CN1303911C - Wood frog high protein calcium powder and producing process thereof - Google Patents
Wood frog high protein calcium powder and producing process thereof Download PDFInfo
- Publication number
- CN1303911C CN1303911C CNB200310109982XA CN200310109982A CN1303911C CN 1303911 C CN1303911 C CN 1303911C CN B200310109982X A CNB200310109982X A CN B200310109982XA CN 200310109982 A CN200310109982 A CN 200310109982A CN 1303911 C CN1303911 C CN 1303911C
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- Prior art keywords
- wood frog
- high protein
- homogenate
- supernatant
- calcium
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Links
- 241000191896 Rana sylvatica Species 0.000 title claims abstract description 25
- 239000000843 powder Substances 0.000 title claims abstract description 20
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 title claims abstract description 19
- 239000011575 calcium Substances 0.000 title claims abstract description 19
- 229910052791 calcium Inorganic materials 0.000 title claims abstract description 19
- 102000004169 proteins and genes Human genes 0.000 title claims abstract description 15
- 108090000623 proteins and genes Proteins 0.000 title claims abstract description 15
- 238000000034 method Methods 0.000 title claims abstract description 12
- 238000005516 engineering process Methods 0.000 claims abstract description 11
- 108090000790 Enzymes Proteins 0.000 claims abstract description 8
- 102000004190 Enzymes Human genes 0.000 claims abstract description 8
- 239000006228 supernatant Substances 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 230000007062 hydrolysis Effects 0.000 claims abstract description 5
- 238000006460 hydrolysis reaction Methods 0.000 claims abstract description 5
- 229940088598 enzyme Drugs 0.000 claims description 6
- 239000004365 Protease Substances 0.000 claims description 5
- 238000000247 postprecipitation Methods 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 108010001682 Dextranase Proteins 0.000 claims description 3
- 108090000526 Papain Proteins 0.000 claims description 3
- 238000007710 freezing Methods 0.000 claims description 3
- 230000008014 freezing Effects 0.000 claims description 3
- 229940055729 papain Drugs 0.000 claims description 3
- 235000019834 papain Nutrition 0.000 claims description 3
- 230000001954 sterilising effect Effects 0.000 claims description 3
- 238000004659 sterilization and disinfection Methods 0.000 claims description 3
- 235000007983 food acid Nutrition 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- 239000000155 melt Substances 0.000 claims 1
- 235000015097 nutrients Nutrition 0.000 abstract description 4
- 239000000047 product Substances 0.000 abstract description 3
- 239000002253 acid Substances 0.000 abstract 1
- 230000007774 longterm Effects 0.000 abstract 1
- 238000001556 precipitation Methods 0.000 abstract 1
- 239000013589 supplement Substances 0.000 abstract 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
- 239000007788 liquid Substances 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- 238000002372 labelling Methods 0.000 description 4
- 235000016709 nutrition Nutrition 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 3
- 239000012634 fragment Substances 0.000 description 3
- 238000000227 grinding Methods 0.000 description 3
- 238000001694 spray drying Methods 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- ZKHQWZAMYRWXGA-KQYNXXCUSA-J ATP(4-) Chemical compound C1=NC=2C(N)=NC=NC=2N1[C@@H]1O[C@H](COP([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O)[C@@H](O)[C@H]1O ZKHQWZAMYRWXGA-KQYNXXCUSA-J 0.000 description 2
- ZKHQWZAMYRWXGA-UHFFFAOYSA-N Adenosine triphosphate Natural products C1=NC=2C(N)=NC=NC=2N1C1OC(COP(O)(=O)OP(O)(=O)OP(O)(O)=O)C(O)C1O ZKHQWZAMYRWXGA-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 108091005804 Peptidases Proteins 0.000 description 2
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 description 2
- 235000019419 proteases Nutrition 0.000 description 2
- 208000008128 pulmonary tuberculosis Diseases 0.000 description 2
- 239000011573 trace mineral Substances 0.000 description 2
- 235000013619 trace mineral Nutrition 0.000 description 2
- 239000011782 vitamin Substances 0.000 description 2
- 229940088594 vitamin Drugs 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 206010031240 Osteodystrophy Diseases 0.000 description 1
- 208000001132 Osteoporosis Diseases 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 206010038519 Renal rickets Diseases 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 210000000988 bone and bone Anatomy 0.000 description 1
- 230000002308 calcification Effects 0.000 description 1
- 235000001465 calcium Nutrition 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- 238000001631 haemodialysis Methods 0.000 description 1
- 230000000322 hemodialysis Effects 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- 230000037257 muscle growth Effects 0.000 description 1
- 201000000585 muscular atrophy Diseases 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
Landscapes
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The present invention relates to a technology for producing wood frog powder with high protein and calcium, which is characterized in that the method comprises the following steps: wood frogs are taken and cut into small pieces, and the small pieces are dried and pulverized; acid is added to the small pieces to obtain homogenate, and the homogenate is sterilized by refrigerating at a low temperature; the sterilized homogenate is rapidly heated till the temperature is higher than 100DEG C and dissolved, and the dissolved homogenate is kept standing for precipitation; the supernatant is taken, water is added to the supernatant to adjust the pH value till the pH value reaches 2.5 to 7.5, biologic enzymes accounting for 5 to 10% of weight of the solution is added to the supernatant to hydrolyze the solution for 48 to 168 hours, the hydrolyzed solution is filtered and dried to make powder, and the wood frog powder with high protein and calcium is obtained. The nutrient components in the wood frog are reserved and not damaged to a maximum degree by the process of adding enzymes for hydrolysis by the technology, the state of abundant nutrient components of calcium, protein, etc. is converted, so the nutrient components in the state are easy for human bodies to absorb, and the purpose of supplement is achieved. The present invention has simple technology, and the product is convenient to eat, and can be preserved for a long term.
Description
Technical field:
The present invention relates to a kind of is the method that raw material is made nutrient and healthcare products with the wood frog, says clearly to have provided Wood frog high protein calcium powder and production technology, belongs to wood frog deep process technology field.
Background technology:
Wood frog is a kind of edibility pollution-free food, is loved by the people as the delicacies on the dining table usually, still, in the wood frog of common cooking methods processing, has a lot of nutritional labelings to be difficult for being absorbed by human body comprehensively, does not reach the purpose of nourishing.
Summary of the invention:
The invention provides a kind of Wood frog high protein calcium powder, contain the nutritional labeling that is easy to absorption of human body in a large number.
The present invention also further provides the production technology of Wood frog high protein powder.
Technical solution of the present invention is as follows: get wood frog and be divided into fritter, crushed after being dried adds the food acids homogenate of 4～8% weight, the cryogenic freezing sterilization, 5～20 minutes, Fast Heating was dissolved more than 100 ℃, place post precipitation, get supernatant and add water to transfer pH value be 2.5～7.5, add 5～10% biology enzymes by solution weight part ratio, hydrolysis 48～168 hours, filter, get Wood frog high protein calcium powder after the dry powder process.
Above-mentioned biology enzyme comprises: biological hydrolysis enzymes such as protease, papain, dextranase, trypsase.
Per 100 grams of high protein calcium powder of the present invention contain: the multivitamin and the various trace elements of albumen 85.1g, calcium 6.2g, sodium 0.25g, potassium 0.19g, fat, two, adenosine triphosphate and needed by human body.
Good effect of the present invention is: wood frog is by adding process such as enzyme hydrolysis, its nutritional labeling is not destroyed, and convert nutritional labelings such as abundant calcium, albumen to the state that easily is absorbed by the body, reach the effect of better nourishing, technology of the present invention is simple, product instant, but long preservation.
Adopt technology of the present invention, because the bone in the forest frog body does not deposit best age, should be still behind HTHP exist with the form of calcium, and contained two in the muscle, adenosine triphosphate and several amino acids, micro-vitamin destroy seldom, and be that carrier is absorbed by the body easily with albumen, increase additional calcium, vitamin, trace element effect, promoted human muscle's growth.For treatment pulmonary tuberculosis osteodystrophy (hemodialysis is analysed the patient), rachitis renalis has better curative effect.Reach and promote the pulmonary tuberculosis calcification, climacteric osteoporosis, muscular atrophy, motion back physical efficiency recovery, old, teenager's effect of supplemented calcium
The specific embodiment:
The following example is intended to further describe for example the present invention, rather than limit the present invention by any way, under the prerequisite that does not deviate from the spirit and principles in the present invention, any change or change that the ability city those of ordinary skill that the present invention did is realized easily all will fall within the claim scope that awaits the reply of the present invention.
Embodiment 1
Go wood frog 10kg to be divided into fragment, the crushed after being dried powdering, the acetic acid that adds 0.7kg carries out homogenized, sterilizes under-30 ℃ of conditions, quickly heats up to after the taking-up more than 100 ℃ and dissolves, it is 3.0 that the placement post precipitation is got supernatant adding distil water accent pH value, add protease by 5% of liquid, the reaction 50 hours that is hydrolyzed that stirs is filtered to remove and is gone up liquid, spray-drying powder process gets Wood frog high protein calcium powder.
Embodiment 2
Go wood frog 10kg to be divided into fragment, the crushed after being dried powdering adds the hydrochloric acid homogenate of 0.5kg, cryogenic freezing sterilization under-35 ℃ of conditions, quickly heat up to after the taking-up more than 100 ℃ and dissolve, place post precipitation, getting supernatant adding distil water accent pH value is 7.5, adds dextranase by 10% of liquid, the reaction 158 hours that is hydrolyzed stirs, filter to remove and go up liquid, spray-drying powder process gets Wood frog high protein calcium powder.
Embodiment 3
Go wood frog 10kg to be divided into fragment, the crushed after being dried powdering, the acetic acid that adds 0.8kg carries out homogenate, sterilizes under-30 ℃ of conditions, quickly heats up to after the taking-up more than 100 ℃ and dissolves, it is 6.0 that the placement post precipitation is got supernatant adding distil water accent pH value, add papain by 8% of liquid, the reaction 90 hours that is hydrolyzed that stirs is filtered to remove and is gone up liquid, spray-drying powder process gets Wood frog high protein calcium powder.
Claims (1)
1, a kind of production technology of Wood frog high protein calcium powder, it is characterized in that comprising following processing step: get wood frog and be divided into fritter, crushed after being dried adds the food acids homogenate of 4～8% weight, low temperature-30 ℃ or-35 ℃ of freezing sterilizations, and Fast Heating melts more than 100 ℃, place post precipitation, get supernatant and add water to transfer pH value be 2.5～7.5, add 5～10% biology enzymes by solution weight part ratio, hydrolysis 48～168 hours, filter, get Wood frog high protein calcium powder after the dry powder process; Described biology enzyme is selected from: a kind of in papain, dextranase, the trypsase.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB200310109982XA CN1303911C (en) | 2003-11-10 | 2003-11-10 | Wood frog high protein calcium powder and producing process thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB200310109982XA CN1303911C (en) | 2003-11-10 | 2003-11-10 | Wood frog high protein calcium powder and producing process thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1543866A CN1543866A (en) | 2004-11-10 |
| CN1303911C true CN1303911C (en) | 2007-03-14 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB200310109982XA Expired - Fee Related CN1303911C (en) | 2003-11-10 | 2003-11-10 | Wood frog high protein calcium powder and producing process thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1303911C (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101822374A (en) * | 2010-04-20 | 2010-09-08 | 吉林省长白山生态食品有限公司 | Method for preparing wood frog living-body high-calcium albumen powder by isostatic cool pressing |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102628004A (en) * | 2012-04-25 | 2012-08-08 | 吉林大学 | Enrichment method of omega-3 unsaturated fatty acid in rana japonica oil |
| CN104212862A (en) * | 2013-06-03 | 2014-12-17 | 吉林省现代中药工程研究中心有限公司 | Wood frog protein and bone calcium extraction method |
| CN103689607A (en) * | 2013-11-26 | 2014-04-02 | 雷家荃 | Application of wood frog high protein calcium powder in preparation of calcium-supplementing health-care products or drugs |
| CN103690564A (en) * | 2013-11-26 | 2014-04-02 | 雷家荃 | Application of wood frog high protein calcium powder in preparation of anti-fatigue health-care products or drugs |
| CN103690565A (en) * | 2013-12-29 | 2014-04-02 | 吉林省力荣生物科技有限公司 | Application of wood frog extracting solution to preparation of medicine for treating and preventing haemorrhoids |
| CN116855309B (en) * | 2023-08-04 | 2023-12-19 | 通化康元生物科技有限公司 | Instant oviductus ranae and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1324620A (en) * | 2000-05-19 | 2001-12-05 | 华泽庆 | production process of biological active toad capsule |
| CN1328777A (en) * | 2000-06-15 | 2002-01-02 | 姜文京 | Puffed wood frog meat strip |
-
2003
- 2003-11-10 CN CNB200310109982XA patent/CN1303911C/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1324620A (en) * | 2000-05-19 | 2001-12-05 | 华泽庆 | production process of biological active toad capsule |
| CN1328777A (en) * | 2000-06-15 | 2002-01-02 | 姜文京 | Puffed wood frog meat strip |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101822374A (en) * | 2010-04-20 | 2010-09-08 | 吉林省长白山生态食品有限公司 | Method for preparing wood frog living-body high-calcium albumen powder by isostatic cool pressing |
| CN101822374B (en) * | 2010-04-20 | 2013-04-03 | 吉林省长白山生态食品有限公司 | Method for preparing wood frog living-body high-calcium albumen powder by isostatic cool pressing |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1543866A (en) | 2004-11-10 |
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