CN116120999A - Insulating electronic component cleaning agent and preparation method and application thereof - Google Patents
Insulating electronic component cleaning agent and preparation method and application thereof Download PDFInfo
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- CN116120999A CN116120999A CN202211639690.6A CN202211639690A CN116120999A CN 116120999 A CN116120999 A CN 116120999A CN 202211639690 A CN202211639690 A CN 202211639690A CN 116120999 A CN116120999 A CN 116120999A
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- electronic component
- cleaning agent
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- component cleaning
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- 239000012459 cleaning agent Substances 0.000 title claims abstract description 67
- 238000002360 preparation method Methods 0.000 title abstract description 11
- 239000002904 solvent Substances 0.000 claims abstract description 22
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- BOSAWIQFTJIYIS-UHFFFAOYSA-N 1,1,1-trichloro-2,2,2-trifluoroethane Chemical compound FC(F)(F)C(Cl)(Cl)Cl BOSAWIQFTJIYIS-UHFFFAOYSA-N 0.000 description 1
- COAUHYBSXMIJDK-UHFFFAOYSA-N 3,3-dichloro-1,1,1,2,2-pentafluoropropane Chemical compound FC(F)(F)C(F)(F)C(Cl)Cl COAUHYBSXMIJDK-UHFFFAOYSA-N 0.000 description 1
- 241000207199 Citrus Species 0.000 description 1
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Images
Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/825—Mixtures of compounds all of which are non-ionic
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/162—Organic compounds containing Si
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/18—Hydrocarbons
- C11D3/188—Terpenes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2006—Monohydric alcohols
- C11D3/201—Monohydric alcohols linear
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2068—Ethers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/28—Heterocyclic compounds containing nitrogen in the ring
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/43—Solvents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
-
- C11D2111/22—
Abstract
The invention relates to an insulating electronic component cleaning agent, a preparation method and application thereof, and the cleaning agent comprises oil-soluble agent, N-methyl pyrrolidone, D-limonene, diethylene glycol butyl ether, siloxane, nonionic surfactant and antistatic agent. The insulating electronic component cleaning agent has good compatibility with all electronic components, excellent electrical insulation performance, capability of realizing uninterrupted power cleaning of electrified equipment, good cleaning power and certain anti-fouling capability; and the product has low odor, no residue, no aromatic hydrocarbon solvent and no ODS component, and is double friendly to environment and cleaning personnel.
Description
Technical Field
The invention belongs to the technical field of cleaning agents, and particularly relates to an insulating electronic component cleaning agent, a preparation method and application thereof.
Background
All-weather continuous acquisition, identification, modulation, conversion, transmission and processing of various forms and various types of information are carried out on various charged devices. In the long-term continuous operation process of the equipment, various dust, moisture, oil smoke, acid gas, salt, metal dust, static electricity and various charged particles are deposited on the surface of the equipment by physical adsorption, so that serious pollution of the equipment is caused, the heat radiation capability of the equipment is reduced, and the operation quality and the operation reliability are reduced. These contaminants also create additional "microcircuitry effects" on the circuitry within the device, resulting in "corrosion-inhibiting" effects, causing poor contact with the device, reduced impedance, leakage, short circuits, bit errors, bad plates, etc., and also causing soft failures such as increased line energy loss, signal attenuation, malfunction, rate and quality instability.
There are two ways to clean the electrification equipment: firstly, the traditional physical method is that blowing, sweeping and wiping after power failure, and the power-on operation is continued after the cleaning agent and/or water are completely evaporated; the cleaning mode affects the normal operation of the equipment, and once cleaning agent or water remains on the equipment, short circuit and damage to the equipment can be caused. And secondly, the electric power is continuously cut off, and chemical cleaning with excellent electric insulation is used for carrying out electrified cleaning. However, the ODS solvent is added into the product at present, so that the substance has extremely strong damage to the ozone layer, has certain toxicity and is not friendly to operators and the environment. For example, CN202110306874 discloses a cleaning agent for electrical equipment, wherein dichloroethane and trifluorotrichloroethane are used as ODS, and dichloroethane is a medium and high toxic substance, has carcinogenic effect, and can generate paralysis effect on central nervous system after long-term use. Can cause damage to liver, kidney, heart and trigeminal nerve. For example, the patent application with the application number of CN202110156661 discloses a cleaning agent for a power transformer, and the dichloropentafluoropropane in the raw material belongs to halogen-containing substances and has a depletion effect on an ozone layer; more than 50 parts of tetrachloroethylene is also used, and high concentrations of tetrachloroethylene can lead to dizziness, headache, drowsiness, confusion, nausea, difficulty speaking and walking, loss of consciousness and death. On 10 and 27 days 2017, the world health organization international cancer research institute published a list of carcinogens, tetrachloroethylene (perchloroethylene) was in the class 2A carcinogen list. Tetrachloroethylene (perchloroethylene) was listed in the list of toxic and hazardous water contaminants (first lot) at day 7 and 23 of 2019.
Therefore, how to obtain a cleaning agent which is friendly to the environment and cleaning personnel and is used for cleaning electrical equipment without power failure is a problem to be solved.
Disclosure of Invention
In order to overcome the problems in the prior art, the invention provides an insulating electronic component cleaning agent, a preparation method and application thereof, wherein the cleaning agent has good compatibility with all electronic components, excellent electrical insulation performance, and can realize uninterrupted cleaning of electrified equipment, and meanwhile, the cleaning agent has good cleaning power and certain anti-fouling capability; and the product has low odor, no residue, no aromatic hydrocarbon solvent and no ODS component, and is double friendly to environment and cleaning personnel.
The purpose of the invention is realized in the following way:
the invention provides an insulating electronic component cleaning agent, which comprises the following raw materials in parts by weight:
solvent oil | 40-70 |
N-methylpyrrolidone | 3-10 |
D-limonene | 2-15 |
Diethylene glycol butyl ether | 5-15 |
Silicone | 2-5 |
Nonionic surfactant | 1-5 |
Antistatic agent | 0.1-3 |
。
Further, the raw materials of the cleaning agent also comprise alcohols, and the weight ratio of the alcohols is as follows:
alcohols | 2-10 |
。
Further, the solvent oil is low-odor environment-friendly solvent oil with desulfurization, denitrification and dearomatization, and specifically one or more of D30, D40, D60, D70 and D80 (commercial brand of solvent oil). Wherein, D30 volatilizes fast, the flash point is low, can be used in the open space; if in a closed space, a formula with high D80 proportion can be adopted.
Further, the alcohol is one or two of ethanol or glycol. The micromolecular alcohols have good permeability, are easier to permeate into dirt, and provide conditions for subsequent cleaning.
Further, the siloxane is one or a mixture of more than one of polydimethylsiloxane, tetramethyl cyclotetrasiloxane and octamethyl cyclotetrasiloxane. The siloxane has good electrical insulation property, certain anti-fouling capability, and can improve the pressure resistance of the cleaning agent, and meanwhile, a layer of protective film with high insulation property is formed on the surface of the electronic equipment, so that the electronic equipment can be hydrophobic and dustproof. The cleaning frequency can be reduced after long-term use.
Further, the nonionic surfactant is any one or a mixture of several of fatty alcohol polyoxyethylene ether, alkylphenol polyoxyethylene ether and alkyl glycoside.
Further, the antistatic agent is ethoxy cocoalkylamine.
The second aspect of the invention provides a preparation method of the insulating electronic component cleaning agent, which comprises the following steps:
all the raw materials in the cleaning agent are added into a normal pressure closed container according to the weight portion ratio, and stirred for 0.5-1h at the speed of 50-200r/min under the condition of 20+/-10 ℃ to obtain the insulating electronic component cleaning agent.
The third aspect of the invention provides a method for using the insulating electronic component cleaning agent, wherein compressed dry air is needed when spray cleaning is selected, sundries including dust and iron powder on the surface of an electronic component to be cleaned are blown off, and then a spray gun is used for sucking the insulating electronic component cleaning agent to spray clean the electronic component; for small-sized electrical equipment or parts, a soaking method is adopted, the electronic component to be cleaned is directly soaked in the insulating electronic component cleaning agent, and the electronic component is fished out after 5-15 minutes.
According to a fourth aspect of the invention, there is provided the use of an oil-solubilizing agent, N-methylpyrrolidone composition for improving detergency of a cleaning agent and avoiding swelling of plastics, wherein the oil-solubilizing agent, N-methylpyrrolidone composition comprises the following components in parts by weight:
solvent oil | 40-70 |
N-methylpyrrolidone | 3-10 |
Preferably, the weight part ratio of the nonpolar solvent-solvent oil to the polar solvent-N-methyl pyrrolidone is 9-12: 1.
compared with the prior art, the invention has the advantages that:
1. the raw materials of the insulating electronic component cleaning agent disclosed by the invention are environment-friendly solvents, do not contain aromatic solvents or ODS components, and are double-friendly to the environment and cleaning personnel; meanwhile, the cleaning agent has good electrical insulation performance, has higher volume resistivity and dielectric constant, is safe to use, does not influence the normal operation of equipment under the condition of charged cleaning, and can ensure the absolute safety of personnel and equipment;
2. according to the invention, the non-polar solvent-solvent oil and the polar solvent-N-methyl pyrrolidone are found to have good cleaning effect on various polar or non-polar pollutants on equipment according to a similar compatibility principle under the condition of reasonable proportion (40-70:3-10, more preferably 9-12:1), and have good compatibility on plastics, paint, metal, ceramic and the like in various components of the equipment through tests;
3. the insulating electronic component cleaning agent disclosed by the invention has the advantages that a proper amount of siloxane is added, so that the pressure resistance value of the cleaning agent can be improved, and meanwhile, a layer of high-insulativity protective film is formed on the surface of electronic equipment, so that the cleaning agent can be prevented from being subjected to hydrophobic and dust. The cleaning frequency can be reduced after long-term use; the nonionic surfactant selected in the system is not ionized and is not easy to be adsorbed on the surface of an object, so that the electric performance of a cleaning object is not affected, and meanwhile, the nonionic surfactant has good detergency, the permeability of the system is increased in the cleaning process, dirt is more soluble in being emulsified and stripped, and the cleaning force of a product is improved.
4. The preparation method of the insulating electronic component cleaning agent has the advantages of simple process, energy conservation and consumption reduction.
Drawings
The invention is further described below with reference to the drawings and examples.
FIG. 1 is a picture of a circuit board before cleaning;
fig. 2 is a photograph of a circuit board cleaned with the cleaning agent for insulating electronic components according to example 4 of the present invention.
Detailed Description
In the following examples, unless otherwise specified, the materials and experimental equipment involved are commercially available.
The raw materials are shown in Table 1.
TABLE 1
The experimental apparatus is shown in Table 2.
TABLE 2
Device name/model | Source |
Atmospheric pressure closed container | Tin-free Dongqi mechanical Co Ltd |
In the following examples, the performance test methods involved are as follows:
ODS content and benzene solvent content: the test was conducted according to JIS K0123-2006 standard.
Volume resistivity: the test was carried out according to DL/T421 "volume resistivity method for Electrical oil".
Power frequency breakdown voltage: according to GB/T507 'insulation oil breakdown voltage measurement'.
Cleaning rate: the test was carried out according to GB/T25097-2010 "live cleaning agent for insulator" 6.7.
Corrosion characteristics: the test was carried out according to GB/T25097-2010 "live cleaning agent for insulator" 6.4.
Example 1:
the embodiment provides an insulating electronic component cleaning agent, which comprises oil-soluble agent, N-methyl pyrrolidone, D-limonene, diethylene glycol butyl ether, alcohols, siloxane, nonionic surfactant and ethoxy coco alkylamine, wherein the weight parts of the raw materials are shown in table 3.
The solvent oil is low-odor environment-friendly solvent oil with desulfurization, denitrification and dearomatization, has low odor, is nontoxic and non-irritating, and is safer for users; meanwhile, the solvent is a nonpolar solvent, and can effectively dissolve oil stains on the surface of an object according to a similar compatibility principle, so as to achieve a certain cleaning effect. The solvent oil used in this example was a mixture of three of D40, D60 and D80.
The N-methyl pyrrolidone is a polar solvent with good stability, and is an excellent cleaning agent for high-precision electronics, circuit boards and lithium batteries. The two are matched for use, so that the detergency of the cleaning agent can be improved, and the swelling of plastics can be avoided.
The D-limonene is a natural ingredient in a variety of fruits (mainly citrus), vegetables and spices, has very good permeability, and can rapidly remove dirt on hard surfaces. In addition, the raw material is lemon-flavored liquid, and the lemon-flavored liquid can bring pleasant smell to the product when being added into a system.
The ethoxy coco alkylamine is used as an antistatic agent, can effectively disinfect static accumulation generated by equipment friction, prevent static interference and dust adhesion, and can effectively enhance the anti-fouling performance of equipment.
The preparation method of the insulating electronic component cleaning agent comprises the following steps:
all raw materials in the cleaning agent are added into a normal pressure closed container according to the weight part ratio shown in the table 3, and stirred for 0.5-1h at the speed of 50-200r/min under the condition of 20+/-10 ℃ to obtain the insulating electronic component cleaning agent.
The application method of the insulating electronic component cleaning agent comprises the following steps: spray washing or soaking method is adopted. Specifically, when a spray washing method is selected, compressed dry air is needed to blow off dust, iron powder and other impurities on the surface of the circuit board to be washed, and then a spray gun is used for sucking a cleaning agent for spray washing. If the equipment is seriously polluted, repeated spray washing is needed. After cleaning, the cleaning agent is quickly dried, and can be dried by using dry air to help the cleaning agent to volatilize quickly. For small-sized electrical equipment or parts, the small-sized electrical equipment or parts can be directly soaked for 10 minutes and then fished out.
Examples 2 to 5:
examples 2 to 5 respectively provide an insulating electronic component cleaning agent, the types of raw materials, the preparation method and the using method are the same as those of example 1, and the weight parts of the raw materials are shown in Table 3.
The effect patterns before and after cleaning the circuit board by using the insulating electronic component cleaning agent described in example 4 are shown in fig. 1 and 2, respectively. After cleaning, the circuit board is cleaned as new, and the upper coating layer, the IC chip, various metal components, plastics and metal tube shells are free from corrosion.
Comparative examples 1 to 2:
in order to explore the influence of the proportioning relation of the oil-soluble agent and N-methyl pyrrolidone on the cleaning agent of the insulating electronic components, the decontamination capability and the corrosiveness of the electrical equipment, the cleaning agent of the electronic components is prepared according to the raw materials and the preparation method used in the example 1, and the weight parts of the raw materials are shown in the table 3.
TABLE 3 Table 3
The insulating electronic component cleaning agent prepared by the above examples and comparative examples was used to test key indexes, and the results are shown in table 4 below.
TABLE 4 Performance test results
Comparative examples 3 to 4:
to investigate the influence of D-limonene on corrosiveness of an insulating electronic component cleaning agent, the electronic component cleaning agent was prepared according to the raw materials and the preparation method used in example 1, and the weight parts of the raw materials are shown in Table 5.
TABLE 5
The insulating electronic component cleaning agents prepared in comparative examples 3 and 4 were subjected to key index tests, and the results are shown in Table 6 below.
TABLE 6 Performance test results
D-limonene is excessively added, and has an obvious swelling effect on PVC materials due to excellent permeation effect, so that the risk of damaging the wire materials exists.
Finally, it should be noted that the above only illustrates the technical solution of the present invention and is not limiting, and although the present invention has been described in detail with reference to the preferred arrangement, it should be understood by those skilled in the art that modifications and equivalents may be made to the technical solution of the present invention without departing from the spirit and scope of the technical solution of the present invention.
Claims (10)
1. The insulating electronic component cleaning agent is characterized by comprising the following raw materials in parts by weight:
。
2. The insulating electronic component cleaning agent according to claim 1, wherein the cleaning agent further comprises alcohols in parts by weight:
。
3. The insulating electronic component cleaning agent according to claim 1, wherein the solvent oil is a low-odor environment-friendly solvent oil for desulfurizing, denitrifying, and dearomatizing.
4. The insulating electronic component cleaning agent according to claim 2, wherein the alcohol is one or a mixture of two of ethanol and ethylene glycol.
5. The insulating electronic component cleaning agent according to claim 1, wherein the siloxane is one or a mixture of a plurality of polydimethyl siloxane, tetramethyl cyclotetrasiloxane, and octamethyl cyclotetrasiloxane.
6. The insulating electronic component cleaning agent according to claim 1, wherein the nonionic surfactant is any one or a mixture of several of fatty alcohol polyoxyethylene ether, alkylphenol polyoxyethylene ether, and alkyl glycoside.
7. The insulating electronic component cleaning agent according to claim 1, wherein the antistatic agent is ethoxycocoalkylamine.
8. A method for preparing the insulating electronic component cleaning agent according to any one of claims 1 to 7, comprising the steps of:
all raw materials in the cleaning agent are added into a normal pressure closed container according to the weight part ratio as described in claim 1 or 2, and stirred for 0.5-1h at the speed of 50-200r/min under the condition of 20+/-10 ℃ to obtain the insulating electronic component cleaning agent.
9. A method for using the insulating electronic component cleaning agent as claimed in any one of claims 1 to 7, comprising the specific steps of: when spray washing is selected, compressed dry air is needed to blow off sundries including dust and iron powder on the surface of the electronic component to be washed, and then a spray gun is used for sucking the insulating electronic component cleaning agent according to any one of claims 1-7 to spray wash the electronic component; for small-sized electrical equipment or parts, a soaking method is adopted, the electronic component to be cleaned is directly soaked in the insulating electronic component cleaning agent according to any one of claims 1 to 7, and the electronic component is fished out after 5 to 15 minutes.
10. The application of the oil-soluble agent and N-methyl pyrrolidone composition in improving the detergency of a cleaning agent and avoiding the swelling of plastics is characterized in that the oil-soluble agent and the N-methyl pyrrolidone are in weight percentage:
。
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