CN116214664A - Deep cavity welding wedge-shaped riving knife material and preparation method thereof - Google Patents
Deep cavity welding wedge-shaped riving knife material and preparation method thereof Download PDFInfo
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- CN116214664A CN116214664A CN202211630832.2A CN202211630832A CN116214664A CN 116214664 A CN116214664 A CN 116214664A CN 202211630832 A CN202211630832 A CN 202211630832A CN 116214664 A CN116214664 A CN 116214664A
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- 238000003466 welding Methods 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title abstract description 17
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- 238000000280 densification Methods 0.000 claims abstract description 18
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- UONOETXJSWQNOL-UHFFFAOYSA-N tungsten carbide Chemical compound [W+]#[C-] UONOETXJSWQNOL-UHFFFAOYSA-N 0.000 claims abstract description 17
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- H01L24/74—Apparatus for manufacturing arrangements for connecting or disconnecting semiconductor or solid-state bodies
- H01L24/78—Apparatus for connecting with wire connectors
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- B28—WORKING CEMENT, CLAY, OR STONE
- B28B—SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
- B28B1/00—Producing shaped prefabricated articles from the material
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Abstract
The invention belongs to the technical field of microelectronic tools, and particularly relates to a deep cavity welding wedge-shaped riving knife material and a preparation method thereof. The chopper is characterized in that the chopper is made of a cylindrical rod body, a transitional wire passing hole is formed in the chopper along the central axis, the transitional wire passing hole is changed from a thick wire passing hole to a thin wire passing hole, and a horn-shaped transitional hole is formed in the middle of the transitional wire passing hole. Meanwhile, the preparation method of the deep cavity welding wedge-shaped chopper material is provided, a powder bed is prepared after tungsten carbide, titanium carbide or ceramic powder is mixed with solid acid, and the high-performance molding of the tungsten carbide, titanium carbide or ceramic material deep cavity welding wedge-shaped chopper bar is realized by adopting a binder injection molding process and subsequent densification treatment. The invention provides a preparation method of a deep cavity welding wedge-shaped chopper with high precision, high efficiency and high cleanliness, which breaks through the difficult problem of machining a hard material complex-shape threading hole, improves the density and strength of parts prepared by a binder injection molding process, and prolongs the service life of chopper materials.
Description
Technical Field
The invention belongs to the technical field of microelectronic tools, and particularly relates to a deep cavity welding wedge-shaped riving knife material and a preparation method thereof.
Background
The wedge-shaped chopper is an important tool for the wire bonding process link in the integrated circuit production, and has the characteristics of small bonding wire distance, low bonding temperature, good bonding quality and the like. The special diagnosis size of the riving knife is small, and the tolerance requirement is strict, so that extremely high perforation machining precision is required when the riving knife is machined. Based on the existing numerical control processing punching equipment and technology, the numerical control processing technology is adopted to carry out punching processing on the riving knife, and a series of problems of low processing precision, high processing difficulty, low processing efficiency and the like exist. If the electric spark machining is adopted for threading the holes, the requirements on the depth-diameter ratio and the precision of the chopper machining can be met, but the machining time is extremely long, and the loss on the tool electrode is extremely high. The cost is high, the efficiency is low, and the method is not suitable for the production of a large number of riving knives. Moreover, the electric spark technology can only process vertical threading holes, and threading holes with transition structures cannot be directly prepared.
At present, the method for preparing the wire-hole rod with the transition structure mainly comprises a welding method and a compression molding method. The welding method is to connect and shape a plurality of parts which are processed separately through brazing. The method can prepare the riving knife bar with a complex threading hole structure, but has the advantages of complex processing process, long production period and weaker strength of the produced riving knife bar at the brazing joint. The pressing forming method is to lay powder in a pressed die, the die is provided with a die core with a transition structure threading hole, the powder is pressed to obtain a blank, and the blank is sintered to obtain a bar stock. The pressing forming method can obtain the riving knife bar with an integral structure, but has high precision requirements on a die and assembly, and is only suitable for preparing parts with simpler internal structures.
Disclosure of Invention
The invention provides a deep cavity welding wedge-shaped riving knife material and a preparation method thereof, which aim to solve the technical problems in the existing riving knife processing process.
The invention aims at providing a deep cavity welding wedge-shaped chopper material, which is a cylindrical rod body (1), wherein a transitional wire through hole (2) is formed in the deep cavity welding wedge-shaped chopper material along a central axis, and a thick wire through hole (3), a transitional hole (4) and a thin wire through hole (5) are formed in the middle of the transitional wire through hole (2).
Further, a transition hole (4) is arranged between the thick threading hole (3) and the thin threading hole (5); the aperture of the rough threading hole (3) is 0.3-1.5 mm; the straightness of the rough threading hole (3) is less than or equal to 0.01 and mm, the coaxiality is less than or equal to 0.01 and mm, and the true roundness is less than or equal to 0.005 and mm; the transition hole (4) is in a horn mouth shape with an included angle of 40-120 degrees and a depth of 0.2-2.0 mm degrees; the aperture of the fine threading hole (5) is 0.1-0.2 and mm; the straightness of the fine wire through hole (5) is less than or equal to 0.01 and mm, the coaxiality is less than or equal to 0.01 and mm, and the true roundness is less than or equal to 0.005 and mm.
Further, the deep cavity welding wedge-shaped chopper material is made of tungsten carbide, titanium carbide or ceramic.
Further, the deep cavity welding wedge-shaped chopper material is a perforated rod material with the outer diameter of 1.5-4.5 mm and the length of 62.0 mm.
The second aim of the invention is to provide a preparation method of the deep cavity welding wedge-shaped riving knife material.
In order to achieve the above purpose, the present invention is realized by the following technical scheme:
a preparation method of a deep cavity welding wedge-shaped chopper material comprises the following steps:
s1, ball-milling and mixing tungsten carbide powder, titanium carbide powder or ceramic powder and solid acid to obtain required powder, and spreading the powder to obtain a powder bed;
s2, selectively spraying an adhesive layer by layer on the powder bed obtained in the step S1, printing and forming the adhesive, keeping a printing piece in the powder bed, evaporating a solvent, solidifying, and removing scattered powder to obtain a green round bar with transitional wire holes;
s3, degreasing the green round bar obtained in the step S2 to obtain a presintered round bar;
s4, sintering the presintered round bar obtained in the step S3 in vacuum to obtain a sintered round bar;
and S5, performing densification treatment on the sintered round bar obtained in the step S4, and performing hot isostatic pressing sintering in an argon atmosphere to obtain the deep cavity welding wedge-shaped chopper material.
Further, the powder of step S1Laser particle size D 50 0.1-35 μm.
Further, the solid acid in step S1 is one of boric acid, borax, succinic acid or maleic acid.
Further, the adhesive in the step S2 is one or a mixture of several of polyvinyl alcohol, hydroxyethyl cellulose, polyamide and polyacrylamide.
Further, the curing process temperature in the step S2 is 90-200 ℃ and the curing time is 1-4 h.
Further, the degreasing process in the step S3 is carried out in a vacuum degreasing furnace at the temperature of 400-600 ℃.
Further, when the pre-sintered round rod in the step S4 is tungsten carbide, the sintering temperature is 1350-2000 ℃; when the presintered round bar is a titanium carbide degreasing round bar, the sintering temperature is 1300-1750 ℃; when the presintered round bar is a ceramic degreasing round bar, the sintering temperature is 1400-1950 ℃.
Further, the sintering temperature of the hot isostatic pressing process in the step S5 is 1200-2000 ℃, and the sintering pressure is 80-120 MPa.
The invention adopts the binder injection molding technology and densification treatment to directly prepare the riving knife bar with the transitional structure threading hole. The binder injection molding technology is that a special printer is used for injecting the binder onto a special powder bed, green bodies are printed layer by layer, the green bodies are solidified and presintered, and in order to further improve the compactness and strength of the material, the presintered parts are densified in a hot isostatic pressing furnace to obtain the rod with the wire-through hole chopper with higher strength. The technology solves the difficulty of batch processing of the threading holes, has the characteristics of short production period, high flexibility and the like, and can prepare parts with complex internal structures. By combining the binder injection molding technology with the hot isostatic pressing sintering technology, the compactness of the bar is improved, and the riving knife material with high strength and long service life is prepared.
Compared with the prior art, the invention has the beneficial effects that:
1. the invention provides a wedge-shaped riving knife material for deep cavity welding and a preparation method thereof, which have the advantages of high precision, high efficiency and low cost, and compared with the machining manufacturing yield, the manufactured riving knife bar material has the advantages of saving a large amount of process time and improving the production efficiency. The adhesive injection molding technology is adopted to produce bars for preparing the deep cavity welded wedge-shaped cleaver in a large batch, and the customized and personalized production can be carried out. The prepared material performance is similar to that of the conventional commercial fine-grained hard alloy and ceramic material by adopting the binder injection molding technology and subsequent densification treatment.
2. In the invention, solid polybasic acid and powder are fully ball-milled and mixed to prepare a powder bed. Because the components of the adhesive contain hydroxyl functional groups, the water-soluble high molecular polymer with the hydroxyl functional groups can react with solid polybasic acid with carboxyl groups at room temperature or under heating conditions to form a crosslinked network. After the treatment of the step S2, the printing part sprayed with the water-based adhesive solution is heated and solidified to form a stable cross-linked network, and the powder bed is removed from the scattered powder, so that the printing green body has good heat resistance and mechanical properties.
3. The bar prepared by the preparation method of the wedge-shaped riving knife bar has high densification degree, and the wedge-shaped riving knife processed by the bar has good bonding quality, effectively ensures the bonding quality of a metal lead and a substrate, has long service life, and improves the welding quality and the welding efficiency of wedge-shaped welding.
Drawings
FIG. 1 is a schematic view of a wedge riving knife material with transitional wire holes prepared in accordance with the present invention.
FIG. 2 is a schematic diagram of a wedge riving knife material with transitional wire holes prepared according to the present invention.
Detailed Description
The technical solutions of the present invention will be clearly and completely described in conjunction with the embodiments of the present invention, and it is apparent that the described embodiments are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
The test methods used in the embodiment of the invention are all conventional methods unless specified otherwise; the materials, reagents and the like used, unless otherwise specified, are those commercially available.
Example 1
As shown in fig. 1, the deep cavity welding wedge-shaped riving knife material is of an integrated structure, and the structure is shown in fig. 2, and comprises a cylindrical rod body (1) and a transitional wire through hole (2) arranged along the central axis inside. The high-strength ceramic tile is manufactured by adopting a binder injection molding technology and subsequent densification treatment.
The preparation method of the tungsten carbide bar comprises the following steps: 1) Particle size of the laser is D 50 Ball milling and mixing tungsten carbide powder with the diameter of 1.0 mu m with maleic acid, and spreading the powder to obtain a powder bed; 2) Using 20 wt% polyvinyl alcohol aqueous solution as adhesive, selectively spraying on powder bed layer by layer, printing and forming adhesive, retaining the printed piece in powder bed, evaporating solvent, solidifying 2 h, solidifying temperature is 110 o C, removing scattered powder to obtain a printed green round bar with a wire through hole; 3) Degreasing the green round bar to obtain a presintered round bar; 4) Sintering the presintered round bar in a sintering furnace under argon atmosphere at 1420 o C, obtaining a sintered round bar; 5) Densification treatment is carried out on the sintered round bar in the argon atmosphere in a hot isostatic pressing furnace, and the sintering temperature is 1360 o And C, sintering the steel bars under the pressure of 100 MPa to obtain the wedge-shaped chopper bars.
The wedge-shaped riving knife bar comprises a cylindrical bar body (1) and a transition type threading hole (2) arranged along a central axis in the bar body, wherein a thick threading hole (3), a transition hole (4) and a thin threading hole (5) are arranged in the middle of the transition type threading hole (2). A transition hole (4) is arranged between the thick threading hole (3) and the thin threading hole (5); the aperture of the rough threading hole (3) is 1.21 mm; the straightness of the thick threading hole (3) is 0.01 and mm, the coaxiality is 0.01 and mm, and the roundness is 0.005 and mm; the transition hole (4) is in an included angle of 91 o Horn mouth shape with depth of 0.51 mm; the aperture of the fine threading hole (5) is 0.10 mm; the straightness of the fine threading hole (5) is 0.01 and mm, the coaxiality is 0.01 and mm, and the roundness is 0.005 and mm. The round bar is made of tungsten carbide, the length of the round bar is 62.1 and mm, and the diameter of the outer circle is1.81 mm, with micron-sized threading holes.
The result shows that according to GB/T3851-2015 method for measuring transverse rupture Strength of hard alloy, under the process, the bending strength of the obtained tungsten carbide green round rod is 3.63 MPa. The bending strength of the tungsten carbide bar after the hot isostatic pressing treatment is 2581 MPa.
Example 2
As shown in fig. 1, the deep cavity welding wedge-shaped riving knife material is of an integrated structure, and the structure is shown in fig. 2, and comprises a cylindrical rod body (1) and a transitional wire through hole (2) arranged along the central axis inside. The high-strength ceramic tile is manufactured by adopting a binder injection molding technology and subsequent densification treatment.
The preparation method of the titanium carbide bar comprises the following steps: 1) Particle size of the laser is D 50 Ball milling and mixing titanium carbide powder with the diameter of 1.0 mu m with maleic acid, and spreading the powder to obtain a powder bed; 2) Using 20 wt% polyvinyl alcohol aqueous solution as adhesive, selectively spraying on powder bed layer by layer, printing and forming adhesive, retaining the printed piece in powder bed, evaporating solvent, solidifying 2 h, solidifying temperature is 110 o C, removing scattered powder to obtain a printed green round bar with a wire through hole; 3) Degreasing the green round bar to obtain a presintered round bar; 4) Sintering the presintered round bar in a sintering furnace under argon atmosphere at 1450 o C, obtaining a sintered round bar; 5) Densification treatment is carried out on the sintered round bar in a hot isostatic pressing furnace under argon atmosphere, and the sintering temperature is 1350 o And C, sintering the steel bars under the pressure of 100 MPa to obtain the wedge-shaped chopper bars.
The wedge-shaped riving knife bar comprises a cylindrical bar body (1) and a transition type threading hole (2) arranged along a central axis in the bar body, wherein a thick threading hole (3), a transition hole (4) and a thin threading hole (5) are arranged in the middle of the transition type threading hole (2). A transition hole (4) is arranged between the thick threading hole (3) and the thin threading hole (5). The aperture of the rough threading hole (3) is 1.19 and mm; the straightness of the thick threading hole (3) is 0.01 and mm, the coaxiality is 0.01 and mm, and the roundness is 0.005 and mm; the transition hole (4) has an included angle of 90 DEG o Horn mouth shape with a depth of 0.50 mm; the aperture of the fine threading hole (5) is 0.10 mm; the straightness of the fine threading hole (5) is 0.01 mm, coaxiality 0.01 mm and roundness 0.005 mm. The round bar is made of titanium carbide, the length of the round bar is 62.0 mm, the diameter of the outer circle is 1.80 mm, and the round bar is provided with micron-sized wire holes.
The result shows that according to GB/T3851-2015 method for measuring transverse rupture Strength of hard alloy, under the process, the obtained titanium carbide green round bar has the bending strength of 3.78 MPa. The bending strength of the titanium carbide bar after the hot isostatic pressing treatment is 1734 MPa.
Example 3
As shown in fig. 1, the deep cavity welding wedge-shaped riving knife material is of an integrated structure, and the structure is shown in fig. 2, and comprises a cylindrical rod body (1) and a transitional wire through hole (2) arranged along the central axis inside. The high-strength ceramic tile is manufactured by adopting a binder injection molding technology and subsequent densification treatment.
The preparation method of the ceramic bar comprises the following steps: 1) Particle size of the laser is D 50 Ball milling and mixing ceramic powder with the diameter of 2.0 mu m with boric acid, and spreading the powder to obtain a powder bed; 2) Using 30 wt% hydroxyethyl cellulose water solution as adhesive, selectively spraying on powder bed layer by layer, printing and molding with adhesive, retaining the printed part in powder bed, evaporating solvent, and solidifying 2 h at a solidifying temperature of 120 deg.F o C, removing scattered powder to obtain a printed green round bar with a wire through hole; 3) Degreasing the green round bar to obtain a presintered round bar; 4) Sintering the presintered round bar in a sintering furnace under argon atmosphere at a sintering temperature of 1410 o C, obtaining a sintered round bar; 5) Densification treatment is carried out on the sintered round bar in a hot isostatic pressing furnace under argon atmosphere, and the sintering temperature is 1370 o And C, sintering the steel bars under the pressure of 100 MPa to obtain the wedge-shaped chopper bars.
The wedge-shaped riving knife bar comprises a cylindrical bar body (1) and a transition type threading hole (2) arranged along a central axis in the bar body, wherein a thick threading hole (3), a transition hole (4) and a thin threading hole (5) are arranged in the middle of the transition type threading hole (2). A transition hole (4) is arranged between the thick threading hole (3) and the thin threading hole (5); the aperture of the rough threading hole (3) is 1.20 mm; the straightness of the thick threading hole (3) is 0.01 and mm, the coaxiality is 0.01 and mm, and the roundness is 0.005 and mm; the transition hole (4) has an included angle of 89 o Depth of0.51 A horn mouth shape of mm; the aperture of the fine threading hole (5) is 0.10 mm; the straightness of the fine threading hole (5) is 0.01 and mm, the coaxiality is 0.01 and mm, and the roundness is 0.005 and mm. The round bar is made of ceramic, the length of the round bar is 62.0 mm, the diameter of the outer circle is 3.90 mm, and the round bar is provided with micron-sized wire holes.
The result shows that according to GB/T3851-2015 method for measuring transverse rupture Strength of hard alloy, under the process, the obtained ceramic green round rod has bending strength of 3.51 MPa. The ceramic bar after hot isostatic pressing treatment has the bending strength of 661 MPa.
Comparative example 1
As shown in fig. 1, the deep cavity welding wedge-shaped riving knife material is of an integrated structure, and the structure is shown in fig. 2, and comprises a cylindrical rod body (1) and a transitional wire through hole (2) arranged along the central axis inside. The high-strength ceramic tile is manufactured by adopting a binder injection molding technology and subsequent densification treatment. The preparation method of the tungsten carbide bar comprises the following steps: 1) Particle size of the laser is D 50 Ball milling and mixing tungsten carbide powder with the particle size of 1.0 mu m, and spreading the powder to obtain a powder bed; 2) Using 20 wt% polyvinyl alcohol aqueous solution as adhesive, selectively spraying on powder bed layer by layer, printing and forming adhesive, retaining the printed piece in powder bed, evaporating solvent, solidifying 2 h, solidifying temperature is 110 o C, removing scattered powder to obtain a printed green round bar with a wire through hole; 3) Degreasing the green round bar to obtain a presintered round bar; 4) Sintering the presintered round bar in a sintering furnace under argon atmosphere at 1420 o C, obtaining a sintered round bar; 5) Densification treatment is carried out on the sintered round bar in the argon atmosphere in a hot isostatic pressing furnace, and the sintering temperature is 1360 o And C, sintering the steel bars under the pressure of 100 MPa to obtain the wedge-shaped chopper bars.
The wedge-shaped riving knife bar comprises a cylindrical bar body (1) and a transition type threading hole (2) arranged along a central axis in the bar body, wherein a thick threading hole (3), a transition hole (4) and a thin threading hole (5) are arranged in the middle of the transition type threading hole (2). A transition hole (4) is arranged between the thick threading hole (3) and the thin threading hole (5); the aperture of the rough threading hole (3) is 1.21 mm; the straightness of the thick threading hole (3) is 0.01 and mm, the coaxiality is 0.01 and mm, and the roundness is 0.005 and mm; the transition isThe included angle of the holes (4) is 90 o Horn mouth shape with depth of 0.49 mm; the aperture of the fine threading hole (5) is 0.10 mm; the straightness of the fine threading hole (5) is 0.01 and mm, the coaxiality is 0.01 and mm, and the roundness is 0.005 and mm. The round bar is made of tungsten carbide, the length of the round bar is 62.0 and mm, the diameter of the outer circle is 1.81 and mm, and the round bar is provided with micron-sized wire holes.
The result shows that according to GB/T3851-2015 method for measuring transverse rupture Strength of hard alloy, under the process, the bending strength of the obtained tungsten carbide green round rod is 3.09 MPa. The bending strength of the tungsten carbide bar after the hot isostatic pressing treatment is 2194 MPa.
Comparative example 2
As shown in fig. 1, the deep cavity welding wedge-shaped riving knife material is of an integrated structure, and the structure is shown in fig. 2, and comprises a cylindrical rod body (1) and a transitional wire through hole (2) arranged along the central axis inside. The high-strength ceramic tile is manufactured by adopting a binder injection molding technology and subsequent densification treatment.
The preparation method of the titanium carbide bar comprises the following steps: 1) Particle size of the laser is D 50 Ball milling and mixing titanium carbide powder with the particle size of 1.0 mu m, and spreading the powder to obtain a powder bed; 2) Using 20 wt% polyvinyl alcohol aqueous solution as adhesive, selectively spraying on powder bed layer by layer, printing and forming adhesive, retaining the printed piece in powder bed, evaporating solvent, solidifying 2 h, solidifying temperature is 110 o C, removing scattered powder to obtain a printed green round bar with a wire through hole; 3) Degreasing the green round bar to obtain a presintered round bar; 4) Sintering the presintered round bar in a sintering furnace under argon atmosphere at 1450 o C, obtaining a sintered round bar; 5) Densification treatment is carried out on the sintered round bar in a hot isostatic pressing furnace under argon atmosphere, and the sintering temperature is 1350 o And C, sintering the steel bars under the pressure of 100 MPa to obtain the wedge-shaped chopper bars.
The wedge-shaped riving knife bar comprises a cylindrical bar body (1) and a transition type threading hole (2) arranged along a central axis in the bar body, wherein a thick threading hole (3), a transition hole (4) and a thin threading hole (5) are arranged in the middle of the transition type threading hole (2). A transition hole (4) is arranged between the thick threading hole (3) and the thin threading hole (5). The aperture of the rough threading hole (3) is 1.21 mm; the straightness of the thick threading hole (3) is 0.01 and mm, the coaxiality is 0.01 and mm, and the roundness is 0.005 and mm; the transition hole (4) is in an included angle of 91 o Horn mouth shape with depth of 0.49 mm; the aperture of the fine threading hole (5) is 0.10 mm; the straightness of the fine threading hole (5) is 0.01 and mm, the coaxiality is 0.01 and mm, and the roundness is 0.005 and mm. The round bar is made of titanium carbide, the length of the round bar is 62.0 and mm, the diameter of the outer circle is 1.79 and mm, and the round bar is provided with micron-sized wire holes.
The result shows that according to GB/T3851-2015 method for measuring transverse rupture Strength of hard alloy, under the process, the bending strength of the obtained titanium carbide green round bar is 2.67 MPa. The bending strength of the titanium carbide bar after the hot isostatic pressing treatment is 1263 MPa.
Comparative example 3
As shown in fig. 1, the deep cavity welding wedge-shaped riving knife material is of an integrated structure, and the structure is shown in fig. 2, and comprises a cylindrical rod body (1) and a transitional wire through hole (2) arranged along the central axis inside. The high-strength ceramic tile is manufactured by adopting a binder injection molding technology and subsequent densification treatment.
The preparation method of the ceramic bar comprises the following steps: 1) Particle size of the laser is D 50 Ball milling and mixing ceramic powder with the diameter of 2.0 mu m, and spreading the powder to obtain a powder bed; 2) Using 30 wt% hydroxyethyl cellulose water solution as adhesive, selectively spraying on powder bed layer by layer, printing and molding with adhesive, retaining the printed part in powder bed, evaporating solvent, and solidifying 2 h at a solidifying temperature of 120 deg.F o C, removing scattered powder to obtain a printed green round bar with a wire through hole; 3) Degreasing the green round bar to obtain a presintered round bar; 4) Sintering the presintered round bar in a sintering furnace under argon atmosphere at a sintering temperature of 1410 o C, obtaining a sintered round bar; 5) Densification treatment is carried out on the sintered round bar in a hot isostatic pressing furnace under argon atmosphere, and the sintering temperature is 1370 o And C, sintering the steel bars under the pressure of 100 MPa to obtain the wedge-shaped chopper bars.
The wedge-shaped riving knife bar comprises a cylindrical bar body (1) and a transition type threading hole (2) arranged along a central axis in the bar body, wherein a thick threading hole (3), a transition hole (4) and a thin threading hole (5) are arranged in the middle of the transition type threading hole (2). The said coarseA transition hole (4) is arranged between the threading hole (3) and the fine threading hole (5); the aperture of the rough threading hole (3) is 1.20 mm; the straightness of the thick threading hole (3) is 0.01 and mm, the coaxiality is 0.01 and mm, and the roundness is 0.005 and mm; the transition hole (4) is in an included angle of 91 o Horn mouth shape with a depth of 0.50 mm; the aperture of the fine threading hole (5) is 0.11 mm; the straightness of the fine threading hole (5) is 0.01 and mm, the coaxiality is 0.01 and mm, and the roundness is 0.005 and mm. The round bar is made of ceramic, the length of the round bar is 62.0 mm, the diameter of the outer circle is 3.91 mm, and the round bar is provided with micron-sized wire holes.
The result shows that according to GB/T3851-2015 method for measuring transverse rupture Strength of hard alloy, under the process, the obtained ceramic green round rod has bending strength of 2.94 MPa. The ceramic bar after hot isostatic pressing treatment has a bending strength of 580 MPa.
By comparing the embodiment 1 with the comparative embodiment 1, the embodiment 2 with the comparative embodiment 2 and the embodiment 3 with the comparative embodiment 3, it can be seen that the solid acid added in the invention can make the thermoplastic binder exert better bonding effect, provide enough strength for subsequent treatment of the green compact, and have better mechanical properties, and can prepare hard alloy and metal ceramic parts with higher precision and complex internal structure through the process of the invention.
It should be understood that the foregoing description of the specific embodiments is merely illustrative of the invention, and is not intended to limit the invention, and that any modifications, equivalents, improvements, etc. that fall within the spirit and principles of the invention are intended to be included within the scope of the invention.
Claims (10)
1. The deep cavity welding wedge-shaped chopper material is characterized in that the deep cavity welding wedge-shaped chopper material is a cylindrical rod body (1), a transitional wire through hole (2) is formed in the deep cavity welding wedge-shaped chopper material along a central axis, and a thick wire through hole (3), a transitional hole (4) and a thin wire through hole (5) are formed in the middle of the transitional wire through hole (2).
2. The deep cavity welding wedge chopper material according to claim 1, wherein a transition hole (4) is arranged between the thick wire through hole (3) and the thin wire through hole (5); the aperture of the rough threading hole (3) is 0.3-1.5 mm; the straightness of the rough threading hole (3) is less than or equal to 0.01 and mm, the coaxiality is less than or equal to 0.01 and mm, and the true roundness is less than or equal to 0.005 and mm; the transition hole (4) is in a horn mouth shape with an included angle of 40-120 degrees and a depth of 0.2-2.0 mm degrees; the aperture of the fine threading hole (5) is 0.1-0.2 and mm; the straightness of the fine wire through hole (5) is less than or equal to 0.01 and mm, the coaxiality is less than or equal to 0.01 and mm, and the true roundness is less than or equal to 0.005 and mm.
3. The deep cavity welded wedge chopper material of claim 1, wherein the deep cavity welded wedge chopper material is a perforated rod material with an outer diameter of 1.5-4.5 mm and a length of 62.0 mm, and is made of tungsten carbide, titanium carbide or ceramic.
4. A method of preparing a deep cavity welded wedge cleaver material in accordance with any one of claims 1-3, comprising the steps of:
s1, ball-milling and mixing tungsten carbide powder, titanium carbide powder or ceramic powder and solid acid to obtain required powder, and spreading the powder to obtain a powder bed;
s2, selectively spraying an adhesive layer by layer on the powder bed obtained in the step S1, printing and forming the adhesive, keeping a printing piece in the powder bed, evaporating a solvent, solidifying, and removing scattered powder to obtain a green round bar with transitional wire holes;
s3, degreasing the green round bar to obtain a presintered round bar;
s4, sintering the presintered round bar in vacuum to obtain a sintered round bar;
and S5, carrying out densification treatment on the sintered round bar, and carrying out hot isostatic pressing sintering in an argon atmosphere to obtain the riving knife.
5. The method according to claim 4, wherein the powder of step S1 has a laser particle size D 50 0.1-35 μm.
6. The method according to claim 4, wherein the solid acid in step S1 is one of boric acid, borax, succinic acid and maleic acid.
7. The method according to claim 4, wherein the binder in step S2 is one or more of polyvinyl alcohol, hydroxyethyl cellulose, polyamide, and polyacrylamide.
8. The method according to claim 4, wherein the curing process temperature in step S2 is 90-200deg.C and the curing time is 1-4 h.
9. The method according to claim 4, wherein the degreasing process in step S3 is performed in a vacuum degreasing furnace at 400-600 ℃.
10. The method according to claim 4, wherein the sintering temperature of the hot isostatic pressing process in step S5 is 1200-2000 ℃ and the sintering pressure is 80-120 MPa.
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