CN116254061A - Preparation method of water-soluble powdery carbon-aluminum binding agent - Google Patents
Preparation method of water-soluble powdery carbon-aluminum binding agent Download PDFInfo
- Publication number
- CN116254061A CN116254061A CN202310284890.2A CN202310284890A CN116254061A CN 116254061 A CN116254061 A CN 116254061A CN 202310284890 A CN202310284890 A CN 202310284890A CN 116254061 A CN116254061 A CN 116254061A
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- CN
- China
- Prior art keywords
- water
- aluminum
- carbon black
- soluble
- carbon
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000011230 binding agent Substances 0.000 title claims abstract description 81
- RQMIWLMVTCKXAQ-UHFFFAOYSA-N [AlH3].[C] Chemical compound [AlH3].[C] RQMIWLMVTCKXAQ-UHFFFAOYSA-N 0.000 title claims abstract description 77
- 238000002360 preparation method Methods 0.000 title claims abstract description 24
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims abstract description 108
- 239000006229 carbon black Substances 0.000 claims abstract description 99
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims abstract description 54
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims abstract description 54
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 45
- 239000007788 liquid Substances 0.000 claims abstract description 37
- 238000006243 chemical reaction Methods 0.000 claims abstract description 33
- 235000019832 sodium triphosphate Nutrition 0.000 claims abstract description 33
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims abstract description 30
- 239000007787 solid Substances 0.000 claims abstract description 30
- 238000003756 stirring Methods 0.000 claims abstract description 25
- 238000001694 spray drying Methods 0.000 claims abstract description 22
- 239000003054 catalyst Substances 0.000 claims abstract description 18
- 235000006408 oxalic acid Nutrition 0.000 claims abstract description 18
- 230000004913 activation Effects 0.000 claims abstract description 13
- 239000002270 dispersing agent Substances 0.000 claims abstract description 13
- 238000004873 anchoring Methods 0.000 claims abstract description 12
- 238000004090 dissolution Methods 0.000 claims abstract description 12
- 238000010438 heat treatment Methods 0.000 claims abstract description 12
- 230000020477 pH reduction Effects 0.000 claims abstract description 11
- 230000005484 gravity Effects 0.000 claims description 14
- 238000000034 method Methods 0.000 claims description 12
- 239000007864 aqueous solution Substances 0.000 claims description 11
- 238000001132 ultrasonic dispersion Methods 0.000 claims description 11
- 239000000243 solution Substances 0.000 claims description 8
- 239000011734 sodium Substances 0.000 claims description 7
- 238000007865 diluting Methods 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 5
- 239000011229 interlayer Substances 0.000 claims description 3
- 239000007858 starting material Substances 0.000 claims description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 239000007767 bonding agent Substances 0.000 abstract description 26
- RGPUVZXXZFNFBF-UHFFFAOYSA-K diphosphonooxyalumanyl dihydrogen phosphate Chemical compound [Al+3].OP(O)([O-])=O.OP(O)([O-])=O.OP(O)([O-])=O RGPUVZXXZFNFBF-UHFFFAOYSA-K 0.000 abstract description 20
- 239000006185 dispersion Substances 0.000 abstract description 11
- 229920005989 resin Polymers 0.000 description 15
- 239000011347 resin Substances 0.000 description 15
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 12
- 229910052799 carbon Inorganic materials 0.000 description 12
- 239000002245 particle Substances 0.000 description 10
- 239000000853 adhesive Substances 0.000 description 8
- 230000001070 adhesive effect Effects 0.000 description 8
- 230000001276 controlling effect Effects 0.000 description 8
- 239000000463 material Substances 0.000 description 7
- 239000011819 refractory material Substances 0.000 description 7
- 238000005266 casting Methods 0.000 description 6
- 230000003628 erosive effect Effects 0.000 description 6
- 239000002783 friction material Substances 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 6
- 239000012778 molding material Substances 0.000 description 6
- 241000872198 Serjania polyphylla Species 0.000 description 5
- 229910052782 aluminium Inorganic materials 0.000 description 5
- 230000007797 corrosion Effects 0.000 description 5
- 238000005260 corrosion Methods 0.000 description 5
- 239000002609 medium Substances 0.000 description 5
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 description 4
- 230000002378 acidificating effect Effects 0.000 description 4
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 4
- 230000009286 beneficial effect Effects 0.000 description 4
- 238000000576 coating method Methods 0.000 description 4
- 125000000524 functional group Chemical group 0.000 description 4
- 230000003647 oxidation Effects 0.000 description 4
- 238000007254 oxidation reaction Methods 0.000 description 4
- 229920001568 phenolic resin Polymers 0.000 description 4
- 239000005011 phenolic resin Substances 0.000 description 4
- 239000002694 phosphate binding agent Substances 0.000 description 4
- 239000007921 spray Substances 0.000 description 4
- 238000002441 X-ray diffraction Methods 0.000 description 3
- 238000005054 agglomeration Methods 0.000 description 3
- 230000002776 aggregation Effects 0.000 description 3
- 239000002131 composite material Substances 0.000 description 3
- 238000005336 cracking Methods 0.000 description 3
- 230000007547 defect Effects 0.000 description 3
- 238000011065 in-situ storage Methods 0.000 description 3
- 230000035939 shock Effects 0.000 description 3
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000010494 dissociation reaction Methods 0.000 description 2
- 230000005593 dissociations Effects 0.000 description 2
- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 description 2
- 239000011810 insulating material Substances 0.000 description 2
- 239000003973 paint Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 229920000388 Polyphosphate Polymers 0.000 description 1
- 238000005411 Van der Waals force Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 229910021502 aluminium hydroxide Inorganic materials 0.000 description 1
- 229910003481 amorphous carbon Inorganic materials 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 239000002612 dispersion medium Substances 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000003317 industrial substance Substances 0.000 description 1
- 239000012774 insulation material Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000011821 neutral refractory Substances 0.000 description 1
- 230000009965 odorless effect Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000010587 phase diagram Methods 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000001205 polyphosphate Substances 0.000 description 1
- 235000011176 polyphosphates Nutrition 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000012744 reinforcing agent Substances 0.000 description 1
- 230000003014 reinforcing effect Effects 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 238000000859 sublimation Methods 0.000 description 1
- 230000008022 sublimation Effects 0.000 description 1
- 238000012876 topography Methods 0.000 description 1
- 239000003232 water-soluble binding agent Substances 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J1/00—Adhesives based on inorganic constituents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Landscapes
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Ceramic Products (AREA)
Abstract
Description
Claims (9)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN202310284890.2A CN116254061B (en) | 2023-03-22 | 2023-03-22 | Preparation method of water-soluble powdery carbon-aluminum binding agent |
Applications Claiming Priority (1)
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CN202310284890.2A CN116254061B (en) | 2023-03-22 | 2023-03-22 | Preparation method of water-soluble powdery carbon-aluminum binding agent |
Publications (2)
Publication Number | Publication Date |
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CN116254061A true CN116254061A (en) | 2023-06-13 |
CN116254061B CN116254061B (en) | 2024-04-19 |
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CN202310284890.2A Active CN116254061B (en) | 2023-03-22 | 2023-03-22 | Preparation method of water-soluble powdery carbon-aluminum binding agent |
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Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4358500A (en) * | 1981-08-20 | 1982-11-09 | Subtex, Inc. | Flame resistant insulating fabric compositions containing inorganic bonding agent |
CN1120059A (en) * | 1994-09-16 | 1996-04-10 | 淄博市新材料研究所 | Inorganic binder and its preparation method and usage |
KR20110050851A (en) * | 2009-11-09 | 2011-05-17 | 조용호 | Friendly environment inorganic adhesive composition and manufacturing method thereof |
US20120174828A1 (en) * | 2007-02-15 | 2012-07-12 | Dalian Rino Environment Engineering Science And Technology Co., Ltd. | Inorganic composite binders with high-temperature resistance |
-
2023
- 2023-03-22 CN CN202310284890.2A patent/CN116254061B/en active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4358500A (en) * | 1981-08-20 | 1982-11-09 | Subtex, Inc. | Flame resistant insulating fabric compositions containing inorganic bonding agent |
CN1120059A (en) * | 1994-09-16 | 1996-04-10 | 淄博市新材料研究所 | Inorganic binder and its preparation method and usage |
US20120174828A1 (en) * | 2007-02-15 | 2012-07-12 | Dalian Rino Environment Engineering Science And Technology Co., Ltd. | Inorganic composite binders with high-temperature resistance |
KR20110050851A (en) * | 2009-11-09 | 2011-05-17 | 조용호 | Friendly environment inorganic adhesive composition and manufacturing method thereof |
Also Published As
Publication number | Publication date |
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CN116254061B (en) | 2024-04-19 |
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PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
CB03 | Change of inventor or designer information |
Inventor after: Zeng Xianxin Inventor after: Zhang Xinying Inventor after: Li Qiang Inventor after: Li Zhiqiang Inventor after: Hou Gaolin Inventor after: Zeng Qingyang Inventor after: Fan Xuesen Inventor after: Cao Keyuan Inventor after: Zhang Yuhang Inventor after: Wang Dajun Inventor before: Zeng Xianxin Inventor before: Zeng Qingyang Inventor before: Li Zhiqiang Inventor before: Hou Gaolin Inventor before: Fan Xuesen Inventor before: Cao Keyuan Inventor before: Zhang Yuhang Inventor before: Wang Dajun Inventor before: Zhang Xinying |
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