CN116676131A - Lotus-flavored special essence and application thereof in cigarettes - Google Patents
Lotus-flavored special essence and application thereof in cigarettes Download PDFInfo
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- CN116676131A CN116676131A CN202310536710.5A CN202310536710A CN116676131A CN 116676131 A CN116676131 A CN 116676131A CN 202310536710 A CN202310536710 A CN 202310536710A CN 116676131 A CN116676131 A CN 116676131A
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- lotus
- essence
- lotus leaf
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 67
- 240000002853 Nelumbo nucifera Species 0.000 claims abstract description 114
- 235000006508 Nelumbo nucifera Nutrition 0.000 claims abstract description 114
- 235000006510 Nelumbo pentapetala Nutrition 0.000 claims abstract description 114
- 239000000284 extract Substances 0.000 claims abstract description 64
- 239000000796 flavoring agent Substances 0.000 claims abstract description 53
- YEJRWHAVMIAJKC-UHFFFAOYSA-N 4-Butyrolactone Chemical compound O=C1CCCO1 YEJRWHAVMIAJKC-UHFFFAOYSA-N 0.000 claims abstract description 32
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 claims abstract description 24
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 claims abstract description 24
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 claims abstract description 24
- ZRSNZINYAWTAHE-UHFFFAOYSA-N p-methoxybenzaldehyde Chemical compound COC1=CC=C(C=O)C=C1 ZRSNZINYAWTAHE-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000005711 Benzoic acid Substances 0.000 claims abstract description 12
- 235000010233 benzoic acid Nutrition 0.000 claims abstract description 12
- IMKHDCBNRDRUEB-UHFFFAOYSA-N dihydroactinidiolide Chemical compound C1CCC(C)(C)C2=CC(=O)OC21C IMKHDCBNRDRUEB-UHFFFAOYSA-N 0.000 claims abstract description 9
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 claims abstract description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 27
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 24
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 24
- 235000019634 flavors Nutrition 0.000 claims description 24
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 21
- WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 claims description 18
- 239000002904 solvent Substances 0.000 claims description 17
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 claims description 16
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 16
- 239000008103 glucose Substances 0.000 claims description 13
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims description 8
- 229930091371 Fructose Natural products 0.000 claims description 8
- 239000005715 Fructose Substances 0.000 claims description 8
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims description 8
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 8
- 235000021314 Palmitic acid Nutrition 0.000 claims description 8
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 8
- 239000004310 lactic acid Substances 0.000 claims description 8
- 235000014655 lactic acid Nutrition 0.000 claims description 8
- 239000001630 malic acid Substances 0.000 claims description 8
- 235000011090 malic acid Nutrition 0.000 claims description 8
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- UFLHIIWVXFIJGU-ARJAWSKDSA-N (Z)-hex-3-en-1-ol Chemical compound CC\C=C/CCO UFLHIIWVXFIJGU-ARJAWSKDSA-N 0.000 claims description 6
- 235000019445 benzyl alcohol Nutrition 0.000 claims description 6
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 5
- 150000002596 lactones Chemical class 0.000 claims description 3
- 244000061176 Nicotiana tabacum Species 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 16
- 239000002994 raw material Substances 0.000 abstract description 15
- 235000013599 spices Nutrition 0.000 abstract description 2
- 238000011156 evaluation Methods 0.000 description 40
- 239000000779 smoke Substances 0.000 description 38
- 239000003205 fragrance Substances 0.000 description 37
- 230000001953 sensory effect Effects 0.000 description 15
- 230000014759 maintenance of location Effects 0.000 description 8
- 239000000047 product Substances 0.000 description 8
- 235000009508 confectionery Nutrition 0.000 description 7
- 239000002304 perfume Substances 0.000 description 7
- 230000007547 defect Effects 0.000 description 6
- 230000000391 smoking effect Effects 0.000 description 6
- 238000004458 analytical method Methods 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- 241000208125 Nicotiana Species 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 238000000605 extraction Methods 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 239000004480 active ingredient Substances 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000009776 industrial production Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000002253 acid Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000012512 characterization method Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 210000000214 mouth Anatomy 0.000 description 1
- 210000003928 nasal cavity Anatomy 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/36—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a heterocyclic ring
- A24B15/40—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a heterocyclic ring having only oxygen or sulfur as hetero atoms
- A24B15/403—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a heterocyclic ring having only oxygen or sulfur as hetero atoms having only oxygen as hetero atoms
- A24B15/406—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a heterocyclic ring having only oxygen or sulfur as hetero atoms having only oxygen as hetero atoms in a five-membered ring
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0042—Essential oils; Perfumes compounds containing condensed hydrocarbon rings
- C11B9/0046—Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings
- C11B9/0049—Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings the condensed rings sharing two common C atoms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention belongs to the field of essence and spice, and particularly relates to lotus-flavored special essence and application thereof in cigarettes. The lotus-flavored special essence comprises the following components in parts by weight: 1 to 5 parts of gamma-butyrolactone, 1 to 8 parts of caproic acid, 0.1 to 1.4 parts of benzyl alcohol, 0.1 to 2.6 parts of phenethyl alcohol, 1 to 5.2 parts of benzoic acid, 0.1 to 1.3 parts of 4-methoxybenzaldehyde, 2 to 11.5 parts of dihydroactinolide and 0.1 to 0.7 part of phyllitol. The lotus-flavor special essence provided by the invention utilizes food-grade raw materials to prepare lotus-flavor essence capable of having the style of lotus leaf extract, can be applied to cigarette flavoring and cigarette perfuming, and can avoid fluctuation of the quality of the lotus leaf extract of natural fragrant raw materials caused by unstable factors such as lotus leaf variety, planting condition, climate and the like while reducing the use effect of the lotus leaf extract in cigarettes.
Description
Technical Field
The invention belongs to the field of essence and spice, and particularly relates to lotus-flavored special essence and application thereof in cigarettes.
Background
The lotus leaf has the characteristics of delicate fragrance, the sensory odor fragrance comprises green fragrance, faint scent, sweet fragrance, sour fragrance and the like, and the lotus leaf extract can effectively reduce the irritation of smoke, improve the comfort level and the moisture retention and improve the overall quality characteristics of a cigarette product while endowing the cigarette with the fragrance-loading characteristics of the cigarette smoke in the cigarette flavoring.
The Chinese patent application publication No. CN109007740A discloses a preparation method of natural lotus leaf essence by pretreatment of raw materials and supercritical CO 2 Extracting, dissolving and refining to obtain natural extract.
As a natural fragrant raw material, the lotus leaf extract is influenced by a plurality of factors, the fluctuation of the product quality is large, for example, the constraints and the influences of lotus leaf varieties, planting conditions, environmental factors and the like, the fluctuation of the quality can greatly influence the end product, and the influence is not acceptable for industrial production and current standardized commodity supply. In addition, the content of volatile components in the lotus leaf is low, the perfuming effect of the lotus leaf extract processed by the lotus leaf is not obvious, the defects of weak fragrance intensity, short fragrance retention time and the like are obvious, and the essence product capable of comprehensively reducing the fragrance style and the action effect of the lotus leaf is prepared directly through the fragrance mixing experience, so that the lotus leaf essence product is a challenging work.
Disclosure of Invention
The invention aims to provide lotus-flavor special essence, which solves the problems of quality fluctuation and lack of essence extract style of natural-flavor lotus leaf extract.
The second purpose of the invention is to provide the application of the lotus-leaf special essence in cigarettes and solve the defects of the natural lotus leaf extract in the application of cigarettes.
In order to achieve the above purpose, the technical scheme adopted by the invention is as follows:
the lotus-flavored special essence comprises the following components in parts by weight: 1 to 5 parts of gamma-butyrolactone, 1 to 8 parts of caproic acid, 0.1 to 1.4 parts of benzyl alcohol, 0.1 to 2.6 parts of phenethyl alcohol, 1 to 5.2 parts of benzoic acid, 0.1 to 1.3 parts of 4-methoxybenzaldehyde, 2 to 11.5 parts of dihydroactinolide and 0.1 to 0.7 part of phyllitol.
The lotus-flavor special essence provided by the invention utilizes food-grade raw materials to prepare lotus-flavor essence capable of having the style of lotus leaf extract, can be applied to cigarette flavoring and cigarette perfuming, and can avoid fluctuation of the quality of the lotus leaf extract of natural fragrant raw materials caused by unstable factors such as lotus leaf variety, planting condition, climate and the like while reducing the use effect of the lotus leaf extract in cigarettes.
Preferably, the lotus-flavor special essence consists of the following components in parts by weight: 1 to 5 parts of gamma-butyrolactone, 1 to 7 parts of caproic acid, 0.1 to 0.4 part of benzyl alcohol, 0.1 to 0.9 part of phenethyl alcohol, 1 to 3 parts of benzoic acid, 0.1 to 0.6 part of 4-methoxybenzaldehyde, 2 to 6 parts of dihydro-kiwi lactone, 0.1 to 0.5 part of phyllitol, 11 to 22 parts of palmitic acid, 11 to 22 parts of fructose, 10 to 15 parts of glucose, 4 to 7 parts of myose, 2 to 8 parts of lactic acid, 0.1 to 0.8 part of acetic acid, 0.6 to 2.8 parts of malic acid, 0.05 to 0.2 part of citric acid and 10 to 30 parts of solvent. By adopting the optimized formula, all components in the formula are sensory active ingredients in high-quality lotus leaves and lotus leaf extracts, the comfort and the smoke state of the cigarette are obviously improved on the basis of endowing the cigarette with the lotus leaf fragrance and the action style of the smoke of the cigarette, and simultaneously, the sensory negative effect of natural fragrant raw materials in the flavoring process is effectively avoided.
In order to further improve the quality of the fragrance and improve the natural feeling and harmony of the fragrance, preferably, the lotus-fragrance special essence comprises the following components in parts by weight: 1 to 1.3 portions of gamma-butyrolactone; 2 to 2.7 portions of caproic acid; 0.2 to 0.4 part of benzyl alcohol; 0.5 to 0.9 portion of phenethyl alcohol; 1 to 1.8 portions of benzoic acid; 0.2 to 0.4 portion of 4-methoxybenzaldehyde; 3 to 4.0 portions of dihydroactinolide; 0.1 to 0.2 part of leaf alcohol; 15-18.3 parts of palmitic acid; 19-21.8 parts of fructose; 10-12.4 parts of glucose; 5 to 6.3 portions of myo-glucose; 4 to 4.6 portions of lactic acid; 0.3 to 0.5 part of acetic acid; 1 to 1.4 portions of malic acid; 0.05 to 0.1 part of citric acid; 20-22.9 parts of solvent.
To further ensure the stability of the raw materials, the action styles of the components are coordinated, preferably the solvent is selected from one or more of water, ethanol and propylene glycol. In order to further enhance the above effect, it is further preferable that the solvent is composed of water, ethanol and propylene glycol in a mass ratio of (10-15): (1-3).
The lotus-flavored special essence is applied to cigarettes.
When the lotus-flavor special essence is applied to cigarette flavoring and cigarette flavoring, the use effect of the lotus leaf extract in the cigarette can be reduced, the fluctuation of the quality of the lotus leaf extract which is a natural fragrant raw material and is caused by unstable factors such as lotus leaf varieties, planting conditions, climate and the like can be avoided, and meanwhile, the defects of weak fragrance of the lotus leaf extract, short fragrance retention time and the like can be effectively overcome.
Preferably, the lotus-leaf special essence and the lotus-leaf extract are added into the cigarette together. The lotus-flavor special essence can be further used together with the lotus leaf extract to further strengthen the lotus-flavor characteristic of the lotus leaf extract and make up for the shortages of weak fragrance and short fragrance retention time of natural perfume.
More preferably, the weight ratio of the lotus characteristic essence and the lotus leaf extract based on the mass of the gamma-butyrolactone is (1-5): (10-15). By adopting the proportion to perfume the cigarettes, the characteristics, coordination and comfort of the lotus fragrance of the smoke can reach higher level.
Preferably, the flavoring is carried out according to 10-1000 ppm of the weight of the cut tobacco of the cigarette. The cigarette is flavored according to the additive amount, so that the cigarette smoke comfortableness can be correspondingly improved and the smoking quality of the cigarette can be improved while the cigarette is endowed with the fragrance-carrying characteristic.
Drawings
FIG. 1 is a diagram of a radar chart for evaluating the smell of a lotus leaf extract in the invention;
fig. 2 is a diagram of a smell evaluation radar of lotus flavor No. 1 in example 1 of the present invention;
fig. 3 is a smell evaluation radar chart of lotus flavor No. 2 essence in example 2 of the present invention;
fig. 4 is a smell evaluation radar chart of lotus flavor No. 3 in example 3 of the present invention.
Detailed Description
The invention utilizes modern analytical chemistry and food sensory analysis technology, combines the aroma simulation and aroma creation technology in the aroma mixing field on the basis of the lotus leaf extract chemical analysis data, prepares the tobacco essence with lotus aroma characteristics, not only strengthens the aroma style and efficacy of lotus leaves, but also has better coordination effect with smoke, and simultaneously, the essence obviously improves the defects of weak aroma strength, lasting aroma and the like of the lotus leaf extract, and can be used for direct aroma mixing and flavoring of cigarettes, but also strengthening the style of the lotus leaf extract.
Specifically, the lotus-flavored special essence disclosed by the invention comprises the following components in parts by weight: 1 to 5 parts of gamma-butyrolactone, 1 to 7 parts of caproic acid, 0.1 to 0.4 part of benzyl alcohol, 0.1 to 0.9 part of phenethyl alcohol, 1 to 3 parts of benzoic acid, 0.1 to 0.6 part of 4-methoxybenzaldehyde, 2 to 6 parts of dihydro-kiwi lactone, 0.1 to 0.5 part of phyllitol, 11 to 22 parts of palmitic acid, 11 to 22 parts of fructose, 10 to 15 parts of glucose, 4 to 7 parts of myose, 2 to 8 parts of lactic acid, 0.1 to 0.8 part of acetic acid, 0.6 to 2.8 parts of malic acid, 0.05 to 0.2 part of citric acid and 10 to 30 parts of solvent.
In the lotus-flavor special essence, all components of the lotus-flavor essence for cigarettes are food-grade flavors sold in the market, the purity and quality of the product are stable and reliable, and the style characteristics and the quality of the lotus-flavor essence and the stability of cigarette products can be effectively ensured. Meanwhile, as each component in the lotus leaf essence is the sensory active ingredient in the lotus leaf with high quality and the lotus leaf extract, the essence prepared based on the components effectively avoids the sensory negative effect of natural perfume raw materials in the perfuming process on the basis of ensuring the fragrance and action style of the lotus leaf.
Most preferably, the lotus-flavored special essence consists of the following components in parts by weight: 1.2 to 1.3 portions of gamma-butyrolactone; 2.4 to 2.7 parts of caproic acid; 0.3 to 0.4 part of benzyl alcohol; 0.8 to 0.9 portion of phenethyl alcohol; 1.6 to 1.8 portions of benzoic acid; 0.3 to 0.4 portion of 4-methoxybenzaldehyde; 3.6 to 4.0 parts of dihydroactinolide; 0.1 to 0.2 part of leaf alcohol; 16.4 to 18.3 parts of palmitic acid; 19.5 to 21.8 portions of fructose; 11.2 to 12.4 portions of glucose; 5.7-6.3 parts of myo-glucose; 4.1 to 4.6 portions of lactic acid; 0.4 to 0.5 part of acetic acid; 1.2 to 1.4 portions of malic acid; 0.05 to 0.1 part of citric acid; 20.5 to 22.9 portions of solvent.
The lotus-flavor special essence can be further used together with the lotus leaf extract to further strengthen the lotus-flavor characteristic of the lotus leaf extract and make up for the shortages of weak fragrance and short fragrance retention time of natural perfume. Preferably, when the lotus-flavor special essence and the lotus leaf extract are used together, the mass ratio of the lotus-flavor special essence to the lotus leaf extract based on the mass of gamma-butyrolactone is (1-5): (10-15). More preferably, the mass ratio of the lotus-flavor special essence and the lotus leaf extract based on the mass of the gamma-butyrolactone is (1.2-1.3): (10-11).
In short, the invention realizes the blending of lotus-flavor special essence based on the comprehensive chemical analysis data of lotus leaves and lotus leaf extracts for the first time, effectively avoids the defects of natural fragrance raw materials while reducing the aroma and the action effect of the lotus leaves, simultaneously can reduce the cost and ensures the stability and the safety of the product quality.
The following describes the practice of the invention in detail with reference to specific examples.
1. The specific examples of the lotus-flavored special essence of the invention are as follows:
example 1
The lotus-flavor special essence (lotus-flavor No. 1 essence) of the embodiment comprises the following components in parts by weight: 3.8 parts of gamma-butyrolactone; 7.7 parts of caproic acid; benzyl alcohol 1.3 parts; 2.6 parts of phenethyl alcohol; 5.2 parts of benzoic acid; 1.3 parts of 4-methoxybenzaldehyde; 11.5 parts of dihydroactinolide; 0.7 parts of leaf alcohol; 66.1 parts of solvent. Wherein the solvent is a mixture of ethanol, water and propylene glycol, and the mass ratio is 10:1:1.
Example 2
The lotus-flavor special essence (lotus-flavor No. 2 essence) of the embodiment comprises the following components in parts by weight: 1.3 parts of gamma-butyrolactone; 2.7 parts of caproic acid; 0.4 parts of benzyl alcohol; 0.9 part of phenethyl alcohol; 1.8 parts of benzoic acid; 0.4 parts of 4-methoxybenzaldehyde; 4.0 parts of dihydroactinolide; 0.2 parts of leaf alcohol; 18.3 parts of palmitic acid; 21.8 parts of fructose; 12.4 parts of glucose; 6.3 parts of myo-glucose; 4.6 parts of lactic acid; 0.5 parts of acetic acid; 1.4 parts of malic acid; 0.1 part of citric acid; 22.9 parts of solvent. Wherein the solvent is a mixture of ethanol, water and propylene glycol, and the mass ratio is 10:1:1.
Example 3
The lotus-flavor special essence (lotus-flavor No. 3 essence) of the embodiment consists of a recombinant and lotus leaf extract in a mass ratio of 10:1, wherein the recombinant consists of the following components in parts by weight: 1.2 parts of gamma-butyrolactone; 2.4 parts of caproic acid; 0.4 parts of benzyl alcohol; 0.8 parts of phenethyl alcohol; 1.6 parts of benzoic acid; 0.4 parts of 4-methoxybenzaldehyde; 3.6 parts of dihydroactinolide; 0.2 parts of leaf alcohol; 16.4 parts of palmitic acid; 19.5 parts of fructose; 11.2 parts of glucose; 5.7 parts of myo-glucose; 4.1 parts of lactic acid; 0.4 parts of acetic acid; 1.2 parts of malic acid; 0.1 part of citric acid; 20.5 parts of solvent. Wherein the solvent is a mixture of ethanol, water and propylene glycol, and the mass ratio is 10:1:1.
The lotus leaf extract in this example was prepared as follows:
(1) First extraction conditions: cleaning commercially available dried lotus leaves, naturally airing, putting 350g of crushed lotus leaves into a 10L round-bottom flask with a feed liquid ratio of 1:8, adding 2800g of 85% ethanol, placing on a rotary evaporator, heating and extracting at a water temperature of 26.1 ℃ for 19 minutes, then heating to 60 ℃, and extracting for 2 hours to obtain 1673.6g of extracting solution.
(2) Second extraction conditions: the extract was poured out, 2400g of 85% ethanol was added thereto, and the temperature was 60℃and the extraction was carried out for 2 hours, thereby obtaining 2591.5g of an extract.
(3) Concentration conditions: mixing the two extractive solutions, pouring into 1000ml round bottom flask, concentrating on rotary evaporator, controlling temperature at 38deg.C, vacuum degree at 58mbar, and rotation speed at 0.5r/min; after concentrating to 658g, the mixture was transferred to a 500ml round-bottomed flask, the initial temperature was adjusted to 40℃at a speed of 0.5r/min and the concentration was completed when the extract had a viscosity as observed at a vacuum of 48 mbar. 74.2g of concentrate was obtained, and 21.5g of black residue was adhered to the bottle wall at the time of pouring, and the total yield was 21.2%.
2. Application of lotus-flavored special essence in cigarettes
The lotus leaf flavor 1-3 is used for flavoring cigarettes, the cigarettes are flavored according to 100ppm of the weight of tobacco shreds, the cigarettes are balanced in a constant temperature and humidity room for 48 hours and then subjected to sensory evaluation, lotus leaf extracts are added according to the same proportion in comparison with the cigarettes, and the cigarettes are balanced under the same conditions after being flavored.
10 sensory evaluation staff with provincial evaluation staff or more are established to form a cigarette surface aroma evaluation and cigarette smoking evaluation group. Smell evaluation: the evaluation was carried out by the flavor profile method with reference to the methods specified in general theory of sensory analysis methods of GB/T10220-2012/ISO 6658-2005, and the respective indices were scored according to Table 1. And (3) evaluating cigarettes: referring to YC/T496-2014 cigarette sensory comfort evaluation method and YC/T497-2014 cigarette Chinese style sensory evaluation method, sensory evaluation is carried out on cigarettes from three aspects of smoke aroma characteristics, comfort characteristics and smoke characteristics, each index is scored according to the requirements of tables 2, 3 and 4, and the evaluation score range of each index is 0-10 points, wherein the minimum scoring unit is 0.5 point. The final evaluation results gave the average of scores to 10 sensory evaluators.
Table 1 odor evaluation scoring table
Table 2 cigarette smoke aroma characteristic score index
Table 3 cigarette smoke comfort feature score index
Table 4 cigarette smoke characteristic scoring index
(1) Evaluation result of lotus fragrance No. 1 essence
The odor evaluation radar chart of lotus leaf extract obtained by the method is shown in figure 1, and the odor evaluation radar chart of lotus leaf No. 1 essence is shown in figure 2.
The evaluation result shows that the lotus leaf essence No. 1 in the embodiment 1 has a certain aroma style characteristic of the lotus leaf extract in the aspect of smell aroma, wherein green aroma, faint scent, sour aroma and sweet aroma are obvious, the characteristics of the lotus leaf extract can be highlighted in the whole, the whole aroma strength or aroma is higher than that of the lotus leaf extract, however, the quality of the aroma is slightly weaker than that of the lotus leaf extract, and the natural feeling and harmony are not as good as those of the lotus leaf extract.
The smoking evaluation results of the lotus-flavored No. 1 essence flavored cigarettes are shown in Table 5.
Table 5 Smoke scoring table for lotus-flavored No. 1 essence flavored cigarettes
The cigarette evaluation result shows that the lotus leaf flavor 1 essence can endow the cigarette with lotus leaf flavor characteristics, the green aroma, the faint scent and the sweet aroma in the smoke are obvious, meanwhile, the smoke has better coordination with the smoke, the effect of reducing miscellaneous gases and the like, and compared with the lotus leaf extract, the lotus leaf flavor 1 essence has no obvious improvement effect on the state and the comfort level of the smoke.
(2) Evaluation result of lotus fragrance No. 2 essence
The sensory evaluation method is implemented by referring to the evaluation scheme and standard of lotus flavor No. 1 essence, so that the personnel of the evaluation group are ensured to be unchanged. The lotus leaf extract smell evaluation radar chart is shown in fig. 1, and the lotus leaf extract smell evaluation radar chart of lotus leaf No. 2 essence is shown in fig. 3.
The evaluation result shows that the lotus leaf essence No. 2 in the embodiment 2 has a certain aroma style characteristic of the lotus leaf extract in the aspect of smell aroma, wherein green aroma, faint scent, sour aroma and sweet aroma are obvious, the characteristics of the lotus leaf extract can be highlighted in the whole, the aroma intensity is higher than that of the lotus leaf extract, the aroma intensity and the aroma retention time are effectively improved, the natural sense and harmony are consistent with those of the lotus leaf extract, and the lotus leaf essence has higher aroma quality.
The smoking evaluation results of the lotus-flavored No. 2 essence flavored cigarettes are shown in Table 6.
Table 6 Smoke scoring table for lotus-flavored No. 2 essence flavored cigarettes
The cigarette evaluation result shows that the lotus leaf flavor No. 2 essence can endow the lotus leaf flavor characteristics of the cigarette smoke, the green flavor, the faint scent and the sweet flavor in the smoke are obvious, the smoke quality and the smoke quantity are obviously improved, meanwhile, the smoke quality and the smoke quantity can be better coordinated with the smoke (the mutual coordination of various flavors is not carried out, the natural feeling is poor if the smoke quality is not coordinated, the overall aroma is not elegant), the miscellaneous gas effect is reduced, and compared with the lotus leaf extract, the lotus leaf flavor No. 2 essence has more obvious improvement effect on the smoke state and the comfort level (the comfort level of the oral cavity and the nasal cavity, the stimulation residue and the like are smaller).
(3) Evaluation result of lotus fragrance No. 3 essence
The sensory evaluation method is implemented by referring to the evaluation scheme and standard of lotus flavor No. 1 essence, so that the personnel of the evaluation group are ensured to be unchanged. The lotus leaf extract smell evaluation radar chart is shown in fig. 1, and the lotus leaf extract smell evaluation radar chart of lotus leaf No. 3 essence is shown in fig. 4.
The evaluation result shows that the lotus fragrance No. 3 essence in the embodiment 3 has typical fragrance style characteristics of the lotus leaf extract in the aspect of smell fragrance, wherein green fragrance, faint scent, sour fragrance and sweet fragrance are very obvious, the characteristics of the lotus leaf extract can be highlighted overall, the fragrance intensity is higher than that of the lotus leaf extract, the fragrance intensity and fragrance retention time are effectively improved, the natural sense and harmony are consistent with those of the lotus leaf extract, and the lotus leaf extract has very high fragrance quality.
The smoking evaluation results of the lotus-flavored No. 3 essence flavored cigarettes are shown in Table 7.
Table 7 Smoke scoring table for lotus-flavored No. 3 essence flavored cigarettes
The cigarette evaluation result shows that the lotus leaf flavor 3 essence can endow the lotus leaf flavor characteristics of the cigarette smoke, the green aroma, the faint scent and the sweet aroma in the smoke are obvious, the smoke quality and the smoke quantity are obviously improved, meanwhile, the smoke quality and the smoke quantity can be well coordinated with the smoke, the effect of miscellaneous gases and the like is reduced, and compared with the lotus leaf extract, the lotus leaf flavor 3 essence has more obvious improvement effect on the smoke state and the comfort level.
From the above description, the lotus-flavored special essence of the invention has the following characteristics:
1. the components of the lotus leaf essence are additive raw materials which are allowed to be used in foods, so that the lotus leaf essence is safe and effective.
2. The lotus leaf essence is based on comprehensive characterization and analysis results of lotus leaves and lotus leaf extract moisture, common solvents, sugar components, acid components and volatile components, has high similarity of product style and lotus leaves, and simultaneously has strong natural sense and good harmony, and can effectively solve the problems of weak fragrance, short fragrance retention time and the like of the lotus leaf extract.
3. The lotus essence can effectively avoid the defects of natural perfume raw materials: quality fluctuation of natural perfume caused by raw material difference; meanwhile, as all the components in the essence are commercial food-grade perfume raw materials, the prepared lotus-flavored essence has stable quality, is beneficial to large-scale and industrial production, and can effectively reduce the cost.
4. The main components of the lotus-flavor essence exist in tobacco leaves, the overall flavor and the smoke harmony are good after the cigarettes are flavored, the lotus-flavor characteristics of the cigarettes are endowed, the smoke comfortableness of the cigarettes can be effectively improved, and the smoking quality of the cigarettes is improved.
Claims (9)
1. The lotus-flavored special essence is characterized by comprising the following components in parts by weight: 1 to 5 parts of gamma-butyrolactone, 1 to 8 parts of caproic acid, 0.1 to 1.4 parts of benzyl alcohol, 0.1 to 2.6 parts of phenethyl alcohol, 1 to 5.2 parts of benzoic acid, 0.1 to 1.3 parts of 4-methoxybenzaldehyde, 2 to 11.5 parts of dihydroactinolide and 0.1 to 0.7 part of phyllitol.
2. The lotus-flavor special essence according to claim 1, wherein the lotus-flavor special essence is composed of the following components in parts by weight: 1 to 5 parts of gamma-butyrolactone, 1 to 7 parts of caproic acid, 0.1 to 0.4 part of benzyl alcohol, 0.1 to 0.9 part of phenethyl alcohol, 1 to 3 parts of benzoic acid, 0.1 to 0.6 part of 4-methoxybenzaldehyde, 2 to 6 parts of dihydro-kiwi lactone, 0.1 to 0.5 part of phyllitol, 11 to 22 parts of palmitic acid, 11 to 22 parts of fructose, 10 to 15 parts of glucose, 4 to 7 parts of myose, 2 to 8 parts of lactic acid, 0.1 to 0.8 part of acetic acid, 0.6 to 2.8 parts of malic acid, 0.05 to 0.2 part of citric acid and 10 to 30 parts of solvent.
3. The lotus-flavored special essence according to claim 2, wherein the lotus-flavored special essence is composed of the following components in parts by weight: 1 to 1.3 portions of gamma-butyrolactone; 2 to 2.7 portions of caproic acid; 0.2 to 0.4 part of benzyl alcohol; 0.5 to 0.9 portion of phenethyl alcohol; 1 to 1.8 portions of benzoic acid; 0.2 to 0.4 portion of 4-methoxybenzaldehyde; 3 to 4.0 portions of dihydroactinolide; 0.1 to 0.2 part of leaf alcohol; 15-18.3 parts of palmitic acid; 19-21.8 parts of fructose; 10-12.4 parts of glucose; 5 to 6.3 portions of myo-glucose; 4 to 4.6 portions of lactic acid; 0.3 to 0.5 part of acetic acid; 1 to 1.4 portions of malic acid; 0.05 to 0.1 part of citric acid; 20-22.9 parts of solvent.
4. A lotus-like feature flavor according to claim 2 or 3, wherein the solvent is selected from one or more of water, ethanol, propylene glycol.
5. The lotus-flavored special essence according to claim 4, wherein the solvent consists of water, ethanol and propylene glycol according to the mass ratio of (10-15): (1-3).
6. Use of the lotus-flavored special essence according to any one of claims 1 to 5 in cigarettes.
7. The use according to claim 6, wherein the lotus leaf extract and the lotus leaf flavor are added together to the cigarette.
8. The use according to claim 7, characterized in that the weight ratio of lotus leaf extract to the lotus leaf flavor of gamma-butyrolactone mass is (1-5): (10-15).
9. Use according to any one of claims 6 to 8, wherein the perfuming is carried out in an amount of 10 to 1000ppm based on the weight of the cut tobacco of the cigarette.
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