CN117665041A - Radio frequency heating oil-rich coal in-situ pyrolysis simulation test device and method - Google Patents
Radio frequency heating oil-rich coal in-situ pyrolysis simulation test device and method Download PDFInfo
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- CN117665041A CN117665041A CN202410143116.4A CN202410143116A CN117665041A CN 117665041 A CN117665041 A CN 117665041A CN 202410143116 A CN202410143116 A CN 202410143116A CN 117665041 A CN117665041 A CN 117665041A
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- 238000010438 heat treatment Methods 0.000 title claims abstract description 67
- 239000003245 coal Substances 0.000 title claims abstract description 61
- 238000000197 pyrolysis Methods 0.000 title claims abstract description 42
- 238000011065 in-situ storage Methods 0.000 title claims abstract description 33
- 238000012360 testing method Methods 0.000 title claims abstract description 23
- 238000004088 simulation Methods 0.000 title claims abstract description 22
- 238000000034 method Methods 0.000 title claims abstract description 21
- 238000005192 partition Methods 0.000 claims abstract description 5
- 238000002474 experimental method Methods 0.000 claims description 6
- 238000012856 packing Methods 0.000 claims description 6
- 238000009529 body temperature measurement Methods 0.000 claims description 5
- -1 polytetrafluoroethylene Polymers 0.000 claims description 3
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims description 3
- 239000004810 polytetrafluoroethylene Substances 0.000 claims description 3
- 239000007788 liquid Substances 0.000 abstract description 10
- 238000000926 separation method Methods 0.000 abstract description 3
- 238000005516 engineering process Methods 0.000 description 11
- 238000006243 chemical reaction Methods 0.000 description 5
- 238000012546 transfer Methods 0.000 description 5
- 230000005855 radiation Effects 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 229910052799 carbon Inorganic materials 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- 238000012544 monitoring process Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000004064 recycling Methods 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 230000002159 abnormal effect Effects 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000002817 coal dust Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
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Abstract
The invention relates to a radio frequency heating oil-rich coal in-situ pyrolysis simulation test device and method, comprising the following steps: the device comprises a cavity, a gas inlet pipe, a gas outlet pipe and a gas inlet pipe, wherein the cavity is of a cylindrical structure with one end open, a porous partition plate is arranged in the cavity, and divides the cavity into a rich oil coal accommodating cavity and a tar accommodating cavity; the gas collecting bag is connected with the cavity through a gas collecting valve; the cavity cover is covered at the opening of the cavity; and the radio frequency antenna of the radio frequency control device is inserted into the cavity and used for heating the oil-rich coal in the oil-rich coal accommodating cavity. The experimental device can control the power and the frequency of radio frequency heating through the radio frequency control device, can judge whether the pyrolysis process in the cavity is finished through the simple device of the gas collecting bag, and can realize dry-wet separation of liquid and residual residues generated in the pyrolysis process of the oil-rich coal, thereby better collecting the liquid.
Description
Technical Field
The invention relates to a radio frequency heating oil-rich coal in-situ pyrolysis simulation test device and method, and belongs to the technical field of oil-rich coal in-situ pyrolysis.
Background
The in-situ pyrolysis technology of the oil-rich coal is an environment-friendly sustainable coal resource exploitation, conversion and utilization technology. The in-situ pyrolysis technology of oil-rich coal is characterized in that the oil-rich coal is directly heated underground through heat transfer of an external heat carrier, when the temperature reaches a certain degree, macromolecular organic matters can break chain links, so that small molecular oil gas components are generated, and the obtained oil gas products are led out of the ground through a collecting well to be separated and further processed. The advantages are that: in-situ pyrolysis directly realizes underground carbon sealing; in situ pyrolysis greatly reduces damage to the formation; the underground in-situ pyrolysis oil extraction reduces accumulation of ground solid semicoke, improves energy utilization efficiency and can remarkably reduce carbon emission in the process.
The in-situ heating technology can be divided into conduction heating, convection heating, chemical heating and radiation heating according to a heating principle, wherein the conduction heating is suitable for an operation scene with high heat conductivity, low pyrolysis temperature and long heating time, and the heat conductivity of coal is extremely low and is not suitable for the operation scene; the convection heating technology has the advantages of high heating efficiency, recycling of heat transfer medium and great heat loss in the injection process; the chemical heating technology has the advantages of high heating speed and high energy utilization rate in the heat release target layer, but has the defects of complex reaction control process and high reaction raw materials and operation cost; the radiation heating technology can directly raise the temperature of a target layer, does not need conduction or convection type heat transfer, has high energy utilization rate, but is in a starting stage at present, and lacks related experimental study.
Disclosure of Invention
Aiming at the technical problems, the invention provides a radio frequency heating oil-rich coal in-situ pyrolysis simulation test device which is used for researching the effect of radio frequency heating on the oil-rich coal in-situ pyrolysis.
In order to achieve the above purpose, the present invention adopts the following technical scheme:
an in-situ pyrolysis simulation test device for radio frequency heating of oil-rich coal, comprising:
the device comprises a cavity, a gas inlet pipe, a gas outlet pipe and a gas inlet pipe, wherein the cavity is of a cylindrical structure with one end open, a porous partition plate is arranged in the cavity, and divides the cavity into a rich oil coal accommodating cavity and a tar accommodating cavity;
the gas collecting bag is connected with the cavity through a gas collecting valve;
the cavity cover is covered at the opening of the cavity;
and the radio frequency antenna of the radio frequency control device is inserted into the cavity and used for heating the oil-rich coal in the oil-rich coal accommodating cavity.
In-situ pyrolysis simulation test device for radiofrequency heating of oil-rich coal, preferably, temperature measuring holes are formed in the side wall of the cavity, and a tar collecting valve is arranged at the bottom of the cavity.
In-situ pyrolysis simulation test device for radiofrequency heating of oil-rich coal, preferably, the cavity cover is provided with a groove, and packing is arranged in the groove.
In-situ pyrolysis simulation test device for radio frequency heating oil-rich coal, preferably, the cavity cover is provided with a through hole for the radio frequency antenna to penetrate, the cavity is also internally provided with an antenna protection cylinder, and the antenna protection cylinder is sleeved outside the radio frequency antenna.
In the radio-frequency heating oil-rich coal in-situ pyrolysis simulation test device, preferably, the antenna protection cylinder is a protection cylinder which does not absorb electromagnetic waves.
In the radio-frequency heating oil-rich coal in-situ pyrolysis simulation test device, preferably, the antenna protection cylinder is a polytetrafluoroethylene protection cylinder.
An experimental method based on the radio frequency heating oil-rich coal in-situ pyrolysis simulation test device comprises the following steps:
placing oil-rich coal on the perforated partition plate in the cavity;
connecting the gas collecting bag with the gas collecting valve and opening the gas collecting valve;
covering the cavity cover and closing the tar collecting valve;
the radio frequency control device is opened to perform radio frequency heating on the oil-rich coal in the cavity and perform temperature measurement through the temperature measurement hole;
collecting gas by using the gas collecting bag;
stopping radio frequency heating, opening the tar collecting valve, and taking out tar from the bottom of the cavity;
and opening the cavity cover to dissipate heat and cleaning the inside of the cavity.
In the experimental method, preferably, a high-temperature resistant temperature measuring rod is used for extending into the temperature measuring hole to measure the temperature.
In the experimental method, preferably, the high temperature resistance temperature of the high temperature resistant temperature measuring rod is 450 ℃.
Due to the adoption of the technical scheme, the invention has the following advantages:
1. the experimental device can perform a large-volume radio-frequency heating oil-rich coal in-situ pyrolysis experiment and collect gas and liquid generated in the process.
2. The experimental device can control the power and the frequency of radio frequency heating through the radio frequency control device, can judge whether the pyrolysis process in the cavity is finished through the simple device of the gas collecting bag, and can realize dry-wet separation of liquid and residual residues generated in the pyrolysis process of the oil-rich coal, thereby better collecting the liquid.
Drawings
FIG. 1 is a schematic diagram of an in-situ pyrolysis simulation test device for RF heating of oil-rich coal according to an embodiment of the present invention;
FIG. 2 is a top view of a perforated baffle plate within a chamber according to this embodiment of the invention;
the figures are marked as follows:
1-an air collecting bag; 2-1-gas collection valve; 2-2-tar collection valve; 3-a temperature measuring hole; 4-oil-rich coal; 5-a cavity; 6-a separator with holes; 7-packing; 8-a cavity cover; 9-an antenna protection cylinder; 10-a radio frequency antenna; 11-radio frequency control device.
Detailed Description
For the purpose of making the objects, technical solutions and advantages of the present invention more apparent, the technical solutions in the present invention will be clearly and completely described below, and it is apparent that the described embodiments are some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by one of ordinary skill in the art without undue burden from the present disclosure, are intended to be within the scope of the present disclosure.
Unless defined otherwise, technical or scientific terms used herein should be given the ordinary meaning as understood by one of ordinary skill in the art to which this invention belongs. The terms "first," "second," "third," "fourth," and the like as used herein do not denote any order, quantity, or importance, but rather are used to distinguish one element from another. The word "comprising" or "comprises", and the like, means that elements or items preceding the word are included in the element or item listed after the word and equivalents thereof, but does not exclude other elements or items. The terms "connected" or "connected," and the like, are not limited to physical or mechanical connections, but may include electrical connections, whether direct or indirect.
For ease of description, spatially relative terms, such as "inner," "outer," "lower," "upper," and the like, may be used herein to describe one element or feature's relationship to another element or feature as illustrated in the figures. Such spatially relative terms are intended to encompass different orientations of the device in use or operation in addition to the orientation depicted in the figures.
The existing in-situ heating technology can be divided into conduction heating, convection heating, chemical heating and radiation heating according to the heating principle, wherein the conduction heating is suitable for operation scenes with high heat conductivity, low pyrolysis temperature and long heating time, and the heat conductivity of coal is extremely low and is not suitable for use; the convection heating technology has the advantages of high heating efficiency, recycling of heat transfer medium and great heat loss in the injection process; the chemical heating technology has the advantages of high heating speed and high energy utilization rate in the heat release target layer, but has the defects of complex reaction control process and high reaction raw materials and operation cost; the radiation heating technology can directly raise the temperature of a target layer, does not need conduction or convection type heat transfer, has high energy utilization rate, but is in a starting stage at present, and lacks related experimental study.
Based on the problems, the invention provides a radio frequency heating oil-rich coal in-situ pyrolysis simulation test device which is used for researching the effect of radio frequency heating on in-situ pyrolysis of oil-rich coal.
As shown in fig. 1 and fig. 2, the in-situ pyrolysis simulation test device for the radio frequency heating oil-rich coal provided by the invention comprises: the cavity 5 is of a cylindrical structure with one end open, a perforated baffle 6 is arranged in the cavity 5, and the perforated baffle 6 divides the cavity 5 into a rich coal accommodating cavity and a tar accommodating cavity; the gas collecting bag 1 is connected with the cavity 5 through a gas collecting valve 2-1; a cavity cover 3 covering an opening of the cavity 5; the radio frequency control device 11, the radio frequency antenna 10 of the radio frequency control device 11 inserts in the cavity 5, is used for heating the rich coal 4 in the rich coal holding cavity. The side wall of the cavity 5 is provided with a temperature measuring hole 3, and the bottom of the cavity 5 is provided with a tar collecting valve 2-2.
Further, a groove is formed in the cavity cover 8, a packing 7 is arranged in the groove, a through hole for the radio frequency antenna 10 to penetrate is formed in the cavity cover 8, an antenna protection barrel 9 is further arranged in the cavity 5, and the antenna protection barrel 9 is sleeved outside the radio frequency antenna 10.
Further, the antenna protection tube 9 is a protection tube that does not absorb electromagnetic waves, and is preferably a polytetrafluoroethylene protection tube.
The invention also relates to an experimental method based on the radio frequency heating oil-rich coal in-situ pyrolysis simulation test device, which comprises the following steps:
step 1: preparing the rich oil coal, detecting the components of the rich oil coal sample in advance, and estimating pyrolysis products according to the existing literature data. The placed rich oil coal is a blocky coal sample, so that excessive coal dust is prevented from entering the space below the porous partition plate to influence tar collection.
Step 2: the oil-rich coal sample is placed on the perforated baffle plate 6 in the cavity 5 as regularly as possible, and the oil-rich coal sample is placed lightly in the placing process, so that the experimental device is prevented from being damaged. Because the oil-rich coal is placed on the perforated baffle plate 6 in the cavity 5, tar generated after pyrolysis of the oil-rich coal is collected in a space below the perforated baffle plate 6.
The method comprises the following steps: the connection of the gas collecting bag 1 is carried out, the connection of the gas collecting bag 1 is ensured to ensure that the gas collecting bag 1 is intact and the connection with the gas collecting valve 2-1 is stable, and the valve is confirmed to be opened.
Step 4: checking whether the cavity cover 8 and the packing 7 of the cavity 5 are intact, covering the cavity cover 8 and ensuring fixation, and checking whether the tar collecting valve 2-2 at the bottom of the cavity 5 is closed. Before the cavity cover 8 is covered, the integrity of the graphite packing 7 is ensured to achieve a certain sealing effect, and the cavity cover 8 needs a certain fixing measure.
Step 5: the power is set according to the actual requirement through the radio frequency control device 11, the device is started after all equipment is normal, the professional equipment (leakage detector) is used for monitoring whether electromagnetic waves leak at any time after the device is started, the temperature of the inside of the cavity 5 is measured through the temperature measuring hole 3 after the device is heated for a certain time, if the heating should be stopped due to abnormal high temperature, if the temperature in the cavity 5 is required to be continuously monitored, the temperature measuring rod is inserted into the cavity 5 and is not taken out, but the temperature measuring rod is required to be resistant to high temperature (450 ℃). The temperature measurement through the temperature measuring hole 3 is carried out by using a high temperature resistant temperature measuring rod which enters the cavity 5 through the temperature measuring hole 3, and the temperature of the cavity 5 at different radial distances is measured. In this process, since high temperature is generated in the cavity 5, the temperature cannot be monitored by the built-in thermometer, and if the purpose of real-time temperature monitoring is to be achieved, the temperature must be measured by the high temperature resistant thermometer.
Step 6: the gas was collected. When heating starts, the condition of the gas collecting bag 1 must be paid attention to, when the gas collecting bag 1 has a large expansion range, the gas collecting valve 2-1 must be closed to replace the gas collecting bag 1, and then the valve is opened, so that the gas collecting bag 1 needs to have special storage protection measures to prevent damage and leakage. The gas collection bag 1 or other devices capable of visually observing the gas collection phenomenon are used for collecting the gas. When the gas collecting bag 1 is used for collecting, if the gas collecting bag 1 is observed to be greatly inflated, the valve is closed to replace the gas collecting bag 1, and the gas is inflammable and explosive, so that the collected gas is required to be properly stored.
Step 7: heating is stopped when no gas is generated or the experimental requirements have been met. Here, no gas is generated, that is, the gas collecting bag 1 does not continue to expand.
Step 8: after stopping the heating, the liquid product is taken out from the bottom of the cavity 5. The container for holding the liquid has the characteristic of high temperature resistance, and the heat-insulating glove is worn when the valve is opened.
Step 9: the cavity cover 8 is opened by wearing the heat-insulating glove, and the heat is dissipated to the room temperature. At this time, the remaining gas in the chamber 5 is not discharged, and a certain protection measure is performed when the chamber cover 8 is opened.
Step 10: the remainder of the cavity 5 is removed and the interior of the cavity 5 is cleaned with professional equipment. It should be noted that, the liquid below the perforated baffle plate 6 in the cavity 5 cannot be completely discharged through the valve at the bottom of the cavity 5, and the perforated baffle plate 6 needs to be removed to collect the residual liquid after cleaning the residues in the cavity 5.
The experimental device can control the power and the frequency of radio frequency heating through the radio frequency control device, can judge whether the pyrolysis process in the cavity is finished through the simple device of the gas collecting bag, and can realize dry-wet separation of liquid and residual residues generated in the pyrolysis process of the oil-rich coal, thereby better collecting the liquid.
Finally, it should be noted that: the above embodiments are only for illustrating the technical solution of the present invention, and are not limiting; although the invention has been described in detail with reference to the foregoing embodiments, it will be understood by those of ordinary skill in the art that: the technical scheme described in the foregoing embodiments can be modified or some technical features thereof can be replaced by equivalents; such modifications and substitutions do not depart from the spirit and scope of the technical solutions of the embodiments of the present invention.
Claims (9)
1. The utility model provides a radio frequency heating oil-rich coal normal position pyrolysis analogue test device which characterized in that includes:
the device comprises a cavity (5) which is of a cylindrical structure with one end open, wherein a perforated baffle (6) is arranged in the cavity (5), and the perforated baffle (6) divides the cavity (5) into a rich coal accommodating cavity and a tar accommodating cavity;
the gas collecting bag (1) is connected with the cavity (5) through a gas collecting valve (2-1);
a cavity cover (8) covering the opening of the cavity (5);
the radio frequency control device (11), the radio frequency antenna (10) of the radio frequency control device (11) is inserted into the cavity (5) and is used for heating the rich coal (4) in the rich coal accommodating cavity.
2. The radio frequency heating oil-rich coal in-situ pyrolysis simulation test device according to claim 1, wherein a temperature measuring hole (3) is formed in the side wall of the cavity (5), and a tar collecting valve (2-2) is arranged at the bottom of the cavity (5).
3. The radio frequency heating oil-rich coal in-situ pyrolysis simulation test device according to claim 1, wherein a groove is formed in the cavity cover (8), and a packing (7) is arranged in the groove.
4. The radio frequency heating oil-rich coal in-situ pyrolysis simulation test device according to claim 3, wherein a through hole for the radio frequency antenna (10) to penetrate is formed in the cavity cover (8), an antenna protection cylinder (9) is further arranged in the cavity (5), and the antenna protection cylinder (9) is sleeved outside the radio frequency antenna (10).
5. The radio frequency heating oil-rich coal in-situ pyrolysis simulation test device according to claim 4, wherein the antenna protection cylinder (9) is a protection cylinder which does not absorb electromagnetic waves.
6. The radio frequency heating oil-rich coal in-situ pyrolysis simulation test device according to claim 5, wherein the antenna protection cylinder (9) is a polytetrafluoroethylene protection cylinder.
7. An experimental method of an in-situ pyrolysis simulation test device for radiofrequency heating oil-rich coal according to any one of claims 2 to 6, comprising the following steps:
placing oil-rich coal on the perforated partition plate (6) in the cavity (5);
connecting the gas collecting bag (1) with the gas collecting valve (2-1) and opening the gas collecting valve (2-1);
covering the cavity cover (8) and closing the tar collection valve (2-2);
the radio frequency control device (11) is opened to perform radio frequency heating on the oil-rich coal in the cavity (5) and perform temperature measurement through the temperature measurement hole (3);
collecting gas by the gas collecting bag (1);
stopping radio frequency heating, opening the tar collecting valve (2-2), and taking out tar from the bottom of the cavity (5);
and opening the cavity cover (8) to dissipate heat and clean the interior of the cavity (5).
8. The method according to claim 7, characterized in that the temperature is measured by means of a temperature-resistant thermometer extending into the temperature measuring hole (3).
9. The method according to claim 8, wherein the high temperature resistant temperature of the high temperature resistant temperature measuring rod is 450 ℃.
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CN204086253U (en) * | 2014-10-01 | 2015-01-07 | 西安科技大学 | A kind of pour to strain to test device of gangue |
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