CN117187976A - Preparation method of negative ion artificial fiber cosmetic yarn - Google Patents
Preparation method of negative ion artificial fiber cosmetic yarn Download PDFInfo
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- CN117187976A CN117187976A CN202311193186.2A CN202311193186A CN117187976A CN 117187976 A CN117187976 A CN 117187976A CN 202311193186 A CN202311193186 A CN 202311193186A CN 117187976 A CN117187976 A CN 117187976A
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- polybutylene terephthalate
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- 239000002537 cosmetic Substances 0.000 title claims abstract description 87
- 229920002994 synthetic fiber Polymers 0.000 title claims abstract description 63
- 238000002360 preparation method Methods 0.000 title claims abstract description 39
- 229920001707 polybutylene terephthalate Polymers 0.000 claims abstract description 107
- -1 polybutylene terephthalate Polymers 0.000 claims abstract description 60
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 58
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims abstract description 58
- 239000007822 coupling agent Substances 0.000 claims abstract description 41
- 150000001450 anions Chemical class 0.000 claims abstract description 37
- 241001474374 Blennius Species 0.000 claims abstract description 31
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 31
- 239000003242 anti bacterial agent Substances 0.000 claims abstract description 29
- 239000011347 resin Substances 0.000 claims abstract description 29
- 229920005989 resin Polymers 0.000 claims abstract description 29
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 29
- 239000011787 zinc oxide Substances 0.000 claims abstract description 29
- 235000012239 silicon dioxide Nutrition 0.000 claims abstract description 18
- 150000002500 ions Chemical class 0.000 claims abstract description 17
- 238000003756 stirring Methods 0.000 claims abstract description 17
- 238000002156 mixing Methods 0.000 claims abstract description 15
- 239000000463 material Substances 0.000 claims abstract description 5
- 238000002074 melt spinning Methods 0.000 claims abstract description 3
- 239000004594 Masterbatch (MB) Substances 0.000 claims description 28
- 238000000034 method Methods 0.000 claims description 7
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 238000009987 spinning Methods 0.000 claims description 3
- 238000007909 melt granulation Methods 0.000 claims description 2
- 239000002245 particle Substances 0.000 claims description 2
- 229920000297 Rayon Polymers 0.000 claims 1
- 125000000129 anionic group Chemical group 0.000 claims 1
- 239000002964 rayon Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 5
- 238000012423 maintenance Methods 0.000 abstract description 3
- 238000002844 melting Methods 0.000 abstract description 2
- 230000008018 melting Effects 0.000 abstract description 2
- 230000003115 biocidal effect Effects 0.000 abstract 1
- 230000002045 lasting effect Effects 0.000 abstract 1
- 239000004753 textile Substances 0.000 abstract 1
- 239000002994 raw material Substances 0.000 description 15
- 230000000844 anti-bacterial effect Effects 0.000 description 14
- 238000010035 extrusion spinning Methods 0.000 description 12
- 239000000835 fiber Substances 0.000 description 7
- 210000002268 wool Anatomy 0.000 description 4
- 241000894006 Bacteria Species 0.000 description 3
- 241001465754 Metazoa Species 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 230000004071 biological effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 230000001877 deodorizing effect Effects 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 210000004709 eyebrow Anatomy 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 210000000653 nervous system Anatomy 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
Abstract
The application relates to the field of textile materials, and particularly discloses an anion artificial fiber cosmetic yarn and a preparation method thereof, wherein the anion artificial fiber cosmetic yarn comprises two components: the component A is 50-70 parts of polybutylene terephthalate (PBT) resin, 10-20 parts of nano zinc oxide, 5-10 parts of nano seaweed carbon powder, 5-10 parts of silicon dioxide, 1-3 parts of antibacterial agent and 1-5 parts of coupling agent, and the component B is a polybutylene terephthalate (PBT) slice. The mixing ratio of the component A to the component B is 1:3-5. The preparation method comprises the steps of putting the dried A-component material into a high-speed stirrer according to a certain proportion, uniformly stirring, granulating in a melting way through a double-screw basic machine, uniformly stirring with polybutylene terephthalate slices according to a certain proportion, and carrying out melt spinning to obtain the artificial fiber cosmetic yarn. The negative ion artificial fiber cosmetic filament provided by the application can be used for lasting antibiosis and releasing negative ions, and has good effects on maintenance and cosmetic hygiene of a human body.
Description
Background
The cosmetic brush is one of the most commonly used cosmetic tools in the field of cosmetic, and concretely comprises an eye shadow brush, a blush brush, a face-repairing brush, a eyebrow brush, a lip brush and the like, and comprises a brush head and a brush head, wherein the brush head consists of cosmetic filaments, the cosmetic brushes with different usage have different performance requirements on the cosmetic filaments, and when in cosmetic, the face-repairing brush can be used for dipping the cosmetic with the brush head and completing the face-repairing at a cosmetic position.
The negative ions are called as vitamins in the air, have important biological effects on human bodies, can stimulate the nervous system to generate good response, improve the immunity, promote health and the like. The anion fiber has excellent physical and chemical properties, has the functions of purifying air, inhibiting bacteria and deodorizing, and has important functions in environmental protection and health care because the anion fiber can release anions for a long time. The cosmetic silk prepared from the anion fiber can be used for resisting bacteria and releasing anions for a long time, and has good effects on the maintenance of human bodies and the sanitation of cosmetics.
At present, the main raw materials of the cosmetic filaments in the cosmetic brush comprise artificial wool fibers and animal wool fibers, wherein the animal wool fibers have good performance, but a large amount of animal wool fibers are used for manufacturing the cosmetic filaments, which is not beneficial to the protection of ecological environment, so that the research of the cosmetic brush filaments with good softness and powder grabbing force is particularly important.
Disclosure of Invention
The application provides a preparation method of an anion artificial fiber cosmetic silk, which adopts the following technical scheme:
an anion artificial fiber cosmetic silk is composed of two components: the component A is 50-70 parts of polybutylene terephthalate (PBT) resin, 10-20 parts of nano zinc oxide, 5-10 parts of nano seaweed carbon powder, 5-10 parts of silicon dioxide, 1-3 parts of antibacterial agent and 1-5 parts of coupling agent, and the component B is a polybutylene terephthalate (PBT) slice. The mixing ratio of the component A to the component B is 1:3-5
The application provides a preparation method of an anion artificial fiber cosmetic silk for solving the problems, which comprises the following steps:
and (3) placing the dried component A material into a high-speed stirrer according to a certain proportion, uniformly stirring, and carrying out melt granulation by a double-screw basic machine to obtain master batch.
And uniformly stirring the master batch A and the polybutylene terephthalate slice according to a certain proportion, and carrying out melt spinning to obtain the artificial fiber cosmetic yarn.
As a preferred embodiment of the method for producing a negative ion artificial fiber cosmetic filament of the present application, the granulation temperature is 230 to 270 ℃.
As a preferred embodiment of the method for preparing the negative ion artificial fiber cosmetic filament, the spinning temperature is 250-280 ℃.
As a preferable scheme of the preparation method of the negative ion artificial fiber cosmetic filament, the preparation method comprises the following raw materials in parts by weight:
and (3) a component A: 50-70 parts of polybutylene terephthalate (PBT) resin,
10-20 parts of nano zinc oxide,
5-10 parts of nano seaweed carbon powder,
5-10 parts of silicon dioxide
1-3 parts of antibacterial agent,
1-5 parts of a coupling agent,
and the component B comprises the following components: polybutylene terephthalate (PBT) slice.
By adopting the technical scheme, under the range, each performance of the cosmetic yarn is excellent, and meanwhile, the antibacterial performance of the cosmetic yarn is good.
As a preferable scheme of the preparation method of the negative ion artificial fiber cosmetic filament, the proportion of the component A to the component B is 1:3-5
As a preferable scheme of the preparation method of the negative ion artificial fiber cosmetic yarn, the viscosity [ eta ] =0.960 dL/g of the PBT slice
As a preferable scheme of the preparation method of the anion artificial fiber cosmetic filament, the particle size of the nano seaweed carbon powder is 100-300 nanometers.
Compared with the prior art, the application has the following beneficial effects:
the negative ion artificial fiber cosmetic filament provided by the application can be used for resisting bacteria and releasing negative ions for a long time, and has good effects on maintenance and cosmetic hygiene of a human body.
The specific embodiment is as follows:
in order that the above-recited objects, features and advantages of the present application will become more apparent, a more particular description of the application will be rendered by reference to specific embodiments thereof which are illustrated in the appended drawings.
In the following description, numerous specific details are set forth in order to provide a thorough understanding of the present application, but the present application may be practiced in other ways other than those described herein, and persons skilled in the art will readily appreciate that the present application is not limited to the specific embodiments disclosed below.
Further, reference herein to "one embodiment" or "an embodiment" means that a particular feature, structure, or characteristic can be included in at least one implementation of the application. The appearances of the phrase "in one embodiment" in various places in the specification are not necessarily all referring to the same embodiment, nor are separate or alternative embodiments mutually exclusive of other embodiments.
Unless otherwise indicated, all starting materials used in the examples were commercially available.
Embodiment one:
the preparation method of the anion artificial fiber cosmetic yarn comprises the following raw materials in parts by mass:
and (3) a component A: 70 parts of polybutylene terephthalate (PBT) resin,
15 parts of nano zinc oxide,
5 parts of nano seaweed carbon powder,
Silica 5 parts
2 parts of antibacterial agent,
3 parts of a coupling agent, namely a coupling agent,
and the component B comprises the following components: polybutylene terephthalate (PBT) slice.
A preparation method of anion artificial fiber cosmetic silk, which comprises the following steps:
step one: polybutylene terephthalate (PBT) resin, nano zinc oxide, nano seaweed carbon powder, silicon dioxide, an antibacterial agent and a coupling agent are put into a high-speed stirrer to be stirred uniformly, and melted and granulated by a double-screw basic machine at the temperature of 250 ℃ to obtain master batch.
Step two: and (3) taking 1 part of the master batch prepared in the step one, uniformly stirring with 2 parts of polybutylene terephthalate slices, carrying out melt blending, and carrying out extrusion spinning at 260 ℃ to obtain the antibacterial artificial fiber cosmetic yarn.
Embodiment two:
the preparation method of the anion artificial fiber cosmetic yarn comprises the following raw materials in parts by mass:
and (3) a component A: 50 parts of polybutylene terephthalate (PBT) resin,
15 parts of nano zinc oxide,
5 parts of nano seaweed carbon powder,
Silica 5 parts
2 parts of antibacterial agent,
3 parts of a coupling agent, namely a coupling agent,
and the component B comprises the following components: polybutylene terephthalate (PBT) slice.
A preparation method of anion artificial fiber cosmetic silk, which comprises the following steps:
step one: polybutylene terephthalate (PBT) resin, nano zinc oxide, nano seaweed carbon powder, silicon dioxide, an antibacterial agent and a coupling agent are put into a high-speed stirrer to be stirred uniformly, and melted and granulated by a double-screw basic machine at the temperature of 250 ℃ to obtain master batch.
Step two: and (3) taking 1 part of the master batch prepared in the step one, uniformly stirring with 2 parts of polybutylene terephthalate slices, carrying out melt blending, and carrying out extrusion spinning at 260 ℃ to obtain the antibacterial artificial fiber cosmetic yarn.
Embodiment III:
the preparation method of the anion artificial fiber cosmetic yarn comprises the following raw materials in parts by mass:
and (3) a component A: 60 parts of polybutylene terephthalate (PBT) resin,
15 parts of nano zinc oxide,
5 parts of nano seaweed carbon powder,
Silica 5 parts
2 parts of antibacterial agent,
3 parts of a coupling agent, namely a coupling agent,
and the component B comprises the following components: polybutylene terephthalate (PBT) slice.
A preparation method of anion artificial fiber cosmetic silk, which comprises the following steps:
step one: polybutylene terephthalate (PBT) resin, nano zinc oxide, nano seaweed carbon powder, silicon dioxide, an antibacterial agent and a coupling agent are put into a high-speed stirrer to be stirred uniformly, and melted and granulated by a double-screw basic machine at the temperature of 250 ℃ to obtain master batch.
Step two: and (3) taking 1 part of the master batch prepared in the step one, uniformly stirring with 2 parts of polybutylene terephthalate slices, carrying out melt blending, and carrying out extrusion spinning at 260 ℃ to obtain the antibacterial artificial fiber cosmetic yarn.
Embodiment four:
the preparation method of the anion artificial fiber cosmetic yarn comprises the following raw materials in parts by mass:
and (3) a component A: 70 parts of polybutylene terephthalate (PBT) resin,
10 parts of nano zinc oxide,
5 parts of nano seaweed carbon powder,
Silica 5 parts
2 parts of antibacterial agent,
3 parts of a coupling agent, namely a coupling agent,
and the component B comprises the following components: polybutylene terephthalate (PBT) slice.
A preparation method of anion artificial fiber cosmetic silk, which comprises the following steps:
step one: polybutylene terephthalate (PBT) resin, nano zinc oxide, nano seaweed carbon powder, silicon dioxide, an antibacterial agent and a coupling agent are put into a high-speed stirrer to be stirred uniformly, and melted and granulated by a double-screw basic machine at the temperature of 250 ℃ to obtain master batch.
Step two: and (3) taking 1 part of the master batch prepared in the step one, uniformly stirring with 2 parts of polybutylene terephthalate slices, carrying out melt blending, and carrying out extrusion spinning at 260 ℃ to obtain the antibacterial artificial fiber cosmetic yarn.
Fifth embodiment:
the preparation method of the anion artificial fiber cosmetic yarn comprises the following raw materials in parts by mass:
and (3) a component A: 70 parts of polybutylene terephthalate (PBT) resin,
20 parts of nano zinc oxide,
5 parts of nano seaweed carbon powder,
Silica 5 parts
2 parts of antibacterial agent,
3 parts of a coupling agent, namely a coupling agent,
and the component B comprises the following components: polybutylene terephthalate (PBT) slice.
A preparation method of anion artificial fiber cosmetic silk, which comprises the following steps:
step one: polybutylene terephthalate (PBT) resin, nano zinc oxide, nano seaweed carbon powder, silicon dioxide, an antibacterial agent and a coupling agent are put into a high-speed stirrer to be stirred uniformly, and melted and granulated by a double-screw basic machine at the temperature of 250 ℃ to obtain master batch.
Step two: and (3) taking 1 part of the master batch prepared in the step one, uniformly stirring with 2 parts of polybutylene terephthalate slices, carrying out melt blending, and carrying out extrusion spinning at 260 ℃ to obtain the antibacterial artificial fiber cosmetic yarn.
Example six:
the preparation method of the anion artificial fiber cosmetic yarn comprises the following raw materials in parts by mass:
and (3) a component A: 70 parts of polybutylene terephthalate (PBT) resin,
15 parts of nano zinc oxide,
5 parts of nano seaweed carbon powder,
10 parts of silicon dioxide
2 parts of antibacterial agent,
3 parts of a coupling agent, namely a coupling agent,
and the component B comprises the following components: polybutylene terephthalate (PBT) slice.
A preparation method of anion artificial fiber cosmetic silk, which comprises the following steps:
step one: polybutylene terephthalate (PBT) resin, nano zinc oxide, nano seaweed carbon powder, silicon dioxide, an antibacterial agent and a coupling agent are put into a high-speed stirrer to be stirred uniformly, and melted and granulated by a double-screw basic machine at the temperature of 250 ℃ to obtain master batch.
Step two: and (3) taking 1 part of the master batch prepared in the step one, uniformly stirring with 2 parts of polybutylene terephthalate slices, carrying out melt blending, and carrying out extrusion spinning at 260 ℃ to obtain the antibacterial artificial fiber cosmetic yarn.
Embodiment seven:
the preparation method of the anion artificial fiber cosmetic yarn comprises the following raw materials in parts by mass:
and (3) a component A: 70 parts of polybutylene terephthalate (PBT) resin,
15 parts of nano zinc oxide,
5 parts of nano seaweed carbon powder,
Silica 5 parts
2 parts of antibacterial agent,
3 parts of a coupling agent, namely a coupling agent,
and the component B comprises the following components: polybutylene terephthalate (PBT) slice.
A preparation method of anion artificial fiber cosmetic silk, which comprises the following steps:
step one: polybutylene terephthalate (PBT) resin, nano zinc oxide, nano seaweed carbon powder, silicon dioxide, an antibacterial agent and a coupling agent are put into a high-speed stirrer to be stirred uniformly, and melted and granulated by a double-screw basic machine at the temperature of 250 ℃ to obtain master batch.
Step two: and 1 part of the master batch prepared in the first step and 1 part of polybutylene terephthalate slice are uniformly stirred, melt blending is carried out, extrusion spinning is carried out at 260 ℃ to obtain the antibacterial artificial fiber cosmetic yarn.
Example eight:
the preparation method of the anion artificial fiber cosmetic yarn comprises the following raw materials in parts by mass:
and (3) a component A: 70 parts of polybutylene terephthalate (PBT) resin,
15 parts of nano zinc oxide,
5 parts of nano seaweed carbon powder,
Silica 5 parts
2 parts of antibacterial agent,
3 parts of a coupling agent, namely a coupling agent,
and the component B comprises the following components: polybutylene terephthalate (PBT) slice.
A preparation method of anion artificial fiber cosmetic silk, which comprises the following steps:
step one: polybutylene terephthalate (PBT) resin, nano zinc oxide, nano seaweed carbon powder, silicon dioxide, an antibacterial agent and a coupling agent are put into a high-speed stirrer to be stirred uniformly, and melted and granulated by a double-screw basic machine at the temperature of 250 ℃ to obtain master batch.
Step two: and (3) taking 1 part of the master batch prepared in the step one, uniformly stirring with 5 parts of polybutylene terephthalate slices, carrying out melt blending, and carrying out extrusion spinning at 260 ℃ to obtain the antibacterial artificial fiber cosmetic yarn.
Example nine:
the preparation method of the anion artificial fiber cosmetic yarn comprises the following raw materials in parts by mass:
and (3) a component A: 70 parts of polybutylene terephthalate (PBT) resin,
15 parts of nano zinc oxide,
5 parts of nano seaweed carbon powder,
Silica 5 parts
2 parts of antibacterial agent,
3 parts of a coupling agent, namely a coupling agent,
and the component B comprises the following components: polybutylene terephthalate (PBT) slice.
A preparation method of anion artificial fiber cosmetic silk, which comprises the following steps:
step one: polybutylene terephthalate (PBT) resin, nano zinc oxide, nano seaweed carbon powder, silicon dioxide, an antibacterial agent and a coupling agent are put into a high-speed stirrer to be uniformly stirred, and melted and granulated by a double-screw basic machine at 240 ℃ to obtain master batch.
Step two: and (3) taking 1 part of the master batch prepared in the step one, uniformly stirring with 2 parts of polybutylene terephthalate slices, carrying out melt blending, and carrying out extrusion spinning at 260 ℃ to obtain the antibacterial artificial fiber cosmetic yarn.
Example ten:
the preparation method of the anion artificial fiber cosmetic yarn comprises the following raw materials in parts by mass:
and (3) a component A: 70 parts of polybutylene terephthalate (PBT) resin,
15 parts of nano zinc oxide,
5 parts of nano seaweed carbon powder,
Silica 5 parts
2 parts of antibacterial agent,
3 parts of a coupling agent, namely a coupling agent,
and the component B comprises the following components: polybutylene terephthalate (PBT) slice.
A preparation method of anion artificial fiber cosmetic silk, which comprises the following steps:
step one: polybutylene terephthalate (PBT) resin, nano zinc oxide, nano seaweed carbon powder, silicon dioxide, an antibacterial agent and a coupling agent are put into a high-speed stirrer to be uniformly stirred, and melted and granulated by a double-screw basic machine at 260 ℃ to obtain master batch.
Step two: and (3) taking 1 part of the master batch prepared in the step one, uniformly stirring with 2 parts of polybutylene terephthalate slices, carrying out melt blending, and carrying out extrusion spinning at 260 ℃ to obtain the antibacterial artificial fiber cosmetic yarn.
Example eleven:
the preparation method of the anion artificial fiber cosmetic yarn comprises the following raw materials in parts by mass:
and (3) a component A: 70 parts of polybutylene terephthalate (PBT) resin,
15 parts of nano zinc oxide,
5 parts of nano seaweed carbon powder,
Silica 5 parts
2 parts of antibacterial agent,
3 parts of a coupling agent, namely a coupling agent,
and the component B comprises the following components: polybutylene terephthalate (PBT) slice.
A preparation method of anion artificial fiber cosmetic silk, which comprises the following steps:
step one: polybutylene terephthalate (PBT) resin, nano zinc oxide, nano seaweed carbon powder, silicon dioxide, an antibacterial agent and a coupling agent are put into a high-speed stirrer to be stirred uniformly, and melted and granulated by a double-screw basic machine at the temperature of 250 ℃ to obtain master batch.
Step two: and (3) taking 1 part of the master batch prepared in the step one, uniformly stirring with 2 parts of polybutylene terephthalate slices, carrying out melt blending, and carrying out extrusion spinning at the temperature of 250 ℃ to obtain the antibacterial artificial fiber cosmetic yarn.
Embodiment twelve:
the preparation method of the anion artificial fiber cosmetic yarn comprises the following raw materials in parts by mass:
and (3) a component A: 70 parts of polybutylene terephthalate (PBT) resin,
15 parts of nano zinc oxide,
5 parts of nano seaweed carbon powder,
Silica 5 parts
2 parts of antibacterial agent,
3 parts of a coupling agent, namely a coupling agent,
and the component B comprises the following components: polybutylene terephthalate (PBT) slice.
A preparation method of anion artificial fiber cosmetic silk, which comprises the following steps:
step one: polybutylene terephthalate (PBT) resin, nano zinc oxide, nano seaweed carbon powder, silicon dioxide, an antibacterial agent and a coupling agent are put into a high-speed stirrer to be stirred uniformly, and melted and granulated by a double-screw basic machine at the temperature of 250 ℃ to obtain master batch.
Step two: and (3) taking 1 part of the master batch prepared in the step one, uniformly stirring with 2 parts of polybutylene terephthalate slices, carrying out melt blending, and carrying out extrusion spinning at 270 ℃ to obtain the antibacterial artificial fiber cosmetic yarn.
Performance testing
The artificial cosmetic filaments prepared in examples one to twelve were examined to observe the antibacterial property, the powder-catching rate, the rebound resilience and the negative ion release amount of the artificial fiber cosmetic filaments.
According to the combination of the first to eighth examples, the performance of the finally prepared cosmetic yarn is affected by changing the amounts of the raw materials, and the prepared cosmetic yarn with the best effect is prepared by selecting 70 parts of polybutylene terephthalate (PBT) resin, 15 parts of nano zinc oxide, 5 parts of nano seaweed carbon powder, 5 parts of silicon dioxide, 2 parts of antibacterial agent and 3 parts of coupling agent.
As can be seen from the combination of the first embodiment and the ninth to twelfth embodiments, changing the conditions in the preparation process can change the powder grabbing rate, rebound resilience and other properties of the finally prepared cosmetic filament, while the artificial fiber cosmetic filament obtained by melting the blended yarn at the granulating temperature of 250 ℃ and the spinning temperature of 260 ℃ in the first embodiment has the best effect.
The application discloses a preparation method of an anion artificial fiber cosmetic silk, which comprises the steps of selecting materials and designing process conditions, wherein the specific embodiment is only for explaining the application and is not limiting to the application, and a person skilled in the art can make modifications to the embodiment without creative contribution according to the need after reading the specification, but only the scope of the claims of the application is protected by patent laws.
Claims (7)
1. A preparation method of anion artificial fiber cosmetic silk is characterized in that: consists of two components: the component A is 50-70 parts of polybutylene terephthalate (PBT) resin, 10-20 parts of nano zinc oxide, 5-10 parts of nano seaweed carbon powder, 5-10 parts of silicon dioxide, 1-3 parts of antibacterial agent and 1-5 parts of coupling agent, and the component B is a polybutylene terephthalate (PBT) slice. The mixing ratio of the component A to the component B is 1:3-5.
2. The method for preparing the negative ion artificial fiber cosmetic filament according to claim one, which is characterized in that: the preparation method of the negative ion artificial fiber cosmetic silk comprises the following steps:
(1) And (3) placing the dried component A material into a high-speed stirrer according to a certain proportion, uniformly stirring, and carrying out melt granulation by a double-screw basic machine to obtain master batch.
(2) And uniformly stirring the master batch A and the polybutylene terephthalate slice according to a certain proportion, and carrying out melt spinning to obtain the artificial fiber cosmetic yarn.
3. The method for producing an anionic rayon cosmetic silk according to claim 1, wherein said granulating temperature is 230-270 ℃.
4. The method of claim one, wherein the spinning temperature is 250-280 ℃.
5. The method for preparing the negative ion artificial fiber cosmetic filament according to claim one, which is characterized in that: the ratio of the component A to the component B is 1:3-5.
6. The method for preparing the negative ion artificial fiber cosmetic filament according to claim one, which is characterized in that: the PBT slice viscosity [ eta ] =0.960 dL/g.
7. The method for preparing the negative ion artificial fiber cosmetic filament according to claim one, which is characterized in that: the particle size of the nano seaweed carbon powder is 100-300 nanometers.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202311193186.2A CN117187976A (en) | 2023-09-15 | 2023-09-15 | Preparation method of negative ion artificial fiber cosmetic yarn |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202311193186.2A CN117187976A (en) | 2023-09-15 | 2023-09-15 | Preparation method of negative ion artificial fiber cosmetic yarn |
Publications (1)
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| CN117187976A true CN117187976A (en) | 2023-12-08 |
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Country Status (1)
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