CN116411218A - Manufacturing process of corrosion-resistant rotating shaft for computer - Google Patents

Manufacturing process of corrosion-resistant rotating shaft for computer Download PDF

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Publication number
CN116411218A
CN116411218A CN202111643913.1A CN202111643913A CN116411218A CN 116411218 A CN116411218 A CN 116411218A CN 202111643913 A CN202111643913 A CN 202111643913A CN 116411218 A CN116411218 A CN 116411218A
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rotating shaft
corrosion
blank
computer
resistant
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方国章
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Suzhou Texin Precision Electronics Co ltd
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Suzhou Texin Precision Electronics Co ltd
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    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/04Ferrous alloys, e.g. steel alloys containing manganese
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23PMETAL-WORKING NOT OTHERWISE PROVIDED FOR; COMBINED OPERATIONS; UNIVERSAL MACHINE TOOLS
    • B23P15/00Making specific metal objects by operations not covered by a single other subclass or a group in this subclass
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D183/00Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
    • C09D183/04Polysiloxanes
    • C09D183/08Polysiloxanes containing silicon bound to organic groups containing atoms other than carbon, hydrogen, and oxygen
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/08Anti-corrosive paints
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/18Hardening; Quenching with or without subsequent tempering
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D6/00Heat treatment of ferrous alloys
    • C21D6/004Heat treatment of ferrous alloys containing Cr and Ni
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D6/00Heat treatment of ferrous alloys
    • C21D6/005Heat treatment of ferrous alloys containing Mn
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D6/00Heat treatment of ferrous alloys
    • C21D6/008Heat treatment of ferrous alloys containing Si
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/0068Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for particular articles not mentioned below
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/001Ferrous alloys, e.g. steel alloys containing N
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/002Ferrous alloys, e.g. steel alloys containing In, Mg, or other elements not provided for in one single group C22C38/001 - C22C38/60
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/008Ferrous alloys, e.g. steel alloys containing tin
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/02Ferrous alloys, e.g. steel alloys containing silicon
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/06Ferrous alloys, e.g. steel alloys containing aluminium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/40Ferrous alloys, e.g. steel alloys containing chromium with nickel
    • C22C38/48Ferrous alloys, e.g. steel alloys containing chromium with nickel with niobium or tantalum
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/40Ferrous alloys, e.g. steel alloys containing chromium with nickel
    • C22C38/50Ferrous alloys, e.g. steel alloys containing chromium with nickel with titanium or zirconium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/40Ferrous alloys, e.g. steel alloys containing chromium with nickel
    • C22C38/58Ferrous alloys, e.g. steel alloys containing chromium with nickel with more than 1.5% by weight of manganese
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C8/00Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C8/06Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using gases
    • C23C8/08Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using gases only one element being applied
    • C23C8/20Carburising
    • C23C8/22Carburising of ferrous surfaces
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D2211/00Microstructure comprising significant phases
    • C21D2211/001Austenite
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D2211/00Microstructure comprising significant phases
    • C21D2211/009Pearlite

Abstract

The invention relates to the technical field of computer accessories, and discloses a manufacturing process of a corrosion-resistant rotating shaft for a computer, which comprises the following steps: (1) Proportioning, namely preparing the percentages of the components in the corrosion-resistant rotating shaft system for the computer: 0.03-0.09% of carbon, 2-4% of aluminum, 0.1-0.4% of silicon, 1.2-1.6% of manganese, 0.02-0.03% of phosphorus, 0.8-1.2% of chromium, 0.01-0.03% of nitrogen, 0.05-0.07% of nickel, 1.5-2.5% of zinc, 1.2-1.8% of titanium, 0.2-0.4% of tin, 0.1-0.3% of niobium and the balance of iron. According to the manufacturing process of the corrosion-resistant rotating shaft for the computer, through solid solution strengthening of nickel and chromium and precipitation strengthening of microalloying elements niobium and titanium carbide, original austenite grains can be kept refined to ensure that the structure of a quenched and tempered building steel plate is sufficiently refined, so that excellent toughness is obtained, the addition of phosphorus can improve the atmospheric corrosion resistance of the rotating shaft, and silicon can be matched with the alloy to further improve the atmospheric corrosion resistance of steel, and the reason is probably that: the steel is not peeled off at high temperature, so that the steel has strong oxidation resistance, corrosion resistance and heat resistance, and is suitable for computers.

Description

Manufacturing process of corrosion-resistant rotating shaft for computer
Technical Field
The invention relates to the technical field of computer accessories, in particular to a manufacturing process of a corrosion-resistant rotating shaft for a computer.
Background
The computer is commonly called as a computer, is a modern electronic computing machine for high-speed computation, can perform numerical computation, can perform logic computation, and has a memory function. The intelligent electronic device is modern intelligent electronic equipment which can automatically and rapidly process mass data according to program operation.
A computer, which is composed of a hardware system and a software system, without any software installed, is called a bare metal. The method can be divided into five types of super computers, industrial control computers, network computers, personal computers and embedded computers, and more advanced computers include biological computers, photon computers, quantum computers and the like.
The existing rotating shaft for the computer is usually formed by polishing an iron rod, the iron rod consists of iron and carbon, and the iron rod is hard in texture, but after long-time use, the outer surface of the iron rod is extremely easy to oxidize and corrode, and the computer cannot be normally used, so that the corrosion-resistant rotating shaft for the computer is provided with a manufacturing process for solving the problems
Disclosure of Invention
(one) solving the technical problems
Aiming at the defects of the prior art, the invention provides a manufacturing process of a corrosion-resistant rotating shaft for a computer, which has the advantages of corrosion resistance and the like, and solves the problems that the outer surface of an iron rod is extremely easy to be oxidized and corroded after long-time use and the computer cannot be normally used.
(II) technical scheme
In order to achieve the purpose of corrosion resistance, the invention provides the following technical scheme: a manufacturing process of a corrosion-resistant rotating shaft for a computer comprises the following steps:
(1) Proportioning, namely preparing the percentages of the components in the corrosion-resistant rotating shaft system for the computer: 0.03-0.09% of carbon, 2-4% of aluminum, 0.1-0.4% of silicon, 1.2-1.6% of manganese, 0.02-0.03% of phosphorus, 0.8-1.2% of chromium, 0.01-0.03% of nitrogen, 0.05-0.07% of nickel, 1.5-2.5% of zinc, 1.2-1.8% of titanium, 0.2-0.4% of tin, 0.1-0.3% of niobium and the balance of iron;
(2) Preparing a blank, namely preparing the ingredients in the step (1) into metal wires through smelting, and cutting the metal wires through unidirectional movement of movable scissors to prepare the blank;
(3) Sintering: preheating the blank for 20 minutes at the preheating temperature of 500-700 ℃, and then heating to 1500 ℃ for sintering treatment to obtain a rotating shaft rough blank A;
(4) Punching: taking out the sintered rotary shaft rough blank A, upsetting for the first time, removing the outer oxide skin, quickly performing hot upsetting for a plurality of times to obtain a round blank, then placing a tooth nail in the middle of the round blank, and continuously hammering and nailing teeth by using a press to perform punching treatment until the tooth nail penetrates through the round blank to obtain a round through hole in the middle of the round blank to obtain a rotary shaft rough blank B;
(5) Carburizing: introducing protective atmosphere into a heat treatment furnace with controllable atmosphere for the rotating shaft rough blank B, preheating at 600-800 ℃, then heating to 800-900 ℃ for heat preservation in a pre-carburization stage, then heating to 900-1000 ℃ for reaction for the second time, and introducing into the heat treatment furnace simultaneously: carbon monoxide enables the carbon potential in the heat treatment furnace to reach 1.2, the furnace gas pressure is controlled to be 400-600Pa, and the temperature is reduced after the reaction is finished, so that a rotating shaft rough blank C is obtained;
(6) Quenching: placing the rotating shaft rough blank B into a salt bath furnace, raising the temperature to 900 ℃ at a heating rate of 50 ℃/h, preserving heat for 3-5h, and placing into quenching liquid for cooling to obtain a rotating shaft rough blank D:
(7) Tempering: tempering the rotating shaft rough blank D at 400-600 ℃, and naturally cooling to room temperature in air;
(8) And (3) coating treatment: immersing the shaft rough blank D in anti-corrosion liquid for 30 minutes through a lifting appliance, driving the bolt to slowly rotate in the immersing process, enabling the bolt to be in contact with the anti-corrosion liquid more uniformly and thoroughly, carrying out surface modification such as hanging drop on the bolt coated with the anti-corrosion liquid, and then drying to obtain a rotating shaft rough blank E;
(9) Cleaning: repeatedly flushing the rotating shaft rough blank E with clear water for 3-5 times to obtain a corrosion-resistant rotating shaft for a computer;
(10) And (3) detection: detecting whether cracks exist in the corrosion-resistant rotating shaft for the computer by using an ultrasonic nondestructive flaw detector, if so, the corrosion-resistant rotating shaft is a waste product, and if the corrosion-resistant rotating shaft is qualified, the corrosion-resistant rotating shaft is a finished product and is put in storage.
Preferably, the feed comprises the following raw materials in parts by weight: 0.03% of carbon, 2% of aluminum, 0.1% of silicon, 1.2% of manganese, 0.02% of phosphorus, 0.8% of chromium, 0.01% of nitrogen, 0.05% of nickel, 1.5% of zinc, 1.2% of titanium, 0.2% of tin, and 0.1% of niobium, with the balance being iron.
Preferably, the feed comprises the following raw materials in parts by weight: 0.06% of carbon, 3% of aluminum, 0.25% of silicon, 1.4% of manganese, 0.025% of phosphorus, 1% of chromium, 0.02% of nitrogen, 0.06% of nickel, 2% of zinc, 1.6% of titanium, 0.3% of tin, and 0.2% of niobium and the balance of iron.
Preferably, the feed comprises the following raw materials in parts by weight: 0.09% of carbon, 2-4% of aluminum, 0.4% of silicon, 1.6% of manganese, 00.03% of phosphorus, 0.8-1.2% of chromium, 0.03% of nitrogen, 0.07% of nickel, 2.5% of zinc, 1.8% of titanium, 0.2-0.4% of tin, and 0.3% of niobium, with the balance being iron.
Preferably, the protective atmosphere is one of methanol, nitrogen or argon
Preferably, the quenching liquid is PAG quenching agent, and the concentration is 10%.
Preferably, the second heating process in the step (5) is divided into a strong diffusion stage and a diffusion stage, the temperature of the strong diffusion stage is controlled to be 900-950 ℃, the temperature of the diffusion stage is controlled to be 950-990 ℃, the carburizing time of the strong diffusion stage is 200-300min, and the diffusion time of the diffusion stage is 60-180min
Preferably, the anti-corrosion liquid in the step (8) is a silicon fluorine high-temperature solution, and the concentration is 20-30%.
(III) beneficial effects
Compared with the prior art, the invention provides a manufacturing process of a corrosion-resistant rotating shaft for a computer, which has the following beneficial effects:
1. according to the manufacturing process of the corrosion-resistant rotating shaft for the computer, manganese, nitrogen and nickel elements are added, so that austenite in alloy steel can be promoted to form, the alloy steel has good high temperature resistance, meanwhile, N element can stabilize a high temperature structure, high temperature strength is improved, and therefore the thermal expansion coefficient of the alloy steel is reduced.
2. The manufacturing process of the corrosion-resistant rotating shaft for the computer ensures that the pearlite structure formed by austenite is more uniform through the heat treatment process of carburizing, quenching and tempering, avoids forming the structure which is not completely the same, and ensures that the rotating shaft has higher strength and toughness.
3. The manufacturing process of the corrosion-resistant rotating shaft for the computer has excellent spreadability, wear resistance and corrosion resistance by adding tin; chromium can enhance the toughness of the metal material and reduce the effective pressure during forming; palladium can enhance the ductility and plasticity of the material, facilitating forging, calendaring, and wire drawing.
4. According to the manufacturing process of the corrosion-resistant rotating shaft for the computer, the rotating shaft is soaked in the corrosion-resistant liquid, the corrosion-resistant liquid is a silicon-fluorine high-temperature solution, and an anti-corrosion coating is formed on the outer surface of the rotating shaft, so that the rotating shaft has high hardness, is smooth and self-cleaning, resists acid and alkali corrosion for a long time, can resist corrosion of an organic solvent, can be used for a long time, and is not easy to age, wear and corrode.
5. According to the manufacturing process of the corrosion-resistant rotating shaft for the computer, through solid solution strengthening of nickel and chromium and precipitation strengthening of microalloying elements niobium and titanium carbide, original austenite grains can be kept refined to ensure that the structure of a quenched and tempered building steel plate is sufficiently refined, so that excellent toughness is obtained, the addition of phosphorus can improve the atmospheric corrosion resistance of the rotating shaft, and silicon can be matched with the alloy to further improve the atmospheric corrosion resistance of steel, and the reason is probably that: the unit cells at the boundary between the silicon oxide and the metal are easily and tightly combined together, and are tightly adhered to the metal and do not peel off even at high temperature, so that the steel has strong oxidation resistance, corrosion resistance and heat resistance, and is suitable for computers.
Detailed Description
The technical solutions of the embodiments of the present invention will be clearly and completely described below in conjunction with the embodiments of the present invention, and it is apparent that the described embodiments are only some embodiments of the present invention, not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Embodiment one:
the manufacturing process of the corrosion-resistant rotating shaft for the computer is characterized by comprising the following steps of:
(1) Proportioning, namely preparing the percentages of the components in the corrosion-resistant rotating shaft system for the computer: 0.09% of carbon, 2-4% of aluminum, 0.4% of silicon, 1.6% of manganese, 00.03% of phosphorus, 0.8-1.2% of chromium, 0.03% of nitrogen, 0.07% of nickel, 2.5% of zinc, 1.8% of titanium, 0.2-0.4% of tin, and 0.3% of niobium, with the balance being iron;
(2) Preparing a blank, namely preparing the ingredients in the step (1) into metal wires through smelting, and cutting the metal wires through unidirectional movement of movable scissors to prepare the blank;
(3) Sintering: preheating the blank for 20 minutes at the preheating temperature of 700 ℃, and then heating to 1500 ℃ for sintering treatment to obtain a rotating shaft rough blank A;
(4) Punching: taking out the sintered rotary shaft rough blank A, upsetting for the first time, removing the outer oxide skin, quickly performing hot upsetting for a plurality of times to obtain a round blank, then placing a tooth nail in the middle of the round blank, and continuously hammering and nailing teeth by using a press to perform punching treatment until the tooth nail penetrates through the round blank to obtain a round through hole in the middle of the round blank to obtain a rotary shaft rough blank B;
(5) Carburizing: introducing protective atmosphere into a heat treatment furnace with controllable atmosphere for the rotating shaft rough blank B, preheating at 800 ℃, then entering a pre-carburizing stage, heating to 900 ℃ for heat preservation, then raising the temperature to 1000 ℃ for the second time for reaction, and introducing into the heat treatment furnace simultaneously: carbon monoxide enables the carbon potential in the heat treatment furnace to reach 1.2, the furnace gas pressure is controlled at 600Pa, and the temperature is reduced after the reaction is finished to obtain a rotating shaft rough blank C;
(6) Quenching: placing the rotating shaft rough blank B into a salt bath furnace, raising the temperature to 900 ℃ at a heating rate of 50 ℃/h, then preserving heat for 5h, and placing into quenching liquid for cooling to obtain a rotating shaft rough blank D:
(7) Tempering: tempering the rotating shaft rough blank D at 600 ℃, and naturally cooling to room temperature in air;
(8) And (3) coating treatment: immersing the shaft rough blank D in anti-corrosion liquid for 30 minutes through a lifting appliance, driving the bolt to slowly rotate in the immersing process, enabling the bolt to be in contact with the anti-corrosion liquid more uniformly and thoroughly, carrying out surface modification such as hanging drop on the bolt coated with the anti-corrosion liquid, and then drying to obtain a rotating shaft rough blank E;
(9) Cleaning: repeatedly washing the rotating shaft rough blank E with clear water for 5 times to obtain a corrosion-resistant rotating shaft for a computer;
(10) And (3) detection: detecting whether cracks exist in the corrosion-resistant rotating shaft for the computer by using an ultrasonic nondestructive flaw detector, if so, the corrosion-resistant rotating shaft is a waste product, and if the corrosion-resistant rotating shaft is qualified, the corrosion-resistant rotating shaft is a finished product and is put in storage.
Preferably, the protective atmosphere is one of methanol, nitrogen or argon
Preferably, the quenching liquid is PAG quenching agent, and the concentration is 10%.
Preferably, the second heating process in the step (5) is divided into a strong diffusion stage and a diffusion stage, the temperature of the strong diffusion stage is controlled at 950 ℃, the temperature of the diffusion stage is controlled at 990 ℃, the carburizing time of the strong diffusion stage is 300min, and the diffusion time of the diffusion stage is 180min
Preferably, the anti-corrosion liquid in the step (8) is a silicon fluorine high-temperature solution with the concentration of 30%
Embodiment two:
the manufacturing process of the corrosion-resistant rotating shaft for the computer is characterized by comprising the following steps of:
(1) Proportioning, namely preparing the percentages of the components in the corrosion-resistant rotating shaft system for the computer: 0.03% of carbon, 2% of aluminum, 0.1% of silicon, 1.2% of manganese, 0.02% of phosphorus, 0.8% of chromium, 0.01% of nitrogen, 0.05% of nickel, 1.5% of zinc, 1.2% of titanium, 0.2% of tin, and 0.1% of niobium, with the balance being iron;
(2) Preparing a blank, namely preparing the ingredients in the step (1) into metal wires through smelting, and cutting the metal wires through unidirectional movement of movable scissors to prepare the blank;
(3) Sintering: preheating the blank for 20 minutes at the preheating temperature of 500 ℃, and then heating to 1500 ℃ for sintering treatment to obtain a rotating shaft rough blank A;
(4) Punching: taking out the sintered rotary shaft rough blank A, upsetting for the first time, removing the outer oxide skin, quickly performing hot upsetting for a plurality of times to obtain a round blank, then placing a tooth nail in the middle of the round blank, and continuously hammering and nailing teeth by using a press to perform punching treatment until the tooth nail penetrates through the round blank to obtain a round through hole in the middle of the round blank to obtain a rotary shaft rough blank B;
(5) Carburizing: introducing protective atmosphere into a heat treatment furnace with controllable atmosphere for the rotating shaft rough blank B, preheating at 600 ℃, then heating to 800 ℃ in a pre-carburization stage, preserving heat, then heating to 900 ℃ for the second time for reaction, and introducing into the heat treatment furnace simultaneously: carbon monoxide enables the carbon potential in the heat treatment furnace to reach 1.2, the furnace gas pressure is controlled at 400Pa, and the temperature is reduced after the reaction is finished to obtain a rotating shaft rough blank C;
(6) Quenching: placing the rotating shaft rough blank B into a salt bath furnace, raising the temperature to 900 ℃ at a heating rate of 50 ℃/h, then preserving heat for 3h, and placing into quenching liquid for cooling to obtain a rotating shaft rough blank D:
(7) Tempering: tempering the rotating shaft rough blank D at 400 ℃, and naturally cooling to room temperature in air;
(8) And (3) coating treatment: immersing the shaft rough blank D in anti-corrosion liquid for 30 minutes through a lifting appliance, driving the bolt to slowly rotate in the immersing process, enabling the bolt to be in contact with the anti-corrosion liquid more uniformly and thoroughly, carrying out surface modification such as hanging drop on the bolt coated with the anti-corrosion liquid, and then drying to obtain a rotating shaft rough blank E;
(9) Cleaning: repeatedly washing the rotating shaft rough blank E with clear water for 3 times to obtain a corrosion-resistant rotating shaft for a computer;
(10) And (3) detection: detecting whether cracks exist in the corrosion-resistant rotating shaft for the computer by using an ultrasonic nondestructive flaw detector, if so, the corrosion-resistant rotating shaft is a waste product, and if the corrosion-resistant rotating shaft is qualified, the corrosion-resistant rotating shaft is a finished product and is put in storage.
Preferably, the protective atmosphere is one of methanol, nitrogen or argon
Preferably, the quenching liquid is PAG quenching agent, and the concentration is 10%.
Preferably, the second heating process in the step (5) is divided into a strong diffusion stage and a diffusion stage, the temperature of the strong diffusion stage is controlled to 900 ℃, the temperature of the diffusion stage is controlled to 960 ℃, the carburizing time of the strong diffusion stage is 200min, and the diffusion time of the diffusion stage is 60min
Preferably, the anti-corrosion liquid in the step (8) is a silicon fluorine high-temperature solution with the concentration of 20%
Embodiment III:
the manufacturing process of the corrosion-resistant rotating shaft for the computer is characterized by comprising the following steps of:
(1) Proportioning, namely preparing the percentages of the components in the corrosion-resistant rotating shaft system for the computer: the material comprises the following raw materials in parts by weight: 0.06% of carbon, 3% of aluminum, 0.25% of silicon, 1.4% of manganese, 0.025% of phosphorus, 1% of chromium, 0.02% of nitrogen, 0.06% of nickel, 2% of zinc, 1.6% of titanium, 0.3% of tin, and 0.2% of niobium and the balance of iron;
(2) Preparing a blank, namely preparing the ingredients in the step (1) into metal wires through smelting, and cutting the metal wires through unidirectional movement of movable scissors to prepare the blank;
(3) Sintering: preheating the blank for 20 minutes at the preheating temperature of 600 ℃, and then heating to 1500 ℃ for sintering treatment to obtain a rotating shaft rough blank A;
(4) Punching: taking out the sintered rotary shaft rough blank A, upsetting for the first time, removing the outer oxide skin, quickly performing hot upsetting for a plurality of times to obtain a round blank, then placing a tooth nail in the middle of the round blank, and continuously hammering and nailing teeth by using a press to perform punching treatment until the tooth nail penetrates through the round blank to obtain a round through hole in the middle of the round blank to obtain a rotary shaft rough blank B;
(5) Carburizing: introducing protective atmosphere into a heat treatment furnace with controllable atmosphere for the rotating shaft rough blank B, preheating at 600-800 ℃, then entering a pre-carburizing stage, heating to 850 ℃ for heat preservation, then raising the temperature to 950 ℃ for the second time for reaction, and simultaneously introducing into the heat treatment furnace: carbon monoxide enables the carbon potential in the heat treatment furnace to reach 1.2, the furnace gas pressure is controlled to be 500Pa, and the temperature is reduced after the reaction is finished to obtain a rotating shaft rough blank C;
(6) Quenching: placing the rotating shaft rough blank B into a salt bath furnace, raising the temperature to 900 ℃ at a heating rate of 50 ℃/h, then preserving heat for 4h, and placing into quenching liquid for cooling to obtain a rotating shaft rough blank D:
(7) Tempering: tempering the rotating shaft rough blank D at 500 ℃, and naturally cooling to room temperature in air;
(8) And (3) coating treatment: immersing the shaft rough blank D in anti-corrosion liquid for 30 minutes through a lifting appliance, driving the bolt to slowly rotate in the immersing process, enabling the bolt to be in contact with the anti-corrosion liquid more uniformly and thoroughly, carrying out surface modification such as hanging drop on the bolt coated with the anti-corrosion liquid, and then drying to obtain a rotating shaft rough blank E;
(9) Cleaning: repeatedly washing the rotating shaft rough blank E with clear water for 4 times to obtain a corrosion-resistant rotating shaft for a computer;
(10) And (3) detection: detecting whether cracks exist in the corrosion-resistant rotating shaft for the computer by using an ultrasonic nondestructive flaw detector, if so, the corrosion-resistant rotating shaft is a waste product, and if the corrosion-resistant rotating shaft is qualified, the corrosion-resistant rotating shaft is a finished product and is put in storage.
Preferably, the protective atmosphere is one of methanol, nitrogen or argon
Preferably, the quenching liquid is PAG quenching agent, and the concentration is 10%.
Preferably, the second heating process in the step (5) is divided into a strong diffusion stage and a diffusion stage, the temperature of the strong diffusion stage is controlled at 930 ℃, the temperature of the diffusion stage is controlled at 980 ℃, the carburizing time of the strong diffusion stage is 250min, and the diffusion time of the diffusion stage is 120min
Preferably, the anti-corrosion liquid in the step (8) is a silicon fluorine high-temperature solution with the concentration of 25%
1. According to the manufacturing process of the corrosion-resistant rotating shaft for the computer, manganese, nitrogen and nickel elements are added to promote the formation of austenite in alloy steel, so that the alloy steel has good high temperature resistance, meanwhile, N element can stabilize a high temperature structure, improve high temperature strength, reduce the thermal expansion coefficient of the alloy steel, in addition, mn element can be used as a desulfurizing agent and a deoxidizing agent, desulfurization and deoxidizing effects can be generated during smelting, the content of sulfur element and oxygen element in the alloy steel is reduced, manganese can enhance the hardness of iron, the ductility and toughness of the iron are not reduced, the high temperature stability and creep effect of the alloy steel are improved, and the influence of temperature difference on the alloy steel is reduced
2. The manufacturing process of the corrosion-resistant rotating shaft for the computer ensures that the pearlite structure formed by austenite is more uniform through the heat treatment process of carburizing, quenching and tempering, avoids forming the structure which is not completely the same, and ensures that the rotating shaft has higher strength and toughness.
3. The manufacturing process of the corrosion-resistant rotating shaft for the computer has excellent spreadability, wear resistance and corrosion resistance by adding tin; chromium can enhance the toughness of the metal material and reduce the effective pressure during forming; palladium can enhance the ductility and plasticity of the material, facilitating forging, calendaring, and wire drawing.
4. According to the manufacturing process of the corrosion-resistant rotating shaft for the computer, the rotating shaft is soaked in the corrosion-resistant liquid, the corrosion-resistant liquid is a silicon-fluorine high-temperature solution, and an anti-corrosion coating is formed on the outer surface of the rotating shaft, so that the rotating shaft has high hardness, is smooth and self-cleaning, resists acid and alkali corrosion for a long time, can resist corrosion of an organic solvent, can be used for a long time, and is not easy to age, wear and corrode.
5. According to the manufacturing process of the corrosion-resistant rotating shaft for the computer, through solid solution strengthening of nickel and chromium and precipitation strengthening of microalloying elements niobium and titanium carbide, original austenite grains can be kept refined to ensure that the structure of a quenched and tempered building steel plate is sufficiently refined, so that excellent toughness is obtained, the addition of phosphorus can improve the atmospheric corrosion resistance of the rotating shaft, and silicon can be matched with the alloy to further improve the atmospheric corrosion resistance of steel, and the reason is probably that: the unit cells at the boundary between the silicon oxide and the metal are easily and tightly combined together, and are tightly adhered to the metal and do not peel off even at high temperature, so that the steel has strong oxidation resistance, corrosion resistance and heat resistance, and is suitable for computers.
Although embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (8)

1. The manufacturing process of the corrosion-resistant rotating shaft for the computer is characterized by comprising the following steps of:
(1) Proportioning, namely preparing the percentages of the components in the corrosion-resistant rotating shaft system for the computer: 0.03-0.09% of carbon, 2-4% of aluminum, 0.1-0.4% of silicon, 1.2-1.6% of manganese, 0.02-0.03% of phosphorus, 0.8-1.2% of chromium, 0.01-0.03% of nitrogen, 0.05-0.07% of nickel, 1.5-2.5% of zinc, 1.2-1.8% of titanium, 0.2-0.4% of tin, 0.1-0.3% of niobium and the balance of iron;
(2) Preparing a blank, namely preparing the ingredients in the step (1) into metal wires through smelting, and cutting the metal wires through unidirectional movement of movable scissors to prepare the blank;
(3) Sintering: preheating the blank for 20 minutes at the preheating temperature of 500-700 ℃, and then heating to 1500 ℃ for sintering treatment to obtain a rotating shaft rough blank A;
(4) Punching: taking out the sintered rotary shaft rough blank A, upsetting for the first time, removing the outer oxide skin, quickly performing hot upsetting for a plurality of times to obtain a round blank, then placing a tooth nail in the middle of the round blank, and continuously hammering and nailing teeth by using a press to perform punching treatment until the tooth nail penetrates through the round blank to obtain a round through hole in the middle of the round blank to obtain a rotary shaft rough blank B;
(5) Carburizing: introducing protective atmosphere into a heat treatment furnace with controllable atmosphere for the rotating shaft rough blank B, preheating at 600-800 ℃, then heating to 800-900 ℃ for heat preservation in a pre-carburization stage, then heating to 900-1000 ℃ for reaction for the second time, and introducing into the heat treatment furnace simultaneously: carbon monoxide enables the carbon potential in the heat treatment furnace to reach 1.2, the furnace gas pressure is controlled to be 400-600Pa, and the temperature is reduced after the reaction is finished, so that a rotating shaft rough blank C is obtained;
(6) Quenching: placing the rotating shaft rough blank B into a salt bath furnace, raising the temperature to 900 ℃ at a heating rate of 50 ℃/h, preserving heat for 3-5h, and placing into quenching liquid for cooling to obtain a rotating shaft rough blank D:
(7) Tempering: tempering the rotating shaft rough blank D at 400-600 ℃, and naturally cooling to room temperature in air;
(8) And (3) coating treatment: immersing the shaft rough blank D in anti-corrosion liquid for 30 minutes through a lifting appliance, driving the bolt to slowly rotate in the immersing process, enabling the bolt to be in contact with the anti-corrosion liquid more uniformly and thoroughly, carrying out surface modification such as hanging drop on the bolt coated with the anti-corrosion liquid, and then drying to obtain a rotating shaft rough blank E;
(9) Cleaning: repeatedly flushing the rotating shaft rough blank E with clear water for 3-5 times to obtain a corrosion-resistant rotating shaft for a computer;
(10) And (3) detection: detecting whether cracks exist in the corrosion-resistant rotating shaft for the computer by using an ultrasonic nondestructive flaw detector, if so, the corrosion-resistant rotating shaft is a waste product, and if the corrosion-resistant rotating shaft is qualified, the corrosion-resistant rotating shaft is a finished product and is put in storage.
2. The process for manufacturing the corrosion-resistant rotating shaft for the computer according to claim 1, which is characterized by comprising the following raw materials in parts by weight: 0.03% of carbon, 2% of aluminum, 0.1% of silicon, 1.2% of manganese, 0.02% of phosphorus, 0.8% of chromium, 0.01% of nitrogen, 0.05% of nickel, 1.5% of zinc, 1.2% of titanium, 0.2% of tin, and 0.1% of niobium, with the balance being iron.
3. The process for manufacturing the corrosion-resistant rotating shaft for the computer according to claim 1, which is characterized by comprising the following raw materials in parts by weight: 0.06% of carbon, 3% of aluminum, 0.25% of silicon, 1.4% of manganese, 0.025% of phosphorus, 1% of chromium, 0.02% of nitrogen, 0.06% of nickel, 2% of zinc, 1.6% of titanium, 0.3% of tin, and 0.2% of niobium and the balance of iron.
4. The process for manufacturing the corrosion-resistant rotating shaft for the computer according to claim 1, which is characterized by comprising the following raw materials in parts by weight: 0.09% of carbon, 2-4% of aluminum, 0.4% of silicon, 1.6% of manganese, 00.03% of phosphorus, 0.8-1.2% of chromium, 0.03% of nitrogen, 0.07% of nickel, 2.5% of zinc, 1.8% of titanium, 0.2-0.4% of tin, and 0.3% of niobium, with the balance being iron.
5. The process of claim 1, wherein the protective atmosphere is one of methanol, nitrogen and argon.
6. The process for manufacturing a corrosion-resistant rotating shaft for a computer according to claim 1, wherein the quenching liquid is a PAG quenching agent with a concentration of 10%.
7. The process of claim 1, wherein the second heating step in the carburizing process in step (5) is divided into a strong infiltration stage and a diffusion stage, the temperature of the strong infiltration stage is controlled to 900-950 ℃, the temperature of the diffusion stage is controlled to 950-990 ℃, the carburizing time of the strong infiltration stage is 200-300min, and the diffusion time of the diffusion stage is 60-180min.
8. The process for manufacturing the corrosion-resistant rotating shaft for the computer according to claim 1, wherein the corrosion-resistant liquid in the step (8) is a silicon-fluorine high-temperature solution, and the concentration is 20-30%.
CN202111643913.1A 2021-12-29 2021-12-29 Manufacturing process of corrosion-resistant rotating shaft for computer Withdrawn CN116411218A (en)

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