CN116020393B - Production equipment for preparing calcitol by using plant sterol - Google Patents
Production equipment for preparing calcitol by using plant sterol Download PDFInfo
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- CN116020393B CN116020393B CN202310171294.3A CN202310171294A CN116020393B CN 116020393 B CN116020393 B CN 116020393B CN 202310171294 A CN202310171294 A CN 202310171294A CN 116020393 B CN116020393 B CN 116020393B
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- bottom plate
- stirring
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- 238000004519 manufacturing process Methods 0.000 title claims abstract description 27
- 235000002378 plant sterols Nutrition 0.000 title claims abstract description 10
- 238000003756 stirring Methods 0.000 claims abstract description 47
- 238000006243 chemical reaction Methods 0.000 claims abstract description 35
- 238000010992 reflux Methods 0.000 claims abstract description 17
- 238000009833 condensation Methods 0.000 claims abstract description 15
- 230000005494 condensation Effects 0.000 claims abstract description 15
- 238000009434 installation Methods 0.000 claims description 15
- 238000007789 sealing Methods 0.000 claims description 11
- 238000003760 magnetic stirring Methods 0.000 claims description 10
- 238000004321 preservation Methods 0.000 claims description 8
- 150000002009 diols Chemical class 0.000 claims description 7
- 238000002360 preparation method Methods 0.000 claims description 3
- 230000002146 bilateral effect Effects 0.000 claims description 2
- 238000004140 cleaning Methods 0.000 abstract description 31
- 239000007789 gas Substances 0.000 abstract description 20
- 239000002912 waste gas Substances 0.000 abstract description 11
- 230000001105 regulatory effect Effects 0.000 description 9
- 230000005540 biological transmission Effects 0.000 description 7
- 230000001699 photocatalysis Effects 0.000 description 5
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- YJVFFLUZDVXJQI-UHFFFAOYSA-L palladium(ii) acetate Chemical compound [Pd+2].CC([O-])=O.CC([O-])=O YJVFFLUZDVXJQI-UHFFFAOYSA-L 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 229910021532 Calcite Inorganic materials 0.000 description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- 238000013375 chromatographic separation Methods 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000013032 photocatalytic reaction Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- WRLFSJXJGJBFJQ-WPUCQFJDSA-N Calcifediol monohydrate Chemical compound O.C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@@H](CCCC(C)(C)O)C)=C\C=C1\C[C@@H](O)CCC1=C WRLFSJXJGJBFJQ-WPUCQFJDSA-N 0.000 description 1
- 208000013038 Hypocalcemia Diseases 0.000 description 1
- 208000029725 Metabolic bone disease Diseases 0.000 description 1
- 208000001132 Osteoporosis Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000001631 haemodialysis Methods 0.000 description 1
- 230000000322 hemodialysis Effects 0.000 description 1
- 230000000705 hypocalcaemia Effects 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 238000010030 laminating Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000011164 ossification Effects 0.000 description 1
- 208000005368 osteomalacia Diseases 0.000 description 1
- 238000007146 photocatalysis Methods 0.000 description 1
- 229940068065 phytosterols Drugs 0.000 description 1
- 208000007442 rickets Diseases 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Abstract
The invention discloses production equipment for preparing calcitol by using plant sterol, which comprises an equipment bottom plate, a stirring and adjusting assembly, an exhaust gas treatment assembly, a cleaning assembly, a condensation reflux reaction kettle, an electric reactor shell and a photoreaction kettle shell, wherein an operation table and a first bottom plate are respectively arranged on one side of the top of the equipment bottom plate; the effective action range of the stirring frame is enlarged by utilizing the stirring adjusting component in production, and the production quality of equipment is improved; the waste gas generated by the equipment is collected and treated in a concentrated way by using the arranged waste gas treatment assembly, so that the damage to the environment caused by direct discharge of the waste gas is avoided; the inner wall of the reaction kettle is cleaned by the aid of the cleaning assembly, and labor intensity of cleaning equipment for workers is relieved.
Description
Technical Field
The invention relates to the technical field of calcitol production, in particular to production equipment for preparing calcitol by using plant sterols.
Background
The ossified diol is also called 25-hydroxyvitamin D3 monohydrate, is a chemical intermediate, is suitable for treating metabolic bone diseases such as osteoporosis, rickets, osteomalacia and the like, can be used for treating hypocalcemia caused by hemodialysis, needs to be processed and produced by using ossified diol production equipment in the preparation process, can basically meet the use requirement of production, but still has certain defects, firstly, the stirring structure of the existing ossified diol production equipment is simple, the position of a stirring frame in a reaction kettle cannot be adjusted in the reaction stirring process, the effective acting range of the stirring frame is limited, the uniformity of stirring treatment of the reaction kettle is influenced, and the production quality of the equipment is reduced; secondly, the existing ossified diol production equipment lacks an automatic cleaning function, and in order to prevent the reaction agent from being stuck inside the reaction kettle, the reaction kettle needs to be cleaned manually and regularly, so that the labor intensity of cleaning equipment for staff is increased; thirdly, the existing ossified diol production equipment lacks a tail gas treatment function, and the waste gas always generated in the medicament reaction process is directly discharged into the air without being collected and treated, so that the surrounding environment is damaged; it is therefore necessary to design a production facility for preparing calcitol using phytosterols.
Disclosure of Invention
The invention aims to provide a production device for preparing calcitol by using plant sterol, which solves the problems in the background art.
In order to achieve the above purpose, the present invention provides the following technical solutions: the utility model provides a use production facility of phytosterol preparation ossification diol, includes equipment bottom plate, operation panel, first bottom plate, display screen, magnetic stirring subassembly, stirring regulation subassembly, exhaust-gas treatment subassembly, cleaning subassembly, second bottom plate, third bottom plate, jar body support, condensation reflux reaction cauldron, heat preservation shell, electric reactor casing, agitator motor, first stirring frame, closing cap, second stirring frame, photoreaction kettle casing and mount table, top one side of equipment bottom plate is provided with operation panel and first bottom plate respectively, and the top embedding of operation panel installs the display screen, and the top opposite side of equipment bottom plate is provided with second bottom plate and third bottom plate respectively, and the top of second bottom plate is provided with jar body support, and the top of jar body support is provided with condensation reflux reaction cauldron, cup joints the first collecting pipe in the exhaust-gas treatment subassembly in the through-hole that condensation reflux reaction cauldron's top one side was seted up.
Preferably, the exhaust gas treatment assembly comprises a first collecting pipe, a second collecting pipe, a third collecting pipe, a first collecting pump, a second collecting pump, a third collecting pump, a gas collecting shell and a treatment pipe, one end of the first collecting pipe is connected to the first collecting pump in a matched mode, the output end of the first collecting pump is sleeved in a through hole formed in the bottom of the gas collecting shell, the top of the gas collecting shell is sleeved on the treatment pipe, and the gas collecting shell is fixedly installed at the center of the top of the equipment bottom plate.
Preferably, the top of first bottom plate is provided with the heat preservation shell, has cup jointed the electric reactor casing in the heat preservation shell, and the lateral wall top of electric reactor casing is provided with the alignment jig in the stirring adjustment subassembly, stirring adjustment subassembly comprises alignment jig, accommodate motor, adjusting screw, connecting block, connecting plate and bracing piece, is connected with adjusting screw through the bearing cooperation in the alignment jig, and the bottom of alignment jig is provided with accommodate motor, and accommodate motor's output runs through the bottom of alignment jig fixed connection adjusting screw.
Preferably, the adjusting screw is provided with the connecting block, and the ball nut of connecting block inside embedding installation is connected with adjusting screw mutually supporting, is provided with the connecting plate between the connecting block, and sliding connection has the bracing piece in the through-hole that connecting plate top bilateral symmetry was seted up, and the top of bracing piece is fixed on the alignment jig, and the bottom mounting of bracing piece is at the top of electric reactor casing, and the agitator motor is installed in the embedding in the recess of connecting plate top center department seting up, and the top of agitator motor's output fixed connection first stirring frame.
Preferably, the top sliding connection of first stirring frame is in the through-hole of seting up at closing cap top, and the closing cap is fixed at the top of electric reactor casing, has cup jointed the second collecting pipe in the through-hole of seting up at electric reactor casing one side top, and the cooperation of second collecting pipe is connected on the second collecting pump, and the output of second collecting pump cup joints in the through-hole of seting up bottom the gas collecting shell.
Preferably, the top of third bottom plate is provided with the installation shell among the magnetic stirring subassembly, the magnetic stirring subassembly comprises installation shell, rotation power group, first support, first magnetic force piece, the support frame, the second support, second magnetic force piece and enclosure, the inside bottom of installation shell is provided with rotation power group, and first support has been cup jointed on rotation power group's the output, first magnetic force piece is installed to the symmetry on the first support, the top of installation shell is provided with the support frame, and the top center department rotation of support frame is connected with the second support, the second magnetic force piece is installed to the bottom symmetry of second support, and the top of second support is provided with the second stirring frame, be provided with the enclosure on the support frame, and the junction of enclosure and second stirring frame is provided with the sealing washer.
Preferably, the top of enclosure is provided with the photoreaction kettle casing, and the top of photoreaction kettle casing is provided with the mount table, and the bottom of mount table is provided with the illuminator body, and the illuminator body is located the inside of photoreaction kettle casing, and the rotation ring in the clean subassembly has been cup jointed on the inside top of photoreaction kettle casing, has cup jointed the third collecting pipe in the through-hole of seting up on one side of photoreaction kettle casing top, and the cooperation of third collecting pipe is connected on the third collecting pump, and the output of third collecting pump cup joints in the through-hole of seting up in the gas collecting shell bottom.
Preferably, the cleaning assembly comprises a rotating ring, a cleaning toothed ring, a transmission gear, a cleaning motor, a motor support and a cleaning support, wherein the cleaning toothed ring is connected to the bottom of the rotating ring in a rotating manner, the cleaning toothed ring is meshed with the transmission gear, the transmission gear is fixed on the output end of the cleaning motor, the cleaning motor is fixed on the motor support, the motor support is symmetrically arranged on the inner wall of the shell of the photoreaction kettle, the cleaning support is uniformly arranged at the bottom of the cleaning toothed ring, and the cleaning support is mutually attached to the inner wall of the shell of the photoreaction kettle.
Compared with the prior art, the invention has the beneficial effects that: the production equipment for preparing the calcite glycol by using the plant sterol uses the plant sterol as a raw material to perform condensation reflux, then ultraviolet rays with specific wavelength are used for photocatalysis treatment in a shell of a photoreaction kettle, palladium acetate is added for continuous stirring after condensation reflux, and finally the calcite glycol is sent to chromatographic separation and extraction; in the production process, the adjusting motor is used for driving the adjusting screw rod to rotate, the connecting block and the connecting plate are driven to move up and down by the adjusting screw rod, the position of the first stirring frame in the electric reactor shell is adjusted, the effective acting range of the stirring frame in the reaction kettle is enlarged, the uniformity of stirring treatment is ensured, and the production quality of equipment is improved; the waste gas generated in the electric reactor shell, the photoreaction kettle shell and the condensation reflux reaction kettle in the reaction process is collected into the gas collecting shell by the aid of the first collecting pump, the second collecting pump and the third collecting pump, and is treated by spraying treatment liquid through the treatment pipe, so that the damage to the surrounding environment caused by direct discharge of production waste gas into the air is avoided; the cleaning motor that utilizes the setting drives the drive gear and rotates, drives the bottom rotation of clean ring gear at the swivel becket through the drive gear meshing, and then utilizes the clean support of drive gear bottom to clean the inner wall of reation kettle, need not the manual work and participated in clean process, has alleviateed staff cleaning equipment's intensity of labour.
Drawings
FIG. 1 is an exploded view of the overall structure of the present invention;
FIG. 2 is an enlarged view of a portion of area A of FIG. 1;
FIG. 3 is an enlarged view of a portion of region B of FIG. 1;
FIG. 4 is a three-dimensional view of the overall structure of the present invention;
FIG. 5 is an enlarged view of a portion of region C of FIG. 4;
FIG. 6 is a top view of the overall structure of the present invention;
in the figure: 1. an equipment base plate; 2. an operation table; 3. a first base plate; 4. a display screen; 5. a magnetic stirring assembly; 6. a stirring adjustment assembly; 7. an exhaust treatment assembly; 8. a cleaning assembly; 9. a second base plate; 10. a third base plate; 11. a tank bracket; 12. condensing and refluxing the reaction kettle; 13. a thermal insulation shell; 14. an electric reactor housing; 15. a stirring motor; 16. a first stirring frame; 17. a closing cap; 18. a second stirring frame; 19. a photoreaction kettle shell; 20. a mounting table; 501. a mounting shell; 502. a rotary power pack; 503. a first bracket; 504. a first magnetic block; 505. a support frame; 506. a second bracket; 507. a second magnetic block; 508. a closed shell; 601. an adjusting frame; 602. adjusting a motor; 603. adjusting a screw rod; 604. a connecting block; 605. a connecting plate; 606. a support rod; 701. a first collection tube; 702. a second collection tube; 703. a third collection tube; 704. a first collection pump; 705. a second collection pump; 706. a third collection pump; 707. a gas collecting shell; 708. a treatment tube; 801. a rotating ring; 802. cleaning the toothed ring; 803. a transmission gear; 804. cleaning a motor; 805. a motor bracket; 806. and cleaning the bracket.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Referring to fig. 1-6, an embodiment of the present invention is provided: a production device for preparing calcitol by using plant sterol comprises a device bottom plate 1, an operation table 2, a first bottom plate 3, a display screen 4, a magnetic stirring assembly 5, a stirring adjusting assembly 6, an exhaust gas treatment assembly 7, a cleaning assembly 8, a second bottom plate 9, a third bottom plate 10, a tank support 11, a condensation reflux reaction kettle 12, a heat preservation shell 13, an electric reactor shell 14, a stirring motor 15, a first stirring frame 16, a sealing cover 17, a second stirring frame 18, a light reaction kettle shell 19 and an installation table 20, wherein one side of the top of the device bottom plate 1 is respectively provided with the operation table 2 and the first bottom plate 3, the display screen 4 is embedded and installed at the top of the operation table 2, the other side of the top of the device bottom plate 1 is respectively provided with the second bottom plate 9 and the third bottom plate 10, the top of the second bottom plate 9 is provided with the tank support 11, the top of the tank support 11 is provided with the condensation reflux reaction kettle 12, the first collecting pipe 701 in the waste gas treatment component 7 is sleeved in a through hole formed in one side of the top of the condensation reflux reaction kettle 12, the waste gas treatment component 7 consists of the first collecting pipe 701, the second collecting pipe 702, the third collecting pipe 703, the first collecting pump 704, the second collecting pump 705, the third collecting pump 706, the gas collecting shell 707 and the treatment pipe 708, one end of the first collecting pipe 701 is connected to the first collecting pump 704 in a matched manner, the output end of the first collecting pump 704 is sleeved in a through hole formed in the bottom of the gas collecting shell 707, the top of the gas collecting shell 707 is sleeved in the treatment pipe 708, the gas collecting shell 707 is fixedly installed at the center of the top of the equipment bottom plate 1, the heat preservation shell 13 is arranged at the top of the first bottom plate 3, the electric reactor shell 14 is sleeved in the heat preservation shell 13, the side wall top of the electric reactor shell 14 is provided with the regulating frame 601 in the stirring regulating component 6, the stirring regulating component 6 consists of the regulating frame 601, the adjusting motor 602, adjusting screw 603, connecting block 604, connecting plate 605 and bracing piece 606 constitute, be connected with adjusting screw 603 through the bearing cooperation in the regulating frame 601, and the bottom of regulating frame 601 is provided with adjusting motor 602, the output of adjusting motor 602 runs through the bottom of regulating screw 603 of regulating frame 601 fixed connection, be provided with connecting block 604 on the adjusting screw 603, and the ball nut of the inside embedding installation of connecting block 604 and mutually support with adjusting screw 603 and connect, be provided with connecting plate 605 between the connecting block 604, and the through-hole that the symmetry was seted up in connecting plate 605 top is equipped with bracing piece 606 in the sliding connection, the top of bracing piece 606 is fixed on regulating frame 601, and the bottom mounting of bracing piece 606 is at the top of electric reactor shell 14, the embedded agitator motor 15 of installing in the recess that sets up in the central department of connecting plate 605 top, and the output fixed connection first agitator 16 of agitator motor 15's top, the top of the first stirring frame 16 is slidably connected in a through hole formed in the top of the sealing cover 17, the sealing cover 17 is fixed on the top of the electric reactor shell 14, a second collecting pipe 702 is sleeved in the through hole formed in the top of one side of the electric reactor shell 14, the second collecting pipe 702 is connected on the second collecting pump 705 in a matched mode, the output end of the second collecting pump 705 is sleeved in the through hole formed in the bottom of the gas collecting shell 707, the top of the third bottom plate 10 is provided with a mounting shell 501 in the magnetic stirring assembly 5, the magnetic stirring assembly 5 consists of the mounting shell 501, a rotating power group 502, a first bracket 503, a first magnetic block 504, a supporting frame 505, a second bracket 506, a second magnetic block 507 and a sealing shell 508, the inner bottom end of the mounting shell 501 is provided with the rotating power group 502, the output end of the rotating power group 502 is sleeved with the first bracket 503, the first magnetic block 504 is symmetrically arranged on the first bracket 503, the top of the installation shell 501 is provided with a support frame 505, the center of the top of the support frame 505 is rotationally connected with a second bracket 506, the bottom of the second bracket 506 is symmetrically provided with a second magnetic block 507, the top of the second bracket 506 is provided with a second stirring frame 18, the support frame 505 is provided with a sealing shell 508, the joint of the sealing shell 508 and the second stirring frame 18 is provided with a sealing ring, the top of the sealing shell 508 is provided with a photoreaction kettle shell 19, the top of the photoreaction kettle shell 19 is provided with an installation table 20, the bottom of the installation table 20 is provided with a light emitter body, the light emitter body is positioned inside the photoreaction kettle shell 19, the inner top end of the photoreaction kettle shell 19 is sleeved with a rotating ring 801 in a cleaning component 8, a through hole formed in one side of the top of the photoreaction kettle shell 19 is sleeved with a third collecting pipe 703, the third collecting pipe 703 is matched and connected to a third collecting pump 706, the output of third collecting pump 706 cup joints in the through-hole of seting up in gas-collecting vessel 707 bottom, clean subassembly 8 comprises rotation ring 801, clean ring gear 802, drive gear 803, clean motor 804, motor support 805 and clean support 806, the bottom rotation of rotation ring 801 is connected with clean ring gear 802, and clean ring gear 802 meshing is connected drive gear 803, drive gear 803 is fixed on the output of clean motor 804, and clean motor 804 is fixed on motor support 805, motor support 805 installs on the inner wall of photoreaction kettle shell 19 symmetrically, the bottom of clean ring gear 802 evenly is provided with clean support 806, and clean support 806 and the inner wall of photoreaction kettle shell 19 laminating each other, utilize the motor support 805 of setting to be favorable to fixing clean motor 804 on the inner wall of photoreaction kettle shell 19, the structural stability of equipment has been improved.
Working principle: when the ultraviolet light photocatalytic treatment device is used, phytosterol is used as a raw material for condensation reflux, ultraviolet light with specific wavelength is used for photocatalytic treatment in a photocatalytic reaction kettle shell 19, a rotary power set 502 drives a first bracket 503 and a first magnetic block 504 to rotate in the photocatalytic treatment process, then magnetic force drives a second magnetic block 507 and a second bracket 506 to rotate on a supporting frame 505, and further magnetic force drives a second stirring frame 18 at the top of the second bracket 506 to rotate, so that a medicament in the photocatalytic reaction kettle is magnetically stirred, and meanwhile ultraviolet light with specific wavelength is emitted by a light emitter body at the bottom of a mounting table 20 for photocatalytic treatment; then, after condensing and refluxing, the mixture enters an electric reactor shell 14, palladium acetate is added into the electric reactor shell 14, then, the electric reactor in the electric reactor shell 14 regulates and controls the temperature in the electric reactor shell 14 to be 45 ℃, meanwhile, the electric reactor regulates and controls the charge flow in the electric reactor shell 14 to be 1equiv, the charge flow and the temperature are kept unchanged in the electric reactor shell 14 to be continuously stirred, the palladium acetate is utilized to carry out catalytic reaction, acetic acid and hydrogen peroxide are added into the electric reactor shell 14 after the electric reaction treatment for 1h, then, the electric reactor regulates and controls the charge flow in the electric reactor shell 14 to be 1equiv, the charge flow is kept unchanged in the electric reactor shell 14 to be continuously stirred, and the electric reactor is sent to chromatographic separation for extraction of calcitol after the electric reaction treatment for 1h, and meanwhile, the palladium acetate is recovered to be reused; in the production process, the adjusting motor 602 is used for driving the adjusting screw 603 to rotate, the connecting block 604 and the connecting plate 605 are driven to move up and down by the adjusting screw 603, the position of the first stirring frame 16 in the electric reactor shell 14 is adjusted, the effective acting range of the stirring frame in the reaction kettle is enlarged, the uniformity of stirring treatment is ensured, and the production quality of equipment is improved; the waste gas generated in the electric reactor shell 14, the photoreaction kettle shell 19 and the condensation reflux reaction kettle 12 in the reaction process is respectively collected into the gas collecting shell 707 by using the first collecting pump 704, the second collecting pump 705 and the third collecting pump 706, and the waste gas is treated by spraying the treatment liquid through the treatment pipe 708, so that the damage to the surrounding environment caused by directly discharging the production waste gas into the air is avoided; the cleaning motor 804 drives the transmission gear 803 to rotate, the transmission gear 803 is meshed to drive the cleaning toothed ring 802 to rotate at the bottom of the rotating ring 801, and then the cleaning support 806 at the bottom of the transmission gear 803 is used for cleaning the inner wall of the reaction kettle, so that the cleaning process is not needed to be manually participated, and the labor intensity of cleaning equipment for staff is reduced.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential characteristics thereof. The present embodiments are, therefore, to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Claims (3)
1. Use production facility of phytosterol preparation ossified diol, including equipment bottom plate (1), operation panel (2), first bottom plate (3), display screen (4), magnetic stirring subassembly (5), stirring regulation subassembly (6), exhaust-gas treatment subassembly (7), clean subassembly (8), second bottom plate (9), third bottom plate (10), jar body support (11), condensation reflux reaction cauldron (12), heat preservation shell (13), electric reactor casing (14), agitator motor (15), first stirring frame (16), closing cap (17), second stirring frame (18), light reaction kettle casing (19) and mount table (20), its characterized in that: an operation table (2) and a first bottom plate (3) are respectively arranged on one side of the top of the equipment bottom plate (1), a display screen (4) is embedded and installed at the top of the operation table (2), a second bottom plate (9) and a third bottom plate (10) are respectively arranged on the other side of the top of the equipment bottom plate (1), a tank support (11) is arranged at the top of the second bottom plate (9), a condensation reflux reaction kettle (12) is arranged at the top of the tank support (11), a first collecting pipe (701) in an exhaust gas treatment assembly (7) is sleeved in a through hole formed in one side of the top of the condensation reflux reaction kettle (12), the exhaust gas treatment assembly (7) consists of the first collecting pipe (701), a second collecting pipe (702), a third collecting pipe (703), a first collecting pump (704), a second collecting pump (705), a third collecting pump (706), a gas collecting shell (707) and a treatment pipe (708), one end of the first collecting pipe (701) is connected to the first collecting pump (704) in a matched mode, the output end of the first collecting pipe is sleeved at the bottom of the gas collecting shell (707), the first collecting pipe (704) is sleeved at the bottom of the gas collecting shell (707), the top of the first collecting pipe (708) is provided at the top of the equipment bottom (1), and an electric reactor shell (14) is sleeved in the heat preservation shell (13), an adjusting frame (601) in a stirring adjusting component (6) is arranged at the top of the side wall of the electric reactor shell (14), the stirring adjusting component (6) consists of an adjusting frame (601), an adjusting motor (602), an adjusting screw (603), a connecting block (604), a connecting plate (605) and a supporting rod (606), the adjusting screw (603) is connected in the adjusting frame (601) through bearing fit, an adjusting motor (602) is arranged at the bottom of the adjusting frame (601), the output end of the adjusting motor (602) penetrates through the bottom end of the adjusting frame (601) to be fixedly connected with the adjusting screw (603), an installation shell (501) in a magnetic stirring component (5) is arranged at the top of a third bottom plate (10), the magnetic stirring component (5) consists of an installation shell (501), a rotating power set (502), a first bracket (503), a first magnetic block (504), a supporting frame (505), a second bracket (506), a second magnetic block (507) and a sealing shell (508), the inner bottom end of the installation shell (601) is provided with the rotating power set (503), and the first bracket (503) is symmetrically sleeved on the first bracket (503), the top of installation shell (501) is provided with support frame (505), and the top center department of support frame (505) rotates and is connected with second support (506), second magnetic force piece (507) is installed to the bottom symmetry of second support (506), and the top of second support (506) is provided with second stirring frame (18), be provided with enclosure shell (508) on support frame (505), and the junction of enclosure shell (508) and second stirring frame (18) is provided with the sealing washer, the top of enclosure shell (508) is provided with light reaction kettle casing (19), and the top of light reaction kettle casing (19) is provided with mount table (20), the bottom of mount table (20) is provided with the illuminator body, the illuminator body is located the inside of light reaction kettle casing (19), inside top of light reaction kettle casing (19) cup joints rotation ring (801) in clean subassembly (8), cup joint third collecting pipe (703) in the through-hole of seting up in one side of light reaction kettle casing (19) top, and third collecting pump (706) cooperation connect on third collecting pump (706), output of third collecting pump (706) is provided with mount table (20), clean ring (803) in clean ring (804), clean ring (804) is seted up by rotation ring (803), clean ring (803) is seted up in clean ring (804) bottom (803), clean ring (804) is equipped with in the through-up of motor (803) Motor support (805) and clean support (806) are constituteed, the bottom rotation of swivel ring (801) is connected with clean ring gear (802), and clean ring gear (802) meshing is connected drive gear (803), drive gear (803) are fixed on the output of clean motor (804), and clean motor (804) are fixed on motor support (805), motor support (805) symmetry is installed on the inner wall of photoreaction kettle casing (19), the bottom of clean ring gear (802) evenly is provided with clean support (806), and clean support (806) are laminated each other with the inner wall of photoreaction kettle casing (19).
2. The production apparatus for preparing calcitol using plant sterols according to claim 1, characterized in that: be provided with connecting block (604) on adjusting screw (603), and ball nut and adjusting screw (603) of connecting block (604) inside embedding installation are mutually supported and are connected, be provided with connecting plate (605) between connecting block (604), and sliding connection has bracing piece (606) in the through-hole of seting up of connecting plate (605) top bilateral symmetry, the top of bracing piece (606) is fixed on alignment jig (601), and the bottom mounting of bracing piece (606) is at the top of electric reactor casing (14), embedding is installed agitator motor (15) in the recess of seting up in connecting plate (605) top center department, and the top of agitator motor (15) output fixed connection first stirring frame (16).
3. The production apparatus for preparing calcitol using plant sterols according to claim 2, characterized in that: the top sliding connection of first stirring frame (16) is in the through-hole of seting up at closing cap (17) top, and closing cap (17) are fixed at the top of electric reactor casing (14), cup jointed second collecting pipe (702) in the through-hole of seting up at electric reactor casing (14) one side top, and second collecting pipe (702) cooperation is connected on second collecting pump (705), and the output of second collecting pump (705) cup joints in the through-hole of seting up in gas collecting shell (707) bottom.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310171294.3A CN116020393B (en) | 2023-02-28 | 2023-02-28 | Production equipment for preparing calcitol by using plant sterol |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310171294.3A CN116020393B (en) | 2023-02-28 | 2023-02-28 | Production equipment for preparing calcitol by using plant sterol |
Publications (2)
| Publication Number | Publication Date |
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| CN116020393A CN116020393A (en) | 2023-04-28 |
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