CN1304829C - Production of X-ray stress measuring calibrated sample - Google Patents
Production of X-ray stress measuring calibrated sample Download PDFInfo
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- CN1304829C CN1304829C CNB2005100232921A CN200510023292A CN1304829C CN 1304829 C CN1304829 C CN 1304829C CN B2005100232921 A CNB2005100232921 A CN B2005100232921A CN 200510023292 A CN200510023292 A CN 200510023292A CN 1304829 C CN1304829 C CN 1304829C
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Abstract
The present invention relates to a preparation method of X-ray stress measuring calibrated test samples, which is used in the technical field of material analysis tests. The preparation method comprises the following steps: (1), material quenching and tempering: forging materials and then removing the phenomena of coarse crystal grains and crystal face preferred orientation from the materials through quenching and tempering processing; (2), shot blasting prestressing: processing a workblank of a calibrated test sample, and processing the end surfaces of the workblank by shot blasting prestressing; (3), electrochemical corrosion: stripping the surface layer part with greater stress gradients of the calibrated test sample layer by layer by an electrochemical corrosion method; (4) stress measurement: measuring X-ray stress in the process of stripping layers by the electrochemical corrosion method, and determining the working surface of the calibrated test sample on the relation curve between stress and layer depth. The X-ray stress measuring calibrated test sample prepared by the present invention is used for calibrating an X-ray stress instrument system to ensure the good operating state of instruments. The calibrated test sample has the advantages of beautiful surface, difficult rustiness, easy on-site operation (namely complex auxiliary device saving) and long-term surface stress stabilization, and is capable of improving the reliability of measurement results.
Description
Technical field
That the present invention relates to is a kind of preparation method of calibration sample, specifically, is a kind of preparation method of X ray stress measuring calibrated sample.Be used for the material analysis technical field of measurement and test.
Background technology
Though multiple strain method is arranged at present, the X ray method for measuring stress is the typical case the most.Because this theoretical method basis is more rigorous, experimental technique is becoming better and approaching perfection day by day, and measurement result is very reliable, and is another non-destructive measuring method, thereby all obtains general application at home and abroad.
Before carrying out the X ray stress measurement, at first must detect the calibration sample of known stress, whether normal with the tester system.Therefore, select suitable calibration sample most important to whole surveying work.The preparation method of existing X ray stress measuring calibrated sample is a kind of flaky material of processing, by crooked or unidirectional loading, obtains calibration sample.The common disadvantage of this class calibration sample is, very inconvenient some servicing units that promptly need of execute-in-place, and measurement result repeatability is bad.
Find by prior art documents, people such as A.S.Munsi are at " Strain, 2003, Vol.39, No.1, p3-10 " (strain, 2003,39 volumes, the 1st phase, 3-10 page or leaf) on deliver the paper of " A method fordetermining X-ray elastic constants for the measurement of residual stress " (a kind of X ray Stress Constants measuring method that is used for residual stress measurement), introduce them and prepared the method for calibration sample, at first be processing one steel disc, adopt four-point bending, come the calibrating instrument system with this to the steel disc imposed load.The shortcoming of this calibration sample is to need servicing units such as strainmeter when loading.
Summary of the invention
The present invention is directed to the deficiencies in the prior art and defective, a kind of preparation method of X ray stress measuring calibrated sample is provided, make its calibration sample of preparing, be convenient to execute-in-place, can farthest guarantee the reliability of X ray results of stress.
The present invention is achieved by the following technical solutions, and concrete steps, the course of work and principle are as follows:
(1) material is modified, selects the 2Cr13 ferrite stainless steel material, through modifier treatment, eliminates the thick and texture phenomenon of crystal grain after the forging.
Its principle of work is, owing to contain the 13%Cr element, non-corrosive under atmospheric environment in the 2Cr13 ferritic stainless steel.It is thick to have eliminated crystal grain, makes the debye ring of each family of crystal planes continuous, and when detector swept away each diffraction ring, the diffraction peak intensity fluctuation was little, and measured stress ratio is more accurate.Eliminated texture in the material, made the crystal face of the same clan of different orientations have identical Stress Constants, thereby guarantee the reliability of measurement result.
(2) shot-peening prestress processes the blank of calibration sample, and its end face is carried out the shot-peening autofrettage.
Its principle of work is that the high speed pellet injection causes its top layer plastic strain to calibration sample blank surface, produces a large amount of dislocations, and has obtained unrelieved stress.On the other hand, after the shot-peening autofrettage, the crystal grain refinement more on calibration sample blank top layer, the texture phenomenon further is eliminated, and has improved the material of calibration sample once more.
(3) galvanic corrosion utilizes the method for galvanic corrosion, and the top layer that the stress gradient of calibration sample blank is bigger is successively peeled off.
Its principle of work is, in the zone, original shot-peening top layer of calibration sample blank, stress distribution is very inhomogeneous, and wherein top layer part is not suitable for staking-out work because stress gradient is bigger, need it be peeled off by galvanic corrosion.The principle of work of galvanic corrosion is successively to be peeled off as the calibration sample blank of anode.Adopting the major advantage of galvanic corrosion, is can not introduce other stress.
(4) stress measurement under the different corrosion depths of calibration sample blank, utilizes the X ray stress ga(u)ge to measure.
X ray stress measurement principle, being based on Bragg equation is X diffraction direction theory, by measuring the difference of different azimuth crystal face angle of diffraction of the same clan, determines the size and the direction of stress.In measuring process, observe the variation tendency of relation curve between stress data and the layer depth, when this curve finishes corrosion and stress measurement work, the working surface of calibration sample that Here it is during near horizontal level.
Owing to eliminated the thick and texture of crystal grain in the calibration sample, authenticity that can the proof stress measurement result is not subjected to the restriction of various measuring conditions.Because calibration sample adopts ferritic stainless steel, this material has body-centered cubic crystal structure, and is difficult for getting rusty and surface aesthetic.This calibration sample size is less to be very light in weight, therefore easy to carry and be easy to execute-in-place.The residual compressive stress on standard specimen top layer keeps balance with inner tension all the time, so its surface stress stable for extended periods of time helps improving the reliability of measurement result.
The invention has the beneficial effects as follows: the X ray stress measuring calibrated sample that the present invention is prepared, be used to demarcate X ray stress ga(u)ge system, guarantee the works fine state of instrument.There is not the thick and texture of crystal grain in calibration sample, is difficult for getting rusty, and is easy to carry, and surface aesthetic is easy to execute-in-place and has promptly omitted complicated auxiliary equipment, and the surface stress stable for extended periods of time has improved the reliability of measurement result.
The stress stable for extended periods of time has improved the reliability of measurement result.
Description of drawings
Fig. 1 is the X-ray diffraction spectral line of calibration sample material
Fig. 2 is the shape and the size of calibration sample
Fig. 3 is the distribution of calibration sample unrelieved stress along depth direction
Fig. 4 is the relation of calibration sample stress and room temperature standing time
Embodiment
Provide following examples in conjunction with content of the present invention:
(1) material is modified
Select the 2Cr13 ferrite stainless steel material, through modifier treatment, hardening and tempering process is 1000 ℃ of oil quenching and 660 ℃ of tempering after the forging.As shown in Figure 1, diffract spectral line shows that this material has been removed the thick and texture of crystal grain, owing to contain the 13%Cr element in the material, makes this material non-corrosive under atmospheric environment.
(2) shot-peening prestress
As shown in Figure 2, the end face to the calibration sample blank carries out the shot-peening autofrettage.The shot-peening parameter is: steel ball bullet diameter 0.15～0.25mm, shot peening strength is arc-height 0.2mm, shot-peening time 10min.The calibration sample outermost layer obtained-unrelieved stress of 218MPa.
(3) galvanic corrosion
The stripping layer is corroded on the bigger top layer of calibration sample stress gradient, and every layer thickness is 0.01mm.The galvanic corrosion parameter is: voltage 6V, electric current 1A, saturated NaCl electrolytic solution.In electrochemical corrosion course, other stress is not introduced on the calibration sample surface.
(4) stress measurement
As shown in Figure 3,, utilize the X ray stress ga(u)ge to measure, obtain relation curve between stress and the layer depth in different corrosion depths.X ray stress ga(u)ge parameter is: tube voltage 25kV, tube current 5mA, collimator diameter 2mm, Cr-K
αRadiation, Fe (211) diffraction crystal face.Fig. 3 shows, when corrosion thickness is 0.08mm curve near level, thereby obtained the working surface of calibration sample.
(5) estimation of stability
With above-mentioned calibration sample, under room temperature state, placed for 1 year, regularly carry out stress measurement, the result is as shown in Figure 4.The repeated experiments error of data illustrates that the stress value of calibration sample can stable for extended periods of time among the figure within ± 10MPa.
Claims (4)
1, a kind of preparation method of X ray stress measuring calibrated sample is characterized in that, concrete steps are as follows:
(1) material is modified: calibration sample is selected ferritic stainless steel, through modifier treatment, eliminates the thick and texture phenomenon of crystal grain in the material after the forging;
(2) shot-peening prestress: process the blank of calibration sample, its end face is carried out the shot-peening autofrettage;
(3) galvanic corrosion: utilize electrochemical etching method, the top layer part that the calibration sample stress gradient is bigger is successively peeled off;
(4) stress measurement: in galvanic corrosion stripping layer process, carry out the X ray stress measurement, determine the working surface of calibration sample from relation curve between stress and the layer depth, when stress and layer depth relation curve during, promptly obtain the working surface of calibration sample near level.
2, the preparation method of X ray stress measuring calibrated sample according to claim 1 is characterized in that, described shot-peening parameter is: steel ball bullet diameter 0.15～0.25mm, shot peening strength is arc-height 0.2mm, shot-peening time 15min.
3, the preparation method of X ray stress measuring calibrated sample according to claim 1 is characterized in that, the parameter of described galvanic corrosion: voltage 6V, electric current 1A, saturated NaCl electrolytic solution.
4, according to the preparation method of claim 1 or 3 described X ray stress measuring calibrated samples, it is characterized in that the parameter of described galvanic corrosion: every interlayer of galvanic corrosion stripping layer is divided into 0.01mm thickness.
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| CNB2005100232921A CN1304829C (en) | 2005-01-13 | 2005-01-13 | Production of X-ray stress measuring calibrated sample |
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| CNB2005100232921A CN1304829C (en) | 2005-01-13 | 2005-01-13 | Production of X-ray stress measuring calibrated sample |
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| CN1645091A CN1645091A (en) | 2005-07-27 |
| CN1304829C true CN1304829C (en) | 2007-03-14 |
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| CNB2005100232921A Expired - Fee Related CN1304829C (en) | 2005-01-13 | 2005-01-13 | Production of X-ray stress measuring calibrated sample |
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| CN102169033B (en) * | 2010-12-08 | 2013-04-03 | 北京科技大学 | Fixed-point non-destructive testing method for internal residual stress of aluminum alloy plate |
| CN102590249A (en) * | 2012-01-11 | 2012-07-18 | 上海交通大学 | Method for nondestructively testing micro hardness of shot-blasted layer of metal material |
| CN102628815A (en) * | 2012-04-10 | 2012-08-08 | 上海交通大学 | Method for detecting residual stress of shot-blasted layer on root part of small-curved-surface gear |
| CN102620871B (en) * | 2012-04-17 | 2013-09-18 | 辽宁工程技术大学 | Particle radiation monitoring mine rock stratum stress state system and monitoring method |
| CN102680502B (en) * | 2012-04-27 | 2014-04-09 | 中国航空工业集团公司北京航空材料研究院 | Method for measuring metal bar textures |
| CN102706708B (en) * | 2012-06-06 | 2014-12-10 | 沈阳飞机工业（集团）有限公司 | Calibration test cube manufacturing method for X-ray residual stress testing system |
| CN102941536B (en) * | 2012-11-21 | 2016-04-06 | 上海交通大学 | Finishing composite shot blasting method strengthened in advance by a kind of novel spring |
| US9989496B2 (en) | 2012-11-29 | 2018-06-05 | Beijing Institute Of Technology | Fixed value residual stress test block and manufacturing and preservation method thereof |
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| CN103411714B (en) * | 2013-08-08 | 2015-03-11 | 南京航空航天大学 | Method for measuring residual stress based on local stripping and coefficient modification |
| CN103837603B (en) * | 2014-02-28 | 2017-02-15 | 北京理工大学 | Method for using residual stress gradient calibrating block |
| CN104155036B (en) * | 2014-08-29 | 2017-07-28 | 哈尔滨工业大学 | A kind of method of the large-scale carbon fiber enhancement resin base composite material component residual stress of use X-ray detection |
| CN104359606A (en) * | 2014-11-25 | 2015-02-18 | 盐城工学院 | Method for measuring equivalent internal stress on milled surface and depth of effect of equivalent internal stress on milled surface |
| CN106033037B (en) * | 2015-03-18 | 2018-07-20 | 中国科学院金属研究所 | A kind of residual stress standard specimen preparation method |
| CN105891244A (en) * | 2016-04-12 | 2016-08-24 | 上海理工大学 | Method for evaluating reliability of shot blasting part with X-ray diffraction technology |
| CN108375595B (en) * | 2018-02-27 | 2020-09-01 | 北京工商大学 | Method for testing distribution of surface stress of metal workpiece along depth direction |
| CN109655475B (en) * | 2019-01-23 | 2020-04-07 | 同济大学 | Method for calibrating detection depth of energy spectrometer |
| CN110726386B (en) * | 2019-09-19 | 2020-11-06 | 西安交通大学 | Measuring method of full stress strain tensor of material based on Laue photographic method |
| CN111207869A (en) * | 2020-02-07 | 2020-05-29 | 航天科工防御技术研究试验中心 | Additive product residual stress testing method |
| CN111537127B (en) * | 2020-05-13 | 2022-03-11 | 西北工业大学 | Full-range calibration method of X-ray stress gauge |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4042825A (en) * | 1976-07-09 | 1977-08-16 | Colorado Seminary | Stressed-unstressed standard for X-ray stress analysis and method of making same |
| US6417512B1 (en) * | 1998-07-16 | 2002-07-09 | Seiko Instruments, Inc. | Sample distortion removing method in thin piece forming |
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- 2005-01-13 CN CNB2005100232921A patent/CN1304829C/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4042825A (en) * | 1976-07-09 | 1977-08-16 | Colorado Seminary | Stressed-unstressed standard for X-ray stress analysis and method of making same |
| US6417512B1 (en) * | 1998-07-16 | 2002-07-09 | Seiko Instruments, Inc. | Sample distortion removing method in thin piece forming |
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Application publication date: 20050727 Assignee: Zhejiang Meili Spring Co., Ltd. Assignor: Shanghai Jiao Tong University Contract record no.: 2010330000310 Denomination of invention: Production of X-ray stress measuring calibrated sample Granted publication date: 20070314 License type: Exclusive License Record date: 20100319 |
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