CN117257709A - Gum protecting and whitening tooth paste composition and preparation method thereof - Google Patents
Gum protecting and whitening tooth paste composition and preparation method thereof Download PDFInfo
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- CN117257709A CN117257709A CN202311442250.6A CN202311442250A CN117257709A CN 117257709 A CN117257709 A CN 117257709A CN 202311442250 A CN202311442250 A CN 202311442250A CN 117257709 A CN117257709 A CN 117257709A
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- paste composition
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- whitening tooth
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- 230000002087 whitening effect Effects 0.000 title claims abstract description 46
- 239000000606 toothpaste Substances 0.000 title claims abstract description 39
- 229940034610 toothpaste Drugs 0.000 title claims abstract description 39
- 239000000203 mixture Substances 0.000 title claims abstract description 33
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- ZAKOWWREFLAJOT-CEFNRUSXSA-N D-alpha-tocopherylacetate Chemical compound CC(=O)OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-CEFNRUSXSA-N 0.000 claims abstract description 37
- 210000004195 gingiva Anatomy 0.000 claims abstract description 25
- 244000144730 Amygdalus persica Species 0.000 claims abstract description 18
- 235000006040 Prunus persica var persica Nutrition 0.000 claims abstract description 18
- 229940042585 tocopherol acetate Drugs 0.000 claims abstract description 16
- 235000008331 Pinus X rigitaeda Nutrition 0.000 claims abstract description 15
- 235000011613 Pinus brutia Nutrition 0.000 claims abstract description 15
- 241000018646 Pinus brutia Species 0.000 claims abstract description 15
- 241000241413 Propolis Species 0.000 claims abstract description 15
- 150000002978 peroxides Chemical class 0.000 claims abstract description 15
- 229940069949 propolis Drugs 0.000 claims abstract description 15
- 229940111630 tea tree oil Drugs 0.000 claims abstract description 15
- 239000010677 tea tree oil Substances 0.000 claims abstract description 15
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229930003427 Vitamin E Natural products 0.000 claims abstract description 4
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229940046009 vitamin E Drugs 0.000 claims abstract description 4
- 239000011709 vitamin E Substances 0.000 claims abstract description 4
- 235000019165 vitamin E Nutrition 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 24
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 21
- ZAKOWWREFLAJOT-UHFFFAOYSA-N d-alpha-Tocopheryl acetate Natural products CC(=O)OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-UHFFFAOYSA-N 0.000 claims description 15
- FOYKKGHVWRFIBD-UHFFFAOYSA-N gamma-tocopherol acetate Natural products CC(=O)OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1 FOYKKGHVWRFIBD-UHFFFAOYSA-N 0.000 claims description 15
- 239000000084 colloidal system Substances 0.000 claims description 14
- CKZZREIPBTYJEQ-UHFFFAOYSA-N Totarol Natural products C1CC2C(C)(C)CCCC2(C)C2=C1C(C(C)C)=C(C)C=C2 CKZZREIPBTYJEQ-UHFFFAOYSA-N 0.000 claims description 13
- ZRVDANDJSTYELM-FXAWDEMLSA-N totarol Chemical compound CC([C@@H]1CC2)(C)CCC[C@]1(C)C1=C2C(C(C)C)=C(O)C=C1 ZRVDANDJSTYELM-FXAWDEMLSA-N 0.000 claims description 13
- 229940074347 totarol Drugs 0.000 claims description 13
- ZRVDANDJSTYELM-UHFFFAOYSA-N trans-totarol Natural products C1CC2C(C)(C)CCCC2(C)C2=C1C(C(C)C)=C(O)C=C2 ZRVDANDJSTYELM-UHFFFAOYSA-N 0.000 claims description 13
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 12
- CVHZOJJKTDOEJC-UHFFFAOYSA-N saccharin Chemical compound C1=CC=C2C(=O)NS(=O)(=O)C2=C1 CVHZOJJKTDOEJC-UHFFFAOYSA-N 0.000 claims description 8
- 229940081974 saccharin Drugs 0.000 claims description 8
- 235000019204 saccharin Nutrition 0.000 claims description 8
- 239000000901 saccharin and its Na,K and Ca salt Substances 0.000 claims description 8
- 238000009849 vacuum degassing Methods 0.000 claims description 6
- 239000006072 paste Substances 0.000 claims description 5
- 239000000853 adhesive Substances 0.000 claims description 3
- 230000001070 adhesive effect Effects 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 239000003906 humectant Substances 0.000 claims description 3
- 239000004615 ingredient Substances 0.000 claims 6
- 230000007794 irritation Effects 0.000 abstract description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 18
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 12
- 239000000499 gel Substances 0.000 description 7
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 7
- 239000001267 polyvinylpyrrolidone Substances 0.000 description 7
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 239000004354 Hydroxyethyl cellulose Substances 0.000 description 4
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 description 4
- 229920002565 Polyethylene Glycol 400 Polymers 0.000 description 4
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 230000000295 complement effect Effects 0.000 description 3
- 235000019982 sodium hexametaphosphate Nutrition 0.000 description 3
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 3
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 2
- 229920002125 Sokalan® Polymers 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 229960001631 carbomer Drugs 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 description 2
- AQLJVWUFPCUVLO-UHFFFAOYSA-N urea hydrogen peroxide Chemical compound OO.NC(N)=O AQLJVWUFPCUVLO-UHFFFAOYSA-N 0.000 description 2
- UZJGVXSQDRSSHU-UHFFFAOYSA-N 6-(1,3-dioxoisoindol-2-yl)hexaneperoxoic acid Chemical compound C1=CC=C2C(=O)N(CCCCCC(=O)OO)C(=O)C2=C1 UZJGVXSQDRSSHU-UHFFFAOYSA-N 0.000 description 1
- WINXNKPZLFISPD-UHFFFAOYSA-M Saccharin sodium Chemical compound [Na+].C1=CC=C2C(=O)[N-]S(=O)(=O)C2=C1 WINXNKPZLFISPD-UHFFFAOYSA-M 0.000 description 1
- 239000004098 Tetracycline Substances 0.000 description 1
- 241001122767 Theaceae Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004061 bleaching Methods 0.000 description 1
- 229940078916 carbamide peroxide Drugs 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 239000003479 dental cement Substances 0.000 description 1
- VTIIJXUACCWYHX-UHFFFAOYSA-L disodium;carboxylatooxy carbonate Chemical compound [Na+].[Na+].[O-]C(=O)OOC([O-])=O VTIIJXUACCWYHX-UHFFFAOYSA-L 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 235000013350 formula milk Nutrition 0.000 description 1
- 229960002163 hydrogen peroxide Drugs 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 210000000214 mouth Anatomy 0.000 description 1
- 238000006864 oxidative decomposition reaction Methods 0.000 description 1
- 230000019612 pigmentation Effects 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 229940045872 sodium percarbonate Drugs 0.000 description 1
- 229960002180 tetracycline Drugs 0.000 description 1
- 229930101283 tetracycline Natural products 0.000 description 1
- 235000019364 tetracycline Nutrition 0.000 description 1
- 150000003522 tetracyclines Chemical class 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/347—Phenols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9755—Gymnosperms [Coniferophyta]
- A61K8/9767—Pinaceae [Pine family], e.g. pine or cedar
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Zoology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Emergency Medicine (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to the technical field of a gum-protecting and whitening tooth paste composition, in particular to a gum-protecting and whitening tooth paste composition which comprises a whitening component containing peroxide and a gum-protecting component for protecting gums, wherein the gum-protecting component is one or more of tocopherol acetate (vitamin E), pine needle extract, propolis extract, peach toposide and tea tree oil. Also relates to a preparation method of the gingiva protecting and whitening tooth paste composition. The components which protect the gums and have stable properties in the whitening tooth paste (gel) are added into the whitening tooth paste, so that the irritation of peroxide to the gums is reduced.
Description
Technical Field
The invention relates to the technical field of a gingiva protecting and whitening tooth paste composition, in particular to a gingiva protecting and whitening tooth paste composition and a preparation method of the gingiva protecting and whitening tooth paste composition.
Background
It is well known that whitening patches (gels) mainly contain peroxides (e.g. hydrogen peroxide, sodium percarbonate, carbamide peroxide/percarbamide, phthalimido peroxy caproic acid, etc.). When in use, the tooth paste can help to relieve exogenous and endogenous pigmentation (such as smoke stain, tea stain, tetracycline tooth, fluospot tooth, etc.), and the principle is that peroxide in the tooth paste (gel) releases active oxygen to generate oxidative decomposition with coloring matters on the tooth surface and/or in the tooth body, thereby achieving the bleaching effect.
During the use of the whitening strip (gel), active oxygen released by peroxide can also stimulate gingival tissues in the oral cavity, causing gum discomfort and even redness. In order to alleviate the problem that gum tissues are damaged more or less in the using process of the whitening tooth paste (gel), the invention is based on the conventional whitening tooth paste (gel), and particularly adds components which protect gums and are stable in the whitening tooth paste (gel).
Disclosure of Invention
In view of the above problems, there is provided a gingival-care and whitening tooth paste composition comprising a whitening component containing peroxide and a gingival-care component for protecting gums, the gingival-care component being one or more of tocopherol acetate (vitamin E), pine needle extract, propolis extract, totarol and tea tree oil.
Further, the gum-protecting components are used in the following range (weight percent): tocopherol acetate (VE) 0% or 0.05% -0.5%, pine needle extract 0% or 0.05% -1.0%, propolis extract 0% or 0.05% -2.0%, totarol (content 1%) 0% or 0.05% -1.0%, tea tree oil 0% or 0.05% -1.0%.
As a first specific embodiment of a gum-protecting component in a gum-protecting whitening tooth-paste composition: the gum protecting component is tocopherol acetate (VE), pine needle extract and totarol.
Further, the gingiva protection component specifically comprises: tocopheryl acetate: 0.05% -0.3%, pine needle extract: 0.05% -0.5%, and the content of the peach phenol is 1%): 0.05% -0.5%.
As a second specific embodiment of the gingiva care component in the gingiva care whitening tooth paste composition: the gum protecting component is tocopherol acetate (VE), propolis extract and totarol.
Further, the gingiva protection component specifically comprises: tocopheryl acetate: 0.05% -0.5% propolis extract: 0.05% -2.0%, and the content of the peach phenol is 1%): 0.05% -0.5%.
As a third specific embodiment of the gingiva care component in the gingiva care whitening tooth paste composition: the gum protecting component is tocopherol acetate (VE), tea tree oil and totarol.
Further, the gingiva protection component specifically comprises: tocopheryl acetate: 0.05% -0.5%, tea tree oil: 0.05% -1.0%, and the content of the peach phenol is 1%): 0.05% -0.5%.
A preparation method of a gingiva protecting and whitening tooth paste composition comprises the following steps:
firstly, sequentially adding components such as a humectant, an adhesive, a peroxide whitening agent, saccharin and the like in a whitening tooth paste formula, and uniformly stirring (at normal temperature for 20-30 minutes) to obtain a colloid for standby;
step two, adjusting the pH value of the colloid to be used to 5.5-7.5 (or a specified range) by using sodium hydroxide solution, and uniformly stirring for later use;
and thirdly, adding essence and gum protecting components, continuously stirring, and vacuum degassing (15-20 minutes, wherein the vacuum degree reaches-0.092 mPa) to obtain the uniform bubble-free colloid for the dental paste with moderate viscosity.
Compared with the prior art, the invention has the beneficial effects that: the components which protect the gums and have stable properties in the whitening tooth paste (gel) are added into the whitening tooth paste, so that the irritation of peroxide to the gums is reduced.
Detailed Description
A gingival whitening tooth paste composition comprises a whitening component containing peroxide and a gingival protecting component for protecting gingiva, wherein the gingival protecting component is one or more of tocopherol acetate (vitamin E), pine needle extract, propolis extract, peach topolypus and tea tree oil.
The dosage (weight percentage) range of the gingiva protection component is as follows: tocopherol acetate (VE) 0% or 0.05% -0.5%, pine needle extract 0% or 0.05% -1.0%, propolis extract 0% or 0.05% -2.0%, totarol (content 1%) 0% or 0.05% -1.0%, tea tree oil 0% or 0.05% -1.0%.
As a first specific embodiment of a gum-protecting component in a gum-protecting whitening tooth-paste composition: the gum protecting component is tocopherol acetate (VE), pine needle extract and totarol.
Further, the gingiva protection component specifically comprises: tocopheryl acetate: 0.05% -0.3%, pine needle extract: 0.05% -0.5%, and the content of the peach phenol is 1%): 0.05% -0.5%.
Embodiment one: (the following are weight percentages)
Polyvinylpyrrolidone: 0.2% -2.5%;
carbomer: 0.5% -1.5%;
hydrogen peroxide (30%): 2-5%;
tocopheryl acetate: 0.05-0.3%;
pine needle extract: 0.05% -0.5%;
peach tricuspid (content 1%): 0.05% -0.5%;
sodium hexametaphosphate: 0.2% -3.0%;
saccharin: 0.2%;
essence: 0.3%;
sodium hydroxide: a proper amount of the components;
glycerol: 40-60%;
PEG-400: the complement is 100.0 percent.
In the above formula, polyvinylpyrrolidone and sodium hexametaphosphate can form water-soluble complex with exogenous stain, or loosen dental stain to separate from tooth surface, and the peroxide content in the above formula should be less than or equal to 3.0% (H in presence or release) 2 O 2 Meter).
The preparation process comprises the following steps: adding glycerol, stirring, adding polyvinylpyrrolidone and carbomer, stirring, adding PEG-400, and stirring. Adding saccharin, sodium hexametaphosphate and hydrogen peroxide, stirring at normal temperature for 20-30 min, adjusting the pH value of the colloid to 5.5-7.5 (or a specified range) with sodium hydroxide solution, adding essence and a composition (tocopherol acetate, pine needle extract and peach phenol) for protecting gums after stirring uniformly, continuing stirring and vacuum degassing (15-20 min, vacuum degree reaching-0.092 mPa), and obtaining the uniform bubble-free dental adhesive colloid with moderate viscosity.
As a second specific embodiment of the gingiva care component in the gingiva care whitening tooth paste composition: the gum protecting component is tocopherol acetate (VE), propolis extract and totarol.
Further, the gingiva protection component specifically comprises: tocopheryl acetate: 0.05% -0.5% propolis extract: 0.05% -2.0%, and the content of the peach phenol is 1%): 0.05% -0.5%.
Embodiment two: (the following are weight percentages)
Polyvinylpyrrolidone: 15% -20%;
hydrogen peroxide (30%): 2% -6%;
tocopheryl acetate: 0.05% -0.5%;
propolis extract: 0.05% -2.0%;
peach tricuspid (content 1%): 0.05% -0.5%;
saccharin: 0.2%;
essence: 0.3%;
sodium hydroxide: a proper amount of the components;
hydroxyethyl cellulose: 0.3% -1%;
glycerol: 40%;
PEG-400: the complement is 100.0 percent.
The peroxide is used in the above formulation in an amount of 3.0% or less (H present or released in the form of a mixture) 2 O 2 Meter).
The preparation process comprises the following steps: adding glycerol, adding hydroxyethyl cellulose and polyvinylpyrrolidone under stirring, adding PEG-400, and stirring. Adding saccharin and hydrogen peroxide, stirring at normal temperature for 20-30 min, adjusting the pH value of the colloid to 5.5-7.5 (or a specified range) with sodium hydroxide solution, stirring uniformly, adding essence and composition for protecting gum (tocopherol acetate, propolis extract and peach phenol), stirring continuously, and vacuum degassing (15-20 min, vacuum degree reaching-0.092 mPa), to obtain uniform bubble-free colloid for dental paste with moderate viscosity.
As a third specific embodiment of the gingiva care component in the gingiva care whitening tooth paste composition: the gum protecting component is tocopherol acetate (VE), tea tree oil and totarol.
Further, the gingiva protection component specifically comprises: tocopheryl acetate: 0.05% -0.5%, tea tree oil: 0.05% -1.0%, and the content of the peach phenol is 1%): 0.05% -0.5%.
Embodiment III: (the following are weight percentages)
Polyvinylpyrrolidone: 0.5% -2.5%;
hydrogen peroxide (30%): 1.0% -5.0%;
glycerol: 15% -25%;
hydroxyethyl cellulose: 0.5% -2.5%;
ethanol: 0.5% -8%;
tocopheryl acetate: 0.05% -0.5%;
tea tree oil: 0.05% -1.0%;
peach tricuspid (content 1%): 0.05% -0.5%;
saccharin: 0.2%;
essence: 0.3%;
water: complement to 100.0%;
in order to protect the teeth and gums, the peroxide should be used in an amount of 3.0% or less (based on H2O2 present or released) in the above formulation.
The preparation process comprises the following steps: adding glycerol, adding hydroxyethyl cellulose and polyvinylpyrrolidone under stirring, adding ethanol and water, and stirring. Adding saccharin water solution (dissolved in proper amount of water in advance) and hydrogen peroxide, stirring at normal temperature for 20-30 min, adding essence and composition for protecting gum (tocopherol acetate, tea tree oil and peach phenol), stirring continuously, and vacuum degassing (15-20 min, vacuum degree reaching-0.092 mPa), to obtain uniform bubble-free colloid for dental paste with moderate viscosity.
A preparation method of a gingiva protecting and whitening tooth paste composition, which comprises the following steps:
firstly, sequentially adding components such as a humectant, an adhesive, a peroxide whitening agent, saccharin and the like in a whitening tooth paste formula, and uniformly stirring (at normal temperature for 20-30 minutes) to obtain a colloid for standby;
step two, adjusting the pH value of the colloid to be used to 5.5-7.5 (or a specified range) by using sodium hydroxide solution, and uniformly stirring for later use;
and thirdly, adding essence and gum protecting components, continuously stirring, and vacuum degassing (15-20 minutes, wherein the vacuum degree reaches-0.092 mPa) to obtain the uniform bubble-free colloid for the dental paste with moderate viscosity.
The foregoing examples merely illustrate one or more embodiments of the invention, which are described in greater detail and are not to be construed as limiting the scope of the invention. It should be noted that it will be apparent to those skilled in the art that several variations and modifications can be made without departing from the spirit of the invention, which are all within the scope of the invention. Accordingly, the scope of the invention should be assessed as that of the appended claims.
Claims (9)
1. A gum-protecting and whitening tooth paste composition is characterized by comprising a whitening component containing peroxide and a gum-protecting component for protecting gums, wherein the gum-protecting component is one or more of tocopherol acetate (vitamin E), pine needle extract, propolis extract, peach topol and tea tree oil.
2. The gingiva care and whitening tooth paste composition according to claim 1, wherein the amount of the gingiva care component (weight percent) is in the range of: tocopherol acetate (VE) 0% or 0.05% -0.5%, pine needle extract 0% or 0.05% -1.0%, propolis extract 0% or 0.05% -2.0%, totarol (content 1%) 0% or 0.05% -1.0%, tea tree oil 0% or 0.05% -1.0%.
3. A gum protecting and whitening tooth paste composition according to claim 2, wherein the gum protecting ingredients are tocopheryl acetate (VE) and pine needle extract and totarol.
4. A gingival whitening tooth paste composition according to claim 3, wherein the gingival care ingredients are specifically: tocopheryl acetate: 0.05% -0.3%, pine needle extract: 0.05% -0.5%, and the content of the peach phenol is 1%): 0.05% -0.5%.
5. A gum-protecting whitening tooth-paste composition according to claim 2, wherein the gum-protecting ingredients are tocopheryl acetate (VE) and propolis extract and totarol.
6. The gum-protecting and whitening tooth-paste composition according to claim 5, wherein the gum-protecting ingredients are specifically: tocopheryl acetate: 0.05% -0.5% propolis extract: 0.05% -2.0%, and the content of the peach phenol is 1%): 0.05% -0.5%.
7. A gum care and whitening tooth paste composition according to claim 2, wherein the gum care ingredients are tocopheryl acetate (VE) and tea tree oil and totarol.
8. The gum-protecting and whitening tooth-paste composition according to claim 7, wherein the gum-protecting ingredients are specifically: tocopheryl acetate: 0.05% -0.5%, tea tree oil: 0.05% -1.0%, and the content of the peach phenol is 1%): 0.05% -0.5%.
9. A preparation method of a gingiva protecting and whitening tooth paste composition, which is characterized by comprising the following steps:
firstly, sequentially adding components such as a humectant, an adhesive, a peroxide whitening agent, saccharin and the like in a whitening tooth paste formula, and uniformly stirring (at normal temperature for 20-30 minutes) to obtain a colloid for standby;
step two, adjusting the pH value of the colloid to be used to 5.5-7.5 (or a specified range) by using sodium hydroxide solution, and uniformly stirring for later use;
and thirdly, adding essence and gum protecting components, continuously stirring, and vacuum degassing (15-20 minutes, wherein the vacuum degree reaches-0.092 mPa) to obtain the uniform bubble-free colloid for the dental paste with moderate viscosity.
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