CN117257715A - Make-up spray with oil control effect and preparation method thereof - Google Patents

Make-up spray with oil control effect and preparation method thereof Download PDF

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Publication number
CN117257715A
CN117257715A CN202311493511.7A CN202311493511A CN117257715A CN 117257715 A CN117257715 A CN 117257715A CN 202311493511 A CN202311493511 A CN 202311493511A CN 117257715 A CN117257715 A CN 117257715A
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oil control
hyaluronic acid
parts
mixture
spray
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胡力
杨萍英
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04—Dispersions; Emulsions
    • A61K8/046—Aerosols; Foams
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A61K8/345—Alcohols containing more than one hydroxy group
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/41—Amines
    • A61K8/416—Quaternary ammonium compounds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9728—Fungi, e.g. yeasts
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/008—Preparations for oily skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59—Mixtures
    • A61K2800/592—Mixtures of compounds complementing their respective functions
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/81—Preparation or application process involves irradiation

Abstract

The invention relates to the technical field of cosmetics, and discloses a make-up spray with an oil control effect and a preparation method thereof, wherein the make-up spray comprises the following components in parts by weight: 12-20 parts of hexanediol, 20-25 parts of jasmine water, 10-15 parts of tremella extract, 6-8 parts of lactobacillus, 8-15 parts of oil control agent, 5-10 parts of film forming agent, 2-4 parts of modified hyaluronic acid and 3-6 parts of emollient; according to the invention, the mixture A is obtained by uniformly mixing hexanediol, jasmine water, tremella extract and lactobacillus; mixing an oil control agent, a film forming agent, modified hyaluronic acid and an emollient to obtain a mixture B; and adding the mixture A into the mixture B, uniformly stirring, cooling to normal temperature, and discharging after the mixture A is inspected to be qualified, thereby obtaining the make-up spray with the oil control effect.

Description

Make-up spray with oil control effect and preparation method thereof
Technical Field
The invention relates to the technical field of cosmetics, in particular to a make-up spray with an oil control effect and a preparation method thereof.
Background
The consumer often has the problems of makeup removal, makeup flowers and the like caused by oil or sweat on the face, the image is seriously affected, how to increase the makeup effect of the consumer becomes a problem to be treated urgently, the common make-up product on the market is provided with powder, powder cake, make-up spray and the like, the powder is a product formed by solid powder, the oil-and-luster condition of the face is reduced through the physical adsorption grease effect of the powder, but the powder is easy to fly upwards and pollutes the environment; the pressed powder is a cake-shaped product obtained by compacting the mixture of the components through equipment, has the characteristics of convenience and rapidness, but is easy to clamp after use, and influences the practical effect of dressing; the finishing spray is a product directly sprayed on the face of a consumer, has the characteristics of convenience in use, excellent finishing effect, excellent skin care effect and the like, is popular in the market at the current stage, has fresh skin feel, but has few film forming components and poor finishing actual effect; the actual effect of the make-up is strong, but after the spray is dried, the film is formed tightly, so that the tight feeling of the face is promoted to be obvious; affecting the cosmetic effect; the actual effect of oil control is good, and the solid powder has the effect of physically adsorbing oil, but white foam can be sprayed, so that the feeling is poor; the drying rate is high, but a large amount of ethanol is added to stimulate the skin.
Disclosure of Invention
(one) solving the technical problems
Aiming at the defects of the prior art, the invention provides the make-up spray with the oil control effect and the preparation method thereof, which have better oil control effect and solve the problem of more grease secretion.
(II) technical scheme
In order to achieve the above purpose, the present invention provides the following technical solutions: the make-up spray with the oil control effect comprises the following components in parts by weight: 12-20 parts of hexanediol, 20-25 parts of jasmine water, 10-15 parts of tremella extract, 6-8 parts of lactobacillus, 8-15 parts of oil control agent, 5-10 parts of film forming agent, 2-4 parts of modified hyaluronic acid and 3-6 parts of emollient.
Preferably, the tremella extract is prepared by the following steps: adding 4-6g of tremella powder passing through 60-70 mesh molecular sieve into a reactor, adding tetrabutylammonium chloride solvent into the reactor, placing into a microwave extractor, extracting at 50-70deg.C for 5-10min under microwave power of 450-550W, and collecting supernatant to obtain tremella extract.
Preferably, the oil control agent is one or more of nicotinamide, benzoyl peroxide gel, calendula, tretinoin, fruit acid, lavender and azelaic acid.
Preferably, the film forming agent is any one or more of acrylic resin-trimethyl siloxane copolymer, polyvinylpyrrolidone, trimethyl siloxysilicate and polyvinyl alcohol.
Preferably, the preparation method of the modified hyaluronic acid comprises the following steps:
(1) Adding 2-5g of hyaluronic acid and 1-3g of 3-chloro-2-hydroxypropyl trimethyl ammonium chloride into 0.6-0.8g/ml of sodium hydroxide aqueous alcohol solution, reacting for 1-2h at 40-60 ℃, continuously adding 8-12% of lactic acid-sodium lactate aqueous solution after the reaction is finished, dissolving and diluting a reaction product, filtering, collecting filtrate, adding acetone for precipitation, filtering and collecting the precipitate, washing 2-3 times by absolute ethyl alcohol, and drying to obtain quaternary ammonium salt grafted hyaluronic acid;
(2) Adding 2-4g of quaternary ammonium salt grafted hyaluronic acid into 1, 4-dioxane, uniformly dispersing, adding 1-2g of epoxy chloropropane and 0.01-0.03g of boron trifluoride diethyl ether, reacting for 2-3h at 70-90 ℃, filtering, washing and drying to obtain chloro quaternary ammonium salt grafted hyaluronic acid;
(3) Adding 2-3g of chlorinated quaternary ammonium salt grafted hyaluronic acid into N, N-dimethylformamide solvent, uniformly dispersing, adding N, N-carbonyl diimidazole, reacting at 60-90 ℃ for 20-30h, filtering, washing and drying to obtain modified hyaluronic acid.
Preferably, the emollient is any one or more of octyl dodecanol, polydimethylsiloxane, glycerol and urea.
Preferably, the preparation method of the make-up spray comprises the following steps:
(1) Weighing hexanediol, jasmine water, tremella extract and lactobacillus according to a certain proportion, uniformly mixing, and stirring at 30-50 ℃ for 1-2h to obtain a mixture A;
(2) Weighing oil control agent, film forming agent, modified hyaluronic acid and emollient in proportion, mixing, stirring at 50-60deg.C for 30-60min to obtain mixture B;
(3) And adding the mixture A into the mixture B, uniformly stirring, cooling to normal temperature, and discharging after the mixture A is inspected to be qualified, thereby obtaining the make-up spray with the oil control effect.
(III) beneficial technical effects
According to the invention, the mixture A is obtained by uniformly mixing hexanediol, jasmine water, tremella extract and lactobacillus; mixing an oil control agent, a film forming agent, modified hyaluronic acid and an emollient to obtain a mixture B; and adding the mixture A into the mixture B, uniformly stirring, cooling to normal temperature, and discharging after the mixture A is inspected to be qualified, thereby obtaining the make-up spray with the oil control effect.
The modified hyaluronic acid contains quaternary ammonium salt groups and imidazole groups, the quaternary ammonium salt groups can play roles in moisturizing, thickening, stabilizing and resisting static electricity, the imidazole can play roles in inhibiting the deterioration of the make-up spray with the oil control effect, and the modified hyaluronic acid and other components cooperate to play roles in controlling the oil of the skin and inhibit the secretion of grease.
Drawings
Fig. 1 is a modified hyaluronic acid reaction scheme.
Fig. 2 is a chart of the cosmetic spray performance test for oil control effect.
Detailed Description
Example 1:
(1) Adding 4g of tremella powder passing through a 60-mesh molecular sieve into a reactor, adding tetrabutylammonium chloride solvent into the reactor, placing the mixture into a microwave extractor, extracting the mixture for 5min at the reaction temperature of 50 ℃ under the microwave power of 450W, and sucking the supernatant to obtain tremella extract;
(2) Adding 2g of hyaluronic acid and 1g of 3-chloro-2-hydroxypropyl trimethyl ammonium chloride into 0.6g/ml of sodium hydroxide aqueous alcohol solution, reacting for 1h at 40 ℃, continuously adding 8% of lactic acid-sodium lactate aqueous solution after the reaction is finished, dissolving and diluting a reaction product, filtering, collecting filtrate, adding acetone for precipitation, filtering and collecting precipitate, washing with absolute ethyl alcohol for 2 times, and drying to obtain quaternary ammonium salt grafted hyaluronic acid;
(3) Adding 2g of quaternary ammonium salt grafted hyaluronic acid into 1, 4-dioxane, uniformly dispersing, adding 1g of epoxy chloropropane and 0.01g of boron trifluoride diethyl ether, reacting for 2 hours at 70 ℃, filtering, washing and drying to obtain chlorinated quaternary ammonium salt grafted hyaluronic acid;
(4) Adding 2g of chloro quaternary ammonium salt grafted hyaluronic acid into an N, N-dimethylformamide solvent, uniformly dispersing, adding N, N-carbonyl diimidazole, reacting for 20 hours at 60 ℃, filtering, washing and drying to obtain modified hyaluronic acid;
(5) Weighing hexanediol, jasmine water, tremella extract and lactobacillus according to a certain proportion, uniformly mixing, and stirring for 1h at 30 ℃ to obtain a mixture A;
(6) Weighing oil control agent, film forming agent, modified hyaluronic acid and emollient in proportion, mixing, stirring at 50deg.C for 30min to obtain mixture B;
(7) And adding the mixture A into the mixture B, uniformly stirring, cooling to normal temperature, and discharging after the mixture A is inspected to be qualified, thereby obtaining the make-up spray with the oil control effect.
Example 2:
(1) Adding 6g of tremella powder passing through a 70-mesh molecular sieve into a reactor, adding tetrabutylammonium chloride solvent into the reactor, placing the mixture into a microwave extractor, extracting the mixture for 10min at the reaction temperature of 70 ℃ under the microwave power of 550W to obtain tremella extract;
(2) Adding 5g of hyaluronic acid and 3g of 3-chloro-2-hydroxypropyl trimethyl ammonium chloride into 0.8g/ml of sodium hydroxide aqueous alcohol solution, reacting for 2 hours at 60 ℃, continuously adding 12% lactic acid-sodium lactate aqueous solution after the reaction is finished, dissolving and diluting a reaction product, filtering, collecting filtrate, adding acetone for precipitation, filtering and collecting precipitate, washing with absolute ethyl alcohol for 3 times, and drying to obtain quaternary ammonium salt grafted hyaluronic acid;
(3) Adding 4g of quaternary ammonium salt grafted hyaluronic acid into 1, 4-dioxane, uniformly dispersing, adding 2g of epoxy chloropropane and 0.03g of boron trifluoride diethyl ether, reacting for 3 hours at 90 ℃, filtering, washing and drying to obtain chlorinated quaternary ammonium salt grafted hyaluronic acid;
(4) Adding 3g of chlorinated quaternary ammonium salt grafted hyaluronic acid into an N, N-dimethylformamide solvent, uniformly dispersing, adding N, N-carbonyl diimidazole, reacting for 30 hours at 90 ℃, filtering, washing and drying to obtain modified hyaluronic acid;
(5) Weighing hexanediol, jasmine water, tremella extract and lactobacillus according to a certain proportion, uniformly mixing, and stirring for 2 hours at 50 ℃ to obtain a mixture A;
(6) Weighing oil control agent, film forming agent, modified hyaluronic acid and emollient in proportion, mixing, stirring at 60deg.C for 60min to obtain mixture B;
(7) And adding the mixture A into the mixture B, uniformly stirring, cooling to normal temperature, and discharging after the mixture A is inspected to be qualified, thereby obtaining the make-up spray with the oil control effect.
Example 3:
(1) Adding 5g of tremella powder passing through a 65-mesh molecular sieve into a reactor, adding tetrabutylammonium chloride solvent into the reactor, placing the mixture into a microwave extractor, extracting the mixture for 7.5min at the reaction temperature of 60 ℃ under the microwave power of 500W, and sucking the supernatant to obtain tremella extract;
(2) Adding 3.5g of hyaluronic acid and 2g of 3-chloro-2-hydroxypropyl trimethyl ammonium chloride into 0.7g/ml of sodium hydroxide aqueous alcohol solution, reacting for 1.5 hours at 50 ℃, continuously adding 10% of lactic acid-sodium lactate aqueous solution after the reaction is finished, dissolving and diluting a reaction product, filtering, collecting filtrate, adding acetone for precipitation, filtering, collecting the precipitate, washing with absolute ethyl alcohol for 2.5 times, and drying to obtain quaternary ammonium salt grafted hyaluronic acid;
(3) Adding 3g of quaternary ammonium salt grafted hyaluronic acid into 1, 4-dioxane, uniformly dispersing, adding 1.5g of epoxy chloropropane and 0.02g of boron trifluoride diethyl ether, reacting at 80 ℃ for 2.5h, filtering, washing and drying to obtain chloro quaternary ammonium salt grafted hyaluronic acid;
(4) Adding 2.5g of chlorinated quaternary ammonium salt grafted hyaluronic acid into an N, N-dimethylformamide solvent, uniformly dispersing, adding N, N-carbonyl diimidazole, reacting at 75 ℃ for 25 hours, filtering, washing and drying to obtain modified hyaluronic acid;
(5) Weighing hexanediol, jasmine water, tremella extract and lactobacillus according to a certain proportion, uniformly mixing, and stirring at 40 ℃ for 1.5 hours to obtain a mixture A;
(6) Weighing oil control agent, film forming agent, modified hyaluronic acid and emollient in proportion, mixing, stirring at 55deg.C for 45min to obtain mixture B;
(7) And adding the mixture A into the mixture B, uniformly stirring, cooling to normal temperature, and discharging after the mixture A is inspected to be qualified, thereby obtaining the make-up spray with the oil control effect.
Example 4:
(1) Adding 4g of tremella powder passing through a 60-mesh molecular sieve into a reactor, adding tetrabutylammonium chloride solvent into the reactor, placing the mixture into a microwave extractor, extracting the mixture for 5min at the reaction temperature of 50 ℃ under the microwave power of 450W, and sucking the supernatant to obtain tremella extract;
(2) Adding 5g of hyaluronic acid and 3g of 3-chloro-2-hydroxypropyl trimethyl ammonium chloride into 0.8g/ml of sodium hydroxide aqueous alcohol solution, reacting for 2 hours at 60 ℃, continuously adding 12% lactic acid-sodium lactate aqueous solution after the reaction is finished, dissolving and diluting a reaction product, filtering, collecting filtrate, adding acetone for precipitation, filtering and collecting precipitate, washing with absolute ethyl alcohol for 3 times, and drying to obtain quaternary ammonium salt grafted hyaluronic acid;
(3) Adding 4g of quaternary ammonium salt grafted hyaluronic acid into 1, 4-dioxane, uniformly dispersing, adding 2g of epoxy chloropropane and 0.03g of boron trifluoride diethyl ether, reacting for 3 hours at 90 ℃, filtering, washing and drying to obtain chlorinated quaternary ammonium salt grafted hyaluronic acid;
(4) Adding 2.5g of chlorinated quaternary ammonium salt grafted hyaluronic acid into an N, N-dimethylformamide solvent, uniformly dispersing, adding N, N-carbonyl diimidazole, reacting at 75 ℃ for 25 hours, filtering, washing and drying to obtain modified hyaluronic acid;
(5) Weighing hexanediol, jasmine water, tremella extract and lactobacillus according to a certain proportion, uniformly mixing, and stirring at 40 ℃ for 1.5 hours to obtain a mixture A;
(6) Weighing oil control agent, film forming agent, modified hyaluronic acid and emollient in proportion, mixing, stirring at 55deg.C for 45min to obtain mixture B;
(7) And adding the mixture A into the mixture B, uniformly stirring, cooling to normal temperature, and discharging after the mixture A is inspected to be qualified, thereby obtaining the make-up spray with the oil control effect.
Example 5:
(1) Adding 6g of tremella powder passing through a 70-mesh molecular sieve into a reactor, adding tetrabutylammonium chloride solvent into the reactor, placing the mixture into a microwave extractor, extracting the mixture for 10min at the reaction temperature of 70 ℃ under the microwave power of 550W to obtain tremella extract;
(2) Adding 5g of hyaluronic acid and 3g of 3-chloro-2-hydroxypropyl trimethyl ammonium chloride into 0.8g/ml of sodium hydroxide aqueous alcohol solution, reacting for 2 hours at 60 ℃, continuously adding 12% lactic acid-sodium lactate aqueous solution after the reaction is finished, dissolving and diluting a reaction product, filtering, collecting filtrate, adding acetone for precipitation, filtering and collecting precipitate, washing with absolute ethyl alcohol for 3 times, and drying to obtain quaternary ammonium salt grafted hyaluronic acid;
(3) Adding 3g of quaternary ammonium salt grafted hyaluronic acid into 1, 4-dioxane, uniformly dispersing, adding 1.5g of epoxy chloropropane and 0.02g of boron trifluoride diethyl ether, reacting at 80 ℃ for 2.5h, filtering, washing and drying to obtain chloro quaternary ammonium salt grafted hyaluronic acid;
(4) Adding 2.5g of chlorinated quaternary ammonium salt grafted hyaluronic acid into an N, N-dimethylformamide solvent, uniformly dispersing, adding N, N-carbonyl diimidazole, reacting at 75 ℃ for 25 hours, filtering, washing and drying to obtain modified hyaluronic acid;
(5) Weighing hexanediol, jasmine water, tremella extract and lactobacillus according to a certain proportion, uniformly mixing, and stirring for 1h at 30 ℃ to obtain a mixture A;
(6) Weighing oil control agent, film forming agent, modified hyaluronic acid and emollient in proportion, mixing, stirring at 50deg.C for 30min to obtain mixture B;
(7) And adding the mixture A into the mixture B, uniformly stirring, cooling to normal temperature, and discharging after the mixture A is inspected to be qualified, thereby obtaining the make-up spray with the oil control effect.
Comparative example 1
(1) Adding 5g of tremella powder passing through a 65-mesh molecular sieve into a reactor, adding tetrabutylammonium chloride solvent into the reactor, placing the mixture into a microwave extractor, extracting the mixture for 7.5min at the reaction temperature of 60 ℃ under the microwave power of 500W, and sucking the supernatant to obtain tremella extract;
(2) Weighing hexanediol, jasmine water, tremella extract and lactobacillus according to a certain proportion, uniformly mixing, and stirring for 1h at 30 ℃ to obtain a mixture A;
(3) Weighing oil control agent, film forming agent and emollient in proportion, mixing, stirring at 50deg.C for 30min to obtain mixture B;
(4) And adding the mixture A into the mixture B, uniformly stirring, cooling to normal temperature, and discharging after the mixture A is inspected to be qualified, thereby obtaining the make-up spray with the oil control effect.
120 oily skin volunteers are selected as study objects, the volunteers are divided into six groups, each group comprises 20 people, the test period is 2 weeks, sensory test evaluation is carried out, evaluation is carried out from two dimensions of oil control effect and comfort level, the score ranges from 0 to 9, the higher the score is, the better the product effect is represented, and the test result is shown in figure 2.
The preferred embodiments of the invention disclosed above are intended only to assist in the explanation of the invention. The preferred embodiments are not exhaustive or to limit the invention to the precise form disclosed. Obviously, many modifications and variations are possible in light of the above teaching. The embodiments were chosen and described in order to best explain the principles of the invention and the practical application, to thereby enable others skilled in the art to best understand and utilize the invention. The invention is limited only by the claims and the full scope and equivalents thereof.

Claims (7)

1. The make-up spray with the oil control effect is characterized by comprising the following components in parts by weight: 12-20 parts of hexanediol, 20-25 parts of jasmine water, 10-15 parts of tremella extract, 6-8 parts of lactobacillus, 8-15 parts of oil control agent, 5-10 parts of film forming agent, 2-4 parts of modified hyaluronic acid and 3-6 parts of emollient.
2. The make-up spray with oil control effect according to claim 1, wherein the tremella extract is prepared by the following steps: adding 4-6g of tremella powder passing through 60-70 mesh molecular sieve into a reactor, adding tetrabutylammonium chloride solvent into the reactor, placing into a microwave extractor, extracting at 50-70deg.C for 5-10min under microwave power of 450-550W, and collecting supernatant to obtain tremella extract.
3. The make-up spray with oil control effect according to claim 1, wherein the oil control agent is any one or more of nicotinamide, benzoyl peroxide gel, calendula, tretinoin, fruit acid, lavender, and azelaic acid.
4. The make-up spray with oil control effect according to claim 1, wherein the film forming agent is any one or more of acrylic resin-trimethylsiloxane copolymer, polyvinylpyrrolidone, trimethylsiloxysilicate, and polyvinyl alcohol.
5. The make-up spray with oil control effect according to claim 1, wherein the modified hyaluronic acid preparation method is as follows:
(1) Adding 2-5g of hyaluronic acid and 1-3g of 3-chloro-2-hydroxypropyl trimethyl ammonium chloride into 0.6-0.8g/ml of sodium hydroxide aqueous alcohol solution, reacting for 1-2h at 40-60 ℃, continuously adding 8-12% of lactic acid-sodium lactate aqueous solution after the reaction is finished, dissolving and diluting a reaction product, filtering, collecting filtrate, adding acetone for precipitation, filtering and collecting the precipitate, washing 2-3 times by absolute ethyl alcohol, and drying to obtain quaternary ammonium salt grafted hyaluronic acid;
(2) Adding 2-4g of quaternary ammonium salt grafted hyaluronic acid into 1, 4-dioxane, uniformly dispersing, adding 1-2g of epoxy chloropropane and 0.01-0.03g of boron trifluoride diethyl ether, reacting for 2-3h at 70-90 ℃, filtering, washing and drying to obtain chloro quaternary ammonium salt grafted hyaluronic acid;
(3) Adding 2-3g of chlorinated quaternary ammonium salt grafted hyaluronic acid into N, N-dimethylformamide solvent, uniformly dispersing, adding N, N-carbonyl diimidazole, reacting at 60-90 ℃ for 20-30h, filtering, washing and drying to obtain modified hyaluronic acid.
6. The oil control cosmetic spray of claim 1, wherein the emollient is one or more of octyldodecanol, polydimethylsiloxane, glycerin, and urea.
7. A method for preparing a make-up spray having an oil control effect as claimed in any one of claims 1 to 6, wherein the method for preparing the make-up spray comprises the steps of:
(1) Weighing hexanediol, jasmine water, tremella extract and lactobacillus according to a certain proportion, uniformly mixing, and stirring at 30-50 ℃ for 1-2h to obtain a mixture A;
(2) Weighing oil control agent, film forming agent, modified hyaluronic acid and emollient in proportion, mixing, stirring at 50-60deg.C for 30-60min to obtain mixture B;
(3) And adding the mixture A into the mixture B, uniformly stirring, cooling to normal temperature, and discharging after the mixture A is inspected to be qualified, thereby obtaining the make-up spray with the oil control effect.
CN202311493511.7A 2023-11-10 2023-11-10 Make-up spray with oil control effect and preparation method thereof Pending CN117257715A (en)

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CN202311493511.7A CN117257715A (en) 2023-11-10 2023-11-10 Make-up spray with oil control effect and preparation method thereof

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106074214A (en) * 2016-07-13 2016-11-09 袁春华 A kind of preparation method of the anti-aging facial film of radioprotective
CN108484794A (en) * 2018-03-17 2018-09-04 山东焦点生物科技股份有限公司 A kind of hyaluronic acid quaternary ammonium radical derivative and its prepare and purify method
CN111714691A (en) * 2020-06-30 2020-09-29 常州大学 Preparation method of antibacterial hydrogel dressing containing imidazolium salt and hyaluronic acid
CN114432182A (en) * 2021-12-24 2022-05-06 广州那比昂生物科技有限公司 Make-up fixing spray with oil control effect and preparation method thereof
CN114886787A (en) * 2022-06-02 2022-08-12 杭州配方师科技有限公司 Oil control essence and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106074214A (en) * 2016-07-13 2016-11-09 袁春华 A kind of preparation method of the anti-aging facial film of radioprotective
CN108484794A (en) * 2018-03-17 2018-09-04 山东焦点生物科技股份有限公司 A kind of hyaluronic acid quaternary ammonium radical derivative and its prepare and purify method
CN111714691A (en) * 2020-06-30 2020-09-29 常州大学 Preparation method of antibacterial hydrogel dressing containing imidazolium salt and hyaluronic acid
CN114432182A (en) * 2021-12-24 2022-05-06 广州那比昂生物科技有限公司 Make-up fixing spray with oil control effect and preparation method thereof
CN114886787A (en) * 2022-06-02 2022-08-12 杭州配方师科技有限公司 Oil control essence and preparation method thereof

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