CN1273055C - Processing technique for compound product of kudzu root and bitter gourd - Google Patents
Processing technique for compound product of kudzu root and bitter gourd Download PDFInfo
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- CN1273055C CN1273055C CN 200310111504 CN200310111504A CN1273055C CN 1273055 C CN1273055 C CN 1273055C CN 200310111504 CN200310111504 CN 200310111504 CN 200310111504 A CN200310111504 A CN 200310111504A CN 1273055 C CN1273055 C CN 1273055C
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- balsam pear
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Abstract
The present invention provides a processing technique for a compound product of kudzu root and bitter gourd; raw materials of kudzuvine root and balsam pear of which the fresh materials of proportion by weight are 1 to 4:10 or the dry material of proportion by weight is 1 to 2:2, are leached by the addition of water (if the raw materials are fresh materials, the raw materials are extracted into juice, and slag is leached by the addition of water), and filtered; then, bacteria are removed by microfiltration; filter liquor is concentrated by a reverse osmosis membrane and then frozen and dried to obtain powder of a semi-finished product; the powder is filled in capsules or made into tablets or oral medicinal liquid to a finished product. The present invention is characterized in that the processing technique does not need to be heated; in the whole production process, an advanced membrane separation and freeze-drying technology is used, which effectively maintains the bioactivity of kudzuvine root and balsam pear. The present invention provides novel health-care food for patients with diabetes.
Description
Technical field:
The present invention relates to a kind of production method of health food-Yizhibao, especially a kind of root of kudzu vine, balsam pear joint product processing technology.
Background technology:
The root of kudzu vine, balsam pear are as extract Puerarin (kudzu root flavone) and the Charantin developed separately, existing industry is sold on market at present, but do not see relevant report with the root of kudzu vine, the compound preparation of balsam pear, and the root of kudzu vine on the market, Bitter Melon P.E, all be to make with extra care and get with alcoholic extraction, this technology is the normal reflux extractive technique, utilize normal reflux extraction and drying equipment to make, its shortcoming is the processing through high temperature heating and organic solvent, active material to the root of kudzu vine, balsam pear has destruction, influenced its biologically active, effect reduces.
Summary of the invention:
Purpose of the present invention adopts low temperature not heat exactly, is the extracting method of solvent with water, produces to have the higher bioactive root of kudzu vine, Bitter Melon P.E, and makes the healthy food of new diabetes patients.The present invention adopts modern molecular level isolation technics---membrane separation technique and Freeze Drying Technique, has solved the problem of with an organic solvent separating in the production process and heating extraction well.
The technical solution used in the present invention is: the aquatic foods material weight proportion that the raw material root of kudzu vine, balsam pear is added flooding (if bright material is then squeezed the juice earlier, residue add flooding again), the root of kudzu vine, balsam pear is 1～4: 10, or the siccative weight proportion is 1～2: 2, filter, remove bacterium by micro-filtrate membrane filtration then, filtrate concentrates with reverse osmosis membrane, freeze drying gets the semi-finished product powder, filled capsules or compressing tablet or make oral liquid and get product.
1, principle: the root of kudzu vine is the food of medicine-food two-purpose, has clearing heat and detoxicating, as to quench one's thirst dampness removing effect; Balsam pear is the traditional food vegetables, has clearing heat and detoxicating effect; Two kinds of raw materials are the healthy food as the diabetic in traditional traditional Chinese medicine, and modern pharmacology proves, kudzu root flavone also has to angiocardiopathy etc. effectively, and Charantin has hypoglycemic activity.Both combinations, by flooding, membrane technology separates, and freeze drying improves the biologically active of its active ingredient, develops to have the healthy food that powerful more is suitable for the diabetic.
2, process
(1) technological process
The root of kudzu vine, balsam pear-mix in proportion feed intake-squeeze the juice lixiviate (bright material is squeezed the juice earlier, and residue adds flooding)-leaching liquor (juice and water extract merge) filtrations-micro-filtration-reverse osmosis concentration-freeze drying-filled capsules or compressing tablet or prepare oral liquid-pack finished product.
(2) technological operation main points
A, mixed feeding intake: the root of kudzu vine, balsam pear 1～2: 2 (siccatives) or 1～4: 10 (bright material) in proportion feed intake.
B, water extract: the root of kudzu vine, balsam pear are after squeezing the juice, and residue still contains active ingredient, need add flooding again, and amount of water was as the criterion to soak the residue liquid level, extracted altogether 3 times.
C, filtration: extract need be filtered to earlier clearly, to remove the granule residue.
D, micro-filtration: on go on foot clear liquid and remove bacterium by micro-filtration, to meet the sanitary standard requirement.
E, reverse osmosis concentration: by reverse osmosis concentration, it is 10～15 ° that extract is concentrated into Brix °.
F, freeze drying: on go on foot concentrate through after the freeze drying the dry powder semi-finished product, during freeze drying, be refrigerated to earlier below-45 ℃, distillation then, sublimation temperature is no more than 40 ℃.
G, filled capsules or compressing tablet or the preparation oral liquid: on go on foot gained dry powder semi-finished product, can be used for filling capsule or compressing tablet or the preparation oral liquid, through pack finished product.
Advantage of the present invention or good effect:
Characteristics of the present invention are without heating, all production processes adopt advanced film to separate and Freeze Drying Technique, have effectively kept the biologically active of the root of kudzu vine, balsam pear, for the diabetic provides a kind of new healthy food.
The specific embodiment:
Embodiment 1
Root of kudzu vine 80kg, balsam pear 500kg, squeeze the juice 380kg, add water 3 * 200kg lixiviate, each lixiviate 1 hour merges leaching liquor and bright juice, 950kg.Filtration, micro-filtration, reverse osmosis concentration to Brix ° be 12 °, freeze drying gets semi-finished product 1.3kg, during freeze drying, is cooled to-45 ℃ earlier, distillation then, sublimation temperature is 35 ℃, the dry powder semi-finished product.
Embodiment 2
Root of kudzu vine 250kg, balsam pear 1.5T, squeeze the juice 1.1T, add water 3 * 600kg lixiviate, each lixiviate 1 hour, merge leaching liquor and bright juice and get 2.8T, filtration, micro-filtration, reverse osmosis concentration to Brix ° be 13 °, freeze drying gets semi-finished product 40kg, is chilled to-48 ℃ during freeze drying earlier, distillation then, sublimation temperature is 33 ℃.Fill capsule with semi-finished product, pack finished product.
This product feature: (1) gets 1ml hot water extracting liquid, adds 2～3 of 5%a-naphthols ethanolic solutions, shakes up, and slowly adds the 0.5ml concentrated sulfuric acid along test tube wall; At the interface place of the test tube and the concentrated sulfuric acid, the purplish red colour circle of very fast formation.(2) get this product powder 0.8g, add methyl alcohol 10ml, 2 hours filtration residues are set add methyl alcohol 0.5ml dissolving; Other gets the Puerarin reference substance, adds methyl alcohol and makes the solution that every 1ml contains 1mg; Draw above-mentioned two kinds of each 10ml of solution, put respectively on the silica gel H lamellae that same sodium carboxymethylcellulose is adhesive, make into strips, with chloroform-methanol-water (7: 2.5: 0.25) is solvent, launch, take out, dry, put under the ultraviolet lamp (365nm) and inspect, manifest the fluorescence streak of same color on sample chromatogram and the corresponding position of contrast chromatogram.
Claims (2)
1, the preparation method of a kind of root of kudzu vine, balsam pear joint product is characterized in that:
The aquatic foods material weight proportion of the root of kudzu vine, balsam pear is 1～4: 10, or the siccative weight proportion is 1～2: 2;
Production process does not heat, adopt the flooding residue then of earlier raw material being squeezed the juice on the technology, filter extract, again micro-filtrate membrane filtration, concentrate with reverse osmosis membrane, it is 10～15 ° that extract is concentrated into Brix °, is refrigerated to then below-45 ℃, distillation again, sublimation temperature is no more than 40 ℃, gets the dry powder semi-finished product after the freeze drying.
2, the preparation method of the root of kudzu vine according to claim 1, balsam pear joint product, dried semi-finished product can be used for processing capsule, tablet or oral liquid formulation.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200310111504 CN1273055C (en) | 2003-11-28 | 2003-11-28 | Processing technique for compound product of kudzu root and bitter gourd |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200310111504 CN1273055C (en) | 2003-11-28 | 2003-11-28 | Processing technique for compound product of kudzu root and bitter gourd |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1545943A CN1545943A (en) | 2004-11-17 |
| CN1273055C true CN1273055C (en) | 2006-09-06 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200310111504 Expired - Fee Related CN1273055C (en) | 2003-11-28 | 2003-11-28 | Processing technique for compound product of kudzu root and bitter gourd |
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| CN (1) | CN1273055C (en) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102318849A (en) * | 2011-07-01 | 2012-01-18 | 南宁大单生物科技有限责任公司 | Balsam pear vinegar |
| CN102293297B (en) * | 2011-07-18 | 2013-03-27 | 句容茅宝葛业有限公司 | Preparation method of kudzu tea |
| CN103284083B (en) * | 2012-02-24 | 2016-06-08 | 中科云健康科技(天津)有限公司 | Balsam pear dry product of homovitamin C content and preparation method thereof |
| CN102599578B (en) * | 2012-03-28 | 2013-12-25 | 太仓市临江农场专业合作社 | Compound health beverage |
| CN102626452A (en) * | 2012-04-25 | 2012-08-08 | 吴庆林 | Hawthorn, radix puerariae, gingko and balsam pear four-in-one flavone capsule |
| CN103655672A (en) * | 2012-09-25 | 2014-03-26 | 洛阳花瓣舞生物技术有限公司 | Preparation method of loofah stoste |
| CN103478643B (en) * | 2013-09-25 | 2014-12-03 | 湖北省宏源药业有限公司 | Comprehensive utilization method for waste water and fibroid dregs generated from arrowroot production |
| CN104873648A (en) * | 2015-06-05 | 2015-09-02 | 王丽坤 | Medicine for regulating hypertension, hyperglycemia and hyperlipidemia |
| CN109965290B (en) * | 2017-12-27 | 2023-06-20 | 深圳华大生命科学研究院 | Meal replacement powder for improving intestinal flora and application thereof |
| CN112717071A (en) * | 2021-01-26 | 2021-04-30 | 张天亮 | Medicament for treating diabetes |
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2003
- 2003-11-28 CN CN 200310111504 patent/CN1273055C/en not_active Expired - Fee Related
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| Publication number | Publication date |
|---|---|
| CN1545943A (en) | 2004-11-17 |
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Granted publication date: 20060906 Termination date: 20091228 |