CN1274217C - Dry farmland herbicide and its methods of use - Google Patents
Dry farmland herbicide and its methods of use Download PDFInfo
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- CN1274217C CN1274217C CN 03157853 CN03157853A CN1274217C CN 1274217 C CN1274217 C CN 1274217C CN 03157853 CN03157853 CN 03157853 CN 03157853 A CN03157853 A CN 03157853A CN 1274217 C CN1274217 C CN 1274217C
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Abstract
The present invention discloses a once eliminating herbicide which is suitable for various crops, medicinal materials, vegetables and seedlings in dry farmland and an application method thereof. The herbicide is prepared from effective components prepared from the compounds of at least one of A, B1, B2 and B3, wherein A stands for 2-chlorine-1-(3-ethoxy-4-nitrophenoxy)-4-(trifluoromethyl)benzene, B1 stands for 2, 6-dinitro-N, N-di-n-propyl-4-trifluoromethyl aniline, B2 stands for N-1-(ethylpropyl)-2,-6-dinitro-3, 4-dimethylaniline, and B3 stands for N-sec-butyl-4-tert-butyl-2, 6-dinitroaniline. The present invention has the advantages of wide weed eliminating spectrum and high medicinal effect, and can be used for various crops, medicinal materials and vegetables in the dry farmland and nursery gardens to basically prevent and eliminate various grassy weeds, broad-leaved weeds, etc. in crop farmland through using the herbicide once with synergistic effects. The effect holding period of the herbicide is moderate, seasonal crops can not be damaged by the weeds basically after the herbicide is used once with no damage to succession crops, and the herbicide can not be accumulated in soil with high security. Crop tests show that the herbicide has no phytotoxicity.
Description
Technical field:
The present invention relates to herbicidal composition and the using method thereof of a kind of suitable dry land various crop, medicinal material, vegetables, nursery stock, especially relate to once clean herbicidal composition and the using method thereof of dry land various crop, medicinal material, vegetables, nursery stock.
Background technology:
At present, China's dry land herbicide great majority commonly used are single active ingredient, as: 2,4-D, agricultural chemicals such as Acetochlor, atrazine, diclofop-methyl, quizalofop-ethyl are divided into two types substantially: a kind of is closed soil type preemergence herbicide, as acetamide-group herbicides etc.; A kind of is the cauline leaf inorganic agent.Closed soil type weed killer herbicide evenly applies in the field before must or transplanting in the crop sowing, forms a medicine layer and kill the weeds young shoot that is being unearthed in the field; Cauline leaf processing type weed killer herbicide then after weeds emerge, kills the weeds of being unearthed by spraying pesticide.There is following drawback in existing chemical weed control: the one, at the serious northern area of hazards of sand storms, use closed soil type preemergence herbicide early spring, usually because the medicine soil layer of ground wind erosion sealing causes herbicidal effect poor; The 2nd, perennial crop is turned green sprouting early next year, sprays preemergence herbicide and is easy to take place poisoning; The 3rd, crop growth period spray cauline leaf inorganic agent, crop absorbs a large amount of agricultural chemicals, causes residue of pesticide easily and influences plant growth; The 4th, the use that cauline leaf is handled weed killer herbicide mainly is the selective problems of weed killer herbicide, monocotyledon weed in the monocot crops, the broadleaf weed in the dicotyledonous crops are difficult to remove like this, when using weed killer herbicide, still need carry out artificial weeding and just can reach satisfied herbicidal effect, increase the labour like this and dropped into and management cost; The 5th, existing chemical weed control technology mostly is medication several times a year, causes the pesticide pollution of soil, crop, environment easily.
Summary of the invention:
One object of the present invention is to provide a kind of suitable dry land multiple kinds of crops: as corn, cotton, soybean, tobacco etc., medicinal material: as Chinese ephedra, Radix Glycyrrhizae, the Radix Astragali etc., vegetables: as potato, garlic, capsicum, leek, celery etc., fruit tree, nursery: pin, broad-leaved nursery stock etc., and prevent and treat monocotyledon weed and broadleaf weed simultaneously, synergistic effect is obvious, consumption is few, broad weed-killing spectrum is to the herbicidal composition of the little low-residual of succession crop influence.
Another object of the present invention is to provide the using method of this herbicidal composition.
One object of the present invention is implemented by following technical scheme: (1), it includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene and B1 are 2,6-dinitro-N, N-di-4-5-trifluoromethylaniline, B2 are N-1-(ethyl propyl)-2,-6-dinitro-3,4-dimethylaniline, B3 are N-sec-butyl-4-tertiary butyl-2, the active ingredient that one or both of 6-dinitroaniline or two or more compounds are formed;
(2), the active ingredient formed of one or both or the two or more compounds of A and B1, B2, B3 wherein, all in the weight of 100% former medicine, its prescription is as follows respectively:
(a), A: B1=1: 0.01-50; Or
(b), A: B2=1: 0.01-50; Or
(c), A: B3=1: 0.01-50; Or
(d), A: B1: B2=1: (0.01-50): (0.01-50); Or
(e), A: B2: B3=1: (0.01-50): (0.01-50); Or
(f), A: B1: B3=1: (0.01-50): (0.01-50); Or
(g)、A∶B1∶B2∶B3＝1∶(0.01-30)∶(0.01-30)∶(0.01-30)。
The active ingredient formed of one or both or two or more compounds of A and B1, B2, B3 wherein, all in the weight of 100% former medicine, the optimum value of its prescription can be as follows respectively:
(a), A: B1=1: 0.5-20; Or
(b), A: B2=1: 0.5-20; Or
(c), A: B3=1: 0.5-20; Or
(d), A: B1: B2=1: (0.5-10): (0.5-10); Or
(e), A: B2: B3=1: (0.5-10): (0.5-10); Or
(f), A: B1: B3=1: (0.5-10): (0.5-10); Or
(g)、A∶B1∶B2∶B3＝1∶(0.5-10)∶(0.5-10)∶(0.5-10)。
The active ingredient formed of one or both among A and B1, B2, the B3 or two or more compounds wherein, all in the weight of 100% former medicine, the optimum value of its prescription can also be as follows respectively:
(a), A: B1=1: 1.5-4; Or
(b), A: B2=1: 1.5-4; Or
(c), A: B3=1: 1.5-4; Or
(d), A: B1: B2=1: (0.5-2): (0.5-2); Or
(e), A: B2: B3=1: (0.5-2): (0.5-2); Or
(f), A: B1: B3=1: (0.5-2): (0.5-2); Or
(g)、A∶B1∶B2∶B3＝1∶(0.5-1.5)∶(0.5-1.5)∶(0.5-1.5)。
The active ingredient that one or both of described A and B1, B2, B3 or two or more compounds are formed, weight in 100% former medicine, be equipped with solvent, emulsifier is made cream preparation, the percentage by weight of its prescription is: the active ingredient that one or both of described A and B1, B2, B3 or two or more compounds are formed is 10-50, solvent is 30-65, and emulsifier is 5-15.The most preferably value of the percentage by weight of its prescription is: the active ingredient that one or both of described A and B1, B2, B3 or two or more compounds are formed is 20-40, and solvent is 40-55, and emulsifier is 8-12.Described solvent includes water, benzene,toluene,xylene, methyl alcohol, ethanol, propyl alcohol, butanols, ethylene glycol, ether, butyl ether, carrene, tetrachloro-ethylene, acetone, 4-methyl-2 pentanone, cyclohexanone, isopropylidene acetone, isophorone or dimethyl formamide etc.; Described emulsifier is one or more of alkylbenzenesulfonate, agricultural newborn 8203#L-308, agricultural newborn 8209#, agricultural newborn 500#, agricultural newborn 8206#, 8901#, Span-80, tween-80 etc.
The active ingredient that one or both of described A and B1, B2, B3 or two or more compounds are formed, weight in 100% former medicine, be equipped with surfactant, filler is made wetting powder, the percentage by weight of its prescription is: the active ingredient that one or both of described A and B1, B2, B3 or two or more compounds are formed is 5-30, surfactant is 5-10, and filler is 60-80.The most preferably value of the percentage by weight of its prescription is: the active ingredient that one or both of described A and B1, B2, B3 or two or more compounds are formed is 10-25, and surfactant is 7-9, and filler is 65-70.Described surfactant comprises: alkylbenzenesulfonate, peregal, lignin, sulfonate, naphthalene sulfonate, alkyl, phenol polyglycol ether, epoxidized polyether, alkylsulfonate, dispersing agent NNO, MF2, SS, CNF, draw back powder or cleaning agent LS.Described filler comprises: one or more of Attagel, montmorillonite, kaolin, bentonite, zeolite, protruding Attapulgite, precipitated calcium carbonate, white carbon, talcum powder, the plaster of paris, diatomite, magnesium sulfate, potash etc.
The active ingredient that one or both of described A and B1, B2, B3 or two or more compounds are formed, weight in 100% former medicine, be equipped with carrier, auxiliary agent is made granule, wherein said auxiliary agent includes binding agent, dispersant, colouring agent, the percentage by weight of its prescription is: the active ingredient that one or both of described A and B1, B2, B3 or two or more compounds are formed is 0.1-3.0, carrier is 90-98, and binding agent is that 1-2, dispersant are that 1-5, colouring agent are 0.01-0.05 in the auxiliary agent.The most preferably value of the percentage by weight of its prescription is: the active ingredient that one or both of described A and [B1], [B2], [B3] or two or more compounds are formed is 0.5-1.5, carrier is 95-97, and binding agent is 1.5 in the auxiliary agent, dispersant is that 2-4, colouring agent are 0.02.Described carrier is one or more of zeolite, river sand, clay, kaolin, attapulgite or the like.Described surfactant comprises: alkylbenzenesulfonate, peregal, lignin, sulfonate, naphthalene sulfonate, alkyl, phenol polyglycol ether, epoxidized polyether, alkylsulfonate, dispersing agent NNO, MF2, SS, CNF, draw back powder or cleaning agent LS.Binding agent is a polyvinyl alcohol.
Described [A] and [B1], [B2], the active ingredient that one or both of [B3] or two or more compounds are formed, weight in 100% former medicine, be equipped with urea, ammonium nitrate, granulated phosphate fertilizer, MAP, diammonium phosphate, potassium chloride, potassium sulphate, magnesium sulfate and compound fertilizer are done carrier, dose Tween-80, NNO, surfactants such as LS are made auxiliary agent, make agricultural chemicals-chemical fertilizer compound formulation, its weight ratio is, the percentage by weight of its prescription is: described [A] and [B1], [B2], the active ingredient that one or both of [B3] or two or more compounds are formed is 0.1-6.0, compound fertilizer is 92-98, auxiliary agent 1-5.The most preferably value of the percentage by weight of its prescription is that the percentage by weight of its prescription is: the active ingredient that one or both of described [A] and [B1], [B2], [B3] or two or more compounds are formed is 0.5-3.0, and compound fertilizer is 94-96, auxiliary agent 2-4.
Another object of the present invention is implemented by following technical scheme: the using method of this weed killer herbicide on perennial plant adopts soup to spread droplet a method or a particle broadcast application, promptly when pouring water, the once clean weed killer herbicide liquid of dry land splashed into or pour water before this herbicidal composition uniform particles is sprinkled into Tanaka.
The herbicidal composition that the present invention relates to, 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene (being called [A] herbicidal compounds in the literary composition) of more specifically saying so, with the category-B herbicidal compounds, choosing to 2,6-dinitro-N, N one di-4-5-trifluoromethylaniline (claiming [B1] herbicidal compounds in the literary composition), N-1-(ethyl propyl)-2,-6-dinitro-3,4-dimethylaniline (claiming [B2] herbicidal compounds in the literary composition), N-sec-butyl-4-tertiary butyl-2, one or both in the 6-dinitroaniline (claiming [B3] herbicidal compounds in the literary composition) and the compound formulation that can keep various auxiliary agents stable and diffusion rapidly to form.
Advantage of the present invention is: (1), broad weed-killing spectrum, drug effect height.Can be used for dry land multiple kinds of crops, medicinal material, vegetables, nursery, disposable use prevents and treats weeds such as multiple grass family, broad-leaved in the crop field substantially.(2), synergy.Both are mixed, and synergistic effect is remarkable according to surveying.Lasting period is moderate, once uses basic maintenance this season crop to avoid weeds harm, to second stubble crop safety, does not accumulate in soil.(3), safe, trial crops is not all found poisoning.
Embodiment:
Missible oil formulation embodiment one:
Embodiment 1-1:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 3 kilograms, 6-dinitro-N, 42 kilograms of N-dis-4-5-trifluoromethylaniline are equipped with solvent: 49 kilograms of toluene, emulsifier 8901#6 kilogram, make the double centner cream preparation.
Embodiment 1-2:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 6 kilograms, 6-dinitro-N, 36 kilograms of N-dis-4-5-trifluoromethylaniline are equipped with 50 kilograms of solvent xylenes, emulsifier 8901#8 kilogram, make the double centner cream preparation.
Embodiment 1-3:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 9 kilograms, 6-dinitro-N, 30 kilograms of N-dis-4-5-trifluoromethylaniline, be equipped with 51 kilograms of solvent xylenes, 7 kilograms of emulsifier Tween-80,3 kilograms of calcium stearates, make the double centner cream preparation.
Embodiment 1-4:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 12 kilograms, 6-dinitro-N, 24 kilograms of N-dis-4-5-trifluoromethylaniline are equipped with 53 kilograms of solvent benzols, emulsifier 8901#11 kilogram, make the double centner cream preparation.
Embodiment 1-6:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 15 kilograms, 6-dinitro-N, 18 kilograms of N-dis-4-5-trifluoromethylaniline are equipped with 57 kilograms of solvent xylenes, emulsifier 8206#12 kilogram, make the double centner cream preparation.
Embodiment 1-7:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 20 kilograms, 6-dinitro-N, 8 kilograms of N-dis-4-5-trifluoromethylaniline, be equipped with 57 kilograms of solvent xylenes, 7 kilograms of emulsifier op-10s, 8 kilograms of dodecyl octyl phenyl ethers, make the double centner cream preparation.
Embodiment 2-1:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 3 kilograms, 6-dinitro-N, 22 kilograms of N-dis-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,15 kilograms of 4-dimethylanilines are equipped with 54.9 kilograms of solvent xylenes, emulsifier 8901#6 kilogram, make the double centner cream preparation.
Embodiment 2-2:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 4 kilograms, 6-dinitro-N, 20 kilograms of N-dis-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,14 kilograms of 4-dimethylanilines are equipped with 55 kilograms of solvent toluenes, emulsifier 8206#7 kilogram, make cream preparation.
Embodiment 2-3:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 6 kilograms, 6-dinitro-N, 18 kilograms of N-dis-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,12.4 kilograms of 4-dimethylanilines are equipped with 55.6 kilograms of solvent xylenes, emulsifier 8201#8 kilogram), make the double centner cream preparation.
Embodiment 2-4:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 9 kilograms, 6-dinitro-N, 15 kilograms of N-dis-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,10.3 kilograms of 4-dimethylanilines are equipped with 56.7 kilograms of solvent xylenes, emulsifier 8901#9 kilogram, make the double centner cream preparation.
Embodiment 2-5:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 11 kilograms, 6-dinitro-N, 13 kilograms of N-dis-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,8.9 kilograms of 4-dimethylanilines are equipped with 57.1 kilograms of solvent benzols, 7 kilograms of emulsifier op-10s, 5 kilograms of dodecyl octyl phenyl ethers, make the double centner cream preparation.
Embodiment 2-6:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 13 kilograms, 6-dinitro-N, 11 kilograms of N-dis-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,7.6 kilograms of 4-dimethylanilines are equipped with 57.4 kilograms of solvent xylenes, emulsifier Tween-807 kilogram, 4 kilograms of calcium stearates, make the double centner cream preparation.
Embodiment 2-7:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 15 kilograms, 6-dinitro-N, 9 kilograms of N-dis-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,6.2 kilograms of 4-dimethylanilines are equipped with 57.8 kilograms of solvent toluenes, emulsifier 8901#4 kilogram, Span-808 kilogram and make the double centner cream preparation.
Embodiment 3-1:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 6 kilograms, 6-dinitro-N, 14.6 kilograms of N-dis-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,10 kilograms of 4-dimethylanilines, B3 is N-sec-butyl-4-tertiary butyl-2,14.6 kilograms of 6-dinitroanilines are equipped with 52.8 kilograms of solvent toluenes, 2 kilograms of 4 kilograms of calcium stearates of emulsifier Tween-80, make the double centner cream preparation.
Embodiment 3-2:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 4 kilograms, 6-dinitro-N, N-di-13.3 kilograms of 4-5-trifluoromethylanilines, B2 are N-1-(ethyl propyl)-2,-6-dinitro-3,9.2 kilograms of 4-dimethylanilines, B3 are N-sec-butyl-4-tertiary butyl-2,13.3 kilograms of 6-dinitroanilines are equipped with 53.2 kilograms of solvent benzols), emulsifier 8901#7 kilogram), make the double centner cream preparation.
Embodiment 3-3:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 6 kilograms, 6-dinitro-N, 12 kilograms of N-dis-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2 ,-6-dinitro-3,8.3 kilograms of 4-dimethylanilines, B3 is N-sec-butyl-4-tertiary butyl-2,12 kilograms of 6-dinitroanilines are equipped with 53.7 kilograms of solvent xylenes, 8 kilograms of emulsifier 8203#, make the double centner cream preparation.
Embodiment 3-4:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 9 kilograms, 6-dinitro-N, 10 kilograms of N-dis-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,6.9 kilograms of 4-dimethylanilines, B3 are N-sec-butyl-4-tertiary butyl-2,10 kilograms of 6-dinitroanilines are equipped with 55.1 kilograms of solvent benzols, 9 kilograms of emulsifier 8901#, make the double centner cream preparation.
Embodiment 3-5:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 11 kilograms, 6-dinitro-N, 8.7 kilograms of N-dis-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,6 kilograms of 4-dimethylanilines, B3 are N-sec-butyl-4-tertiary butyl-2,8.7 kilograms of 6-dinitroanilines are equipped with 55.6 kilograms of solvent xylenes, 10 kilograms of emulsifier 8206#, make the double centner cream preparation.
Embodiment 3-6:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 13 kilograms, 6-dinitro-N, 7.3 kilograms of N-dis-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,5 kilograms of 4-dimethylanilines, B3 are N-sec-butyl-4-tertiary butyl-2,7.3 kilograms of 6-dinitroanilines are equipped with 56.4 kilograms of solvent toluenes, 6 kilograms of emulsifier 8901#, Span-80 make the double centner cream preparation for 5 kilograms.
Embodiment 3-7:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 15 kilograms, 6-dinitro-N, 6 kilograms of N-dis-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,4 kilograms of 4-dimethylanilines, B3 are N-sec-butyl-4-tertiary butyl-2,6 kilograms of 6-dinitroanilines are equipped with 57 kilograms of solvent xylenes, 12 kilograms of emulsifier 8901#, make the double centner cream preparation.
Wetting powder embodiment two:
Embodiment 1-1:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 3 kilograms, 6-dinitro-N, 7 kilograms of N-dis-4-5-trifluoromethylaniline are equipped with 3 kilograms of surfactant washing agent LS, 2 kilograms of dispersing agent NNOs, filler: 30 kilograms of precipitated calcium carbonates, 55 kilograms of white carbons, make the double centner wetting powder.
Embodiment 1-2:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 4 kilograms, 6-dinitro-N, 11 kilograms of N-dis-4-5-trifluoromethylaniline are equipped with surfactant: 3 kilograms of cleaning agent LS, 3 kilograms of dispersing agent NNOs, filler: 29 kilograms in diatomite, 50 kilograms of talcum powder, make the double centner wetting powder.
Embodiment 1-3:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 5 kilograms, 6-dinitro-N, 10 kilograms of N-dis-4-5-trifluoromethylaniline are equipped with surfactant: 4 kilograms of neopelexes, 2 kilograms of odium stearate, filler: 30 kilograms of precipitated calcium carbonates, 49 kilograms of kaolin, make the double centner wetting powder.
Embodiment 1-4:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 8 kilograms, 6-dinitro-N, 12 kilograms of N-dis-4-5-trifluoromethylaniline are equipped with surfactant: 4 kilograms of neopelexes, 3 kilograms of odium stearate, filler: 30 kilograms of kaolin, 43 kilograms in diatomite, make the double centner wetting powder.
Embodiment 1-5:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 5 kilograms, 6-dinitro-N, 15 kilograms of N-dis-4-5-trifluoromethylaniline are equipped with surfactant: 5 kilograms of cleaning agent LS, 3 kilograms of dispersing agent NNOs, filler: 30 kilograms of kaolin, 42 kilograms in diatomite, make the double centner wetting powder.
Embodiment 1-6:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 10 kilograms, 6-dinitro-N, 10 kilograms of N-dis-4-5-trifluoromethylaniline are equipped with surfactant: 3 kilograms of neopelexes, 5 kilograms of odium stearate, filler: 30 kilograms in diatomite, 42 kilograms of precipitated calcium carbonates, make the double centner wetting powder.
Embodiment 1-7:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 13 kilograms, 6-dinitro-N, 7 kilograms of N-dis-4-5-trifluoromethylaniline are equipped with surfactant: 4 kilograms of cleaning agent LS, 4 kilograms of dispersing agent NNOs, filler: 40 kilograms of kaolin, 32 kilograms of bentonites, make the double centner wetting powder.
Embodiment 2-1:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 2 kilograms, 6-dinitro-N, N-di-4 kilograms of 4-5-trifluoromethylanilines, B2 are N-1-(ethyl propyl)-2,-6-dinitro-3,4 kilograms of 4-dimethylanilines are equipped with surfactant: 3 kilograms of neopelexes, 2 kilograms of odium stearate, filler: 30 kilograms of kaolin, 55 kilograms of bentonites, make the double centner wetting powder.
Embodiment 2-1:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 4 kilograms, 6-dinitro-N, N-di-6 kilograms of 4-5-trifluoromethylanilines, B2 are N-1-(ethyl propyl)-2,-6-dinitro-3,5 kilograms of 4-dimethylanilines are equipped with surfactant: 3 kilograms of cleaning agent LS, 2 kilograms of dispersing agent NNOs, filler: 40 kilograms of kaolin, 40 kilograms of bentonites, make the double centner wetting powder.
Embodiment 2-2:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 6 kilograms, 6-dinitro-N, N-di-5 kilograms of 4-5-trifluoromethylanilines, B2 are N-1-(ethyl propyl)-2,-6-dinitro-3,4 kilograms of 4-dimethylanilines are equipped with surfactant: 3 kilograms of neopelexes, 3 kilograms of odium stearate, filler: 29 kilograms of bentonites, 50 kilograms of precipitated calcium carbonates, make the double centner wetting powder.
Embodiment 2-3:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 8 kilograms, 6-dinitro-N, N-di-6 kilograms of 4-5-trifluoromethylanilines, B2 are N-1-(ethyl propyl)-2,-6-dinitro-3,6 kilograms of 4-dimethylanilines are equipped with surfactant: 3 kilograms of cleaning agent LS, 5 kilograms of dispersing agent NNOs, filler: but 30 kilograms of precipitated calcium carbonates, 42 kilograms in diatomite, make the double centner Wettable Powder.
Embodiment 2-4:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 10 kilograms, 6-dinitro-N, N-di-5 kilograms of 4-5-trifluoromethylanilines, B2 are N-1-(ethyl propyl)-2,-6-dinitro-3,5 kilograms of 4-dimethylanilines are equipped with surfactant: 3 kilograms of neopelexes, 5 kilograms of odium stearate, filler: 30 kilograms of precipitated calcium carbonates, 42 kilograms of white carbons, make the double centner wetting powder.
Embodiment 2-5:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 12 kilograms, 6-dinitro-N, N-di-6 kilograms of 4-5-trifluoromethylanilines, B2 are N-1-(ethyl propyl)-2,-6-dinitro-3,2 kilograms of 4-dimethylanilines are equipped with surfactant: 3 kilograms of cleaning agent LS, 5 kilograms of dispersing agent NNOs, filler: 30 kilograms of white carbons, 42 kilograms in diatomite, make the double centner wetting powder.
Embodiment 2-6:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 2 kilograms, 6-dinitro-N, N-di-8 kilograms of 4-5-trifluoromethylanilines, B2 are N-1-(ethyl propyl)-2,-6-dinitro-3,10 kilograms of 4-dimethylanilines are equipped with surfactant: 5 kilograms of cleaning agent LS, 5 kilograms of dispersing agent NNOs, filler: 40 kilograms of precipitated calcium carbonates, 30 kilograms in diatomite, make the double centner wetting powder.
Embodiment 2-7:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 8 kilograms, 6-dinitro-N, N-di-6 kilograms of 4-5-trifluoromethylanilines, B2 are N-1-(ethyl propyl)-2,-6-dinitro-3,6 kilograms of 4-dimethylanilines are equipped with surfactant: 4 kilograms of neopelexes, 6 kilograms of odium stearate, filler: 40 kilograms of kaolin, 30 kilograms of bentonites, make the double centner wetting powder.
Embodiment 3-1:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 2 kilograms, 6-dinitro-N, N-di-3 kilograms of 4-5-trifluoromethylanilines, B2 are N-1-(ethyl propyl)-2,-6-dinitro-3,2 kilograms of 4-dimethylanilines, B3 are N-sec-butyl-4-tertiary butyl-2,3 kilograms of 6-dinitroanilines are equipped with surfactant: 3 kilograms of neopelexes, 3 kilograms of odium stearate, filler: 40 kilograms of kaolin, 44 kilograms of bentonites, make the double centner wetting powder.
Embodiment 3-2:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 5 kilograms, 6-dinitro-N, N-di-2 kilograms of 4-5-trifluoromethylanilines, B2 are N-1-(ethyl propyl)-2,-6-dinitro-3,2 kilograms of 4-dimethylanilines, B3 are N-sec-butyl-4-tertiary butyl-2,1 kilogram of 6-dinitroaniline, be equipped with surfactant: 3 kilograms of cleaning agent LS, 2 kilograms of dispersing agent NNOs, filler: 40 kilograms of precipitated calcium carbonates, 45 kilograms in diatomite, make the double centner wetting powder.
Embodiment 3-3:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 2 kilograms, 6-dinitro-N, N-di-6 kilograms of 4-5-trifluoromethylanilines, B2 are N-1-(ethyl propyl)-2,-6-dinitro-3,3 kilograms of 4-dimethylanilines, B3 are N-sec-butyl-4-tertiary butyl-2,4 kilograms of 6-dinitroanilines, be equipped with surfactant: 3 kilograms of cleaning agent LS, 4 kilograms of dispersing agent NNOs, filler: 40 kilograms of kaolin, 38 kilograms of bentonites, make the double centner wetting powder.
Embodiment 3-4:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 6 kilograms, 6-dinitro-N, N-di-4 kilograms of 4-5-trifluoromethylanilines, B2 are N-1-(ethyl propyl)-2,-6-dinitro-3,2 kilograms of 4-dimethylanilines, B3 are N-sec-butyl-4-tertiary butyl-2,3 kilograms of 6-dinitroanilines, be equipped with surfactant: 4 kilograms of neopelexes, 4 kilograms of odium stearate, filler: 40 kilograms of precipitated calcium carbonates, 37 kilograms in diatomite, make the double centner wetting powder.
Embodiment 3-5:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 6 kilograms, 6-dinitro-N, N-di-5 kilograms of 4-5-trifluoromethylanilines, B2 are N-1-(ethyl propyl)-2,-6-dinitro-3,4 kilograms of 4-dimethylanilines, B3 are N-sec-butyl-4-tertiary butyl-2,5 kilograms of 6-dinitroanilines are equipped with surfactant: 5 kilograms of neopelexes, 5 kilograms of odium stearate, filler: 30 kilograms of precipitated calcium carbonates, 40 kilograms in diatomite, make the double centner wetting powder.
Embodiment 3-6:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 10 kilograms, 6-dinitro-N, N-di-3 kilograms of 4-5-trifluoromethylanilines, B2 are N-1-(ethyl propyl)-2,-6-dinitro-3,3 kilograms of 4-dimethylanilines, B3 are N-sec-butyl-4-tertiary butyl-2,4 kilograms of 6-dinitroanilines are equipped with surfactant: 5 kilograms of cleaning agent LS, 5 kilograms of dispersing agent NNOs, filler: 30 kilograms of kaolin, 40 kilograms of bentonites, make wetting powder.
Embodiment 3-7:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 8 kilograms, 6-dinitro-N, N-di-4 kilograms of 4-5-trifluoromethylanilines, B2 are N-1-(ethyl propyl)-2,-6-dinitro-3,4 kilograms of 4-dimethylanilines, B3 are N-sec-butyl-4-tertiary butyl-2,4 kilograms of 6-dinitroanilines are equipped with surfactant: 4 kilograms of neopelexes, 6 kilograms of odium stearate, filler: 30 kilograms of precipitated calcium carbonates, 40 kilograms in diatomite, make the double centner wetting powder.
Granule formulation embodiment three:
Embodiment 1-1:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.3 kilogram, 6-dinitro-N, 0.2 kilogram of N-di-4-5-trifluoromethylaniline, be equipped with carrier: binding agent is that 2 kilograms of polyvinyl alcohol, surfactant are that 1 kilogram of lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent are 0.3 kilogram in 5 kilograms of kaolin, 90.2 kilograms of river sands, the auxiliary agent, makes the double centner granule.
Embodiment 1-2:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.5 kilogram, 6-dinitro-N, 0.5 kilogram of N-di-4-5-trifluoromethylaniline, be equipped with carrier: binding agent is that 2 kilograms of polyvinyl alcohol, surfactant are that 1 kilogram of lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent are 0.3 kilogram in 5 kilograms of kaolin, 89.2 kilograms of river sands, the auxiliary agent, makes the double centner granule.
Embodiment 1-3:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.3 kilogram, 6-dinitro-N, 0.7 kilogram of N-di-4-5-trifluoromethylaniline, be equipped with carrier: binding agent is that 2 kilograms of polyvinyl alcohol, surfactant are that 1 kilogram of lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent are 0.3 kilogram in 5 kilograms of kaolin, 89.2 kilograms of river sands, the auxiliary agent, makes the double centner granule.
Embodiment 1-4:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.6 kilogram, 6-dinitro-N, 0.4 kilogram of N-di-4-5-trifluoromethylaniline, be equipped with carrier: binding agent is that 2 kilograms of polyvinyl alcohol, surfactant are that 1 kilogram of lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent are 0.3 kilogram in 5 kilograms of kaolin, 89.2 kilograms of river sands, the auxiliary agent, makes the double centner granule.
Embodiment 1-5:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.5 kilogram, 6-dinitro-N, 1.0 kilograms of N-dis-4-5-trifluoromethylaniline, be equipped with carrier: binding agent is that 2 kilograms of polyvinyl alcohol, surfactant are that 1 kilogram of lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent are 0.3 kilogram in 5 kilograms of kaolin, 88.7 kilograms of river sands, the auxiliary agent, makes the double centner granule.
Embodiment 1-6:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.8 kilogram, 6-dinitro-N, 0.7 kilogram of N-di-4-5-trifluoromethylaniline, be equipped with carrier: binding agent is that 2 kilograms of polyvinyl alcohol, surfactant are that 1 kilogram of lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent are 0.3 kilogram in 5 kilograms of kaolin, 88.7 kilograms of river sands, the auxiliary agent, makes the double centner granule.
Embodiment 1-7:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.8 kilogram, 6-dinitro-N, 1.2 kilograms of N-dis-4-5-trifluoromethylaniline, be equipped with carrier: binding agent is that 2 kilograms of polyvinyl alcohol, surfactant are that 1 kilogram of lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent are 0.3 kilogram in 5 kilograms of kaolin, 88.2 kilograms of river sands, the auxiliary agent, makes the double centner granule.
Embodiment 2-1:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.3 kilogram, 6-dinitro-N, 0.4 kilogram of N-di-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,0.3 kilogram of 4-dimethylaniline, be equipped with carrier: 5 kilograms of kaolin, 89.7 kilograms of river sands, binding agent is 2 kilograms of polyvinyl alcohol in the auxiliary agent, surfactant is 1 kilogram of a lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent is 0.3 kilogram, makes the double centner granule.
Embodiment 2-2:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.5 kilogram, 6-dinitro-N, 0.25 kilogram of N-di-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,0.25 kilogram of 4-dimethylaniline, be equipped with carrier: 5 kilograms of kaolin, 89.7 kilograms of river sands, binding agent is 2 kilograms of polyvinyl alcohol in the auxiliary agent, surfactant is 1 kilogram of a lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent is 0.3 kilogram, makes the double centner granule.
Embodiment 2-3:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.5 kilogram, 6-dinitro-N, 0.5 kilogram of N-di-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,0.5 kilogram of 4-dimethylaniline, be equipped with carrier: 5 kilograms of kaolin, 89.2 kilograms of river sands, binding agent is 2 kilograms of polyvinyl alcohol in the auxiliary agent, surfactant is 1 kilogram of a lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent is 0.3 kilogram, makes the double centner granule.
Embodiment 2-4:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.9 kilogram, 6-dinitro-N, 0.3 kilogram of N-di-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,0.3 kilogram of 4-dimethylaniline, be equipped with carrier: 5 kilograms of kaolin, 89.2 kilograms of river sands, binding agent is 2 kilograms of polyvinyl alcohol in the auxiliary agent, surfactant is 1 kilogram of a lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent is 0.3 kilogram, makes the double centner granule.
Embodiment 2-5:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.3 kilogram, 6-dinitro-N, 0.8 kilogram of N-di-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,0.9 kilogram of 4-dimethylaniline, be equipped with carrier: 5 kilograms of kaolin, 88.7 kilograms of river sands, binding agent is 2 kilograms of polyvinyl alcohol in the auxiliary agent, surfactant is 1 kilogram of a lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent is 0.3 kilogram, makes the double centner granule.
Embodiment 2-6:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.7 kilogram, 6-dinitro-N, 0.7 kilogram of N-di-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,0.6 kilogram of 4-dimethylaniline, be equipped with carrier: 5 kilograms of kaolin, 88.7 kilograms of river sands, binding agent is 2 kilograms of polyvinyl alcohol in the auxiliary agent, surfactant is 1 kilogram of a lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent is 0.3 kilogram, makes the double centner granule.
Embodiment 2-7:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 1.0 kilograms, 6-dinitro-N, 0.5 kilogram of N-di-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,0.5 kilogram of 4-dimethylaniline, be equipped with carrier: 5 kilograms of kaolin, 88.7 kilograms of river sands, binding agent is 2 kilograms of polyvinyl alcohol in the auxiliary agent, surfactant is 1 kilogram of a lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent is 0.3 kilogram, makes the double centner granule.
Embodiment 3-1:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.1 kilogram, 6-dinitro-N, 0.3 kilogram of N-di-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,0.3 kilogram of 4-dimethylaniline, B3 is N-sec-butyl-4-tertiary butyl-2,0.3 kilogram of 6-dinitroaniline, be equipped with carrier: 5 kilograms of kaolin, 89.7 kilograms of river sands, binding agent is 2 kilograms of polyvinyl alcohol in the auxiliary agent, surfactant is 1 kilogram of a lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent is 0.3 kilogram, makes the double centner granule.
Embodiment 3-2:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.5 kilogram, 6-dinitro-N, 0.2 kilogram of N-di-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,0.2 kilogram of 4-dimethylaniline, B3 is N-sec-butyl-4-tertiary butyl-2,0.1 kilogram of 6-dinitroaniline, be equipped with carrier: 5 kilograms of kaolin, 89.7 kilograms of river sands, binding agent is 2 kilograms of polyvinyl alcohol in the auxiliary agent, surfactant is 1 kilogram of a lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent is 0.3 kilogram, makes the double centner granule.
Embodiment 3-3:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.3 kilogram, 6-dinitro-N, 0.3 kilogram of N-di-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,0.2 kilogram of 4-dimethylaniline, B3 is N-sec-butyl-4-tertiary butyl-2,0.2 kilogram of 6-dinitroaniline, be equipped with carrier: 5 kilograms of kaolin, 89.7 kilograms of river sands, binding agent is 2 kilograms of polyvinyl alcohol in the auxiliary agent, surfactant is 1 kilogram of a lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent is 0.3 kilogram, makes the double centner granule.
Embodiment 3-4:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.4 kilogram, 6-dinitro-N, 0.5 kilogram of N-di-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,0.5 kilogram of 4-dimethylaniline, B3 is N-sec-butyl-4-tertiary butyl-2,0.1 kilogram of 6-dinitroaniline, be equipped with carrier: 5 kilograms of kaolin, 89.2 kilograms of river sands, binding agent is 2 kilograms of polyvinyl alcohol in the auxiliary agent, surfactant is 1 kilogram of a lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent is 0.3 kilogram, makes the double centner granule.
Embodiment 3-5:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.6 kilogram, 6-dinitro-N, 0.4 kilogram of N-di-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,0.5 kilogram of 4-dimethylaniline, B3 is N-sec-butyl-4-tertiary butyl-2,0.5 kilogram of 6-dinitroaniline, be equipped with carrier: 5 kilograms of kaolin, 89.2 kilograms of river sands, binding agent is 2 kilograms of polyvinyl alcohol in the auxiliary agent, surfactant is 1 kilogram of a lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent is 0.3 kilogram, makes the double centner granule.
Embodiment 3-6:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.8 kilogram, 6-dinitro-N, 0.4 kilogram of N-di-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,0.4 kilogram of 4-dimethylaniline, B3 is N-sec-butyl-4-tertiary butyl-2,0.4 kilogram of 6-dinitroaniline, be equipped with carrier: 5 kilograms of kaolin, 88.7 kilograms of river sands, binding agent is 2 kilograms of polyvinyl alcohol in the auxiliary agent, surfactant is 1 kilogram of a lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent is 0.3 kilogram, makes the double centner granule.
Embodiment 3-7:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.3 kilogram, 6-dinitro-N, 0.5 kilogram of N-di-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,0.5 kilogram of 4-dimethylaniline, B3 is N-sec-butyl-4-tertiary butyl-2,0.7 kilogram of 6-dinitroaniline, be equipped with carrier: 5 kilograms of kaolin, 88.7 kilograms of river sands, binding agent is 2 kilograms of polyvinyl alcohol in the auxiliary agent, surfactant is 1 kilogram of a lignin calcium sulfonate, 0.6 kilogram of cleaning agent LS, 0.4 kilogram of dispersing agent NNO, colouring agent is 0.3 kilogram, makes the double centner granule.
Agricultural chemicals-chemical fertilizer compound formulation embodiment four:
Embodiment 1-1:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.1 kilogram, 6-dinitro-N, 0.4 kilogram of N-di-4-5-trifluoromethylaniline, being equipped with 23.5 kilograms of 30 kilograms in urea, 30 kilograms of MAPs, 15 kilograms of fertilizer of potassium sulphate and fluorspar powders does carrier, 0.3 kilogram of surfactant neopelex, odium stearate and makees auxiliary agent for 0.2 kilogram, make binding agent for 0.5 kilogram with polyvinyl alcohol, make agricultural chemicals-chemical fertilizer compound formulation.
Embodiment 1-2:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.3 kilogram, 6-dinitro-N, 0.3 kilogram of N-di-4-5-trifluoromethylaniline, be equipped with 23.5 kilograms in 75 kilograms in compound fertilizer, fluorspar powder and do 0.2 kilogram in carrier, 0.3 kilogram of surfactant neopelex, odium stearate and make auxiliary agent, make binding agent for 0.4 kilogram, make agricultural chemicals-chemical fertilizer compound formulation with polyvinyl alcohol.
Embodiment 1-3:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.4 kilogram, 6-dinitro-N, 0.6 kilogram of N-di-4-5-trifluoromethylaniline, be equipped with 27.5 kilograms in 70 kilograms in urea, fluorspar powder and do carrier, 0.6 kilogram of surfactant neopelex, odium stearate and make auxiliary agent for 0.4 kilogram, make binding agent with 0.5 kilogram of polyvinyl alcohol and make agricultural chemicals-chemical fertilizer compound formulation.
Embodiment 1-4:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.7 kilogram, 6-dinitro-N, 0.3 kilogram of N-di-4-5-trifluoromethylaniline is equipped with 40 kilograms of 30 kilograms of diammonium phosphate of urea, 27.5 kilograms of compound fertilizers of fluorspar powder and does 0.5 kilogram in carrier, 0.5 kilogram of surface active agent neopelex, odium stearate and make auxiliary agent, make binding agent with 0.5 kilogram of polyvinyl alcohol and make agricultural chemicals-chemical fertilizer compound formulation.
Embodiment 1-5:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.9 kilogram, 6-dinitro-N, 0.1 kilogram of N-di-4-5-trifluoromethylaniline is equipped with 98 kilograms in phosphate fertilizer and does carrier, 0.5 kilogram of surfactant neopelex, odium stearate and make auxiliary agent for 0.5 kilogram and make agricultural chemicals-chemical fertilizer compound formulation.
Embodiment 1-6:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.6 kilogram, 6-dinitro-N, 0.9 kilogram of N-di-4-5-trifluoromethylaniline is equipped with 26.5 kilograms of 40 kilograms of 30 kilograms of diammonium phosphate of urea, fluorspar powder and does 0.5 kilogram in carrier, 0.5 kilogram of surfactant neopelex, odium stearate and make auxiliary agent, make binding agent with 0.5 kilogram of polyvinyl alcohol and make agricultural chemicals-chemical fertilizer compound formulation.
Embodiment 1-7:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.8 kilogram, 6-dinitro-N, 1.2 kilograms of N-dis-4-5-trifluoromethylaniline, be equipped with 26.5 kilograms in 30 kilograms in urea, 40 kilograms of MAPs, potassium sulphate and do carrier, 0.5 kilogram of surfactant neopelex, odium stearate and make auxiliary agent for 0.5 kilogram, make agricultural chemicals-chemical fertilizer compound formulation with 0.5 kilogram of polyvinyl alcohol.
Embodiment 2-1:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.3 kilogram, 6-dinitro-N, N-di-0.4 kilogram of 4-5-trifluoromethylaniline, B2 are N-1-(ethyl propyl)-2,-6-dinitro-3,0.3 kilogram of 4-dimethylaniline, be equipped with 27.5 kilograms in 30 kilograms in urea, 40 kilograms of MAPs, potassium sulphate and do carrier, 0.5 kilogram of surfactant neopelex, odium stearate and make auxiliary agent for 0.5 kilogram, make agricultural chemicals-chemical fertilizer compound formulation with 0.5 kilogram of polyvinyl alcohol.
Embodiment 2-2:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.6 kilogram, 6-dinitro-N, N-di-0.4 kilogram of 4-5-trifluoromethylaniline, B2 are N-1-(ethyl propyl)-2,-6-dinitro-3,0.5 kilogram of 4-dimethylaniline is equipped with 27 kilograms in 30 kilograms in urea, 40 kilograms of MAPs, potassium sulphate and does carrier, 0.5 kilogram of surfactant neopelex, odium stearate and make auxiliary agent for 0.5 kilogram, makes agricultural chemicals-chemical fertilizer compound formulation with 0.5 kilogram of polyvinyl alcohol.
Embodiment 2-3:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.8 kilogram, 6-dinitro-N, N-di-0.6 kilogram of 4-5-trifluoromethylaniline, B2 are N-1-(ethyl propyl)-2,-6-dinitro-3,0.6 kilogram of 4-dimethylaniline, be equipped with 26.5 kilograms in 30 kilograms in urea, 40 kilograms of MAPs, potassium sulphate and do carrier, 0.5 kilogram of surfactant neopelex, odium stearate and make auxiliary agent for 0.5 kilogram, make agricultural chemicals-chemical fertilizer compound formulation with 0.5 kilogram of polyvinyl alcohol.
Embodiment 3-1:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.3 kilogram, 6-dinitro-N, 0.2 kilogram of N-di-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,0.2 kilogram of 4-dimethylaniline, B3 is N-sec-butyl-4-tertiary butyl-2,0.2 kilogram of 6-dinitroaniline, be equipped with 75 kilograms in compound fertilizer, fluorspar powder is done carrier for 23 kilograms, 0.3 kilogram of surfactant neopelex, odium stearate is made auxiliary agent for 0.2 kilogram, make binding agent for 0.5 kilogram with polyvinyl alcohol, make agricultural chemicals-chemical fertilizer compound formulation.
Embodiment 3-2:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.6 kilogram, 6-dinitro-N, 0.3 kilogram of N-di-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,0.3 kilogram of 4-dimethylaniline, B3 is N-sec-butyl-4-tertiary butyl-2,0.3 kilogram of 6-dinitroaniline, be equipped with 75 kilograms in compound fertilizer, fluorspar powder is done carrier for 22.5 kilograms, 0.3 kilogram of surfactant neopelex, odium stearate is made auxiliary agent for 0.2 kilogram, make binding agent for 0.5 kilogram with polyvinyl alcohol, make agricultural chemicals-chemical fertilizer compound formulation.
Embodiment 3-3:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 0.8 kilogram, 6-dinitro-N, 0.4 kilogram of N-di-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,0.4 kilogram of 4-dimethylaniline, B3 is N-sec-butyl-4-tertiary butyl-2, the 6-dinitroaniline is equipped with 75 kilograms in compound fertilizer for 0.4 kilogram, fluorspar powder is done carrier for 22 kilograms, 0.3 kilogram of surfactant neopelex, odium stearate is made auxiliary agent for 0.2 kilogram, make binding agent for 0.5 kilogram with polyvinyl alcohol, make agricultural chemicals-chemical fertilizer compound formulation.
Embodiment 3-4:
All in former medicine purity 100%, the quantity of other component is in the actual industrial product for the quantity of weed killer herbicide in the following prescription.
Herbicidal composition includes: A is that 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene is 2 with B1 for 1.0 kilograms, 6-dinitro-N, 0.5 kilogram of N-di-4-5-trifluoromethylaniline, B2 is N-1-(ethyl propyl)-2,-6-dinitro-3,0.5 kilogram of 4-dimethylaniline, B3 is N-sec-butyl-4-tertiary butyl-2,0.5 kilogram of 6-dinitroaniline, be equipped with 75 kilograms in compound fertilizer, fluorspar powder is done carrier for 21.5 kilograms, 0.3 kilogram of surfactant neopelex, odium stearate is made auxiliary agent for 0.2 kilogram, make binding agent for 0.5 kilogram with polyvinyl alcohol, make agricultural chemicals-chemical fertilizer compound formulation.
Embodiment five:
For the control efficiency of explanation serial herbicide composition of the present invention, in following embodiment 5, detect following index to upland field weed.
(1) weeds preventive effect (%)=(X-Y)/Y100
Wherein X is the weeds fresh weight that does not deal with, and Y is with the weeds fresh weight after the herbicide treatment.
(2) expection preventive effect (%) adopts the CoLby method, i.e. X+Y-XY/100, the weeds preventive effect when wherein X, Y are respectively single kind of weed killer herbicide.When surveying the weeds preventive effect, show the generation synergistic effect greater than the expection preventive effect.
(3) crop fresh weight inhibiting rate (%)=(R-S)/R100
Crop fresh weight when wherein R represents not use herbicide treatment, S are represented with herbicide treatment ensuing crop fresh weight.
Be used to measure the extent of injury (with blank compare) of weed killer herbicide to crop
Embodiment 5:
With A compound and the composite herbicidal composition of the present invention of category-B compound (B1, B2, B3), as follows to the control efficiency experiment condition of dry crop weeds as effective ingredient:
(1) experimental field basic condition: soil is neutral alkali sand soil partially, the content of organic matter 0.45～0.63%, preceding crop wheat, potato, corn.
(2) for studying thing: corn, Chinese ephedra, capsicum, willow cutting nursery.
(3) experimental condition: sowing on corn April 30, the Chinese ephedra late March is transplanted, and willow is transplanted a cutting cuttage mid-April, and capsicum is transplanted the first tenday period of a month in May, and dispenser applies with pouring water before late May broadleaf weed 4 leaves.Measure the control of weeds effect in time to the influence of target crop mid-August after the medication.
(4) experimental field weeds kind: broadleaf weed mainly contains lamb's-quarters, amaranth, wormwood artemisia etc., and monocotyledon weed mainly contains barnyard grass, india lovegrass, green foxtail, speedwell etc.Result of the test sees Table 1,2, and 3,4.
Table 1 cornfield weeding result
| Classes of compounds | Effective ingredient consumption (gram/mu) | Herbicidal effect (%) | Expection preventive effect (%) | Corn fresh weight inhibiting rate (%) | Influence (%) to corn field output | ||
| Unifacial leaf | Dicotyledonous | Average preventive effect | |||||
| A | 8 | 56.0 | 89.0 | 72.5 | 0 | +8.9 | |
| B1 | 20 | 52.0 | 23.0 | 37.5 | 0 | +3.2 | |
| 40 | 89.0 | 36.0 | 62.5 | 0 | +6.7 | ||
| B2 | 30 | 41.0 | 28.0 | 34.5 | 0 | +3.1 | |
| 60 | 90.5 | 37.1 | 63.8 | 0 | +6.6 | ||
| B3 | 50 | 60.2 | 24.1 | 42.2 | 0 | +3.3 | |
| 100 | 88.9 | 38.2 | 63.6 | 0 | +6.1 | ||
| A+B1 | 8+40 | 94.2 | 93.3 | 93.8 | 89.7 | 0 | +14.1 |
| A+B2 | 8+60 | 93.1 | 90.9 | 92.0 | 90.0 | 0 | +13.2 |
| A+B3 | 8+100 | 91.6 | 89.9 | 90.8 | 90.0 | 0 | +13.4 |
| A+B1+B2 | 8+20+30 | 96.0 | 94.2 | 95.1 | 88.7 | 0 | +14.7 |
| A+B2+B3 | 8+20+30 | 93.8 | 95.1 | 94.5 | 89.6 | 0 | +13.7 |
| A+B1+B3 | 8+20+50 | 96.3 | 94.7 | 95.5 | 89.9 | 0 | +14.3 |
| Blank | 0 | 0 | 0 | 0 | 0 | 0 | 0 |
The using method of composition series of herbicides of the present invention, be behind the crop seedling weeds 1-4 leaf phase use, adopt following method to use:
1, soup spreads the method for dripping.Mainly be that missible oil, aqueous emulsion, wetting powder evenly spread soup according to the mu consumption when pouring water and splash in the water.
2, spread fertilizer over the fields the particle method.Directly spread fertilizer over the fields into the farmland according to the mu consumption for Manufactured granule, agrochemical fertilizer mixture particle; For elder generations such as missible oil, aqueous emulsion, wetting powder with coated pesticidal be impregnated into granular fertilizer or carrier on, after evenly be sprinkled in the field.Pour water immediately after the dispenser, form one deck medicine film to guarantee the soil face of land.
Table 2 Chinese ephedra field herbicidal effect
| Classes of compounds | Effective ingredient consumption (gram/mu) | Herbicidal effect (%) | Expection preventive effect (%) | Chinese ephedra height inhibiting rate (%) | Influence (%) to Chinese ephedra output | ||
| Unifacial leaf | Dicotyledonous | Average preventive effect | |||||
| A | 10 | 51.0 | 93.0 | 72.0 | 0 | +9 | |
| B1 | 25 | 56.0 | 26.0 | 41.0 | 0 | +6.2 | |
| 50 | 93.0 | 48.0 | 70.5 | 0 | +8.3 | ||
| B2 | 40 | 46.0 | 32.0 | 39.0 | 0 | +5.7 | |
| 80 | 94.0 | 49.2 | 71.6 | 0 | +7.9 | ||
| B3 | 60 | 59.1 | 33.4 | 46.3 | 0 | +5.9 | |
| 120 | 91.3 | 43.3 | 67.3 | 0 | +7.6 | ||
| A+B1 | 10+50 | 96.0 | 94.0 | 95.0 | 91.7 | 0 | +16.4 |
| A+B2 | 10+80 | 97.0 | 96.0 | 96.5 | 92.0 | 0 | +15.9 |
| A+B3 | 10+120 | 94.0 | 92.0 | 93.0 | 90.8 | 0 | +16.1 |
| A+B1+B2 | 10+25+40 | 96.4 | 94.3 | 95.4 | 89.9 | 0 | +16.5 |
| A+B2+B3 | 10+40+60 | 96.8 | 95.2 | 96.0 | 90.8 | 0 | +15.4 |
| A+B1+B3 | 10,+25 10 | 95.3 | 97.9 | 96.6 | 91.1 | 0 | +15.6 |
| Blank | 0 | 0 | 0 | 0 | 0 | 0 | 0 |
Table 3 capsicum field herbicidal effect
| Classes of compounds | Effective ingredient consumption (gram/mu) | Herbicidal effect (%) | Expection preventive effect (%) | Capsicum fresh weight inhibiting rate (%) | Influence (%) to yield of hot pepper | ||
| Unifacial leaf | Dicotyledonous | Average preventive effect | |||||
| A | 10 | 57.0 | 90.0 | 73.5 | 0 | +11.3 | |
| B1 | 20 | 51.0 | 23.6 | 37.3 | 0 | +6.2 | |
| 40 | 89.0 | 37.0 | 63.0 | 0 | +9.1 | ||
| B2 | 30 | 40.0 | 27.0 | 33.5 | 0 | +5.9 | |
| 60 | 89.3 | 37.6 | 63.5 | 0 | +8.4 | ||
| B3 | 50 | 50.2 | 23.4 | 36.8 | 0 | +4.9 | |
| 100 | 88.6 | 39.7 | 64.2 | 0 | +8.1 | ||
| A+B1 | 10+40 | 94.2 | 93.6 | 93.9 | 90.2 | 0 | +19.2 |
| A+B2 | 10+60 | 93.9 | 92.3 | 93.1 | 90.3 | 0 | +20.3 |
| A+B3 | 10+100 | 92.6 | 90.5 | 91.6 | 90.5 | 0 | +19.2 |
| A+B1+B2 | 10+20+30 | 96.0 | 94.3 | 95.2 | 89.0 | 0 | +17.6 |
| A+B2+B3 | 10+30+50 | 94.8 | 93.6 | 94.2 | 88.9 | 0 | +18.3 |
| A+B1+B3 | 10+20+50 | 95.8 | 94.1 | 95.0 | 89.3 | 0 | +17.9 |
| Blank | 0 | 0 | 0 | 0 | 0 | 0 | 0 |
Table 4 poplar seedlings field herbicidal effect
| Classes of compounds | Effective ingredient consumption (gram/mu) | Herbicidal effect (%) | Expection preventive effect (%) | Influence (%) to the willow leading thread | ||
| Unifacial leaf | Dicotyledonous | Average preventive effect | ||||
| A | 10 | 51.0 | 93.6 | 72.3 | +12.6 | |
| B1 | 30 | 61.0 | 28.0 | 44.5 | +9.1 | |
| 60 | 95.0 | 46.0 | 70.5 | +12.3 | ||
| B2 | 45 | 58.0 | 29.0 | 43.5 | +8.9 | |
| 90 | 94.0 | 45.0 | 69.5 | +13.2 | ||
| B3 | 55 | 57.0 | 30.0 | 43.5 | +9.2 | |
| 110 | 93.0 | 47.0 | 70.0 | +11.4 | ||
| A+B1 | 10+60 | 97.0 | 95.2 | 96.1 | 91.8 | +22.6 |
| A+B2 | 10+90 | 96.8 | 94.9 | 95.9 | 91.6 | +21.4 |
| A+B3 | 10+110 | 95.8 | 94.8 | 95.3 | 91.7 | +20.5 |
| A+B1+B2 | 10+30+45 | 97.2 | 96.3 | 96.8 | 91.3 | +22.3 |
| A+B2+B3 | 10+45+50 | 96.2 | 95.4 | 96.3 | 91.3 | +21.4 |
| A+B1+B3 | 10+30+55 | 96.3 | 96.6 | 96.6 | 91.3 | +20.1 |
| Blank | 0 | 0 | 0 | 0 | 0 | 0 |
Claims (17)
1, a kind of herbicidal composition is characterized in that,
(1), it includes: [A] is 2 for 2-chloro-1-(3-ethyoxyl-4-nitrophenoxy)-4-(trifluoromethyl) benzene with being selected from [B1], 6-dinitro-N, N-di-4-5-trifluoromethylaniline, [B2] are N-sec-butyl-4-tertiary butyl-2, the active ingredient that the compound of one or both B groups of 6-dinitroaniline is formed;
(2), the active ingredient formed of one or both compound of A and B group wherein, all in the weight of 100% former medicine, its prescription is as follows:
A∶B＝1∶0.01-50。
2, herbicidal composition according to claim 1 is characterized in that, wherein A organizes the active ingredient that compound is formed with a kind of B that is selected from [B1], [B2], and all in the weight of 100% former medicine, its prescription is as follows:
A∶B＝1∶0.5-20。
3, herbicidal composition according to claim 1 is characterized in that, wherein A organizes the active ingredients that compound is formed with two kinds of B that are selected from [B1], [B2], and all in the weight of 100% former medicine, its prescription is as follows:
A∶B1∶B2＝1∶(0.5-10)∶(0.5-10)。
4, herbicidal composition according to claim 2 is characterized in that, wherein A organizes the active ingredient that compound is formed with a kind of B that is selected from [B1], [B2], and all in the weight of 100% former medicine, its prescription is as follows:
A∶B＝1∶1.5-4。
5, herbicidal composition according to claim 3 is characterized in that, wherein A organizes the active ingredients that compound is formed with two kinds of B that are selected from [B1], [B2],
A∶B1∶B2＝1∶(0.5-2)∶(0.5-2)。
6, according to the arbitrary described herbicidal composition of claim 1-5, it is characterized in that, described [A] and described B organize the active ingredient of one or both compound composition, weight in 100% former medicine, be equipped with solvent, emulsifier is made cream preparation, the percentage by weight of its prescription is: described [A] is 10-50 with the active ingredient that described B group compound is formed, and solvent is 30-65, and emulsifier is 5-15.
7, herbicidal composition according to claim 6, it is characterized in that, the active ingredient that the compound of one or both of described [A] and described B group is formed, weight in 100% former medicine, be equipped with solvent, emulsifier is made cream preparation, the percentage by weight of its prescription is 20-40, and solvent is 40-55, and emulsifier is 8-12.
8, herbicidal composition according to claim 6, it is characterized in that described solvent includes water, benzene,toluene,xylene, methyl alcohol, ethanol, propyl alcohol, butanols, ethylene glycol, ether, butyl ether, carrene, tetrachloro-ethylene, acetone, 4-methyl-2 pentanone, cyclohexanone, isopropylidene acetone, isophorone or dimethyl formamide; Described emulsifier is alkylbenzenesulfonate, agricultural newborn 8203#L-308, agricultural newborn 8209#, agricultural newborn 8206#, agricultural newborn 8901#, agricultural newborn 500# farming breast or tween-80, Span-80.
9, according to the arbitrary described herbicidal composition of claim 1-5, it is characterized in that, the active ingredient that one or both compounds of described [A] and B group are formed, weight in 100% former medicine, be equipped with surfactant, filler is made wetting powder, the percentage by weight of its prescription is the active ingredient 5-30 that one or both compounds of B group are formed, and surfactant is 5-10, and filler is 60-80.
10, herbicidal composition according to claim 9, it is characterized in that, the active ingredient that one or both compounds of described [A] and B group are formed, weight in 100% former medicine, be equipped with surfactant, filler is made wetting powder, the percentage by weight of its prescription is: the active ingredient that one or both compounds of B group are formed is 10-25, and surfactant is 7-9, and filler is 65-70.
11, herbicidal composition according to claim 9, it is characterized in that described surfactant is: peregal, lignin, sulfonate, naphthalene sulfonate, alkyl, phenol polyglycol ether, epoxidized polyether, alkylsulfonate, dispersing agent NNO, MF2, SS, CNF, draw back one or more of powder or cleaning agent LS; Described filler comprises: one or more of Attagel, montmorillonite, kaolin, bentonite, zeolite, protruding Attapulgite, precipitated calcium carbonate, white carbon, talcum powder, the plaster of paris, diatomite, magnesium sulfate.
12, according to the arbitrary described herbicidal composition of claim 1-5, it is characterized in that, the active ingredient that one or both compounds of described [A] and described B group are formed, weight in 100% former medicine, be equipped with carrier, auxiliary agent is made granule, wherein said auxiliary agent includes binding agent, dispersant, colouring agent, the percentage by weight of its prescription is: described [A] is 0.1-3.0 with the active ingredient that one or both compounds of B group are formed, carrier is 95-98, and binding agent is that 1-2, dispersant are that 1-5, colouring agent are 0.01-0.05 in the auxiliary agent.
13, herbicidal composition according to claim 12, it is characterized in that, the active ingredient that one or both compounds of described [A] and described B group are formed, weight in 100% former medicine, be equipped with carrier, auxiliary agent is made granule, wherein said auxiliary agent includes binding agent, dispersant, colouring agent, the most preferably value of the percentage by weight of its prescription is: described [A] is 0.5-1.5 with the active ingredient that one or both compounds of described B group are formed, carrier is 96-97, and binding agent is 1.5 in the auxiliary agent, dispersant is that 2-4, colouring agent are 0.02.
14, herbicidal composition according to claim 12 is characterized in that, described carrier is zeolite, river sand, clay, kaolin, attapulgite.
15, according to the arbitrary described herbicidal composition of claim 1-5, it is characterized in that, the active ingredient that one or both compounds of described [A] and described B group are formed, weight in 100% former medicine, be equipped with urea, ammonium nitrate, granulated phosphate fertilizer, MAP, diammonium phosphate, potassium chloride, potassium sulphate, magnesium sulfate and compound fertilizer are done carrier, dose Tween-80, NNO, the LS surfactant is made auxiliary agent, make agricultural chemicals-chemical fertilizer compound formulation, the percentage by weight of its prescription is: described [A] is 0.1-6.0 with the active ingredient that one or both compounds of described B group are formed, compound fertilizer is 92-98, auxiliary agent 1-5.
16, herbicidal composition according to claim 15, it is characterized in that, the active ingredient that one or both compounds of described [A] and described B group are formed, weight in 100% former medicine, be equipped with urea, ammonium nitrate, granulated phosphate fertilizer, MAP, diammonium phosphate, potassium chloride, potassium sulphate, magnesium sulfate and compound fertilizer are done carrier, dose Tween-80, NNO, the LS surfactant is made auxiliary agent, make agricultural chemicals-chemical fertilizer compound formulation, the percentage by weight of its prescription is: described [A] is 0.5-3.0 with the active ingredient that described B organizes one or both compounds compositions, compound fertilizer is 94-96, auxiliary agent 2-4.
17, the using method of herbicidal composition according to claim 1, it is characterized in that, in the perennial plant field, adopt soup to spread to drip a method or a particle broadcast application, promptly when pouring water, herbicidal composition liquid splashed into or pour water before this herbicidal composition uniform particles is sprinkled into Tanaka.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 03157853 CN1274217C (en) | 2003-09-10 | 2003-09-10 | Dry farmland herbicide and its methods of use |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 03157853 CN1274217C (en) | 2003-09-10 | 2003-09-10 | Dry farmland herbicide and its methods of use |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1522569A CN1522569A (en) | 2004-08-25 |
| CN1274217C true CN1274217C (en) | 2006-09-13 |
Family
ID=34287174
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 03157853 Expired - Fee Related CN1274217C (en) | 2003-09-10 | 2003-09-10 | Dry farmland herbicide and its methods of use |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1274217C (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103242104A (en) * | 2013-05-22 | 2013-08-14 | 徐应先 | Plant liquid fertilizer |
| TWI598040B (en) * | 2016-10-21 | 2017-09-11 | Liang-Wei Zeng | Compositions for controlling weeds and methods for controlling weeds |
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2003
- 2003-09-10 CN CN 03157853 patent/CN1274217C/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN1522569A (en) | 2004-08-25 |
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