CN1236141C - Making process of Chinese cypress paper with wide-spectrum antiseptic function for cygarette - Google Patents
Making process of Chinese cypress paper with wide-spectrum antiseptic function for cygarette Download PDFInfo
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- CN1236141C CN1236141C CN 02146697 CN02146697A CN1236141C CN 1236141 C CN1236141 C CN 1236141C CN 02146697 CN02146697 CN 02146697 CN 02146697 A CN02146697 A CN 02146697A CN 1236141 C CN1236141 C CN 1236141C
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- antiseptic
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Abstract
The present invention discloses a preparation method of Chinese cypress paper with wide-spectrum antiseptic function for cygarettes, which comprises the following steps: coating printing is carried out to a piece of base Chinese cypress paper by printing compression rollers to realize that the surface of the base Chinese cypress paper is uniformly coated with wide-spectrum antiseptic printing ink containing inorganic antibacterial agents, organic antibacterial agents and traditional Chinese medicine preparations to obtain the Chinese cypress paper with wide-spectrum antiseptic function. The present invention is characterized in that 10PPM to 2000PPM of silver ions or copper ions or ampicillin sodium or traditional Chinese medicine Bazheng mixtures, or two or three or four of the four antibacterial agents are added to the printing ink composed of modified rosin, polyvinyl alcohol, dibutyl phthalate, butyral, anatase titanium dioxide, medical etanol, ferrite yellow calcium carbonate and talc powder; then, the mixture reacts for 0.5 to 24 hours under the condition of 0 to 60 DEG C; a product is ground, pulverized, dispersed and used for coating and printing the base Chinese cypress paper to prepare the Chinese cypress paper with wide-spectrum antiseptic function. The present invention has the advantages of simple procedure, strong applicability, wide antiseptic spectrum, lasting antisepsis, heat and acid and alkali resistance, and human body innocuity.
Description
Technical field
The present invention relates to the preparation method of a kind of cigarette, belong to the technology of preparing of antiseptic China Cypress paper with broad-spectrum antiseptic yew paper.
Background technology
The overwrap of cigarette filter mouth portion is called yew paper, and yew paper has different colours and decorative pattern, all realizes by applying various decorative inks.Yew paper is called tipping base paper before applying printing ink.
As everyone knows, smoking population occupies very big ratio in world population, and still has the trend of rising.Because bacterium extensively is present in people's work and the living environment, people's health has been constituted serious threat.In recent years, smoking was constantly surging with healthy cry, and the consumer has also proposed new requirement to the safety and sanitation of cigarette yew paper.Cigarette yew paper is the cigarette tipping paper that plume is twisted in filter rod, and people put into mouth with the yew paper that scribbles printing ink.Yet cigarette yew paper is easy to catch various bacteriums in production, packed and transported, storage and use, then these bacteriums just from the oral cavity, respiratory tract enters human body, causes multiple disease easily.Following table is sampling cigarette yew paper microorganism detection result:
| B4 | 10 | 5 |
| B5 | 10 | 35 |
| D1 | 10 | 5 |
| D2 | 10 | 15 |
| D4 | 10 | 5 |
| E2 | 310 | Do not detect |
| E4 | 20 | Do not detect |
| F2 | 20 | Do not detect |
Carry out science and technology through Tianjin scientific information Institute of Social Science Information and look into newly (report number is 20021201002375), adopt retrieval methods such as manual information retrieval, light disk retrieval, state's interconnect, international online, in following scope, retrieve:
1. CSTAD (version in 2002)
2. Chinese technical journal piece of writing name database (1989---2002-03)
Chinese science and technology Economic News database (1992---2002-03)
Chinese patent database (1985---2002-08)
5. china academia paper database (version in 2002)
6. china academia meeting paper database (version in 2002)
7. Chinese chemical industry bibliographic data base (version in 2002)
(8.CA chemical industry document) (1967---2002-06)
9.WPI (world patents index) (1963-----2002-08)
10.JAPIO (Japan Patent) (1976------2002-08)
11.EuropeaPatents (European patent) (1978-----2002-08)
12.USPat.Fulltext (United States Patent (USP)) (1971------2002-08)
Looking into new conclusion is:-----but do not see the report that is used for cigarette usefulness yew paper antibacterial treatment.In above-mentioned bibliographical information, do not see the bibliographical information of the antiseptic China Cypress paper research identical with this project research contents.
Summary of the invention
The purpose of this invention is to provide the preparation method of a kind of cigarette yew paper with broad-spectrum antiseptic printing ink.This procedure is simple, and applicability is strong, and has a broad antifungal spectrum is antibiotic lasting, heat-resisting, and acid and alkali-resistance is nontoxic to human body.
The present invention is realized by following technical proposals.A kind of cigarette preparation method of broad-spectrum antiseptic yew paper, this method is with tipping base paper, through the print roller application to printed, apply equably in its surface and contain inorganic antiseptic, the broad-spectrum antiseptic printing ink of organic antibacterial agent and Chinese medicine preparation, make broad-spectrum antiseptic yew paper, it is characterized in that: to modified rosin by percentage by weight 0.5%-5.0%, the polyvinyl alcohol of 1.0%-4.0%, the dibutyl phthalate of 0.01%-0.5%, the butyral of 0.5%-3.0%, the anatase titanium dioxide of 3.0%-7.0%, the medical ethanol of 50%-80% (ethanol content 95%), the iron oxide yellow of 1.5%-5.5%, the calcium carbonate of 3.0%-8.0% and the talcum powder of 4.5%-8.5% are formed, and above each component sum is in 100% the printing ink, the silver ion that adds 10PPM-2000PPM, copper ion, ampicillin sodium or bazheng mixture, bazheng heji, or in the above-mentioned four kinds antiseptic two kinds, three kinds or four kinds, under 0～60 ℃ of condition, react then; 0.5～24 hours, product was used for the application to printed tipping base paper after grinding, pulverize, disperseing, make broad-spectrum antiseptic yew paper.
Above-mentioned silver ion antimicrobial agent is AgNO
3The copper ion antiseptic is CuSO
4.5H
2O; Bazheng mixture, bazheng heji be by fringed pink, plantain seed, pivot hold, rheum officinale, talcum, akebi, cape jasmine and Radix Glycyrrhizae refine the pure Chinese medicinal preparation that forms.
The antiseptic China Cypress paper of the present invention's development, has a broad antifungal spectrum, antibiotic lasting, can prevent bacterium particularly alimentary canal, respiratory infectious disease bacterium and food poisoning pathogen contamination yew paper, prevent to propagate pathogen by yew paper (media), reduce the generation of disease.This preparation method's process is simple, easy to use, and the broad-spectrum antiseptic yew paper anti-microbial property of Using such method preparation is good, and applicability is strong, and heat-resisting, and acid and alkali-resistance is nontoxic to human body.
Below the present invention is described in detail.
Antiseptic silver ion of the present invention, copper ion, ampicillin sodium and bazheng mixture, bazheng heji disperse in printing ink easily, low price, and as antibiotic effective ingredient, this makes this antibacterial ink have the prerequisite of premium properties beyond doubt with this.In the preparation process, should control reaction temperature be 0～60 ℃, be to operate under 5～7 the condition in the pH of solution value, under the effect of stirring, reacted 0.5～24 hour.With the product that reaction obtains, grind and disperse, make cigarette broad-spectrum antiseptic printing ink.Re-use the printing roll broad-spectrum antiseptic printing ink is coated on the tipping base paper surface equably, obtain product one cigarette filter external packing of the present invention broad-spectrum antiseptic yew paper.
The specific embodiment
Embodiment 1
With 2.5g AgNO
3Be dissolved in a spot of water, be transferred in the reactor of 10L, add 95% medicinal alcohol 3.5kg then, stirred 0.5 hour, add 5.0% modified rosin, 1.0% polyvinyl alcohol, 0.5% dibutyl phthalate, 0.9% butyral, 4.7% anatase titanium dioxide, 3.5% iron oxide yellow, 4.6% calcium carbonate, 8.5% talcum powder then at 20 ℃, pH is under 7 the condition, continuous stirring 24 hours.After reaction finishes, grind and disperse.Obtain the antibacterial ink 5kg of argentiferous 634PPM.Use roll to be coated on the tipping base paper surface the above-mentioned antibacterial ink of producing, make antiseptic China Cypress paper.Press the method for " disinfection technology standard " regulation of health ministry promulgation, adopt reference culture antiseptic China Cypress paper to be carried out the sterilization check test, Escherichia coli 4.9 * 10
5Strain, sterilizing rate was 100% in 10 minutes; Staphylococcus aureus 3.1 * 10
4Strain, sterilizing rate was 100% in 10 minutes; Pseudomonas aeruginosa 3.2 * 10
6Strain, sterilizing rate was 100% in 10 minutes; Hay bacillus 4.5 * 10
4Strain, sterilizing rate was 100% in 10 minutes.Acute skin irritation test result: non-stimulated; Toxicity test result: nontoxic; Antibiotic persistence: deposit 12 months sample, sterilizing rate was 100% in 10 minutes.
Embodiment 2
CuSO with 10g
45H
2O is dissolved in a spot of water, be transferred in the reactor of 10L, add 95% medicinal alcohol 3.5kg then, stirred 1.5 hours, add 4.5% modified rosin, 1.5% polyvinyl alcohol, 0.2% dibutyl phthalate, 1.2% butyral, 3.5% anatase titanium dioxide, 4.7% iron oxide yellow, 5.1% calcium carbonate, 8.0% talcum powder then at 20 ℃, pH is under 7 the condition, continuous stirring 24 hours.After reaction finishes, grind dispersion.Obtain the antibacterial ink 5kg of cupric 512PPM.Use roll to be coated on the tipping base paper surface the above-mentioned antibacterial ink of producing, make antiseptic China Cypress paper.Press the method for " disinfection technology standard " regulation of health ministry promulgation, adopt reference culture antiseptic China Cypress paper to be carried out the sterilization check test, Escherichia coli 3.2 * 10
5Strain, sterilizing rate was 100% in 15 minutes; Staphylococcus aureus 4.0 * 10
4Strain, sterilizing rate was 100% in 15 minutes; Pseudomonas aeruginosa 3.7 * 10
6Strain, sterilizing rate was 100% in 15 minutes; Hay bacillus 5.0 * 10
4Strain, sterilizing rate was 100% in 15 minutes.Acute skin irritation test result: non-stimulated; Toxicity test result: nontoxic; Antibiotic persistence: deposit 12 months sample, sterilizing rate was 98% in 15 minutes.
Embodiment 3
The 10mL bazheng mixture, bazheng heji is dissolved in a spot of water, be transferred in the reactor of 10L, add 95% medicinal alcohol 3.5kg then, stirred 1.0 hours, add 3.0% modified rosin, 3.0% polyvinyl alcohol, 0.5% dibutyl phthalate, 0.9% butyral, 4.7% anatase titanium dioxide, 3.5% iron oxide yellow, 4.6% calcium carbonate, 8.5% talcum powder then at 20 ℃, pH is under 7 the condition, continuous stirring 24 hours.After reaction finishes, grind dispersion.Obtain containing the antibacterial ink 5kg of the about 2000PPM of bazheng mixture, bazheng heji.Use roll to be coated on the tipping base paper surface the above-mentioned antibacterial ink of producing, make antiseptic China Cypress paper.Press the method for " disinfection technology standard " regulation of health ministry promulgation, adopt reference culture antiseptic China Cypress paper to be carried out the sterilization check test, Escherichia coli 3.1 * 10
5Strain, sterilizing rate was 98% in 30 minutes; Staphylococcus aureus 4.7 * 10
4Strain, sterilizing rate was 100% in 30 minutes; Pseudomonas aeruginosa 3.9 * 10
6Strain, sterilizing rate was 100% in 30 minutes; Hay bacillus 4.1 * 10
4Strain, sterilizing rate was 100% in 30 minutes.Acute skin irritation test result: non-stimulated; Toxicity test result: nontoxic; Antibiotic persistence: deposit 12 months sample, sterilizing rate was 95% in 30 minutes.
Embodiment 4
The 1.0g ampicillin sodium is dissolved in a spot of water, be transferred in the reactor of 10L, add 95% medicinal alcohol 3.5kg then, stirred 0.5 hour, add 4.5% modified rosin, 1.0% polyvinyl alcohol, 0.5% dibutyl phthalate, 0.9% butyral, 4.7% anatase titanium dioxide, 4.0% iron oxide yellow, 5.0% calcium carbonate, 8.0% talcum powder then at 20 ℃, pH is under 7 the condition, continuous stirring 24 hours.After reaction finishes, grind dispersion.Obtain containing the antibacterial ink 4.2kg of ampicillin sodium 238PPM.Use roll to be coated on the tipping base paper surface the above-mentioned antibacterial ink of producing, make antiseptic China Cypress paper.Press the method for " disinfection technology standard " regulation of health ministry promulgation, adopt reference culture antiseptic China Cypress paper to be carried out the sterilization check test, Escherichia coli 3.5 * 10
5Strain, sterilizing rate was 90% in 40 minutes; Staphylococcus aureus 2.8 * 10
4Strain, sterilizing rate was 95% in 40 minutes; Pseudomonas aeruginosa 4.0 * 10
6Strain, sterilizing rate was 100% in 40 minutes; Hay bacillus 3.8 * 10
4Strain, sterilizing rate was 100% in 40 minutes.Acute skin irritation test result: non-stimulated; Toxicity test result: nontoxic; Antibiotic persistence: deposit 12 months sample, sterilizing rate was 90% in 40 minutes.
Embodiment 5
With 1.0g AgNO
3, the 6mL bazheng mixture, bazheng heji is dissolved in a spot of water, be transferred in the reactor of 10L, add 95% medicinal alcohol 3.5kg then, stirred 0.5 hour, add 4.0% modified rosin, 0.8% polyvinyl alcohol, 0.7% dibutyl phthalate, 0.9% butyral, 4.7% anatase titanium dioxide, 5.5% iron oxide yellow, 5.6% calcium carbonate, 6.5% talcum powder again at 20 ℃, pH is under 7 the condition, continuous stirring 24 hours.After reaction finishes, grind dispersion.Obtain the antibacterial ink 5kg of argentiferous and bazheng mixture, bazheng heji.Use roll to be coated on the tipping base paper surface the above-mentioned antibacterial ink of producing, make antiseptic China Cypress paper.Press the method for " disinfection technology standard " regulation of health ministry promulgation, adopt reference culture antiseptic China Cypress paper to be carried out the sterilization check test, Escherichia coli 4.5 * 10
5Strain, sterilizing rate was 100% in 10 minutes; Staphylococcus aureus 4.0 * 10
4Strain, sterilizing rate was 100% in 10 minutes; Pseudomonas aeruginosa 3.8 * 10
6Strain, sterilizing rate was 100% in 10 minutes; Hay bacillus 5.2 * 10
4Strain, sterilizing rate was 100% in 10 minutes.Acute skin irritation test result: non-stimulated; Toxicity test result: nontoxic; Antibiotic persistence: deposit 12 months sample, sterilizing rate was 100% in 10 minutes.
Embodiment 6
With 5.0gCuSO
45H
2O, 6mL bazheng mixture, bazheng heji are dissolved in a spot of water, be transferred in the reactor of 10L, add 95% medicinal alcohol 3.5kg then, stirred 0.5 hour, add 4.0% modified rosin, 0.8% polyvinyl alcohol, 0.7% dibutyl phthalate, 0.9% butyral, 4.7% anatase titanium dioxide, 5.5% iron oxide yellow, 5.6% calcium carbonate, 6.5% talcum powder again at 20 ℃, pH is under 7 the condition, continuous stirring 24 hours.After reaction finishes, grind dispersion.Obtain the antibacterial ink 5kg of cupric and bazheng mixture, bazheng heji.Use roll to be coated on the tipping base paper surface the above-mentioned antibacterial ink of producing, make antiseptic China Cypress paper.Press the method for " disinfection technology standard " regulation of health ministry promulgation, adopt reference culture antiseptic China Cypress paper to be carried out the sterilization check test, Escherichia coli 4.5 * 10
5Strain, sterilizing rate was 100% in 15 minutes; Staphylococcus aureus 4.0 * 10
4Strain, sterilizing rate was 100% in 15 minutes; Pseudomonas aeruginosa 3.8 * 10
6Strain, sterilizing rate was 100% in 15 minutes; Hay bacillus 5.2 * 10
4Strain, sterilizing rate was 100% in 10 minutes.Acute skin irritation test result: non-stimulated; Toxicity test result: nontoxic; Antibiotic persistence: deposit 12 months sample, sterilizing rate was 98% in 10 minutes.
Claims (2)
1. a cigarette is with the preparation method of broad-spectrum antiseptic yew paper, this method is with tipping base paper, through the print roller application to printed, apply equably in its surface and contain inorganic antiseptic, the broad-spectrum antiseptic printing ink of organic antibacterial agent and Chinese medicine preparation, make broad-spectrum antiseptic yew paper, it is characterized in that: by the modified rosin of percentage by weight 0.5%-5.0%, the polyvinyl alcohol of 1.0%-4.0%, the dibutyl phthalate of 0.01%-0.5%, the butyral of 0.5%-3.0%, the anatase titanium dioxide of 3.0%-7.0%, the medicinal alcohol of 50%-80%, the iron oxide yellow of 1.5%-5.5%, the calcium carbonate of 3.0%-8.0% and the talcum powder of 4.5%-8.5% are formed, and above each component sum is in 100% the printing ink, the silver ion that adds 10PPM-2000PPM, copper ion, ampicillin sodium or bazheng mixture, bazheng heji, or in the above-mentioned four kinds antiseptic two kinds, three kinds or four kinds, under 0～60 ℃ of condition, reacted 0.5～24 hour then, product is through grinding, pulverize, after the dispersion, be used for the application to printed tipping base paper, make broad-spectrum antiseptic yew paper.
2. by the preparation method of the described cigarette of claim 1 with broad-spectrum antiseptic yew paper, it is characterized in that: silver ion antimicrobial agent is AgNO
3The copper ion antiseptic is CuSO
4.5H
2O; Bazheng mixture, bazheng heji be by fringed pink, plantain seed, hold, rheum officinale, talcum, akebi, cape jasmine and Radix Glycyrrhizae refine the pure Chinese medicinal preparation that forms.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 02146697 CN1236141C (en) | 2002-11-05 | 2002-11-05 | Making process of Chinese cypress paper with wide-spectrum antiseptic function for cygarette |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 02146697 CN1236141C (en) | 2002-11-05 | 2002-11-05 | Making process of Chinese cypress paper with wide-spectrum antiseptic function for cygarette |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1417413A CN1417413A (en) | 2003-05-14 |
| CN1236141C true CN1236141C (en) | 2006-01-11 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 02146697 Expired - Fee Related CN1236141C (en) | 2002-11-05 | 2002-11-05 | Making process of Chinese cypress paper with wide-spectrum antiseptic function for cygarette |
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Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1287047C (en) * | 2004-01-16 | 2006-11-29 | 玉溪金灿科技有限公司 | Antibacterial Chinese cypress paper and its preparing method |
| CN100463695C (en) * | 2006-07-06 | 2009-02-25 | 欧阳允武 | Antesepsis processing method for printed matter and antibiotic printed matter processed thereby |
| CN101718056B (en) * | 2009-11-17 | 2011-05-18 | 何金星 | Method for preparing water-based ink tipping paper with anti-bacterial and anti-virus function |
| CN103054188B (en) * | 2012-11-14 | 2014-04-16 | 湖北中烟工业有限责任公司 | Nozzle tipping paper for antibiosis cigarette, preparation method thereof, and nozzle for antibiosis cigarette |
| CN103330286B (en) * | 2013-06-28 | 2014-11-05 | 湖北中烟工业有限责任公司 | Cigarette filter tip comprising natural Chinese herbal medicine antibacterial agent and manufacturing method |
| CN103504481A (en) * | 2013-10-11 | 2014-01-15 | 红塔烟草(集团)有限责任公司 | Electronic cigarette with antibacterial layer cigarette holder |
| CN103590285A (en) * | 2013-10-11 | 2014-02-19 | 金东纸业（江苏）股份有限公司 | Antibacterial coating and antibacterial paper |
| CN105002780A (en) * | 2015-06-26 | 2015-10-28 | 安徽省三环纸业(集团)有限公司 | Production technology of antibacterial tipping paper for cigarettes |
| CN106087570A (en) * | 2016-06-12 | 2016-11-09 | 铜陵锋帆彩色印务有限公司 | Mildew proof board coating based on Modification of kaolin and preparation method thereof |
| CN105926353A (en) * | 2016-06-12 | 2016-09-07 | 铜陵锋帆彩色印务有限公司 | Attapulgite modified mould-proof paperboard and preparation method thereof |
| CN112048942A (en) * | 2020-09-07 | 2020-12-08 | 安徽天翔高新特种包装材料集团有限公司 | Antibacterial cigarette tipping paper and printing process thereof |
-
2002
- 2002-11-05 CN CN 02146697 patent/CN1236141C/en not_active Expired - Fee Related
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| Publication number | Publication date |
|---|---|
| CN1417413A (en) | 2003-05-14 |
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| ASS | Succession or assignment of patent right |
Owner name: YUNNAN YUXI GLYPTOSTROBUS MILL Effective date: 20050304 |
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Effective date of registration: 20050304 Address after: 300072 Tianjin city Wei Jin Road No. 92 Applicant after: Tianjin University Co-applicant after: Yunnan Yuxi Tipping Paper Factory Address before: 300072 Tianjin city Wei Jin Road No. 92 Applicant before: Tianjin University |
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