CN116239952A - Welding slag anti-sticking aerosol and preparation method thereof - Google Patents

Welding slag anti-sticking aerosol and preparation method thereof Download PDF

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Publication number
CN116239952A
CN116239952A CN202310056806.1A CN202310056806A CN116239952A CN 116239952 A CN116239952 A CN 116239952A CN 202310056806 A CN202310056806 A CN 202310056806A CN 116239952 A CN116239952 A CN 116239952A
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CN
China
Prior art keywords
stirring
sticking
aerosol
parts
welding slag
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Pending
Application number
CN202310056806.1A
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Chinese (zh)
Inventor
张为敬
梁高健
谢志平
卢金霞
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Zhongshan Tentop Fine Chemical Co ltd
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Zhongshan Tentop Fine Chemical Co ltd
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Priority to CN202310056806.1A priority Critical patent/CN116239952A/en
Publication of CN116239952A publication Critical patent/CN116239952A/en
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D191/00Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/08Anti-corrosive paints
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/20Diluents or solvents
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/63Additives non-macromolecular organic

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Nonmetallic Welding Materials (AREA)

Abstract

The invention provides a welding slag anti-sticking aerosol and a preparation method thereof, wherein the method comprises the following steps: (1) Adding water and sodium benzoate into a reaction kettle in sequence, and stirring; (2) Then adding monoethanolamine and triethanolamine borate, and stirring; (3) adding phospholipid, heating and stirring; (4) adding soybean oil, and stirring; (5) Cooling under stirring, adding antiseptic, and stirring; (6) And (3) filling the agent in the step (5) into a container to obtain the welding slag anti-sticking aerosol. After the welding slag anti-sticking aerosol prepared by the preparation method of the welding slag anti-sticking aerosol is sprayed on the metal surface, the welding slag anti-sticking aerosol can be quickly attached to and spread on the metal surface, has high film forming speed, can be removed by wiping or flushing, is very efficient, and has no welding slag trace.

Description

Welding slag anti-sticking aerosol and preparation method thereof
Technical Field
The invention relates to the technical field of chemical materials, in particular to a welding slag anti-sticking aerosol and a preparation method thereof.
Background
For welding operations such as electric welding, argon arc welding, laser welding and cutting welding in metal processing, mechanical processing, industrial application and the like, metal is melted in a local range in the welding process, and splashes generated when the temperature of a metal part is suddenly increased under the influence of arc light high temperature generated by external gas and heavy current are easy to splash everywhere, the generated 'slag ash' temperature is up to 500 ℃, and when the slag ash falls on the metal surface, the slag ash is burnt and sintered due to the high temperature of the slag ash, dark color to black color and slag bonding are generated, so that the appearance of equipment is influenced, the original state and even performance of the metal surface are damaged by slag bonding, and the corrosion of a metal matrix is accelerated.
In order to solve the problem, a large number of workers invent various protective and isolation products. At present, two types of products are mainly used, namely, a non-aerosol type product is not convenient to use, brushing is needed, construction is difficult in some special positions or angles, or an air gun is used for spraying, and the air gun is required for field conditions, an air compressor and an air compression gun are needed, so that the operation is inconvenient. The other is an aerosol formulation of a primary formulation, generally an aqueous formulation or an oily formulation, wherein the aqueous formulation has poor anti-sticking effect, the welding slag can be effectively separated by beating, the oily formulation is not environment-friendly and forms an oil film, and the oil film is scrubbed later.
Disclosure of Invention
In view of the above problems, one of the objects of the present invention is to provide a method for preparing a slag anti-sticking aerosol, which can be quickly adhered and spread on a metal surface after spraying, can be removed by wiping or washing, is very efficient, and has no slag trace.
In order to achieve the above object, a first aspect of the present invention provides a method for preparing a welding slag anti-sticking aerosol, comprising the steps of:
(1) Adding water and sodium benzoate into a reaction kettle in sequence, and stirring;
(2) Then adding monoethanolamine and triethanolamine borate, and stirring;
(3) Adding phospholipid, heating, and stirring;
(4) Adding soybean oil, and stirring;
(5) Cooling under stirring, adding antiseptic, and stirring;
(6) And (3) filling the agent in the step (5) into a container to obtain the welding slag anti-sticking aerosol.
In some embodiments, a method of preparing a slag anti-stick aerosol includes the steps of:
(1) Sequentially adding 60-80 parts of water and 0.1-1 part of sodium benzoate into a reaction kettle, and stirring;
(2) Adding 0.05-1 part of monoethanolamine and 0.2-5 parts of triethanolamine borate, and stirring;
(3) Adding 10-40 parts of phospholipid, heating and stirring;
(4) Adding 0.5-5 parts of soybean oil, and stirring;
(5) Cooling under stirring, adding 0.1-2 parts of preservative, and stirring for later use;
(6) And (3) filling the agent in the step (5) into a container to obtain the welding slag anti-sticking aerosol.
As examples, the water content may be 60 parts, 62 parts, 64 parts, 66 parts, 68 parts, 70 parts, 72 parts, 74 parts, 76 parts, 78 parts, 80 parts, etc., but is not limited to the recited values, and other non-recited values within the above ranges are equally applicable.
By way of example, the sodium benzoate content may be 0.1 part, 0.2 part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part, 1 part, etc., but is not limited to the recited values, as other non-recited values within each of the above ranges are equally applicable.
As an example, the content of monoethanolamine may be 0.05 parts, 0.1 parts, 0.2 parts, 0.3 parts, 0.4 parts, 0.5 parts, 0.6 parts, 0.7 parts, 0.8 parts, 0.9 parts, 1 part, etc., but is not limited to the recited values, and other non-recited values within the above ranges are equally applicable.
As an example, the content of triethanolamine borate can be 0.2 part, 0.5 part, 1 part, 1.5 part, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, etc., but is not limited to the recited values, and other non-recited values within the above ranges are equally applicable.
As examples, the content of the phospholipid may be 10 parts, 15 parts, 20 parts, 25 parts, 30 parts, 35 parts, 40 parts, etc., but is not limited to the recited values, and other non-recited values within the above-described respective ranges are equally applicable.
As examples, the content of soybean oil may be 0.5 part, 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, etc., but is not limited to the recited values, and other non-recited values within the above ranges are equally applicable.
As an example, the preservative may be contained in an amount of 0.1 part, 0.2 part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part, 1 part, 1.1 part, 1.2 part, 1.3 part, 1.4 part, 1.5 part, 1.6 part, 1.7 part, 1.8 part, 1.9 part, 2 parts, etc., but is not limited to the recited values, and other non-recited values within the above ranges are equally applicable.
In some embodiments, the heating temperature in step (3) is 60-80 ℃. The heating temperature is, for example, 60 ℃, 62 ℃, 64 ℃, 66 ℃, 68 ℃, 70 ℃, 72 ℃, 74 ℃, 76 ℃, 78 ℃, 80 ℃ or the like, but the heating temperature is not limited to the values listed, and other values not listed in the above-mentioned respective value ranges are equally applicable.
In some embodiments, the temperature in step (5) is reduced to below 40 ℃. The temperature is, for example, 40 ℃, 35 ℃, 30 ℃, 25 ℃, etc., but is not limited to the values listed, and other values not listed in the above-mentioned respective value ranges are equally applicable.
In some embodiments, the phospholipid is a vegetable-based phospholipid. Further, the phospholipid is phosphatidylcholine (also known as lecithin).
In some embodiments, the preservative is calcium propionate or potassium sorbate.
Correspondingly, the invention also provides a welding slag anti-sticking aerosol, which is prepared by adopting the preparation method of the welding slag anti-sticking aerosol.
The invention has the beneficial effects that:
(1) According to the invention, plant phospholipids and soybean oil are respectively used as grease, and are emulsified with water through modification to form an oil-water emulsion film, so that the oil-water emulsion film can be quickly attached to and spread on the metal surface after spraying, and the oil-water emulsion film is very efficient and completely free of welding slag marks after one wiping or one flushing after the welding operation is finished;
(2) The oil-water emulsion film provided by the invention has the advantages that the film forming time is quick, namely, the film is sprayed and used, the film is even, and the film is not wiped or washed, so that the film can be stored for at least more than 24 hours, and a large space is reserved for the flexibility of welding operation;
(3) The welding slag anti-sticking aerosol is green and environment-friendly, is prepared by a water-based formula, is harmless to decompose, has characteristic smell of vegetable oil, is mild and non-irritating, and promotes better working environment and user comfort;
(4) The welding slag anti-sticking aerosol disclosed by the invention has no corrosion to metal, and the triethanolamine borate can bring certain rust and corrosion inhibition capability to welding parts and spraying parts.
Detailed Description
The following description is of the preferred embodiments of the present invention, and it should be noted that, for those skilled in the art, it is possible to make several improvements and modifications without departing from the principle of the embodiments of the present invention, and these improvements and modifications are also considered as the protection scope of the embodiments of the present invention.
Example 1
The preparation method of the welding slag anti-sticking aerosol comprises the following steps:
(1) Adding 70 parts of water and 0.3 part of sodium benzoate into a reaction kettle in sequence, and stirring for 20min;
(2) Then adding 0.2 part of monoethanolamine and 1 part of triethanolamine borate, and stirring until the materials are completely dissolved;
(3) Then adding 25 parts of phosphatidylcholine, heating to 65 ℃, and stirring until the phosphatidylcholine is completely dissolved;
(4) Adding 3 parts of soybean oil under stirring, and stirring until the soybean oil is completely dissolved;
(5) Cooling to below 40 ℃ under stirring, adding 0.8 part of potassium sorbate, stirring for about 10 minutes, and stopping stirring for later use;
(6) And (3) filling the agent in the step (5) into a container to obtain the welding slag anti-sticking aerosol.
The welding slag anti-sticking aerosol is sprayed on a place where a welding star is likely to splash at a welding part, and is wiped after welding is finished, wherein the residual rate is 0.
Example 2
The preparation method of the welding slag anti-sticking aerosol comprises the following steps:
(1) Adding 80 parts of water and 0.5 part of sodium benzoate into a reaction kettle in sequence, and stirring for 30min;
(2) Then adding 0.3 part of monoethanolamine and 1.2 parts of triethanolamine borate, and stirring until the materials are completely dissolved;
(3) Then adding 30 parts of phosphatidylcholine, heating to 70 ℃, and stirring until the phosphatidylcholine is completely dissolved;
(4) Adding 3.5 parts of soybean oil under stirring, and stirring until the soybean oil is completely dissolved;
(5) Cooling to below 40 ℃ under stirring, adding 1 part of potassium sorbate, stirring for about 10 minutes, and stopping stirring for later use;
(6) And (3) filling the agent in the step (5) into a container to obtain the welding slag anti-sticking aerosol.
The welding slag anti-sticking aerosol is sprayed on a place where a welding star is likely to splash at a welding part, and is wiped after welding is finished, wherein the residual rate is 0.
Example 3
The preparation method of the welding slag anti-sticking aerosol comprises the following steps:
(1) Adding 75 parts of water and 0.4 part of sodium benzoate into a reaction kettle in sequence, and stirring for 20min;
(2) Then adding 0.3 part of monoethanolamine and 1 part of triethanolamine borate, and stirring until the materials are completely dissolved;
(3) Then 28 parts of phosphatidylcholine is added, and then the mixture is heated to 70 ℃ and stirred until the mixture is completely dissolved;
(4) Adding 3 parts of soybean oil under stirring, and stirring until the soybean oil is completely dissolved;
(5) Cooling to below 40 ℃ under stirring, adding 0.8 part of potassium sorbate, stirring for about 10 minutes, and stopping stirring for later use;
(6) And (3) filling the agent in the step (5) into a container to obtain the welding slag anti-sticking aerosol.
The welding slag anti-sticking aerosol is sprayed on a place where a welding star is likely to splash at a welding part, and is wiped after welding is finished, wherein the residual rate is 0.
Comparative example 1
(1) Adding 70 parts of water and 0.3 part of sodium benzoate into a reaction kettle in sequence, and stirring for 20min;
(2) Then adding 1 part of triethanolamine borate, and stirring until the triethanolamine borate is completely dissolved;
(3) Then adding 25 parts of phosphatidylcholine, heating to 65 ℃, and stirring until the phosphatidylcholine is completely dissolved;
(4) Adding 3 parts of soybean oil under stirring, and stirring until the soybean oil is completely dissolved;
(5) Cooling to below 40 ℃ under stirring, adding 0.8 part of preservative, stirring for about 10 minutes, and stopping stirring for later use;
(6) And (3) filling the agent in the step (5) into a container to obtain the welding slag anti-sticking aerosol.
The welding slag anti-sticking aerosol is sprayed on a welding part where a welding star is likely to splash, and is wiped after welding is finished, and the residual rate is 2%.
Finally, it should be noted that the above embodiments are only for illustrating the technical solution of the present invention and not for limiting the scope of the present invention, and although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that the present invention can be modified or substituted without departing from the spirit and scope of the technical solution of the present invention.

Claims (8)

1. A preparation method of a welding slag anti-sticking aerosol is characterized by comprising the following steps:
(1) Adding water and sodium benzoate into a reaction kettle in sequence, and stirring;
(2) Then adding monoethanolamine and triethanolamine borate, and stirring;
(3) Adding phospholipid, heating, and stirring;
(4) Adding soybean oil, and stirring;
(5) Cooling under stirring, adding antiseptic, and stirring;
(6) And (3) filling the agent in the step (5) into a container to obtain the welding slag anti-sticking aerosol.
2. The method of preparing a slag anti-stick aerosol as set forth in claim 1, comprising the steps of:
(1) Sequentially adding 60-80 parts of water and 0.1-1 part of sodium benzoate into a reaction kettle, and stirring;
(2) Adding 0.05-1 part of monoethanolamine and 0.2-5 parts of triethanolamine borate, and stirring;
(3) Adding 10-40 parts of phospholipid, heating and stirring;
(4) Adding 0.5-5 parts of soybean oil, and stirring;
(5) Cooling under stirring, adding 0.1-2 parts of preservative, and stirring for later use;
(6) And (3) filling the agent in the step (5) into a container to obtain the welding slag anti-sticking aerosol.
3. The method for preparing a slag anti-sticking aerosol according to claim 1, wherein the heating temperature in step (3) is 60-80 ℃.
4. The method for preparing the welding slag anti-sticking aerosol according to claim 1, wherein in the step (5), the temperature is reduced to below 40 ℃.
5. The method of preparing a solder slag anti-sticking aerosol according to claim 1, wherein the phospholipid is a vegetable-based phospholipid.
6. The method of preparing a solder dross anti-sticking aerosol according to claim 5, wherein the phospholipid is phosphatidylcholine.
7. The method of preparing a slag anti-sticking aerosol according to claim 1, wherein the preservative is calcium propionate or potassium sorbate.
8. A slag anti-sticking aerosol prepared by the method of any one of claims 1 to 7.
CN202310056806.1A 2023-01-18 2023-01-18 Welding slag anti-sticking aerosol and preparation method thereof Pending CN116239952A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202310056806.1A CN116239952A (en) 2023-01-18 2023-01-18 Welding slag anti-sticking aerosol and preparation method thereof

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Application Number Priority Date Filing Date Title
CN202310056806.1A CN116239952A (en) 2023-01-18 2023-01-18 Welding slag anti-sticking aerosol and preparation method thereof

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2443972A1 (en) * 2001-03-30 2002-10-10 J & G Chemical Specialties, Llc Barrier coatings
US20130146571A1 (en) * 2011-12-13 2013-06-13 Gigi P. Streeter Anti-spatter composition
CN105008464A (en) * 2013-03-06 2015-10-28 瓦卢瑞克石油天然气法国有限公司 Threaded tubular component protected by a film
CN112048363A (en) * 2020-09-16 2020-12-08 江苏赢新润滑科技有限公司 Environment-friendly anti-splashing liquid for automobile welding

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2443972A1 (en) * 2001-03-30 2002-10-10 J & G Chemical Specialties, Llc Barrier coatings
US20130146571A1 (en) * 2011-12-13 2013-06-13 Gigi P. Streeter Anti-spatter composition
CN105008464A (en) * 2013-03-06 2015-10-28 瓦卢瑞克石油天然气法国有限公司 Threaded tubular component protected by a film
CN112048363A (en) * 2020-09-16 2020-12-08 江苏赢新润滑科技有限公司 Environment-friendly anti-splashing liquid for automobile welding

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