CN116285491A - Preparation method of low-VOC (volatile organic compound) water-based printing ink for corrugated paper - Google Patents
Preparation method of low-VOC (volatile organic compound) water-based printing ink for corrugated paper Download PDFInfo
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- CN116285491A CN116285491A CN202310342252.1A CN202310342252A CN116285491A CN 116285491 A CN116285491 A CN 116285491A CN 202310342252 A CN202310342252 A CN 202310342252A CN 116285491 A CN116285491 A CN 116285491A
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- 238000007639 printing Methods 0.000 title claims abstract description 33
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 239000012855 volatile organic compound Substances 0.000 title description 41
- 238000003756 stirring Methods 0.000 claims abstract description 30
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims abstract description 20
- 229920001747 Cellulose diacetate Polymers 0.000 claims abstract description 10
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 10
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims abstract description 10
- 239000000440 bentonite Substances 0.000 claims abstract description 10
- 229910000278 bentonite Inorganic materials 0.000 claims abstract description 10
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000000839 emulsion Substances 0.000 claims abstract description 10
- 239000000945 filler Substances 0.000 claims abstract description 10
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims abstract description 10
- 239000000347 magnesium hydroxide Substances 0.000 claims abstract description 10
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims abstract description 10
- 239000000049 pigment Substances 0.000 claims abstract description 10
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 10
- 229920001909 styrene-acrylic polymer Polymers 0.000 claims abstract description 10
- 238000000034 method Methods 0.000 claims abstract description 9
- 239000004114 Ammonium polyphosphate Substances 0.000 claims abstract description 4
- 235000019826 ammonium polyphosphate Nutrition 0.000 claims abstract description 4
- 229920001276 ammonium polyphosphate Polymers 0.000 claims abstract description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 7
- 229910019142 PO4 Inorganic materials 0.000 claims description 7
- 239000010452 phosphate Substances 0.000 claims description 7
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 7
- 238000002156 mixing Methods 0.000 claims description 2
- 238000011161 development Methods 0.000 abstract description 3
- 231100000956 nontoxicity Toxicity 0.000 abstract 1
- 239000000976 ink Substances 0.000 description 24
- 238000000576 coating method Methods 0.000 description 10
- 239000003973 paint Substances 0.000 description 7
- 238000012360 testing method Methods 0.000 description 6
- 239000004115 Sodium Silicate Substances 0.000 description 5
- 229910052911 sodium silicate Inorganic materials 0.000 description 5
- 239000011248 coating agent Substances 0.000 description 4
- 238000010276 construction Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000003373 anti-fouling effect Effects 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 230000003670 easy-to-clean Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000005562 fading Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
- C09D11/037—Printing inks characterised by features other than the chemical nature of the binder characterised by the pigment
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/14—Printing inks based on carbohydrates
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/20—Air quality improvement or preservation, e.g. vehicle emission control or emission reduction by using catalytic converters
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a preparation method of printing ink for low-VOC water-based corrugated paper; firstly, placing a beaker containing sodium water glass in a high-speed dispersing machine, controlling the rotating speed to be 200-550r/min, adding a certain amount of styrene-acrylic emulsion, polyvinyl alcohol and cellulose diacetate, stirring for 15-30min, adding a certain amount of pigment and filler, and stirring for 15-30min to obtain a component A; placing a beaker containing an ammonium polyphosphate solution in a high-speed dispersing machine, controlling the rotating speed to be 400-1500r/min, adding a certain amount of aluminum hydroxide, magnesium hydroxide and bentonite, and stirring for 15-30min to obtain a component B; when in use, the AB component is mixed to obtain the printing ink for the low VOC resistant water-based corrugated paper; the method of the invention has the advantages of safe finished products, no toxicity and harm, guaranteeing the sanitary safety of food, no volatile gas generation and good industrial development prospect.
Description
Technical Field
The invention relates to an application technology for preparing sodium silicate and development of a water-based paint formula, in particular to printing ink for low-VOC water-based corrugated paper.
Background
VOCs (volatile organic compounds) are one of the common coatings, and the coatings contain volatile organic compounds, which are gradually volatilized during the coating construction and later use, thereby polluting the air quality and the environment. Thus, VOC coatings can cause environmental and human health pollution, and long-term exposure can pose a potential threat to human health. Therefore, in the coating industry, low VOC or zero VOC coatings are increasingly being widely popularized.
The sodium water glass paint is produced with sodium water glass as main material and through processing. Sodium water glass coatings offer a great advantage over other conventional coatings. Firstly, the sodium water glass paint has the characteristic of very strong weather resistance under the external climate condition, and can still keep stable color after being used for many years, and the phenomena of fading, falling off and the like can not occur. And secondly, the sodium silicate paint has high surface hardness, is not easy to adhere to dust and dirt, and is easy to clean. Meanwhile, the sodium water glass paint is an inorganic paint, can prevent fire from spreading when a fire disaster occurs, and has good fireproof performance. The sodium water glass paint has the advantages of inorganic environment protection, strong weather resistance, good anti-fouling performance and the like, and is widely applied to the fields of construction, industry and the like.
At present, the same document disclosure as the technical scheme of the invention is not seen.
Disclosure of Invention
The invention aims to provide printing ink for low-VOC water-based corrugated paper, which solves the problem that the traditional VOC coating contains a large amount of volatile organic compounds, reduces the pollution to the environment and meets the environmental protection requirement. Therefore, the development of the environment-friendly low-VOC water-based printing ink is one of the key points of the current environment-friendly ink research; the printing ink for the low-VOC water-based corrugated paper is prepared by a simple and easily controllable method, and the problems of environment, health and the like caused by VOC coating can be effectively solved.
The technical scheme adopted by the invention is as follows:
the preparation method of the printing ink for the low-VOC water-based corrugated paper comprises the following steps:
(1) Placing the beaker containing sodium water glass in a high-speed dispersing machine, controlling the rotating speed to be 200-550r/min, adding a certain amount of styrene-acrylic emulsion, polyvinyl alcohol and cellulose diacetate, and stirring for 15-30min;
the sodium silicate comprises the following components in parts by weight: styrene-acrylic emulsion: polyvinyl alcohol: cellulose diacetate = 100 parts: 20-30 parts of: 2-10 parts of: 2-10 parts; controlling the rotating speed to be 200-550r/min, and stirring for 15-30min;
(2) Adding a certain amount of pigment and filler into the step (1), controlling the rotating speed to be 300-500r/min, and stirring for 15-30min to obtain a component A;
the sodium silicate comprises the following components in parts by weight: pigment filler = 100 parts: 2-15 parts; controlling the rotating speed to be 300-500r/min, and stirring for 15-30min;
(3) Placing a beaker containing an ammonium polyphosphate solution in a high-speed dispersing machine, controlling the rotating speed to be 400-1500r/min, adding a certain amount of aluminum hydroxide, magnesium hydroxide and bentonite, stirring for 15-30min to obtain a component B, and mixing the component AB when in use to obtain the low-VOC-resistant water-based printing ink for corrugated paper;
the concentration of the ammonium oligomeric phosphate solution is 5-25 g/L;
the ammonium polyphosphate solution comprises the following components in parts by weight: aluminum hydroxide: magnesium hydroxide: bentonite = 100 parts: 5-25 parts of: 5-15 parts of: 1-5 parts; controlling the rotating speed to be 400-1500r/min, and stirring for 15-30min;
the component A comprises the following components in parts by mass: component B = 100 parts: 10-50 parts.
Compared with the prior art, the invention has the following advantages:
(1) The preparation method has the advantages of environment-friendly raw materials, simple process and easy industrialized production;
(2) The AB component is separated, namely mixed and used, and the stability of the material is better.
Detailed Description
The present invention will be described in further detail by way of examples, but the scope of the present invention is not limited to the above.
Example 1:
the preparation method of the printing ink for the low-VOC water-based corrugated paper comprises the following steps:
(1) Placing a beaker containing 100 parts of sodium water glass in a high-speed dispersing machine, controlling the rotating speed to be 200r/min, adding 20 parts of styrene-acrylic emulsion, 2 parts of polyvinyl alcohol and 2 parts of cellulose diacetate, and stirring for 15-30min;
(2) Adding 2 parts of pigment and filler into the step (1), controlling the rotating speed to be 300r/min, and stirring for 15min to obtain a component A;
(3) Placing a beaker containing 100 parts of 5g/L ammonium oligomeric phosphate solution in a high-speed dispersing machine, controlling the rotating speed to be 400r/min, adding 5 parts of aluminum hydroxide, 5 parts of magnesium hydroxide and 1 part of bentonite, and stirring for 15min to obtain a component B; when in use, 100 parts of A and 10 parts of B are mixed to obtain the printing ink for the low-VOC-resistant water-based corrugated paper.
The printing ink for low-VOC water-based corrugated paper prepared in the embodiment has VOC of 8g/L according to GB/T38597-2020 standard test.
Example 2:
the preparation method of the printing ink for the low-VOC water-based corrugated paper comprises the following steps:
(1) Placing a beaker containing 100 parts of sodium silicate in a high-speed dispersing machine, controlling the rotating speed to 550r/min, adding 30 parts of styrene-acrylic emulsion, 10 parts of polyvinyl alcohol and 10 parts of cellulose diacetate, and stirring for 30min;
(2) 15 parts of pigment and filler are added in the step (1), the rotating speed is controlled to be 500r/min, and stirring is carried out for 30min, so that a component A is obtained;
(3) Placing a beaker containing 100 parts of 25g/L ammonium oligomeric phosphate solution in a high-speed dispersing machine, controlling the rotating speed to 1500r/min, adding 25 parts of aluminum hydroxide, 15 parts of magnesium hydroxide and 5 parts of bentonite, and stirring for 30min to obtain a component B; when in use, 100 parts of A and 50 parts of B are mixed to obtain the printing ink for the low-VOC-resistant water-based corrugated paper.
The printing ink for low-VOC water-based corrugated paper prepared in the embodiment has VOC of 12g/L according to GB/T38597-2020 standard test.
Example 3:
the preparation method of the printing ink for the low-VOC water-based corrugated paper comprises the following steps:
(1) Placing a beaker containing 100 parts of sodium water glass in a high-speed dispersing machine, controlling the rotating speed to be 300r/min, adding 5 parts of styrene-acrylic emulsion, 4 parts of polyvinyl alcohol and 6 parts of cellulose diacetate, and stirring for 20min;
(2) Adding 4 parts of pigment and filler into the step (1), controlling the rotating speed to be 300r/min, and stirring for 20min to obtain a component A;
(3) Placing a beaker containing 100 parts of 10g/L ammonium oligomeric phosphate solution in a high-speed dispersing machine, controlling the rotating speed to be 600r/min, adding 10 parts of aluminum hydroxide, 5 parts of magnesium hydroxide and 2 parts of bentonite, and stirring for 20min to obtain a component B; when in use, 100 parts of A and 30 parts of B are mixed to obtain the printing ink for the low-VOC-resistant water-based corrugated paper.
The printing ink for low-VOC water-based corrugated paper prepared in the embodiment has VOC of 10g/L according to GB/T38597-2020 standard test.
Example 4:
the preparation method of the printing ink for the low-VOC water-based corrugated paper comprises the following steps:
(1) Placing a beaker containing 100 parts of sodium water glass in a high-speed dispersing machine, controlling the rotating speed to be 400r/min, adding 27.5 parts of styrene-acrylic emulsion, 5 parts of polyvinyl alcohol and 8 parts of cellulose diacetate, and stirring for 25min;
(2) Adding 10 parts of pigment and filler in the step (1), controlling the rotating speed to be 450r/min, and stirring for 25min to obtain a component A;
(3) Placing a beaker containing 100 parts of 20g/L ammonium oligomeric phosphate solution in a high-speed dispersing machine, controlling the rotating speed to be 800r/min, adding 12 parts of aluminum hydroxide, 2.5 parts of magnesium hydroxide and 3 parts of bentonite, and stirring for 30min to obtain a component B; when in use, 100 parts of A and 30 parts of B are mixed to obtain the printing ink for the low-VOC-resistant water-based corrugated paper.
The printing ink for low-VOC water-based corrugated paper prepared in the embodiment has VOC of 9g/L according to GB/T38597-2020 standard test.
Example 5:
the preparation method of the printing ink for the low-VOC water-based corrugated paper comprises the following steps:
(1) Placing a beaker containing 100 parts of sodium water glass in a high-speed dispersing machine, controlling the rotating speed to be 500r/min, adding 22.5 parts of styrene-acrylic emulsion, 4 parts of polyvinyl alcohol and 7.5 parts of cellulose diacetate, and stirring for 28min;
(2) Adding 6 parts of pigment and filler in the step (1), controlling the rotating speed to be 450r/min, and stirring for 30min to obtain a component A;
(3) Placing a beaker containing 100 parts of 8.5g/L ammonium oligomeric phosphate solution in a high-speed dispersing machine, controlling the rotating speed to 1450r/min, adding 20 parts of aluminum hydroxide, 2 parts of magnesium hydroxide and 4.5 parts of bentonite, and stirring for 15min to obtain a component B; when in use, 100 parts of A and 25 parts of B are mixed to obtain the printing ink for the low-VOC-resistant water-based corrugated paper.
The printing ink for low-VOC water-based corrugated paper prepared in the embodiment has VOC of 8g/L according to GB/T38597-2020 standard test.
Table 1 is a data table of VOC test results for the low VOC aqueous corrugated paper printing inks prepared in examples 1-5.
Claims (6)
1. The preparation method of the printing ink for the low-VOC water-based corrugated paper is characterized by comprising the following specific steps:
(1) Placing the beaker containing sodium water glass in a high-speed dispersing machine, controlling the rotating speed to be 200-550r/min, adding a certain amount of styrene-acrylic emulsion, polyvinyl alcohol and cellulose diacetate, and stirring for 15-30min;
(2) Adding a certain amount of pigment and filler into the step (1), controlling the rotating speed to be 300-500r/min, and stirring for 15-30min to obtain a component A;
(3) Placing a beaker containing the ammonium polyphosphate solution in a high-speed dispersing machine, controlling the rotating speed to be 400-1500r/min, adding a certain amount of aluminum hydroxide, magnesium hydroxide and bentonite, stirring for 15-30min to obtain a component B, and mixing the component AB when in use to obtain the low-VOC-resistant water-based printing ink for corrugated paper.
2. The method for preparing the printing ink for the low-VOC aqueous corrugated paper, which is characterized in that: the sodium water glass comprises the following components in parts by weight: styrene-acrylic emulsion: polyvinyl alcohol: cellulose diacetate = 100 parts: 20-30 parts of: 2-10 parts of: 2-10 parts; controlling the rotating speed to be 200-550r/min, and stirring for 15-30min.
3. The method for preparing the printing ink for the low-VOC aqueous corrugated paper, which is characterized in that: the sodium water glass comprises the following components in parts by weight: pigment filler = 100 parts: 2-15 parts; controlling the rotating speed to be 300-500r/min, and stirring for 15-30min.
4. The method for preparing the printing ink for the low-VOC aqueous corrugated paper, which is characterized in that: the concentration of the ammonium oligomeric phosphate solution is 5-25 g/L.
5. The method for preparing the printing ink for the low-VOC aqueous corrugated paper, which is characterized in that: the method comprises the following steps of: aluminum hydroxide: magnesium hydroxide: bentonite = 100 parts: 5-25 parts of: 5-15 parts of: 1-5 parts; controlling the rotating speed to be 400-1500r/min, and stirring for 15-30min.
6. The method for preparing the printing ink for the low-VOC aqueous corrugated paper, which is characterized in that: the component A comprises the following components in parts by weight: component B = 100 parts: 10-50 parts.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310342252.1A CN116285491A (en) | 2023-04-03 | 2023-04-03 | Preparation method of low-VOC (volatile organic compound) water-based printing ink for corrugated paper |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310342252.1A CN116285491A (en) | 2023-04-03 | 2023-04-03 | Preparation method of low-VOC (volatile organic compound) water-based printing ink for corrugated paper |
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| Publication Number | Publication Date |
|---|---|
| CN116285491A true CN116285491A (en) | 2023-06-23 |
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|---|---|---|---|
| CN202310342252.1A Pending CN116285491A (en) | 2023-04-03 | 2023-04-03 | Preparation method of low-VOC (volatile organic compound) water-based printing ink for corrugated paper |
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|---|---|---|---|---|
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2023
- 2023-04-03 CN CN202310342252.1A patent/CN116285491A/en active Pending
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