediol: 20

Fresh milk (after preservative treatment, identical): 30 with embodiment 3

NMF: 0.08

SOD:500 unit

Flos Rosae Davuricae elite: 2

Anticorrisive agent: methyl hydroxybenzoate+propylben=0.1+0.05

Essence: an amount of

Water: complement to 100.

The fresh milk honey of whitening: potassium cetyl phosphate: 2

Laruyl alcohol sulfuric ester triethanolamine salt: 0.5

Stearic acid: 2

18 alcohol: 6

Hydroxyethylcellulose: 1

White oil, vegetable oil, ester class: 20

Glycerine, propane diols, 1,3-butanediol: 25

Fresh milk (after preservative treatment, identical): 40 with embodiment 4

Vitamin C: 0.8

Kojic acid ester: 0.8

Aloe: 2

Sea-buckthorn skims the cream off milk: 4

Anticorrisive agent: methyl hydroxybenzoate+propylben=0.1+0.05

Essence: an amount of

Water: complement to 100.

Fresh milk is bathed the back emulsion: polyoxyethylene (20) fatty alcohol ether: 1

Lauryl sodium sulfate: 0.5

Glycerin monostearate: 2.5

18 alcohol, hydroxyethylcellulose: 2

White oil, vegetable oil, ester class:

Glycerine, propane diols, 1,3-butanediol: 20

Fresh milk (after preservative treatment, identical): 15 with embodiment 4

NMF: 0.1

SOD:500 unit

Plant extract elite: 2

Anticorrisive agent: methyl hydroxybenzoate+propylben=0.1+0.05

Essence: an amount of

Water: complement to 100.

Claims (12)

1, the method for anticorrosion treatment of fresh milk, the fresh milk after the processing can be applicable in the production of cosmetics, and described method comprises:

Raw milk is carried out pasteurization;

Add compound preservative in the fresh milk behind the pasteurization, described compound preservative is selected from least two kinds in the following group: 2-methyl-4-isothiazoline-3-ketone, 2-bromo-2-nitro-1, ammediol, 1,3-dihydroxymethyl-5,5-dimethyl hydantoin, 3-iodo-2-propynyl butyl carbamate and [N-methylol-N-(1,3-dihydroxymethyl-2,5-diketone-4-imidazolidinyl)-the N-methylolurea], and the addition of described compound preservative is the 0.1-1.5% of fresh milk quality.

2, the method for anticorrosion treatment of the described fresh milk of claim 1, wherein, described anticorrisive agent is for being selected from 2-bromo-2-nitro-1, ammediol, 3-iodo-2-propynyl butyl carbamate and [N-methylol-N-(1,3-dihydroxymethyl-2,5-diketone-4-imidazolidinyl)-the N-methylolurea] at least two kinds compound preservative.

3, the method for anticorrosion treatment of the described fresh milk of claim 2, wherein, described compound preservative is following three kinds composite product: 2-bromo-2-nitro-1, ammediol, [N-methylol-N-(1,3-dihydroxymethyl-2,5-diketone-4-imidazolidinyl)-the N-methylolurea] with the compound proportion of 3-iodo-2-propynyl butyl carbamate be 1-2: 3-5: 1.

4, the production method that contains the fresh milk cosmetics, it comprises, make the oil phase and the water of cosmetic material carry out preliminary emulsification earlier, the temperature of adjusting this emulsification system adds when being lower than 60 ℃ to be implemented anticorrosion pretreated fresh-milk material according to each described method of claim 1-3 and adds mutually with other, homogeneous makes the interpolation phased soln not have bubble fully and in the system to system through stirring also, requires complete operation according to prescription after system is further lowered the temperature.

5, the described production method of claim 4, wherein, the addition of described fresh milk is the 5-80% of this cosmetics gross weight.

6, the described production method of claim 5, wherein, the addition of fresh milk is the 5-50% of this cosmetics gross weight.

7, the described production method of claim 4, wherein, fresh-milk material uses in 48 hours after anticorrosion preliminary treatment.

8, claim 4,5 or 7 described production methods, wherein, when producing emulsion cosmetic, the primary emulsion that adds is the combination of at least a anion emulsifier, at least a nonionic emulsifier or anion emulsifier and nonionic emulsifier, and excipients is selected from one or more in 18 alcohol, hydroxyethylcellulose, polyacrylic acid, ceresine, beeswax, paraffin and the microwax.

9, the described production method of claim 8, wherein, the addition of described primary emulsion is the 0.5-5.0% of cosmetics gross mass; The addition of excipients is the 5-10% of cosmetics gross mass.

10, a kind of fresh milk cosmetics that contain, it is that production method manufacturing according to claim 4 forms.

11, the described fresh milk cosmetics that contain of claim 10, be emulsified make-up, gross weight with these cosmetics is a benchmark, the fresh milk that wherein contains 5-80%, and primary emulsion wherein is the combination of at least a anion emulsifier, at least a nonionic emulsifier or anion emulsifier and nonionic emulsifier, and excipients is selected from one or more in 18 alcohol, hydroxyethylcellulose, polyacrylic acid, ceresine, beeswax, paraffin and the microwax.

12, the described fresh milk cosmetics that contain of claim 11, it is the emulsified make-up that is used for skin care, hair care or cleaning.