CN1223265A - Process for preparing stachyose and its products and application - Google Patents
Process for preparing stachyose and its products and application Download PDFInfo
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- CN1223265A CN1223265A CN98100020A CN98100020A CN1223265A CN 1223265 A CN1223265 A CN 1223265A CN 98100020 A CN98100020 A CN 98100020A CN 98100020 A CN98100020 A CN 98100020A CN 1223265 A CN1223265 A CN 1223265A
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Abstract
The preparation method of stachyose is characterized by that it uses stachys sieboldii as raw material, and adopts the processes of water extraction, alcohol precipitation or juice-pressing or uses polar organic solvent to extract the stachyose contained in the raw material stachys sieboldii. The described raw material includes fresh product and/or dried product, if the dried product is used, the dried product must be soaked in 3-6 times (by weight) clear water for 120-300 min., and its digestion extraction time or reflux digestion extraction time is 1-2 times that of fresh product. Said invented stachyose product can be used in the production of cold beverage, milk product, icecream, bread, cake, sweets, chocolate and instant food, also can be made into tablet and effervescent agent of health-care tonic preparation.
Description
The present invention relates to the technical field of protective foods, refer in particular to and a kind ofly utilize artichoke betony extracts stachyose for raw material preparation method and products thereof and use.
Stachyose belongs to protective foods, is present in the root and stem of fabaceous seed and labiate, and molecular formula is C
24H
42O
21, molecular weight is 666, structural formula is
The preparation of stachyose has formed certain scale in states such as Japan and America and Europes, but still gets the brush-off little stachyose product in China.The preparation method of stachyose extracts from fabaceous seed at present; because the main component of the oligose in soybean is a stachyose; raffinose and sucrose; in sophisticated soybean; the content of stachyose is about 4%; raffinose is about 1%; sucrose is about 5%; the preparation method of soybean oligosaccharide commonly used is that usefulness has been removed grease and proteic soybean whey is raw material carbohydrate separation and refining method preparation routinely; concrete technology comprises that soybean whey usefulness is saltoutd by elder generation or residual albumen is removed in ultrafiltration; use activated carbon decolorizing again; then with electrodialysis or ion exchange method desalination; make the syrup of soybean oligosaccharide at last with vacuum concentration; can also further make particle or powder mix powder, main component and content in the soybean oligosaccharide of various forms see Table 1.The composition of table 1 soybean oligosaccharide (% weight)
From seeing Table 1 as seen, be that the soybean oligosaccharide that raw material is produced is the mixture of multiple sugar with the soybean, the stachyose content with health-care effect wherein is below 23%.And from the root of labiate and stem, extract the method for stachyose, not seeing at present has any report.
| Category | Moisture | Stachyose | Raffinose | Sucrose | Other sugar |
| Syrup | ????24 | ????18 | ????6 | ????34 | ????18 |
| Particle | ????3 | ????23 | ????7 | ????44 | ????23 |
| Mixed powder | ????3 | ????11 | ????4 | ????22 | ????60 |
The inventor is engaged in the research-and-development activity of protective foods for a long time, numerous Labiatae betonies has been carried out research and exploration repeatedly, consider from output, price, stachyose content etc. are many-sided determine with the artichoke betony to be that the technical scheme that raw material extracts stachyose is best.
Main purpose of the present invention is to provide a kind of artichoke betony extracts stachyose for raw material preparation method and products thereof that utilizes, and reaches the purpose in exploitation protective foods source.
Another object of the present invention is to provide a kind of technical scheme for preparing multiple stachyose protective foods with the stachyose place of sucrose.
The object of the present invention is achieved like this: a kind of preparation method of stachyose, it is characterized in that this preparation method is is raw material with artichoke betony, by water extract-alcohol precipitation or squeeze the juice or extract wherein contained stachyose with polar organic solvent, described artichoke betony comprise bright product with or dry product, if when using dry product, must be earlier with 3-6 doubly the clear water of (weight) the dry product artichoke betony was soaked 120～300 minutes, it boils carries or refluxes and boil during for bright product 1-2 times of time of carrying.
The extracting method of described water extract-alcohol precipitation comprises that (parts by weight) get 100 parts artichoke betony and smash to pieces, adds 200～1000 parts water, boils 30～600 minutes time of carrying, filter, remove residual quarrel, add the ethanol of 50-90 part in the filtrate, the after-filtration that stirs is removed insolubles; Described extracting method of squeezing the juice comprises that the bright artichoke betony of cleaning is put into juice extractor squeezes the juice and filter, and removes residual quarrel; The described method of extracting with polar organic solvent comprises that the artichoke betony of getting 100 parts smashs to pieces, and the polar organic solvent backflow that adds 50～100 parts is boiled 30～600 minutes time of carrying, and removes by filter residual quarrel; The stachyose of this method preparation can be by decolouring and/or pure ratio method, and the content that improves stachyose reaches 90%; Described polar organic solvent comprises ethanol; Described water extract-alcohol precipitation comprises smashs the artichoke betony of 100 grams to pieces, and the poach that adds 500 grams is carried 120 minutes time, removes by filter residual quarrel, adds 60% aqueous ethanolic solution 100 grams in the filtrate, and the after-filtration that stirs is removed insolubles; Get 100 parts artichoke betony described comprising with organic solvent extraction, smashs to pieces, adds 60% aqueous ethanolic solution 100 grams, refluxes and boil the 150 minutes time of carrying, and removes by filter residual quarrel; This product extracts from artichoke betony with the described preparation method of claim 1; This product can place of sucrose be applied to refreshment drink, milk-product, ice-creams, bread, cake, candy, chocolate, ready-to-eat, or makes tablet, effervescent class health care tonic.
Main positively effect of the present invention is:
1, the present invention has started the raw material resources of extracting the stachyose protective foods, select for use for a long time and do not paid attention to by people, and extensive growth is a raw material in the artichoke betony of limes marginis, roadside, field stalk, prepare stachyose with health-care effect, its concrete technical scheme comprises water extract-alcohol precipitation or squeezes the juice or extract with polar organic solvent that its preparation method is very simple, does not need specific installation, operation is with low cost easily.
2, decolour and drying with the stachyose process of method preparation of the present invention, the content of its stachyose can reach 90% high purity, green health care food for pure natural, because stachyose is not dissolved and absorbs by the human intestines and stomach, directly enter large intestine, be the multiplicaiton factor of beneficial bacteria bifidus bacillus in the large intestine, thereby can suppress the growth and breeding of inherent putrefactive bacterium in external source pathogenic bacterium and the intestines, the effect that reaches health care and prevent and cure diseases.
3, the stachyose of method preparation of the present invention belongs to low-molecular-weight water-soluble dietary fibre, have be easy to add in the food and drink, stable performance, not chelating mineral element, advantage such as low-yield, but place of sucrose is applied in the food such as refreshment drink, milk-product, ice-creams, bread, cake, candy, chocolate, ready-to-eat, also can make health care tonics such as tablet or effervescent.
The present invention is further described below in conjunction with preferred embodiment.
Embodiment 1
Preparation method of the present invention can adopt bright product of artichoke betony or dry product with the concrete technical scheme of water extract-alcohol precipitation, comprises the steps:
1, select materials:
The raw material artichoke betony that the present invention uses belongs to perennial herbaceous plant as the Labiatae wood, wild limes marginis, roadside, field stalk in humidity, spread all over all parts of the country, also can cultivate easily, gather autumn, people get its stem tuber and do salted vegetables usefulness for a long time, ignore its health-care effect, the present invention gets its stem tuber and cleans, it is standby to get its bright product (or drying), the content of stachyose is about 10% in the bright product of artichoke betony stem tuber by analysis, for the 2-3 of content in the soybean doubly, so artichoke betony is the optimum feed stock of extraction stachyose.
2, extract stachyose with the technical scheme of water extract-alcohol precipitation:
Getting bright product 100 grams of artichoke betony smashs to pieces, add water 500 grams, boil the 120 minutes time of carrying, remove by filter residue, add 60% aqueous ethanolic solution 100 grams in the filtrate, after-filtration stirs, remove insolubles, make the stachyose dry product with vacuum-drying, desire prepares highly purified product, available activated carbon decolorizing, the content of its stachyose can reach 90%.
In the present embodiment, if during with the artichoke betony dry product, it must soak 120-300 minute with 500 gram clear water earlier, and it boils the time of carrying is 240 minutes, is fully extracted with assurance stachyose wherein.
Embodiment 2:
The concrete technical scheme extraction stachyose that preparation method of the present invention can adopt the bright product of artichoke betony and squeeze the juice, its method of selecting materials is cleaned for getting the bright product of artichoke betony stem tuber, puts into juice extractor subsequently and squeezes the juice, and filter, and following steps are with embodiment 1, so do not repeat.
Embodiment 3:
Preparation method of the present invention, can also adopt bright product of artichoke betony or dry product to extract stachyose with the concrete technical scheme of polar organic solvent extraction using alcohol, its method of selecting materials does not repeat with embodiment 1 event, the artichoke betonys of getting 100 grams are subsequently smashed to pieces and are added 60% aqueous ethanolic solution 100 grams and reflux and boil the 150 minutes time of carrying and filter, remove residual quarrel, following steps do not repeat with embodiment 1 event.
If when use dry product, must soak with clear water earlier with embodiment 1 in the present embodiment, its backflow is boiled the time of carrying and is prolonged 1～2 times too, is fully extracted with assurance stachyose wherein.
Embodiment 4
The health-care effect of product of the present invention and effect embodiment.
1, stachyose has the effect that promotes bifidus bacillus propagation, and stachyose can promote the propagation of inherent beneficial bacteria bifidus bacillus in the enteron aisle, thereby suppresses the growth of spoilage organism in the intestines and reduce the formation of poisonous fermented product.Test method eats the food that contains stachyose 5～8g for each person every day for selecting grownup 10 people, and the quantity of bifidus bacillus increases by 10～100 times in the two weeks back chemical examination ight soil.Therefore the food that contains stachyose has the nourishing function that suppresses diarrhoea, and specific embodiment suffers from the edible for each person every day food that contains stachyose 3g of cacatory 15 children for giving, and after 7 days, times of defecation obviously reduces, and no longer rushes down rare semiliquid stool.
2, stachyose has the function that protects the liver.
Because stachyose has the formation that makes bifidus bacillus propagation and reduce the toxic metabolite product, thereby has alleviated the burden that liver divides toxolysin greatly.Specific embodiment is to select 12 patients that suffer from chronic hepatitis, the edible for each person every day food that contains stachyose 4g, and after 40 days, the state of an illness generally takes a turn for the better, and appetite increases, weight increase, the protein tolerance increases, and the harmful metabolite concentration in serum and the urine is reduced to normal value.
3, stachyose has the function of reduction serum courage with alcohol.
Because a large amount of propagation of bifidus bacillus in the intestines have changed the equilibrium relationship of microbial cells in the intestines and have suppressed harmful bacteria growing, play the effect that reduces serum cholesterol content.Specific embodiment is to select cholesterol to be higher than the elderly 10 people of normal value, eats the food that contains stachyose 6g for each person every day, and after 3 months, the total serum cholesterol reduces by 20～50dL.
Stachyose is not because of being absorbed by the body in addition, be low-yield and food noenergy, can offer and like sweet food to be reluctant that again the person of getting fat is edible, can place of sucrose be applied in the food such as refreshment drink, milk-product, ice-creams, bread, cake, candy, chocolate, ready-to-eat, can also make health care tonics such as tablet or effervescent.
Claims (10)
1, a kind of preparation method of stachyose, it is characterized in that this preparation method is is raw material with artichoke betony, by water extract-alcohol precipitation or squeeze the juice or extract wherein contained stachyose with polar organic solvent, described artichoke betony comprises bright product and/or dry product, if when using dry product, must be earlier with 3-6 doubly the clear water of (weight) the dry product artichoke betony was soaked 120～300 minutes, it boils carries or refluxes and boil during for bright product 1-2 times of time of carrying.
2, a kind of preparation method who utilizes artichoke betony to extract stachyose according to claim 1, it is characterized in that: the extracting method of described water extract-alcohol precipitation comprises that (parts by weight) get 100 parts artichoke betony and smash to pieces, the water that adds 200～1000 parts, boil 30～600 minutes time of carrying, filter, remove residual quarrel, add the ethanol of 50-90 part in the filtrate, the after-filtration that stirs is removed insolubles.
3, a kind of preparation method who utilizes artichoke betony to extract stachyose according to claim 1 is characterized in that: described extracting method of squeezing the juice comprises that the bright artichoke betony of cleaning is put into juice extractor squeezes the juice and filter, and removes residual quarrel.
4, a kind of preparation method who utilizes artichoke betony to extract stachyose according to claim 1, its feature is stored in: the described method of extracting with polar organic solvent comprises that the artichoke betony of getting 100 parts smashs to pieces, the polar organic solvent backflow that adds 50～100 parts is boiled 30～600 minutes time of carrying, and removes by filter residual quarrel.
5, a kind of preparation method who utilizes artichoke betony to extract stachyose according to claim 1 is characterized in that: the stachyose of this method preparation, can be by decolouring and/or pure ratio method, and the content that improves stachyose reaches 90%.
6, the preparation method of stachyose according to claim 1 is characterized in that: described polar organic solvent comprises ethanol.
7, the preparation method of stachyose according to claim 1, it is characterized in that: described water extract-alcohol precipitation comprises smashs the artichoke betony of 100 grams to pieces, the poach that adds 500 grams is carried 120 minutes time, remove by filter residual quarrel, aqueous ethanolic solution 100 grams of adding 60% in the filtrate, the after-filtration that stirs is removed insolubles.
8, the preparation method of stachyose according to claim 1 is characterized in that: get 100 parts artichoke betony described comprising with organic solvent extraction, smashs to pieces, adds 60% aqueous ethanolic solution 100 grams, refluxes and boil the 150 minutes time of carrying, and removes by filter residual quarrel.
9, a kind of stachyose product is characterized in that: this product extracts from artichoke betony with the described preparation method of claim 1.
10, a kind of application of stachyose product as claimed in claim 9, it is characterized in that this product can place of sucrose be applied to refreshment drink, milk-product, ice-creams, bread, cake, candy, chocolate, ready-to-eat, or make tablet, effervescent class health care tonic.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN98100020A CN1130368C (en) | 1998-01-12 | 1998-01-12 | Process for preparing stachyose and its products and application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN98100020A CN1130368C (en) | 1998-01-12 | 1998-01-12 | Process for preparing stachyose and its products and application |
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| Publication Number | Publication Date |
|---|---|
| CN1223265A true CN1223265A (en) | 1999-07-21 |
| CN1130368C CN1130368C (en) | 2003-12-10 |
Family
ID=5215745
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN98100020A Expired - Fee Related CN1130368C (en) | 1998-01-12 | 1998-01-12 | Process for preparing stachyose and its products and application |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1093544C (en) * | 1999-12-23 | 2002-10-30 | 中国食品发酵工业研究所 | Stachyose and its preparing process |
| US7166582B2 (en) | 2002-05-02 | 2007-01-23 | J-Oil Mills, Inc. | Antiallergic composition |
| CN100335061C (en) * | 2003-06-19 | 2007-09-05 | 张汝学 | Use of stachyose in preparing drug for diabetes and its preparation method |
| CN100354290C (en) * | 2005-05-23 | 2007-12-12 | 青岛国风药业股份有限公司 | Raffinoses oligosaccharide with stachyose as main materials and method for preparing same |
| CN100457765C (en) * | 2007-01-16 | 2009-02-04 | 广东太阳神集团有限公司 | Method for producing stabhyose, and method for producing stabhyose and catalpol by using rehmannia root |
| CN102229627A (en) * | 2011-05-13 | 2011-11-02 | 南京中医药大学 | Method for preparing stachyose by using water-extraction alcohol-precipitation of salvia miltiorrhiza |
| CN102389073A (en) * | 2011-11-17 | 2012-03-28 | 中国食品发酵工业研究院 | Natural plant extract formula for liver protection |
| CN103265583A (en) * | 2013-03-05 | 2013-08-28 | 中国食品发酵工业研究院 | Method for preparing stachyose crystal |
| CN103815224A (en) * | 2014-01-28 | 2014-05-28 | 宁波大学 | Stachyose effervescent tablet and preparation method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1070195A (en) * | 1992-09-04 | 1993-03-24 | 中国人民武装警察部队河北省总队医院 | A kind of method of from soyflour, extracting oligose |
-
1998
- 1998-01-12 CN CN98100020A patent/CN1130368C/en not_active Expired - Fee Related
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1093544C (en) * | 1999-12-23 | 2002-10-30 | 中国食品发酵工业研究所 | Stachyose and its preparing process |
| US7166582B2 (en) | 2002-05-02 | 2007-01-23 | J-Oil Mills, Inc. | Antiallergic composition |
| CN100335061C (en) * | 2003-06-19 | 2007-09-05 | 张汝学 | Use of stachyose in preparing drug for diabetes and its preparation method |
| CN100354290C (en) * | 2005-05-23 | 2007-12-12 | 青岛国风药业股份有限公司 | Raffinoses oligosaccharide with stachyose as main materials and method for preparing same |
| CN100457765C (en) * | 2007-01-16 | 2009-02-04 | 广东太阳神集团有限公司 | Method for producing stabhyose, and method for producing stabhyose and catalpol by using rehmannia root |
| CN102229627B (en) * | 2011-05-13 | 2013-10-16 | 南京中医药大学 | Method for preparing stachyose by using water-extraction alcohol-precipitation of salvia miltiorrhiza |
| CN102229627A (en) * | 2011-05-13 | 2011-11-02 | 南京中医药大学 | Method for preparing stachyose by using water-extraction alcohol-precipitation of salvia miltiorrhiza |
| CN102389073A (en) * | 2011-11-17 | 2012-03-28 | 中国食品发酵工业研究院 | Natural plant extract formula for liver protection |
| CN102389073B (en) * | 2011-11-17 | 2013-01-23 | 中国食品发酵工业研究院 | Natural plant extract formula for liver protection |
| CN103265583A (en) * | 2013-03-05 | 2013-08-28 | 中国食品发酵工业研究院 | Method for preparing stachyose crystal |
| CN103265583B (en) * | 2013-03-05 | 2016-01-13 | 中国食品发酵工业研究院 | A kind of preparation method of stachyose crystal |
| CN103815224A (en) * | 2014-01-28 | 2014-05-28 | 宁波大学 | Stachyose effervescent tablet and preparation method thereof |
| CN103815224B (en) * | 2014-01-28 | 2016-01-20 | 宁波大学 | A kind of stachyose effervescent tablet and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN1130368C (en) | 2003-12-10 |
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