CN117694447A - Sesame deep-processing protein powder and preparation method thereof - Google Patents
Sesame deep-processing protein powder and preparation method thereof Download PDFInfo
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- CN117694447A CN117694447A CN202311758410.8A CN202311758410A CN117694447A CN 117694447 A CN117694447 A CN 117694447A CN 202311758410 A CN202311758410 A CN 202311758410A CN 117694447 A CN117694447 A CN 117694447A
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- 235000003434 Sesamum indicum Nutrition 0.000 title claims abstract description 194
- 108090000623 proteins and genes Proteins 0.000 title claims abstract description 105
- 102000004169 proteins and genes Human genes 0.000 title claims abstract description 105
- 239000000843 powder Substances 0.000 title claims abstract description 61
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 244000000231 Sesamum indicum Species 0.000 title 1
- 241000207961 Sesamum Species 0.000 claims abstract description 193
- 235000018102 proteins Nutrition 0.000 claims abstract description 103
- 239000002994 raw material Substances 0.000 claims abstract description 38
- 238000000605 extraction Methods 0.000 claims abstract description 25
- 235000012054 meals Nutrition 0.000 claims abstract description 23
- 235000007164 Oryza sativa Nutrition 0.000 claims abstract description 17
- 108010084695 Pea Proteins Proteins 0.000 claims abstract description 17
- 108010073771 Soybean Proteins Proteins 0.000 claims abstract description 17
- 108010046377 Whey Proteins Proteins 0.000 claims abstract description 17
- 102000007544 Whey Proteins Human genes 0.000 claims abstract description 17
- 235000019702 pea protein Nutrition 0.000 claims abstract description 17
- 235000009566 rice Nutrition 0.000 claims abstract description 17
- 235000019710 soybean protein Nutrition 0.000 claims abstract description 17
- 235000021119 whey protein Nutrition 0.000 claims abstract description 17
- 238000000034 method Methods 0.000 claims abstract description 12
- 238000002156 mixing Methods 0.000 claims abstract description 6
- 240000007594 Oryza sativa Species 0.000 claims abstract 5
- 238000012216 screening Methods 0.000 claims description 14
- 239000007788 liquid Substances 0.000 claims description 12
- 238000005238 degreasing Methods 0.000 claims description 6
- 238000004140 cleaning Methods 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 5
- 239000002689 soil Substances 0.000 claims description 5
- 239000010902 straw Substances 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 4
- 238000000926 separation method Methods 0.000 claims description 3
- 239000008159 sesame oil Substances 0.000 claims description 3
- 235000011803 sesame oil Nutrition 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims 1
- 238000010521 absorption reaction Methods 0.000 abstract description 4
- 230000001804 emulsifying effect Effects 0.000 abstract description 4
- 230000009102 absorption Effects 0.000 abstract description 2
- 239000006260 foam Substances 0.000 abstract description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 2
- 241000209094 Oryza Species 0.000 description 12
- 238000007710 freezing Methods 0.000 description 4
- 230000008014 freezing Effects 0.000 description 4
- 238000009777 vacuum freeze-drying Methods 0.000 description 4
- MTCFGRXMJLQNBG-REOHCLBHSA-N (2S)-2-Amino-3-hydroxypropansäure Chemical compound OC[C@H](N)C(O)=O MTCFGRXMJLQNBG-REOHCLBHSA-N 0.000 description 1
- 239000004475 Arginine Substances 0.000 description 1
- LEVWYRKDKASIDU-QWWZWVQMSA-N D-cystine Chemical compound OC(=O)[C@H](N)CSSC[C@@H](N)C(O)=O LEVWYRKDKASIDU-QWWZWVQMSA-N 0.000 description 1
- ODKSFYDXXFIFQN-BYPYZUCNSA-P L-argininium(2+) Chemical compound NC(=[NH2+])NCCC[C@H]([NH3+])C(O)=O ODKSFYDXXFIFQN-BYPYZUCNSA-P 0.000 description 1
- HNDVDQJCIGZPNO-YFKPBYRVSA-N L-histidine Chemical compound OC(=O)[C@@H](N)CC1=CN=CN1 HNDVDQJCIGZPNO-YFKPBYRVSA-N 0.000 description 1
- KDXKERNSBIXSRK-YFKPBYRVSA-N L-lysine Chemical compound NCCCC[C@H](N)C(O)=O KDXKERNSBIXSRK-YFKPBYRVSA-N 0.000 description 1
- AYFVYJQAPQTCCC-GBXIJSLDSA-N L-threonine Chemical compound C[C@@H](O)[C@H](N)C(O)=O AYFVYJQAPQTCCC-GBXIJSLDSA-N 0.000 description 1
- 239000004472 Lysine Substances 0.000 description 1
- KDXKERNSBIXSRK-UHFFFAOYSA-N Lysine Natural products NCCCCC(N)C(O)=O KDXKERNSBIXSRK-UHFFFAOYSA-N 0.000 description 1
- MTCFGRXMJLQNBG-UHFFFAOYSA-N Serine Natural products OCC(N)C(O)=O MTCFGRXMJLQNBG-UHFFFAOYSA-N 0.000 description 1
- AYFVYJQAPQTCCC-UHFFFAOYSA-N Threonine Natural products CC(O)C(N)C(O)=O AYFVYJQAPQTCCC-UHFFFAOYSA-N 0.000 description 1
- 239000004473 Threonine Substances 0.000 description 1
- 238000003916 acid precipitation Methods 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- ODKSFYDXXFIFQN-UHFFFAOYSA-N arginine Natural products OC(=O)C(N)CCCNC(N)=N ODKSFYDXXFIFQN-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229960003067 cystine Drugs 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- HNDVDQJCIGZPNO-UHFFFAOYSA-N histidine Natural products OC(=O)C(N)CC1=CN=CN1 HNDVDQJCIGZPNO-UHFFFAOYSA-N 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 238000009700 powder processing Methods 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 238000000751 protein extraction Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
- A23J1/14—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from leguminous or other vegetable seeds; from press-cake or oil-bearing seeds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J3/00—Working-up of proteins for foodstuffs
- A23J3/04—Animal proteins
- A23J3/08—Dairy proteins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J3/00—Working-up of proteins for foodstuffs
- A23J3/14—Vegetable proteins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J3/00—Working-up of proteins for foodstuffs
- A23J3/14—Vegetable proteins
- A23J3/16—Vegetable proteins from soybean
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Polymers & Plastics (AREA)
- Food Science & Technology (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Zoology (AREA)
- Organic Chemistry (AREA)
- Wood Science & Technology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Seeds, Soups, And Other Foods (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses sesame deep-processing protein powder, which comprises sesame protein powder, wherein the sesame protein powder comprises 60% of sesame protein, 11% of soybean protein, 9.5% of pea protein, 9.5% of rice protein and 10% of whey protein; the preparation method of the sesame protein powder comprises the following steps: s1, preparing sesame protein, soybean protein, pea protein, rice protein and whey protein; s2, uniformly mixing the prepared raw material proteins to obtain sesame protein powder; s3, selecting sesame raw materials; s4, crushing the fried sesame raw material: s5, extracting the crushed sesame raw materials; s6, processing the sesame seed meal obtained after extraction; s7, extracting sesame protein from the processed sesame seed meal; s8, processing the extracted sesame protein. The protein powder prepared by the method has better solubility, water absorption, oil absorption, emulsifying property, emulsifying stability and foam stability.
Description
Technical Field
The invention relates to the technical field of sesame protein powder processing, in particular to sesame deep-processing protein powder and a preparation method thereof.
Background
The sesame protein powder is prepared by taking sesame protein as a main component and matching other components, and most of the current sesame protein powder is prepared by extracting protein from sesame residue during processing, wherein the sesame residue is processed into powder, and then extracted by an alkali extraction and acid precipitation method, wherein the sesame residue powder is accurately weighed according to a solid-to-liquid ratio of 1:12, leaching the protein from the sesame residue at the pH value of l1 and the temperature of 70 ℃, wherein the sesame residue is processed in the extraction mode, the protein content in the sesame residue is low, and the extraction mode is easy to damage the structure of the protein, so that the quality of a finished product processed later is affected.
Therefore, we propose a sesame deep-processing protein powder and a preparation method thereof to solve the above problems.
Disclosure of Invention
The invention aims to solve the defects in the prior art and provides sesame deep-processing protein powder and a preparation method thereof.
In order to achieve the above purpose, the present invention adopts the following technical scheme:
a sesame deep-processing protein powder, which comprises sesame protein powder, wherein the sesame protein powder comprises 60% of sesame protein, 11% of soybean protein, 9.5% of pea protein, 9.5% of rice protein and 10% of whey protein;
the preparation method of the sesame protein powder comprises the following steps:
s1, preparing sesame protein, soybean protein, pea protein, rice protein and whey protein;
s2, uniformly mixing the prepared sesame protein, soybean protein, pea protein, rice protein and whey protein to obtain sesame protein powder;
s3, selecting sesame raw materials;
s4, crushing the fried sesame raw material:
s5, extracting the crushed sesame raw materials;
s6, processing the sesame seed meal obtained after extraction;
s7, extracting sesame protein from the processed sesame seed meal;
s8, processing the extracted sesame protein.
S3-1, screening sesame raw materials;
s-3-1, screening out sundries such as stones, crushed soil, crushed sesame straw, crushed leaves and the like in the sesame raw materials, and screening out empty and shrunken sesame in the sesame raw materials screened with the sundries.
S3-2, performing primary processing on the screened sesame raw materials;
s3-2-1, cleaning and drying the screened sesame meeting the processing quality requirement, parching, and then crushing into sesame powder.
S5-1, heating crushed sesame to a critical temperature and extracting sesame oil;
s5-1-1, extraction times of at least three times, extraction pressure of 0.8-1.5MPa, extraction temperature of 45-55deg.C, and ratio of sesame powder heated to critical temperature to extract liquid of 2:6, and extraction time of 1.5-2.5 h.
As a further step in the method of the present invention, S5-2 is extracted to obtain sesame seed meal by solid-liquid separation.
As a further step in the method of the invention, S6-1, the sesame seed meal obtained after extraction is crushed and degreased.
As a further step in the method, S7-1, sesame seed meal after crushing and degreasing treatment is subjected to pH value of 9.5-12, temperature of 40-50 ℃, solid-liquid ratio of 1:36 and time of 20-90 min to prepare sesame protein.
As a further step in the method, S8-1, pre-freezing the prepared sesame protein for two hours at the temperature of twenty ℃ below zero, and then carrying out vacuum freeze drying to obtain a finished product of the sesame deep processed protein.
Compared with the prior art, the invention has the beneficial effects that:
according to the invention, the sesame is subjected to deep processing to extract protein and prepared into protein powder, so that the protein in the sesame can be better extracted, the influence of the protein structure in sesame meal is smaller, and the amino acid components such as threonine, serine, cystine, lysine, histidine and arginine in the sesame protein are high in preservation, so that the sesame deep protein powder has better solubility, water absorption, oil absorption, emulsifying property, emulsifying stability and foam stability.
Detailed Description
The following description of the technical solutions in the embodiments of the present invention will be clear and complete, and it is obvious that the described embodiments are only some embodiments of the present invention, but not all embodiments.
Example 1
A sesame deep-processing protein powder comprises sesame protein powder, wherein the sesame protein powder comprises 60% of sesame protein, 11% of soybean protein, 9.5% of pea protein, 9.5% of rice protein and 10% of whey protein;
the preparation method of the sesame protein powder comprises the following steps:
s1, preparing sesame protein, soybean protein, pea protein, rice protein and whey protein;
s2, uniformly mixing the prepared sesame protein, soybean protein, pea protein, rice protein and whey protein to obtain sesame protein powder;
s3, selecting sesame raw materials;
s3-1, screening sesame raw materials;
s-3-1, screening out sundries such as stones, crushed soil, crushed sesame straw, crushed leaves and the like in the sesame raw materials, and screening out empty and shrunken sesame in the sesame raw materials screened with the sundries.
S3-2, performing primary processing on the screened sesame raw materials;
s3-2-1, cleaning and drying the screened sesame meeting the processing quality requirement, parching, and then crushing into sesame powder;
s4, crushing the fried sesame raw material:
s5, extracting the crushed sesame raw materials;
s5-1, heating crushed sesame to a critical temperature and then extracting sesame oil;
s5-1-1, extraction times of at least three times, extraction pressure of 0.8-1.5MPa, extraction temperature of 45-55deg.C, and ratio of sesame powder heated to critical temperature to extract liquid of 2:6, and extraction time of 1.5-2.5 h.
S5-2, obtaining sesame seed meal after extraction in a solid-liquid separation mode;
s6, processing the sesame seed meal obtained after extraction;
s6-1, crushing and degreasing the sesame seed meal obtained after extraction;
s7, extracting sesame protein from the processed sesame seed meal;
s7-1, preparing sesame protein under the conditions that the pH value of the crushed and defatted sesame meal is 9.5-12, the temperature is 40-50 ℃, the solid-liquid ratio is 1:36 and the time is 20-90 min;
s8, processing the extracted sesame protein;
s8-1, pre-freezing the prepared sesame protein for two hours at the temperature of twenty ℃ below zero, and then performing vacuum freeze drying to obtain a finished product of the sesame deep processed protein.
Example two
Sesame deep-processing protein powder comprises sesame protein powder, wherein the sesame protein powder comprises 60% of sesame protein, 11% of soybean protein, 9.5% of pea protein, 9.5% of rice protein and 10% of whey protein;
the preparation method of the sesame protein powder comprises the following steps:
s1, preparing sesame protein, soybean protein, pea protein, rice protein and whey protein;
s2, uniformly mixing the prepared sesame protein, soybean protein, pea protein, rice protein and whey protein to obtain sesame protein powder;
s3, selecting sesame raw materials;
s3-1, screening sesame raw materials;
s-3-1, screening out sundries such as stones, crushed soil, crushed sesame straw, crushed leaves and the like in the sesame raw materials, and screening out empty and shrunken sesame in the sesame raw materials screened with the sundries;
s3-2, performing primary processing on the screened sesame raw materials;
s3-2-1, cleaning and drying the screened sesame meeting the processing quality requirement, and then crushing the sesame into sesame powder, wherein the sesame powder is required to be careful that the sesame cannot be fried;
s4, crushing the dried sesame raw materials, namely crushing the selected sesame raw materials meeting the quality requirements into sesame powder;
s5, crushing and degreasing sesame powder;
s6, sesame protein extraction is carried out on the sesame powder after the crushing and degreasing treatment;
s7-1, preparing sesame protein under the conditions that the pH value is 10, the temperature is 45 ℃, the solid-liquid ratio is 1:20 and the time is 0 min;
s8, processing the extracted sesame protein;
s8-1, pre-freezing the prepared sesame protein for two hours at the temperature of twenty ℃ below zero, and then performing vacuum freeze drying to obtain a finished product of the sesame deep processed protein.
Example III
Sesame deep-processing protein powder comprises sesame protein powder, wherein the sesame protein powder comprises 60% of sesame protein, 11% of soybean protein, 9.5% of pea protein, 9.5% of rice protein and 10% of whey protein;
the preparation method of the sesame protein powder comprises the following steps:
s1, preparing sesame protein, soybean protein, pea protein, rice protein and whey protein;
s2, uniformly mixing the prepared sesame protein, soybean protein, pea protein, rice protein and whey protein to obtain sesame protein powder;
s3, selecting sesame raw materials;
s3-1, screening sesame raw materials;
s-3-1, screening out sundries such as stones, crushed soil, crushed sesame straw, crushed leaves and the like in the sesame raw materials, and screening out empty and shrunken sesame in the sesame raw materials screened with the sundries;
s3-2, performing primary processing on the screened sesame raw materials;
s3-2-1, cleaning and drying the screened sesame meeting the processing quality requirement, and then crushing the sesame into sesame powder, wherein the sesame powder is required to be careful that the sesame cannot be fried;
s4, crushing the dried sesame raw material into sesame seed meal, and heating the sesame seed meal at a high temperature;
s5, crushing and degreasing the sesame seed meal heated at high temperature;
s6, extracting sesame protein from the processed sesame seed meal;
s6-1, preparing sesame protein from crushed and defatted sesame meal under the conditions of pH12, temperature 40 ℃ and solid-liquid ratio of 1:20 and extraction time of 90 min;
s7, processing the extracted sesame protein;
s7-1, pre-freezing the prepared sesame protein for two hours at the temperature of twenty ℃ below zero, and then performing vacuum freeze drying to obtain a finished product of the sesame deep processed protein.
The above examples are preferred embodiments of the present invention, but the embodiments of the present invention are not limited to the above examples, and any other changes, modifications, substitutions, combinations, and simplifications that do not depart from the spirit and principle of the present invention should be made in the equivalent manner, and the embodiments are included in the protection scope of the present invention.
Claims (8)
1. Sesame deep-processing protein powder comprises sesame protein powder and is characterized by comprising 60% of sesame protein, 11% of soybean protein, 9.5% of pea protein, 9.5% of rice protein and 10% of whey protein;
the preparation method of the sesame protein powder comprises the following steps:
s1, preparing sesame protein, soybean protein, pea protein, rice protein and whey protein;
s2, uniformly mixing the prepared sesame protein, soybean protein, pea protein, rice protein and whey protein to obtain sesame protein powder;
s3, selecting sesame raw materials;
s4, crushing the fried sesame raw material:
s5, extracting the crushed sesame raw materials;
s6, processing the sesame seed meal obtained after extraction;
s7, extracting sesame protein from the processed sesame seed meal;
s8, processing the extracted sesame protein.
2. The method for preparing sesame protein powder according to claim 1, wherein S3-1, sesame raw materials are screened;
s-3-1, screening out sundries such as stones, crushed soil, crushed sesame straw, crushed leaves and the like in the sesame raw materials, and screening out empty and shrunken sesame in the sesame raw materials screened with the sundries.
3. The method for preparing sesame protein powder according to claim 1, wherein S3-2, the screened sesame raw material is subjected to preliminary processing;
s3-2-1, cleaning and drying the screened sesame meeting the processing quality requirement, parching, and then crushing into sesame powder.
4. The method for producing sesame protein powder according to claim 1, wherein S5-1, the sesame oil is extracted by heating crushed sesame to a critical temperature;
s5-1-1, extraction times of at least three times, extraction pressure of 0.8-1.5MPa, extraction temperature of 45-55deg.C, and ratio of sesame powder heated to critical temperature to extract liquid of 2:6, and extraction time of 1.5-2.5 h.
5. The method for preparing sesame protein powder according to claim 1, wherein the sesame seed meal is obtained by solid-liquid separation after the extraction of S5-2.
6. The method for preparing sesame protein powder according to claim 1, wherein the sesame seed meal obtained after the extraction is crushed and defatted in S6-1.
7. The method for preparing sesame protein powder according to claim 1, wherein S7-1, sesame protein is prepared by crushing and degreasing sesame seed meal at a pH of 9.5-12, a temperature of 40-50 ℃, a solid-liquid ratio of 1:36 and a time of 20-90 min.
8. The method for preparing sesame protein powder according to claim 1, wherein S8-1 pre-freezes the prepared sesame protein at twenty degrees below zero for two hours, and then vacuum freeze-dries to obtain the finished sesame protein product after further processing.
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| CN202311758410.8A CN117694447A (en) | 2023-12-20 | 2023-12-20 | Sesame deep-processing protein powder and preparation method thereof |
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| CN202311758410.8A CN117694447A (en) | 2023-12-20 | 2023-12-20 | Sesame deep-processing protein powder and preparation method thereof |
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