CN1185330C - Process for preparing efficient soap without pollution - Google Patents
Process for preparing efficient soap without pollution Download PDFInfo
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- CN1185330C CN1185330C CNB991122968A CN99112296A CN1185330C CN 1185330 C CN1185330 C CN 1185330C CN B991122968 A CNB991122968 A CN B991122968A CN 99112296 A CN99112296 A CN 99112296A CN 1185330 C CN1185330 C CN 1185330C
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Abstract
The present invention relates to a method for efficiently preparing soap without pollution, particularly to a method for soap preparation without waste water discharge in the process of production. The method comprises the processes of material preparation and saponification, and the major constituents include the following raw materials that are prepared according to part by weight: 20 to 25 parts of liquid sodium silicate whose content is 40%, 20 to 25 parts of liquid sodium hydroxide whose content si 30%, 10 to 15 parts of liquid rosin whose content is 30%, 0.5 to 1 part of pasted 102 active agents whose content is 70%, 1 to 2 parts of powdery K12 active agents whose content is 90%, and 45 to 50 parts of solid fatty acid that is mixed. Raw materials in the present invention are reasonably prepared respectively, only the processes of material preparation, sponification and static placement are carried out during processing, and different raw materials are sufficiently reacted during processing, so that no waste water is generated. In addition, redundant processes during processing are omitted, and objects which are required in the processes are removed; therefore, the cost is greatly reduced.
Description
The present invention is a kind of pollution-free working method of efficient soap, need not the working method of the soap of sewage effluent in particularly a kind of production process.
The processing of soap at present generally will through getting the raw materials ready, saponification is left standstill, alkaline hydrolysis leaves standstill, put in order leave standstill, allotment agent, cold drawing are cold puts, cuts, dries by the fire several procedures such as cold, printing packing.Said process is not only comparatively complicated, and need leave standstill at alkaline hydrolysis, re-uses other raw material in the process such as allotment agent, thereby makes the production cost of soap higher.In addition, also need to discharge the waste water that is harmful to environment in process of production, the environment around giving causes great harm.
The objective of the invention is to: the free of contamination working method that discloses a kind of low cost of manufacture, efficient soap.
The present invention also will be through getting the raw materials ready and the saponification process, and its major ingredient comprises following raw material (weight part) by part preparation:
(1) liquid state and content are 40% water glass 20-25,
(2) be in a liquid state and content is 30% sodium hydroxide 20-25,
(3) be in a liquid state and content is 30% rosin liquid 10-15,
(4) being paste and content is 70% 102 promoting agent 0.5-1,
(5) being powdery and content is 90% K12 promoting agent 1-2,
(6) be solid-state mixed fatty acid 45-50.
On the basis of above-mentioned raw materials, generally to add auxiliary materials such as essence, pigment.
The course of processing of the present invention can adopt existing processes, but preferably uses following technological process: above-mentioned raw materials is added in the reactor, maintain the temperature at 100-120 ℃, carrying out the saponification processing and finally reaching saponification degree is 100%.The material that saponification is finished is poured in the predetermined mould, its cooling back is formed solid state.
Each raw material is in the present invention rationally prepared, make in its course of processing only get the raw materials ready, saponification and leave standstill process, and various in this course raw material fully reacts, thereby do not produce waste water.In addition, owing to saved the article of the unnecessary course of processing and the adding of these process needs, thereby its cost reduces greatly.The product alcohol-insoluble substance that adopts present method to process is no more than 8%, and muriate is lower than 0.5%, and is harmful and the mordant free caustic alkali of fabric is lower than 0.3%.
Below in conjunction with embodiment the present invention is elaborated.
Embodiment one:
Get liquid state and content by weight and be 40% water glass 20, be in a liquid state and content is 30% sodium hydroxide 25, be in a liquid state and content is 30% rosin liquid 15, be paste and content and be 70% 102 promoting agents 0.8, be powdery and content and be 90% K12 promoting agent 1, be solid-state mixed fatty acid 45.Above-mentioned each raw material is added in the reactor, maintain the temperature at 115 ℃, carrying out the saponification processing and finally reaching saponification degree is 100%.The material that saponification is finished is poured in the predetermined mould, its cooling back is formed solid state.
Embodiment two:
Get liquid state and content by weight and be 40% water glass 25, be in a liquid state and content is 30% sodium hydroxide 23, be in a liquid state and content is 30% rosin liquid 10, be paste and content and be 70% 102 promoting agents 1, be powdery and content and be 90% K12 promoting agent 1.5, be solid-state mixed fatty acid 48.Above-mentioned each raw material is added in the reactor, maintain the temperature at 110 ℃, carrying out the saponification processing and finally reaching saponification degree is 100%.The material that saponification is finished is poured in the predetermined mould, its cooling back is formed solid state.
Embodiment three:
Get liquid state and content by weight and be 40% water glass 24, be in a liquid state and content is 30% sodium hydroxide 23, be in a liquid state and content is 30% rosin liquid 12, be paste and content and be 70% 102 0.5, be powdery and content and be 90% K12 promoting agent 1.8, be solid-state mixed fatty acid 50, spices, pigment are an amount of.Above-mentioned each raw material is added in the reactor, maintain the temperature at 105 ℃, carrying out the saponification processing and finally reaching saponification degree is 100%.The material that saponification is finished is poured in the predetermined mould, its cooling back is formed solid state.
Embodiment four:
Get liquid state and content by weight and be 40% water glass 22, be in a liquid state and content is 30% sodium hydroxide 22, be in a liquid state and content is 30% rosin liquid 14, be paste and content and be 70% 102 promoting agents 0.6, be powdery and content and be 90% K12 promoting agent 2, be solid-state mixed fatty acid 46, spices, pigment and white dyes are an amount of.Above-mentioned each raw material is added in the reactor, maintain the temperature at 120 ℃, carrying out the saponification processing and finally reaching saponification degree is 100%.The material that saponification is finished is poured in the predetermined mould, its cooling back is formed solid state.
Claims (1)
1, a kind of pollution-free working method of efficient soap comprises and getting the raw materials ready and the saponification process, it is characterized in that: its main component comprises following raw material (weight part) by part preparation:
(1) liquid state and content are 40% water glass 20-25,
(2) be in a liquid state and content is 30% sodium hydroxide 20-25,
(3) be in a liquid state and content is 30% rosin liquid 10-15,
(4) being paste and content is 70% 102 promoting agents (fatty alcohol-polyoxyethylene ether) 0.5-1,
(5) being powdery and content is 90% K12 promoting agent (sodium alkyl sulfate) 1-2,
(6) be solid-state mixed fatty acid 45-50;
Above-mentioned raw materials is added in the reactor, maintain the temperature at 100-120 ℃, carrying out the saponification processing and finally reaching saponification degree is 100%, and the material that saponification is finished is poured in the predetermined mould, and its cooling back is formed solid state.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB991122968A CN1185330C (en) | 1999-07-01 | 1999-07-01 | Process for preparing efficient soap without pollution |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB991122968A CN1185330C (en) | 1999-07-01 | 1999-07-01 | Process for preparing efficient soap without pollution |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1279277A CN1279277A (en) | 2001-01-10 |
| CN1185330C true CN1185330C (en) | 2005-01-19 |
Family
ID=5275618
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB991122968A Expired - Fee Related CN1185330C (en) | 1999-07-01 | 1999-07-01 | Process for preparing efficient soap without pollution |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1185330C (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102242030B (en) * | 2011-06-15 | 2012-08-29 | 陈礼刚 | Method for producing paste toilet soap |
| CN108029465A (en) * | 2017-12-07 | 2018-05-15 | 颍上县上安阳绿色农业发展有限公司 | Cultivation technique and management method without frame Snakegourd Fruit |
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1999
- 1999-07-01 CN CNB991122968A patent/CN1185330C/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN1279277A (en) | 2001-01-10 |
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| CF01 | Termination of patent right due to non-payment of annual fee |