CN116440766B - Gallium oxide powder mixing device and mixing method thereof - Google Patents

Gallium oxide powder mixing device and mixing method thereof Download PDF

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Publication number
CN116440766B
CN116440766B CN202310729851.9A CN202310729851A CN116440766B CN 116440766 B CN116440766 B CN 116440766B CN 202310729851 A CN202310729851 A CN 202310729851A CN 116440766 B CN116440766 B CN 116440766B
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China
Prior art keywords
stirring
stirring tank
gallium oxide
adjusting
component
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CN202310729851.9A
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Chinese (zh)
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CN116440766A (en
Inventor
谈逊
谈谦
刘宁波
刘才
吴曦
王占玲
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Huaxia Semiconductor Shenzhen Co ltd
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Huaxia Semiconductor Shenzhen Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/80Mixing plants; Combinations of mixers
    • B01F33/836Mixing plants; Combinations of mixers combining mixing with other treatments
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/80After-treatment of the mixture
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05Stirrers
    • B01F27/07Stirrers characterised by their mounting on the shaft
    • B01F27/072Stirrers characterised by their mounting on the shaft characterised by the disposition of the stirrers with respect to the rotating axis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/60Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis
    • B01F27/70Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with paddles, blades or arms
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/70Mixers specially adapted for working at sub- or super-atmospheric pressure, e.g. combined with de-foaming
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/80Mixing plants; Combinations of mixers
    • B01F33/836Mixing plants; Combinations of mixers combining mixing with other treatments
    • B01F33/8364Mixing plants; Combinations of mixers combining mixing with other treatments with drying
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/10Maintenance of mixers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/30Driving arrangements; Transmissions; Couplings; Brakes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/30Driving arrangements; Transmissions; Couplings; Brakes
    • B01F35/32Driving arrangements
    • B01F35/321Disposition of the drive
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/30Driving arrangements; Transmissions; Couplings; Brakes
    • B01F35/33Transmissions; Means for modifying the speed or direction of rotation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/40Mounting or supporting mixing devices or receptacles; Clamping or holding arrangements therefor
    • B01F35/42Clamping or holding arrangements for mounting receptacles on mixing devices
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/50Mixing receptacles
    • B01F35/52Receptacles with two or more compartments
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/75Discharge mechanisms
    • B01F35/752Discharge mechanisms with arrangements for converting the mechanism from mixing to discharging, e.g. by either guiding a mixture back into a receptacle or discharging it
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/75Discharge mechanisms
    • B01F35/754Discharge mechanisms characterised by the means for discharging the components from the mixer
    • B01F35/7547Discharge mechanisms characterised by the means for discharging the components from the mixer using valves, gates, orifices or openings
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/75Discharge mechanisms
    • B01F35/754Discharge mechanisms characterised by the means for discharging the components from the mixer
    • B01F35/7548Discharge mechanisms characterised by the means for discharging the components from the mixer using tilting or pivoting means for emptying the mixing receptacle
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/90Heating or cooling systems
    • B01F35/92Heating or cooling systems for heating the outside of the receptacle, e.g. heated jackets or burners
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/90Heating or cooling systems
    • B01F2035/99Heating

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)

Abstract

The application belongs to the technical field of gallium oxide preparation, and particularly relates to a gallium oxide powder mixing device and a gallium oxide powder mixing method. The mixing device comprises a base, wherein a material receiving component, a stirring tank, a suction device and a material feeding component are arranged on the surface of the base, a material inlet, a suction opening and a material discharging opening are formed in the surface of the stirring tank, the suction device is connected with the suction opening to suck out gas in the stirring tank, the material feeding component is connected with the material inlet, the stirring tank is internally provided with the stirring component and an extrusion component, the surface of the stirring tank is sleeved with a heating component, an adjusting component is further arranged on the surface of the base and connected with the stirring tank, the central axis of the stirring tank is parallel to the ground and is marked as a first working state, the central axis of the stirring tank is perpendicular to the ground and is marked as a second working state, and the adjusting component is used for adjusting the mutual switching between the first working state and the second working state; the gallium oxide powder mixing device realizes automatic processing of gallium oxide powder mixing, realizes automatic feeding, stirring, drying and cake making treatment, and has high processing efficiency.

Description

Gallium oxide powder mixing device and mixing method thereof
Technical Field
The application belongs to the technical field of gallium oxide preparation, and particularly relates to a gallium oxide powder mixing device.
Background
Gallium oxide is a transparent oxide semiconductor material, and has been attracting attention for a long time in terms of conductivity and luminescence, and has a wide application prospect in terms of optoelectronic devices, and is used as an insulating layer of a Ga-based semiconductor material, and an ultraviolet filter.
When the titanium-doped gallium oxide crystal is prepared, the titanium oxide and gallium oxide powder are mixed in a vacuum environment and stirred, then the mixture is dried, and then the mixture is made into a cake shape, and then the solid-phase sintering method is adopted to prepare the titanium-doped gallium oxide crystal. The method comprises the steps of preparing a titanium oxide and gallium oxide powder mixture into a cake shape, and drying the titanium oxide and gallium oxide powder mixture in a drying oven, taking out the mixture after drying, and pressing the cake to obtain the titanium doped gallium oxide crystal by sintering.
Disclosure of Invention
The application provides a gallium oxide powder mixing device and a mixing method thereof for solving the problems.
The application realizes the above purpose through the following technical scheme:
the utility model provides a gallium oxide powder mixing arrangement, the on-line screen storage device comprises a base, the surface of base is equipped with receiving subassembly, the agitator tank, suction equipment and material loading subassembly, the feed inlet has been seted up on the surface of agitator tank, extraction opening and bin outlet, suction equipment links to each other with the extraction opening, suction equipment is used for drawing out the interior gas of agitator tank, material loading subassembly links to each other with the feed inlet, be equipped with stirring subassembly and extrusion subassembly in the agitator tank, the surface cover of agitator tank is equipped with heating element, the surface of base still is equipped with adjusting part, adjusting part links to each other with the agitator tank, the axis of agitator tank is parallel with ground, the first operating condition of marking, the axis of agitator tank is perpendicular with ground, the second operating condition of marking, the mutual switching of first operating condition and second operating condition is adjusted to the adjusting part.
As a further optimization scheme of the application, a partition piece is arranged in the stirring tank, the partition piece divides the inner cavity of the stirring tank into two parts, namely a stirring cavity and an extrusion cavity, the stirring assembly and the feeding port are positioned in the stirring cavity, and the extrusion assembly and the discharge port are positioned in the extrusion cavity.
As a further optimization scheme of the application, a chute is further formed in the inner wall surface of the stirring tank, the chute is arranged along the circumferential direction of the inner wall of the stirring tank, the partition piece comprises a fixed plate and a movable plate, the fixed plate is fixedly arranged at the upper half end of the inner wall of the stirring tank, the movable plate slides along the chute, the movable plate covers the lower half section of the stirring cavity and is marked as a stirring state, the discharge port is positioned in the upper half section area of the stirring tank, the partition piece covers the upper half section of the stirring cavity and is marked as a discharging state, an adjusting block is arranged on the surface of the partition piece, the adjusting component comprises a first adjusting part, the first adjusting part is matched with the adjusting block, the partition piece is driven to be in the stirring state when the stirring tank is horizontally distributed, and is driven to be in the discharging state when the stirring tank is vertically distributed.
As a further optimization scheme of the application, the stirring assembly comprises a power part and a shaft rod, the power part drives the shaft rod to rotate, the shaft rod is positioned in the stirring tank, the surfaces of the partition piece and the regulating block are also provided with openings, the shaft rod penetrates through the openings, the surface of the shaft rod is also provided with a plurality of detachable stirring rods, the stirring rods and the shaft rod are distributed in a cross manner, and the stirring rods are distributed in a circumferential array around the shaft rod.
As a further optimization scheme of the application, the extrusion assembly comprises a linear driving part and an extrusion part, wherein the movement direction of the linear driving part is parallel to the axial direction of the shaft rod, and the linear driving part drives the extrusion part to enter the discharge port to press the gallium oxide mixed powder into a cake shape.
As a further optimization scheme of the application, the linear driving part comprises two groups of strokes, namely a first stroke and a second stroke, wherein the distance of the second stroke is larger than that of the first stroke, the first stroke of the linear driving part pushes the extrusion part to enter the discharge port to press the gallium oxide mixed powder into a cake shape, and the second stroke of the linear driving part pushes the extrusion part to push the gallium oxide mixed powder pressed into the cake shape out of the discharge port and into the receiving assembly.
As a further optimization scheme of the application, the surface of the linear driving part is also connected with a stirring piece, the stirring piece comprises a rod piece and a plurality of stirring blocks, the axial direction of the rod piece is coaxial with the shaft rod, the stirring blocks are arranged at intervals along the circumferential direction of the rod piece, the stirring blocks stir the gallium oxide mixed powder to the inside of the discharge hole, and the discharge hole is filled with the gallium oxide mixed powder while the surface of the gallium oxide mixed powder is scraped.
As a further optimization scheme of the application, the adjusting component further comprises a main driving part and a rotating motor, the output end of the rotating motor is connected with the tank body of the stirring tank to drive the stirring tank to switch between a first working state and a second working state, the main driving part drives the first adjusting part to act to drive the stirring state of the partition piece to switch with the discharging state, the main driving part comprises a fixed gear and a penetrating rod, the fixed gear is fixedly arranged on the surface of the base, one end of the penetrating rod penetrates through the tank body of the stirring tank, the end part of the penetrating rod positioned outside the stirring tank is fixedly connected with a driven wheel matched with the fixed gear, the other end of the penetrating rod is provided with a bevel gear, the surface of the bevel gear is meshed with a matched gear, the end face of the matched gear is connected with a cam block, the rotation of the cam block is arranged on the surface of the fixed plate, the side face of the cam block is abutted against the first adjusting part, the first adjusting part is slidably arranged on the surface of the fixed plate through an elastic piece, the first adjusting part moves to drive the adjusting block to act, and the stirring state of the partition piece to switch with the discharging state.
As a further optimization scheme of the application, the linear driving part comprises a cylindrical cam and a limiting plate, one end of the cylindrical cam, which is far away from the discharge port, is connected with the shaft rod, an annular displacement groove is formed in the side surface of the cylindrical cam, the limiting plate is fixedly arranged on the inner wall of the stirring tank, the surface of the limiting plate is penetrated with a moving rod, the moving direction of the moving rod is parallel to the axial direction of the shaft rod, the moving rod is L-shaped, one end of the moving rod is connected with the end part of the extrusion part, the other end of the moving rod is inserted into the displacement groove, when the cylindrical cam rotates for one circle, the moving rod slides along the displacement groove to drive the extrusion part to press gallium oxide mixed powder into a cake shape, then the extrusion part is far away from the discharge port, and finally the extrusion part secondarily enters the discharge port to push the cake-shaped gallium oxide mixed powder into the receiving component.
The gallium oxide powder mixing method specifically comprises the following steps:
s1: the gallium oxide powder and the titanium oxide powder are conveyed to the inside of the stirring tank through the feeding component, the heating component and the pumping equipment work synchronously, the heating component heats the inside of the stirring tank and toasts the mixture of the titanium oxide powder and the gallium oxide powder, the pumping equipment pumps the environment in the stirring tank into a vacuum environment through the pumping hole, and the stirring component mixes the gallium oxide powder and the titanium oxide powder in the stirring tank;
s2: after the mixing treatment of the gallium oxide powder and the titanium oxide powder is completed, the rotating motor acts to drive the stirring tank to rotate, so that the stirring tank is changed from a first working state to a second working state;
s3: while the stirring tank is in working state transition, the driven wheel is meshed with the fixed gear, the driven wheel drives the penetrating rod to rotate, the penetrating rod and the bevel gear synchronously rotate, the bevel gear is meshed with the matched gear to drive the cam block to rotate, the cam block extrudes the first adjusting part to enable the first adjusting part to displace when rotating, the first adjusting part drives the adjusting block to act, and the driving partition piece is converted from the stirring state to the discharging state;
s4: after the state transition of the partition piece is completed, the shaft lever is driven to act along with the power part, the shaft lever drives the cylindrical cam to act synchronously, when the cylindrical cam rotates for a circle, the moving lever acts twice, the extruding part is firstly driven to enter the discharge port to press the gallium oxide mixed powder into a cake shape, and then the extruding part is driven to enter the discharge port for the second time to push the cake-shaped gallium oxide mixed powder into the receiving assembly, so that the collection treatment of the gallium oxide and titanium oxide powder mixture is completed.
The application has the beneficial effects that: the mixing equipment provided by the application can realize automatic processing of mixing gallium oxide and titanium oxide powder, and realize automatic feeding, stirring, drying, cake making and collecting treatment, has high processing efficiency, saves the time required by conversion between different stations, and further improves the production efficiency.
Drawings
FIG. 1 is a schematic view of the overall structure of the present application;
FIG. 2 is a schematic elevational view of the first operating condition of the agitator tank of the present application;
FIG. 3 is a schematic rear view of the first operational state of the agitator tank of the present application;
FIG. 4 is a schematic rear view of a second operational state of the agitator tank of the present application;
FIG. 5 is a schematic view showing the internal structure of the agitation tank of the present application;
fig. 6 is a schematic structural view of the stirring state of the partition member of the present application;
fig. 7 is a schematic view of the structure of the discharging state of the partition member of the present application;
fig. 8 is a side wall plan development schematic view of the cylindrical cam of the present application.
In the figure: 1. a base; 2. a material receiving assembly; 3. a stirring tank; 31. a feed inlet; 32. an extraction opening; 33. a discharge port; 34. a partition member; 341. a fixing plate; 342. a movable plate; 343. an adjusting block; 344. an opening; 35. a stirring cavity; 36. an extrusion chamber; 37. a chute; 4. a suction device; 5. a feeding assembly; 6. a stirring assembly; 61. a power section; 62. a shaft lever; 63. a stirring rod; 7. an extrusion assembly; 71. a linear driving section; 711. a cylindrical cam; 712. a limiting plate; 713. a displacement groove; 714. a moving rod; 72. an extrusion part; 73. a material stirring piece; 731. a rod piece; 732. a shifting block; 8. a heating assembly; 9. an adjustment assembly; 91. a first adjusting part; 92. a main driving part; 921. a fixed gear; 922. a penetrating rod; 923. driven wheel; 924. a bevel gear; 925. a mating gear; 926. a cam block; 93. and rotating the motor.
Detailed Description
The present application will be described in further detail with reference to the accompanying drawings, wherein it is to be understood that the following detailed description is for the purpose of further illustrating the application only and is not to be construed as limiting the scope of the application, as various insubstantial modifications and adaptations of the application to those skilled in the art can be made in light of the foregoing disclosure.
Example 1
As shown in fig. 1 to 8, a gallium oxide powder mixing device, including base 1, the surface of base 1 is equipped with receipts material subassembly 2, agitator tank 3, suction equipment 4 and material loading subassembly 5, feed inlet 31 has been seted up on the surface of agitator tank 3, extraction opening 32 and bin outlet 33, suction equipment 4 links to each other with extraction opening 32, suction equipment 4 is used for evacuating the interior gas of agitator tank 3, material loading subassembly 5 links to each other with feed inlet 31, be equipped with agitator assembly 6 and extrusion subassembly 7 in the agitator tank 3, the surface cover of agitator tank 3 is equipped with heating element 8, the surface of base 1 still is equipped with adjusting part 9, adjusting part 9 links to each other with agitator tank 3, the axis of agitator tank 3 is the first operating condition when keeping in parallel with the ground, the axis of agitator tank 3 is the second operating condition when keeping in perpendicular with the ground, the mutual switching of first operating condition and second operating condition is adjusted to adjusting part 9.
It should be noted that, in this embodiment, the feeding component 5 is connected with the feeding port 31 through a pipe, and the connection state is detachable connection, where the pipe is a flexible pipe, and the pipe can be extended or shortened along with the switching of the first working state and the second working state of the stirring tank 3, so as to ensure that the feeding component 5 carries out continuous feeding treatment inside the stirring tank 3.
It should be noted that, the suction device 4 draws the interior of the stirring tank 3 into a vacuum environment through the air extraction opening 32, wherein the feed opening 31 should be provided with a valve element, and when the suction device 4 performs air extraction treatment, the valve element is closed, and when the material is required to be filled, the valve element is opened.
Wherein, heating element 8 is wrapped up agitator tank 3, and heating element 8 heats agitator tank 3, dries inside gallium oxide and titanium oxide powder, conveniently presses into cake form with the inside mixed material of agitator tank 3.
And, receive material subassembly 2 and base 1 detachable connection, receive material subassembly 2 includes the receipts workbin, receive the surface of workbin and be equipped with the connector, when agitator tank 3 changes to second operating condition, the connector aligns each other with bin outlet 33, and receive the inside of workbin still be equipped with the barrier plate, the barrier plate links to each other with linear telescopic link, when carrying out the cake processing to gallium oxide and titanium oxide mixed powder, the barrier plate blocks the connector, when needing to carry out ejection of compact processing, linear telescopic link drives the barrier plate and leaves the connector, along with the action of extrusion subassembly 7, push the cake-shaped gallium oxide and titanium oxide mixture to the receipts workbin inside, accomplish the collection processing to gallium oxide and titanium oxide mixture.
The inside of agitator tank 3 is equipped with the partition piece 34, and partition piece 34 separates into two parts with the inner chamber of agitator tank 3, is stirring chamber 35 and extrusion chamber 36 respectively, and stirring subassembly 6 and feed inlet 31 are located stirring chamber 35, and extrusion subassembly 7 and bin outlet 33 are located extrusion chamber 36.
The chute 37 has still been seted up to agitator tank 3 internal wall face, the chute 37 sets up along agitator tank 3's inner wall circumference, partition member 34 includes fixed plate 341 and fly leaf 342, fixed plate 341 fixed mounting is in agitator tank 3's inner wall's upper half, fly leaf 342 slides along chute 37, the fly leaf 342 covers the lower half section of agitator chamber 35 and marks as the stirring state, bin outlet 33 is located agitator tank 3's upper half region, partition member 34 covers the upper half section of agitator chamber 35 and marks as the discharge state, partition member 34's surface is equipped with regulating block 343, regulating assembly 9 includes first regulation portion 91, first regulation portion 91 cooperates with regulating block 343, the drive is in the stirring state when agitator tank 3 distributes in the level, when agitator tank 3 vertically, be in the discharge state.
In this embodiment, the first adjusting portion 91 is a rack, the adjusting block 343 is a connecting gear, and when the first adjusting portion 91 moves down, the adjusting block 343 is driven to rotate, so that the movable plate 342 slides along the chute 37, the driving partition 34 is changed from the stirring state to the discharging state, and the stirring cavity 35 is communicated with the extrusion cavity 36.
The stirring assembly 6 comprises a power part 61 and a shaft lever 62, the power part 61 drives the shaft lever 62 to rotate, the shaft lever 62 is positioned in the stirring tank 3, the surfaces of the partition piece 34 and the adjusting block 343 are further provided with openings 344, the shaft lever 62 penetrates through the openings 344, the surface of the shaft lever 62 is further provided with a plurality of detachable stirring rods 63, the stirring rods 63 and the shaft lever 62 are distributed in a cross manner, and the stirring rods 63 are distributed in a circumferential array around the shaft lever 62.
The extrusion assembly 7 comprises a linear driving part 71 and an extrusion part 72, wherein the movement direction of the linear driving part 71 is parallel to the axial direction of the shaft rod 62, and the linear driving part 71 drives the extrusion part 72 to enter the discharge port 33 to press the gallium oxide mixed powder into a cake shape.
The linear driving part 71 includes two sets of strokes, which are a first stroke and a second stroke, wherein the distance of the second stroke is greater than that of the first stroke, the first stroke of the linear driving part 71 pushes the extruding part 72 to enter the discharge port 33 to press the gallium oxide mixed powder into a cake shape, and the second stroke of the linear driving part 71 pushes the extruding part 72 to push the gallium oxide mixed powder pressed into the cake shape out of the discharge port 33 and into the receiving assembly 2.
The surface of the linear driving part 71 is also connected with a stirring piece 73, the stirring piece 73 comprises a rod piece 731 and a plurality of stirring blocks 732, the axial direction of the rod piece 731 is coaxial with the shaft lever 62, the stirring blocks 732 are arranged at intervals along the circumferential direction of the rod piece 731, the stirring blocks 732 stir the gallium oxide mixed powder to the inside of the discharge hole 33, and the surface of the gallium oxide mixed powder is scraped while the discharge hole 33 is full.
It should be further noted that, when the plurality of shifting blocks 732 shift the mixture into the discharge port 33, the content of the mixture pressed each time can be ensured to be consistent, so as to avoid the occurrence of different sizes of cake materials during the production and discharge.
The adjusting component 9 further comprises a main driving part 92 and a rotating motor 93, the output end of the rotating motor 93 is connected with the tank body of the stirring tank 3 to drive the stirring tank 3 to switch between a first working state and a second working state, the main driving part 92 drives the first adjusting part 91 to act to drive the stirring state of the partition piece 34 and the discharging state to switch between each other, the main driving part 92 comprises a fixed gear 921 and a penetrating rod 922, the fixed gear 921 is fixedly arranged on the surface of the base 1, one end of the penetrating rod 922 penetrates through the tank body of the stirring tank 3, the end part of the penetrating rod 922 positioned outside the stirring tank 3 is fixedly connected with a driven wheel 923 matched with the fixed gear 921, the other end of the penetrating rod 922 is provided with a bevel gear 924, the surface of the bevel gear 924 is meshed with a matched gear 925, the end face of the matched gear 925 is connected with a cam block 926, the rotation of the cam block 926 is arranged on the surface of the fixed plate 341, the side face of the cam block 926 abuts against the first adjusting part 91, the first adjusting part 91 is slidably arranged on the surface 341 of the fixed plate through an elastic piece, the first adjusting part 91 moves the driving the adjusting part 343 to act to drive the partition piece 34 and the stirring state and the discharging state to switch between the stirring state and the discharging state.
When the rotation motor 93 drives the tank body of the stirring tank 3 to change from the first working state to the second working state, the driven wheel 923 is meshed with the fixed gear 921 to drive the penetrating rod 922 to rotate, the bevel gear 924 synchronously rotates when the penetrating rod 922 rotates, the bevel gear 924 drives the matched gear 925 to rotate, the cam block 926 is driven to rotate, the cam block 926 extrudes the first adjusting part 91 to move downwards, the adjusting block 343 is driven to act, the driving partition piece 34 is changed from the stirring state to the discharging state, and the stirring cavity 35 is communicated with the extrusion cavity 36.
The linear driving part 71 comprises a cylindrical cam 711 and a limiting plate 712, one end of the cylindrical cam 711, which is far away from the discharge hole 33, is connected with the shaft lever 62, an annular displacement groove 713 is formed in the side surface of the cylindrical cam 711, the limiting plate 712 is fixedly arranged on the inner wall of the stirring tank 3, a moving rod 714 penetrates through the surface of the limiting plate 712, the moving direction of the moving rod 714 is parallel to the axial direction of the shaft lever 62, the moving rod 714 is L-shaped, one end of the moving rod 714 is connected with the end of the extrusion part 72, the other end of the moving rod 714 is inserted into the displacement groove 713, when the cylindrical cam 711 rotates for one circle, the moving rod 714 slides along the displacement groove 713 to drive the extrusion part 72 to press gallium oxide mixed powder into a cake shape, then the extrusion part 72 is far away from the discharge hole 33, the length of the extrusion part 72 is larger than the length of the first entering the discharge hole 33, and then the cake-shaped gallium oxide mixed powder is pushed into the material receiving assembly 2, and the cake-shaped gallium oxide mixed powder is collected and processed.
Example 2
In this embodiment, a gallium oxide powder mixing method is provided, which specifically includes the following steps:
s1: the gallium oxide powder and the titanium oxide powder are conveyed into the stirring tank 3 through the feeding component 5, the heating component 8 and the suction device 4 work synchronously, the heating component 8 heats the interior of the stirring tank 3 and toasts the mixture of the titanium oxide and the gallium oxide powder, the suction device 4 pumps the environment in the stirring tank 3 into a vacuum environment through the air extraction opening 32, and the stirring component 6 mixes the gallium oxide powder and the titanium oxide powder in the stirring tank 3;
s2: after the mixing treatment of the gallium oxide powder and the titanium oxide powder is completed, the rotating motor 93 acts to drive the stirring tank 3 to rotate, so that the stirring tank 3 is changed from the first working state to the second working state;
s3: while the stirring tank 3 is in the working state transition, the driven wheel 923 is meshed with the fixed gear 921, the driven wheel 923 drives the penetrating rod 922 to rotate, the penetrating rod 922 and the bevel gear 924 synchronously rotate, the bevel gear 924 and the matching gear 925 are meshed with each other to drive the cam block 926 to rotate, the cam block 926 extrudes the first adjusting part 91 to enable the first adjusting part 91 to displace when rotating, the first adjusting part 91 drives the adjusting block 343 to act, and the driving partition piece 34 is changed from the stirring state to the discharging state;
s4: after the state transition of the partition piece 34 is completed, along with the action of the shaft lever 62 driven by the power part 61, the shaft lever 62 drives the cylindrical cam 711 to synchronously act, when the cylindrical cam 711 rotates for one circle, the moving rod 714 acts twice, firstly, the extrusion part 72 is driven to enter the discharge port 33 to press gallium oxide mixed powder into a cake shape, then, the extrusion part 72 is driven to enter the discharge port 33 for the second time to push the cake-shaped gallium oxide mixed powder into the receiving assembly 2, and the collection treatment of the gallium oxide and titanium oxide powder mixture is completed.
The foregoing examples illustrate only a few embodiments of the application and are described in detail herein without thereby limiting the scope of the application. It should be noted that it will be apparent to those skilled in the art that several variations and modifications can be made without departing from the spirit of the application, which are all within the scope of the application.

Claims (2)

1. The gallium oxide powder mixing device is characterized by comprising a base (1), wherein a material collecting component (2), a stirring tank (3), a pumping device (4) and a material feeding component (5) are arranged on the surface of the base (1), a material inlet (31), a pumping hole (32) and a material discharging hole (33) are formed in the surface of the stirring tank (3), the pumping device (4) is connected with the pumping hole (32), the pumping device (4) is used for pumping gas in the stirring tank (3), the material feeding component (5) is connected with the material inlet (31), a stirring component (6) and an extrusion component (7) are arranged in the stirring tank (3), a heating component (8) is sleeved on the surface of the stirring tank (3), an adjusting component (9) is further arranged on the surface of the base (1), the adjusting component (9) is connected with the stirring tank (3), when the central axis of the stirring tank (3) is parallel to the ground, the first working state is recorded, and when the central axis of the stirring tank (3) is perpendicular to the ground, the second working state is recorded, the adjusting component (9) is used for adjusting the mutual switching between the first working state and the second working state.
A partition piece (34) is arranged in the stirring tank (3), the partition piece (34) divides the inner cavity of the stirring tank (3) into two parts, namely a stirring cavity (35) and an extrusion cavity (36), a stirring assembly (6) and a feeding hole (31) are positioned in the stirring cavity (35), and an extrusion assembly (7) and a discharge hole (33) are positioned in the extrusion cavity (36);
the stirring tank is characterized in that a chute (37) is further formed in the inner wall surface of the stirring tank (3), the chute (37) is arranged along the circumferential direction of the inner wall of the stirring tank (3), the partition piece (34) comprises a fixed plate (341) and a movable plate (342), the fixed plate (341) is fixedly arranged at the upper half end of the inner wall of the stirring tank (3), the movable plate (342) slides along the chute (37), the lower half section of the stirring cavity (35) is covered by the movable plate (342) and is in a stirring state, the discharge port (33) is located in the upper half section area of the stirring tank (3), the upper half section of the stirring cavity (35) is covered by the partition piece (34) and is in a discharging state, an adjusting block (343) is arranged on the surface of the partition piece (34), the adjusting component (9) comprises a first adjusting part (91), the first adjusting part (91) is matched with the adjusting block (343), and the partition piece (34) is driven to be in the stirring state when the stirring tank (3) is horizontally distributed, and in the discharging state when the stirring tank (3) is vertically distributed;
the stirring assembly (6) comprises a power part (61) and a shaft lever (62), the power part (61) drives the shaft lever (62) to rotate, the shaft lever (62) is positioned in the stirring tank (3), openings (344) are further formed in the surfaces of the partition piece (34) and the adjusting block (343), the shaft lever (62) penetrates through the openings (344), a plurality of detachable stirring rods (63) are further arranged on the surface of the shaft lever (62), the stirring rods (63) and the shaft lever (62) are distributed in a cross mode, and the stirring rods (63) are distributed in a circumferential array around the shaft lever (62);
the extrusion assembly (7) comprises a linear driving part (71) and an extrusion part (72), wherein the movement direction of the linear driving part (71) is parallel to the axial direction of the shaft lever (62), and the linear driving part (71) drives the extrusion part (72) to enter the discharge port (33) to press gallium oxide mixed powder into a cake;
the linear driving part (71) comprises two groups of strokes, namely a first stroke and a second stroke, wherein the distance of the second stroke is larger than that of the first stroke, the first stroke of the linear driving part (71) pushes the extruding part (72) to enter the discharge port (33) to press the gallium oxide mixed powder into a cake shape, and the second stroke of the linear driving part (71) pushes the extruding part (72) to push the gallium oxide mixed powder pressed into the cake shape out of the discharge port (33) and enter the receiving assembly (2);
the surface of the linear driving part (71) is also connected with a stirring piece (73), the stirring piece (73) comprises a rod piece (731) and a plurality of stirring blocks (732), the axial direction of the rod piece (731) is coaxial with the axial rod (62), the stirring blocks (732) are arranged at intervals along the circumferential direction of the rod piece (731), the stirring blocks (732) stir gallium oxide mixed powder into a discharging hole (33), and the discharging hole (33) is filled with the gallium oxide mixed powder while the surface of the gallium oxide mixed powder is scraped;
the adjusting component (9) further comprises a main driving part (92) and a rotating motor (93), the output end of the rotating motor (93) is connected with the tank body of the stirring tank (3), the first working state and the second working state of the stirring tank (3) are driven to be mutually switched, the main driving part (92) drives the first adjusting part (91) to act, the stirring state and the discharging state of the partition piece (34) are driven to be mutually switched, the main driving part (92) comprises a fixed gear (921) and a penetrating rod (922), the fixed gear (921) is fixedly arranged on the surface of the base (1), one end of the penetrating rod (922) penetrates through the tank body of the stirring tank (3), the end part of the penetrating rod (922) positioned outside the stirring tank (3) is fixedly connected with a driven wheel (921) matched with the fixed gear (923), the other end of the penetrating rod (922) is provided with a bevel gear (924), the surface of the bevel gear (924) is meshed with a matched gear (925), the end face of the matched gear (925) is connected with a cam block (926), the rotation of the cam block (926) is arranged on the face of the fixed plate (341), the side face of the cam block (926) is fixedly arranged on the face of the fixed plate (341), the face of the first adjusting part (341) penetrates through the first adjusting part (91) and is fixedly connected with the first adjusting part (91) through the elastic adjusting part, the driving partition piece (34) is mutually switched between a stirring state and a discharging state;
the linear driving part (71) comprises a cylindrical cam (711) and a limiting plate (712), one end of the cylindrical cam (711), which is far away from the discharge opening (33), is connected with the shaft rod (62), an annular displacement groove (713) is formed in the side surface of the cylindrical cam (711), the limiting plate (712) is fixedly arranged on the inner wall of the stirring tank (3), the surface of the limiting plate (712) is provided with a moving rod (714) in a penetrating mode, the moving direction of the moving rod (714) is parallel to the axial direction of the shaft rod (62), the moving rod (714) is L-shaped, one end of the moving rod (714) is connected with the end of the extrusion part (72), the other end of the moving rod (714) is inserted into the displacement groove (713), when the cylindrical cam (711) rotates for one circle, the moving rod (714) slides along the displacement groove (713) to drive the extrusion part (72) to press gallium oxide mixed powder into a cake shape, then the extrusion part (72) is far away from the discharge opening (33), and finally the extrusion part (72) secondarily enters the discharge opening (33) to push the cake-shaped gallium oxide mixed powder into the receiving component (2).
2. A mixing method using the gallium oxide powder mixing apparatus of claim 1, comprising the steps of:
s1: the gallium oxide powder and the titanium oxide powder are conveyed to the inside of the stirring tank (3) through the feeding component (5), the heating component (8) and the suction device (4) work synchronously, the heating component (8) is used for heating the inside of the stirring tank (3) and simultaneously roasting a mixture of the titanium oxide powder and the gallium oxide powder, the suction device (4) is used for vacuumizing the environment inside the stirring tank (3) through the extraction opening (32), and the stirring component (6) is used for mixing the gallium oxide powder and the titanium oxide powder inside the stirring tank (3);
s2: after the mixing treatment of the gallium oxide powder and the titanium oxide powder is completed, a rotating motor (93) acts to drive the stirring tank (3) to rotate, so that the stirring tank (3) is changed from a first working state to a second working state;
s3: while the stirring tank (3) is in working state transition, the driven wheel (923) is meshed with the fixed gear (921), the driven wheel (923) drives the penetrating rod (922) to rotate, the penetrating rod (922) and the bevel gear (924) synchronously rotate, the bevel gear (924) is meshed with the matching gear (925) to drive the cam block (926) to rotate, the cam block (926) extrudes the first adjusting part (91) to enable the first adjusting part (91) to displace when rotating, the first adjusting part (91) drives the adjusting block (343) to act, and the driving partition piece (34) is converted into a discharging state from the stirring state;
s4: after the state transition of the partition piece (34) is completed, along with the action of the shaft lever (62) driven by the power part (61), the cylindrical cam (711) is driven by the shaft lever (62) to synchronously act, when the cylindrical cam (711) rotates for one circle, the moving rod (714) acts twice, the extruding part (72) is firstly driven to enter the discharge port (33) to press gallium oxide mixed powder into a cake shape, and then the extruding part (72) is driven to enter the discharge port (33) to push the cake-shaped gallium oxide mixed powder into the receiving assembly (2) for the second time, so that the collection treatment of the gallium oxide and titanium oxide powder mixture is completed.
CN202310729851.9A 2023-06-20 2023-06-20 Gallium oxide powder mixing device and mixing method thereof Active CN116440766B (en)

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