CN1267690A - Fireproof and waterproof canvas paint and its compounding process - Google Patents
Fireproof and waterproof canvas paint and its compounding process Download PDFInfo
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- CN1267690A CN1267690A CN 00114186 CN00114186A CN1267690A CN 1267690 A CN1267690 A CN 1267690A CN 00114186 CN00114186 CN 00114186 CN 00114186 A CN00114186 A CN 00114186A CN 1267690 A CN1267690 A CN 1267690A
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Abstract
The canvas paint of the present invention is one two-component synthetic rubber slurry paint including component A and component B. The component A consists of synthetic rubber CSM20 or CSM30, liquid epoxy resin, chlorinated resin, sulfurizing promoter, fungicide and mixed solvent; and the component B consists of polymerized rosin or polyamide 300 or polyamide 650, chlorinated rubber or chlorinated polyethylene or vinyl chloride-maleic acid copolymer, fireproof agent, color, defoaming agent, levelling agent and mixed solvent. The canvas material with the paint of the present invention has excellent fireproof, waterproof, weather resisting, aging resisting, acid resisting, alkali resisting, salt resisting and mouldproof performance.
Description
The present invention relates to a kind of synthetic rubber rubber cement coating and preparation method thereof.
For general rainproof tarpaulin is become the fire-proof and water-proof tarpaulin, greatly to expand its Application Areas, people have invented the coating that is used to make fireproof and waterproof canvas of various different ingredients.Chinese patent CN1034943A discloses a kind of " latex of high molecular compounded special triple-prevention material ", and the prescription of its serum is made up of polyvinyl acetate (PVA), polyvinyl alcohol, anti-aging agent, permeate agent, fire retardant, defoamer, water and cationic chloroprene latex.It is said that this invention has solved waterproof, fire prevention, the protection against corrosion problem of tarpaulin coating.But should invent because due to the limitation of rubber cement raw material itself, may exist: the package stability of coating is not so good, and workability is also not ideal, is difficult to obtain level and smooth coatingsurface, and in addition, coating is adsorbed dust easily, tarpaulin needs often to clean.Chinese patent CN1064905A disclosed " dyeing and finishing method of many anti-(waterproof, fire-retardant, anticorrosion, anti-electrostatic etc.) fabric ", its prescription is made up of the same softening agent of polyvinyl chloride (PVC) RESINS, fire retardant, aluminium powder, solvent etc., make material infiltrate fabric by padding method, through high temperature plasticizing and on the fabric yarn surface, form thin film, make fiber and air insulated and obtain multi-functional.It is said that this method is used as tent, drop cloth, protective clothes and protective device fabric usually.The problem that this invention exists is; Because the thermostability of polyvinyl chloride (PVC) RESINS itself is relatively poor, thermolysis easily is so thermotolerance is relatively poor; Next is that complete processing is complicated, plastify under 160～240 ℃ high temperature, and also there is plasticizer migration simultaneously in the energy consumption height, makes coating produce the phenomenon that is clamminess.
The purpose of this invention is to provide a kind of excellent storage stability, good heat resistance, good flame resistance, canvas coating and blending process thereof with fire-proof and water-proof performance.
The objective of the invention is to realize by following measure.
Fireproof and waterproof canvas paint of the present invention is the synthetic rubber rubber cement coating that contains organic solvent of a kind of pair of component subpackage type, and it is made up of first component and component B, wherein,
The first component is formed (weight percentage) by following starting material:
Synthetic rubber CSM20 or CSM30 25～35%
Liquid epoxies 5～8%
Chlorinated resin or vinyl chloride-vinylidene chloride resin 2～4%
Vulcanization accelerator 1～2%
Mould inhibitor 1～2%
Surplus is a mixed solvent;
Component B is formed (weight percentage) by following starting material:
Polymerized rosin (dimer) or polyamide 6 50 or kymene 00 3～9%
Chlorinated rubber or chlorinatedpolyethylene or vinylchlorid-maleate copolymer 8～10%
Fire retardant 20～35%
Smoke suppressor 3～7%
Pigment 15～35%
Defoamer 0.01～0.02%
Flow agent 0.01～0.02%
Surplus is a mixed solvent;
Mixed solvent in first, the component B is formed (weight percentage) by following starting material;
Dimethylbenzene 69%
No. 200 solvents 21%
Butanols 10%;
First component: component B=10: 1 (weight).
The blending process of anti-fire and water-proof paint of the present invention is:
Synthetic rubber CSM20 or CSM30 film are cut into short adhesive tape;
The preparation of first component: by prescription material consumption, with synthetic rubber CSM20 or CSM30 adhesive tape, liquid epoxies, chlorinated resin or vinyl chloride-vinylidene chloride resin, vulcanization accelerator dissolves with mixed solvent stirring under 80 ± 2 ℃, until being dissolved into rubber cement fully, add mould inhibitor then, be cooled to the room temperature after-filtration.Packed for standby use.
The preparation of component B: by prescription material consumption, with polymerized rosin (dimer) or polyamide 6 50 or kymene 00, with, chlorinated rubber or chlorinatedpolyethylene or vinylchlorid-maleate copolymer, dissolve with mixed solvent stirring under 80 ± 2 ℃,, be cooled to the room temperature after-filtration until being dissolved into rubber cement fully, then remaining material is added in the good sizing material of dissolving, be ground to fineness after mixing and reach 20 μ m.Packed for standby use.
Before applying construction, by the first component: the coating of can constructing after the mixed of component B=10: 1 (weight) is even.
When construction applies, regulate execution of coating viscosity of the present invention with aforementioned mixed solvent.Generally, adopt the spraying method construction, about 30 seconds of its viscosity adopts brush application, and about 60～70 seconds of its viscosity adopts the roller painting construction, about 70～80 seconds of its viscosity.
With coating of the present invention be coated in through the cotton of waterborne flame retardant agent arrangement or wash-two surfaces of cotton blending canvas on, after solidification treatment, can obtain to have the canvas product of excellent fire-proof and water-proof performance.
The present invention has following advantage:
1, coating of the present invention has good storing stability, thermostability and good construction performance, can adopt spread coating, spraying method and roller painting to construct, and it is particularly suitable for adopting mechanize, automatic continuous roll coating process to produce fireproof and waterproof canvas;
2, coating of the present invention does not contain heavy metal lead, mercury and radioactivity does not have element, meets environment protection and HUMAN HEALTH safety requirements;
3,, has the performance of following excellence with the canvas matrix material of coating material production of the present invention;
(1) You Yi fire resistance, this material combustion performance reaches the GB8624B1 level;
(2) You Yi water resistance, water pressure resistance 140～200cm (being coated with 2 roads); Hang water test: φ 350mm, depth of water 200mm, the water at 60 ° of angles sprinkle and beat, and be water-tight;
(3) You Yi high temperature resistant, low temperature resistant and high and low temperature resistance, high temperature resistant 120 ℃/6h does not ftracture, and is non-foaming, is not clamminess the outward appearance no change; Low temperature resistant-50 ℃/6h does not ftracture, and is non-foaming, do not come off, crooked nothing be full of cracks, and cloth specimen is felt firmly slightly, recovers former state at normal temperatures; High-low temperature resistant-45～80 ℃ circulates 6 times, does not ftracture, and is non-foaming, do not come off, and crooked do not have a be full of cracks.
(4) You Yi ageing-resistant, acidproof, alkaline-resisting, salt tolerance, oil-proofness, anti-oceanic climate, and fungus resistance (anti-mould reaches 1 grade).
Embodiment one:
Formula table
| Sequence number | Starting material title and model | Weight percentage (%) |
| First component 123456 | Synthetic rubber CSM30 altax chlorinated rubber Resins, epoxy E44 mould inhibitor TMTD mixed solvent | ????27 ????1.5 ????2.5 ????6.5 ????1.2 ????61.3 |
| Component B 123456789 10 11 | Polymerized rosin (dimer) chlorinated rubber fire retardant AP TiO 2R902 red iron oxide (95%) high-carbon black pigment Al 2O 3·3H 2The green mill base defoamer of O flow agent mixed solvent | 5 10 22 14 615 an amount of 0.01 0.01 about 36 |
Mixed solvent is formed the first component by dimethylbenzene 69% (weight), No. 200 solvents 21% (weight) and butanols 10% (weight) in the above-mentioned table: component B=10: 1 (weight)
The blending process of coating:
Synthetic rubber CSM30 film is cut into the long adhesive tape of 10～15cm;
The first component: by the material consumption of above-mentioned formula table, the material of sequence number 1,2,3,4 is inserted in the stainless steel still that has electric mixer and reflux, stirs down at 80 ± 2 ℃ with mixed solvent, until be dissolved into naked eyes do not see particle is arranged till; Add mould inhibitor then, after being cooled to room temperature, filter, in the packing plastics bucket of packing into, stand-by.
Component B: by the material consumption of above-mentioned formula table, the material of sequence number 1,2 is inserted in the stainless steel still that has electric mixer and reflux, with mixed solvent in 80 ± 2 ℃ down constantly stirring dissolve, up to being dissolved into till naked eyes cannot see particle; Through being cooled to room temperature, filter discharging; Then remaining material is added in the good sizing material of dissolving, mix with the high-speed stirring decollator earlier, move to and grind in the triple-roller mill, being milled to fineness, to reach 20 μ m be qualified, packs, stand-by.
In the first component: the coating of can constructing behind the ratio uniform mixing of component B=10: 1 (weight).
Embodiment two
Formula table
| Sequence number | Starting material title and model | Weight percentage (%) |
| First component 123456 | Synthetic rubber CSM20 altax chlorinated polyethylene resin Resins, epoxy E54 mould inhibitor TMTD mixed solvent | ????28 ????1.5 ????3 ????6.5 ????1.0 ????60 |
| Component B 123456789 10 11 | Polyamide 6 50 chlorinated polyethylene resin composite flame-retardant agent F/R P-53 TiO 2R902 red iron oxide (95%) high-carbon black pigment (NH 4) 2MoO 4(95%) green mill base defoamer flow agent mixed solvent | 69 24 13 6 1.0 5 an amount of 0.01 0.01 about 35 |
All the other are identical with embodiment one.
The preparation technology of coating is identical with embodiment one.
Embodiment three
Formula table
| Sequence number | Starting material title and model | Weight percentage (%) |
| First component 123456 | Synthetic rubber CSM30 altax vinylchlorid-maleate copolymer Resins, epoxy E42 mould inhibitor TMTD mixed solvent | ????29 ????1.5 ????2.5 ????7 ????1.0 ????59 |
| Component B 123456789 10 11 | Polymerized rosin (dimer) vinylchlorid-maleate copolymer fire retardant AP TiO 2R902 red iron oxide (95%) Mg (OH) 2(95%) the green mill base defoamer of high-carbon black pigment flow agent mixed solvent | 58 23 14 65 1.0 an amount of 0.01 0.01 about 37 |
All the other are identical with embodiment one.
The preparation technology of coating is identical with embodiment one.
Claims (6)
1, a kind of prescription of fireproof and waterproof canvas paint is characterized in that: it is made up of first component and component B, and described first component is formed (weight percentage) by following starting material:
Synthetic rubber CSM20 or CSM30 25～35%
Liquid epoxies 5～8%
Chlorinated resin or vinyl chloride-vinylidene chloride resin 2～4%
Vulcanization accelerator 1～2%
Mould inhibitor 1～2%
Surplus is a mixed solvent;
Described component B is formed (weight percentage) by following starting material:
Polymerized rosin (dimer) or polyamide 6 50 or kymene 00 3～9%
Chlorinated rubber or chlorinatedpolyethylene or vinylchlorid-maleate copolymer 8～10%
Fire retardant 20～35%
Smoke suppressor 3～7%
Pigment 15～35%
Defoamer 0.01～0.02%
Flow agent 0.01～0.02%
Surplus is a mixed solvent;
Mixed solvent in described first, the component B is formed (weight percentage) by following starting material:
Dimethylbenzene 69%
No. 200 solvents 21%
Butanols 10%
First component: component B=10: 1 (weight).
2, the prescription of fireproof and waterproof canvas paint according to claim 1 is characterized in that fire retardant is fire retardant AP or fire retardant F/R P-53, and smoke suppressor is Mg (OH)
2Or (NH
4)
2MoO
4(95%) or Al
2O
33H
2O.
3, the prescription of fireproof and waterproof canvas paint according to claim 1 and 2 is characterized in that described first component forms (weight percentage) by following starting material:
Synthetic rubber CSM30 27%
Altax 1.5%
Chlorinated rubber 2.5%
Resins, epoxy E44 6.5%
Mould inhibitor TMTD 1.2%
Mixed solvent 61.3%
Described component B is formed (weight percentage) by following starting material:
Polymerized rosin (dimer) 5%
Chlorinated rubber 10%
Fire retardant AP 22%
TiO
2?R902??????????????????14％
Red iron oxide (95%) 6%
High-carbon black pigment 1%
Al
2O
3·3H
2O?????????????5％
Green mill base is an amount of
Defoamer 0.01%
Flow agent 0.01%
Mixed solvent about 36%
4, the prescription of fireproof and waterproof canvas paint according to claim 1 and 2 is characterized in that described first component forms (weight percentage) by following starting material:
Synthetic rubber CSM20 28%
Altax 1.5%
Chlorinated polyethylene resin 3%
Resins, epoxy E54 6.5%
Mould inhibitor TMTD 1.0%
Mixed solvent 60%
Described component B is formed (weight percentage) by following starting material:
Polyamide 6 50 6%
Chlorinated polyethylene resin 9%
Composite flame-retardant agent F/R P-53 24%
TiO
2?R902?????????????????13％
Red iron oxide (95%) 6%
High-carbon black pigment 1.0%
(NH
4)
2MoO
4(95％)????????5％
Green mill base is an amount of
Defoamer 0.01%
Flow agent 0.01%
Mixed solvent about 35%
5, the prescription of fireproof and waterproof canvas paint according to claim 1 and 2 is characterized in that described first component forms (weight percentage) by following starting material:
Synthetic rubber CSM30 29%
Altax 1.5%
Vinylchlorid-maleate copolymer 2.5%
Resins, epoxy E42 7%
Mould inhibitor TMTD 1.0%
Mixed solvent 59%
Described component B is formed (weight percentage) by following starting material:
Polymerized rosin (dimer) 5%
Vinylchlorid-maleate copolymer 8%
Fire retardant AP 23%
TiO
2?R902??????????????14％
Red iron oxide (95%) 6%
Mg(OH)
2(95％)???????????5％
High-carbon black pigment 1.0%
Green mill base is an amount of
Defoamer 0.01%
Flow agent 0.01%
Mixed solvent about 37%
6, fireproof and waterproof canvas paint according to claim 1 and 2, its blending process is characterised in that:
To close rubber CSM20 or the CSM30 film is cut into short adhesive tape;
The preparation of first component: by prescription material consumption, with synthetic rubber CSM20 or CSM30 adhesive tape, Resins, epoxy, chlorinated resin or vinyl chloride-vinylidene chloride resin, vulcanization accelerator dissolves with mixed solvent stirring under about 80 ± 2 ℃, until being dissolved into rubber cement fully, add mould inhibitor then, be cooled to the room temperature after-filtration, packing is waitd upon usefulness;
The preparation of component B: by prescription material consumption, with polymerized rosin (dimer) or polyamide 6 50 or kymene 00, with, chlorinated rubber or chlorinatedpolyethylene or vinylchlorid-maleate copolymer dissolve with mixed solvent stirring under 80 ± 2 ℃, until being dissolved into rubber cement fully, be cooled to the room temperature after-filtration, then remaining material is added in the good sizing material of dissolving, be ground to fineness behind the uniform mixing and reach 20 μ m, packed for standby use;
In the first component: the coating of can constructing behind the ratio uniform mixing of component B=10: 1 (weight).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 00114186 CN1267690A (en) | 2000-04-06 | 2000-04-06 | Fireproof and waterproof canvas paint and its compounding process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 00114186 CN1267690A (en) | 2000-04-06 | 2000-04-06 | Fireproof and waterproof canvas paint and its compounding process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1267690A true CN1267690A (en) | 2000-09-27 |
Family
ID=4583899
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 00114186 Pending CN1267690A (en) | 2000-04-06 | 2000-04-06 | Fireproof and waterproof canvas paint and its compounding process |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1267690A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100451078C (en) * | 2005-08-11 | 2009-01-14 | 中国石油天然气集团公司 | Silver coloured perchloro polyethylene external corrusion resistant paint and its manufacturing method |
| CN101284970B (en) * | 2008-05-30 | 2010-07-28 | 王丹 | Waterproof coating material |
| CN101255306B (en) * | 2007-09-11 | 2011-05-04 | 兰州理工大学 | Paint for composition cloth and preparation thereof |
| CN103073991A (en) * | 2013-01-06 | 2013-05-01 | 葫芦岛市恒通特种漆有限公司 | Method for preparing low temperature resistant and corrosion proof coating |
| CN103952910A (en) * | 2014-03-25 | 2014-07-30 | 安徽柏拉图涂层织物有限公司 | Coating material for ship sail surface material |
-
2000
- 2000-04-06 CN CN 00114186 patent/CN1267690A/en active Pending
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100451078C (en) * | 2005-08-11 | 2009-01-14 | 中国石油天然气集团公司 | Silver coloured perchloro polyethylene external corrusion resistant paint and its manufacturing method |
| CN101255306B (en) * | 2007-09-11 | 2011-05-04 | 兰州理工大学 | Paint for composition cloth and preparation thereof |
| CN101284970B (en) * | 2008-05-30 | 2010-07-28 | 王丹 | Waterproof coating material |
| CN103073991A (en) * | 2013-01-06 | 2013-05-01 | 葫芦岛市恒通特种漆有限公司 | Method for preparing low temperature resistant and corrosion proof coating |
| CN103073991B (en) * | 2013-01-06 | 2016-06-01 | 葫芦岛市恒通特种漆有限公司 | The production method of a kind of coating of resistance to low-temperature corrosion protection |
| CN103952910A (en) * | 2014-03-25 | 2014-07-30 | 安徽柏拉图涂层织物有限公司 | Coating material for ship sail surface material |
| CN103952910B (en) * | 2014-03-25 | 2016-01-20 | 安徽柏拉图涂层织物有限公司 | A kind of sail fabric coating and preparation method thereof |
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| C06 | Publication | ||
| PB01 | Publication | ||
| AD01 | Patent right deemed abandoned | ||
| C20 | Patent right or utility model deemed to be abandoned or is abandoned |