CN1315401C - Preparation for lipoid frame particle - Google Patents
Preparation for lipoid frame particle Download PDFInfo
- Publication number
- CN1315401C CN1315401C CNB2005100423172A CN200510042317A CN1315401C CN 1315401 C CN1315401 C CN 1315401C CN B2005100423172 A CNB2005100423172 A CN B2005100423172A CN 200510042317 A CN200510042317 A CN 200510042317A CN 1315401 C CN1315401 C CN 1315401C
- Authority
- CN
- China
- Prior art keywords
- lipoid
- preparation
- sodium alginate
- gelatin
- particle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/87—Re-use of by-products of food processing for fodder production
Abstract
The present invention provides a method for preparing a phosphatide skeleton granule, which comprises the steps that processing aids are directly added into oil sediment to prepare an oil sediment skeleton granule by utilizing the action among the processing aids and among the processing aids and a salt solution; then the oil sediment skeleton granule is dried under the condition of certain temperature to prepare the dried oil sediment skeleton granule. The present invention has the technical scheme that 1 part by weight of alkalized or hydrated oil sediment of plants and 1 to 5 parts by weight gelatin-sodium alginate mixed solution are uniformly mixed at the temperature below 50 DEG C to prepare granules, and then the granules are solidified or coagulated and dried to prepare the phospholipid skeleton granule.
Description
Technical field
The present invention relates to a kind of by peanut, soybean, alkalization of different plants such as vegetable seed or hydrated oil foot directly produce the method for lipoid frame particle,
Background technology
At present, when alkalization of the accessory substance of soybean system oil or hydrated oil foot are made raw material production phosphatide, generally be to produce emulsus phosphatide by oil foot, extract through the acetone equal solvent by emulsus phosphatide again and produce powder phospholipid.Wen Shiqian etc. (concentrate the development and the pilot production of the anti-tapered horizontal film evaporator of research of soybean lecithin production technology and equipment.Chinese oil 1988 (4) .34～39) to studying by the technology of grease production emulsus phosphatide.Temperature light source etc. (the powder soybean lecithin produce experiment. Chinese oil .1985 (5) 40～47), Zhang Genwang etc. (development of human consumption soybean phosphatide. Zhengzhou Grain College journal 1991 (2) 1～8) carried out the powder phospholipid pilot experiment with acetone as solvent.Up to the present, though the production technology of emulsus phosphatide is generally used in various places, also difficulty is big really, cost is higher to produce powder phospholipid with emulsus phosphatide.
Emulsus phosphatide is difficult to stir evenly when the mixed feed as feed addictive, and usually adhesive aggregation is agglomerating, and it is uneven that phosphatide is disperseed.The production of powdered phospholipid well solves the deficiency that emulsus phosphatide exists in the production of fodder process.But when joining feed, still to add a certain amount of oil as energy, if can directly use not only oil-containing but also phosphorous fatty oil pin formula feed, the cost price of feed is reduced greatly, and the equipment investment of solution emulsus phosphatide and the existence of powdered phospholipid production technology is big, complex process, time is long, energy consumption is big, and solvent load is big, and the production safety problem that exists in producing.
Summary of the invention:
The objective of the invention is to overcome the deficiencies in the prior art, a kind of alkalization of different plants such as soybean, peanut and vegetable seed or preparation method that hydrated oil foot is directly produced lipoid frame particle of utilizing is provided.This method can make the oil foot treatment process simplify greatly, and the time shortens, and cost reduces, and is suitable for producing in batches etc.
Purpose of the present invention can realize by following technical measures:
By in oil foot, directly adding processing aid, utilize the effect that reaches between processing aid and salting liquid between the processing aid to make the oil foot skeleton particle, under the uniform temperature condition, carry out drying then, obtain dry oil foot skeleton particle.The concrete technical solution that adopts is alkalization or the hydrated oil foot according to plant: gelatin-sodium alginate mixed liquor=1: 1～5 weight portion proportionings, mix being lower than under 50 ℃, make particle after solidify or solidify, dry lipoid frame particle.Described gelatin-sodium alginate mixed liquor is that concentration is 1～5% gelatin: concentration is that sodium alginate=1: 0.5～2 weight portion proportionings of 1～5% mix and form.
Purpose of the present invention also can realize by following technical measures:
Described curing is to adopt CaSO
4Or Na
2S0
4Or CaCl
2Or (NH
4)
2SO
4Or the calcium citrate saturated solution is a consolidation liquid; Wherein with CaSO
4Saturated solution is best; Described solidifying is that employing concentration is that 30% above ethanol liquid is solidification liquid; Described curing also can be the mixed liquor that adopts consolidation liquid and solidification liquid; Described drying can adopt natural drying at room temperature or vacuum drying or be lower than 75 ℃ of following heat dryings; Perhaps it is put into ethanol number minute earlier, drying then, other dried forms all can; Only need 5～10 minutes described hardening time.
Technology of the present invention does not need solvent extraction, has solved the problem that the emulsus phosphatide of vegetable soda carburetion pin preparation is difficult to produce powder phospholipid simultaneously.
The processing aid that the present invention adds comprises gelatin, sodium alginate and calcium sulfate etc., the positively charged and CaSO of gelatin
1SO
1 2Promote that the effect of gelling is the strongest, sodium alginate is dissolvable in water water and Ca
+ 2Aggegation immediately becomes micelle when meeting, employed ethanolic solution can make gelatin solidify, help being dried into porose particle again, gelatin-calcium sulfate-sodium alginate forms skeleton jointly in the phosphatide particle, makes moisture, oil-containing, the oil foot that contains phosphatide is filled in the empty frame of skeleton and forms skeleton particle, raw materials used being easy to get, and consumption is few, nontoxic, low price.
The present invention produces the process of powder phospholipid again owing to not adopting alkalization or hydrated oil foot process with plant to make emulsus phosphatide with acetone extraction.The oil foot treatment process is simplified greatly, and the time shortens, and energy consumption reduces, and cost reduces, and product color and quality are higher, are suitable for producing in batches.
The specific embodiment:
Embodiment 1:
A. earlier the gelatin water is carried out swelling, 70 ℃ dissolve and make the gelatin solution that concentration is 1～5% (weight); The sodium alginate water is carried out swelling, and the sodium alginate solution that concentration is 1～5% (weight) is made in 100 ℃ of following dissolvings.
B. be raw material with soybean alkalization oil foot, by gelatin solution: sodium alginate solution=the weight portion proportioning mixed in 1: 0.5, promptly made gelatin-sodium alginate mixed liquor; Press oil foot: gelatin-sodium alginate mixed liquor=1: 5 weight portion proportioning is to mix under 50 ℃ of situations in temperature, is delivered to outlet through auger, makes spheric granules, goes into CaSO
4Stopped in the saturated solution 5 minutes, and took out skeleton particle, under 55 ℃, dry product.
Embodiment 2:
A. with embodiment 1.
B. be raw material with the soybean oil sediment, by gelatin solution: sodium alginate solution=the weight portion proportioning mixed in 1: 2, promptly made gelatin-sodium alginate mixed liquor; Press oil foot: gelatin-sodium alginate mixed liquor=1: 1 weight portion proportioning is to mix under 10 ℃ of situations in temperature, is delivered to outlet through auger, makes spheric granules, goes into Na
2SO
1Stopped 10 minutes in the saturated solution, take out skeleton particle, the at room temperature air-dry product that gets, quality and color and luster are better.
Embodiment 3:
A. with embodiment 1.
B. be raw material with the peanut hydrated oil foot, by gelatin solution: sodium alginate solution=the weight portion proportioning mixed in 1: 0.8, promptly made gelatin-sodium alginate mixed liquor; Press oil foot: gelatin-sodium alginate mixed liquor=1: 3 weight portion proportioning is to mix under 30 ℃ of situations in temperature, through extremely outlet of helical feed, make spheric granules, went into concentration and be 30% ethanol liquid 5 minutes, take out skeleton particle, under 70 ℃, dry then product.
Embodiment 4:
A. with embodiment 1.
B. be raw material with arachine carburetion pin, by gelatin solution: sodium alginate solution=the weight portion proportioning mixed in 1: 1.5, promptly made gelatin-sodium alginate mixed liquor; Press oil foot: gelatin-sodium alginate mixed liquor=1: 2 weight portion proportioning is to mix under 20 ℃ of situations in temperature, is delivered to outlet through auger, makes spheric granules, goes into (NH
4)
2SO
4Stopped 9 minutes in the mixed liquor of saturated solution and 60% ethanol liquid, take out skeleton particle, get product through vacuum drying.
Embodiment 5:
A. with embodiment 1.
B. be raw material with vegetable seed alkalization oil foot, by gelatin solution: sodium alginate solution=the weight portion proportioning mixed in 1: 1.2, promptly made gelatin-sodium alginate mixed liquor; Press oil foot: gelatin-sodium alginate mixed liquor=1: 4 weight portion proportioning is to mix under 40 ℃ of situations in temperature, to outlet, makes spheric granules through helical feed, goes into CaCl
2Stopped 6 minutes in the saturated solution, take out skeleton particle, the at room temperature air-dry product that gets.
Embodiment 6:
A. with embodiment 1.
B. be raw material with the vegetable seed hydrated oil foot, by gelatin solution: sodium alginate solution=the weight portion proportioning mixed in 1: 2, promptly made gelatin-sodium alginate mixed liquor; Press oil foot: gelatin-sodium alginate mixed liquor=1: 2 weight portion proportioning, in temperature is to mix under 50 ℃ of situations, through extremely outlet of helical feed, make spheric granules, go in the mixed liquor of calcium citrate saturated solution and 90% ethanol liquid to stop 5 minutes, take out skeleton particle, under 65 ℃, dry product.
Embodiment 7:
A. with embodiment 1.
B. be raw material with arachine carburetion pin, by gelatin solution: sodium alginate solution=the weight portion proportioning mixed in 1: 1, promptly made gelatin-sodium alginate mixed liquor; Press oil foot: gelatin-sodium alginate mixed liquor=1: 2 weight portion proportioning is to mix under 40 ℃ of situations in temperature, is delivered to outlet through auger, makes spheric granules, goes into concentration and be 95% ethanol liquid 5 minutes, takes out skeleton particle, gets product through vacuum drying.
Claims (6)
1, a kind of preparation method of lipoid frame particle, it is characterized in that alkalization or hydrated oil foot: gelatin-sodium alginate mixed liquor=1: 1～5 weight portion proportionings according to soybean, peanut or vegetable seed, mix being lower than under 50 ℃, make particle after solidify or solidify, dry lipoid frame particle; Described gelatin-sodium alginate mixed liquor is that weight concentration is 1～5% gelatin solution: weight concentration is that sodium alginate solution=1: 0.5～2 weight portion proportionings of 1～5% mix and form.
2,, it is characterized in that described curing is to adopt CaSO according to the preparation method of claims 1 described a kind of lipoid frame particle
4Or Na
2SO
4, CaCl
2, (NH
4)
2SO
4, the calcium citrate saturated solution is consolidation liquid.
3,, it is characterized in that described curing is that employing CaSO4 saturated solution is a consolidation liquid according to the preparation method of claims 2 described a kind of lipoid frame particles.
4,, it is characterized in that described solidifying is that employing concentration is that 30% above ethanol liquid is solidification liquid according to the preparation method of claims 1 described a kind of lipoid frame particle.
5,, it is characterized in that described curing is the mixed liquor that adopts consolidation liquid and solidification liquid according to the preparation method of claims 2 or 4 described a kind of lipoid frame particles.
6,, it is characterized in that described dry employing natural drying at room temperature or vacuum drying or be lower than 75 ℃ of following heat dryings according to the preparation method of claims 1 described a kind of lipoid frame particle.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100423172A CN1315401C (en) | 2005-01-11 | 2005-01-11 | Preparation for lipoid frame particle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100423172A CN1315401C (en) | 2005-01-11 | 2005-01-11 | Preparation for lipoid frame particle |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1644078A CN1644078A (en) | 2005-07-27 |
| CN1315401C true CN1315401C (en) | 2007-05-16 |
Family
ID=34876335
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2005100423172A Expired - Fee Related CN1315401C (en) | 2005-01-11 | 2005-01-11 | Preparation for lipoid frame particle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1315401C (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH706380A1 (en) * | 2012-04-13 | 2013-10-15 | Fluid Solids Ag C O Studio Beat Karrer | A degradable material from biological components. |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5171588A (en) * | 1990-05-21 | 1992-12-15 | Dai-Ichi Kogyo Seiyaku Co., Ltd. | Method for modulating the sedimentation rate of piscicultural dry pellets and product thereof |
| CN1080291A (en) * | 1992-06-26 | 1994-01-05 | 郴州科技实业公司 | From tea waste, extract the method for refined saponin |
-
2005
- 2005-01-11 CN CNB2005100423172A patent/CN1315401C/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5171588A (en) * | 1990-05-21 | 1992-12-15 | Dai-Ichi Kogyo Seiyaku Co., Ltd. | Method for modulating the sedimentation rate of piscicultural dry pellets and product thereof |
| CN1080291A (en) * | 1992-06-26 | 1994-01-05 | 郴州科技实业公司 | From tea waste, extract the method for refined saponin |
Non-Patent Citations (1)
| Title |
|---|
| 间歇式饲用茶籽磷脂的生产 韦会方等，中国油脂，第29卷第1期 2004 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1644078A (en) | 2005-07-27 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| KR100698452B1 (en) | Development of ruminally protected nutrients and their utilization for milk and beef enrichment | |
| CN106699449A (en) | Double-layer coated slow-release nitrogen fertilizer for improving saline-alkali soil and preparation method thereof | |
| CN103102223B (en) | Special lecithin-coated slow release fertilizer for cotton and production method of fertilizer | |
| CN107691770A (en) | A kind of high yield shrimp feed for effectively improving immunity and preparation method thereof | |
| CN106866275A (en) | A kind of granular compound fertilizer for exempting to dry and cool down and preparation method thereof | |
| CN103420732B (en) | Multifunctional sustained-release fertilizer | |
| CN105326797A (en) | Processing process for salinomycin granular preparation | |
| CN101265487A (en) | Preparation method for enriching gamma-aminobutyric acid by using fixed rice bran glutamic acid decarboxylase | |
| CN1315401C (en) | Preparation for lipoid frame particle | |
| CN104692952A (en) | Special melt granulated, rich-selenium and nitre-sulfur based fertilizer for jujube trees and preparation method thereof | |
| CN110041942A (en) | A kind of microencapsulation soil conditioner and preparation method thereof | |
| CN106675057A (en) | Preparation method of hard-shell calcium alginate oil sac | |
| CN109438101A (en) | Preparation method, granulating agent and its application of granulating agent | |
| CN107857621A (en) | A kind of particle magnesium sulfate fertilizer and preparation method thereof | |
| CN104177175A (en) | Coated fertilizer for increasing antioxidant function of strawberries and preparation method thereof | |
| CN104030839B (en) | A kind of Nano capsule slow-release fertilizer and preparation method thereof | |
| CN105214096A (en) | A kind of preparation method of instant branched-chain amino acid | |
| CN102924258A (en) | Method for producing calcium formate from sugar mill filter mud | |
| CN103392908B (en) | Preparation technique of granular phospholipid | |
| CN107082731A (en) | A kind of prilling process of particle nitrogen fertilizer | |
| CN102845616B (en) | Phosphorus supplementing agent and preparation method thereof | |
| CN102219939B (en) | Water retaining agent and preparation method thereof | |
| CN105753645A (en) | Method for preparing powder xylitol with purity being 55% | |
| CN107669652A (en) | A kind of preparation method for extracting species high-viscosity material particle | |
| CN107114564A (en) | The preparation method of premixing feedstuff containing hydrated phospholipids |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |