CN220558645U - Sodium chlorate mother liquor purifier - Google Patents
Sodium chlorate mother liquor purifier Download PDFInfo
- Publication number
- CN220558645U CN220558645U CN202321839662.9U CN202321839662U CN220558645U CN 220558645 U CN220558645 U CN 220558645U CN 202321839662 U CN202321839662 U CN 202321839662U CN 220558645 U CN220558645 U CN 220558645U
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- CN
- China
- Prior art keywords
- mother liquor
- cover
- sodium chlorate
- wall
- machine body
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- BZSXEZOLBIJVQK-UHFFFAOYSA-N 2-methylsulfonylbenzoic acid Chemical compound CS(=O)(=O)C1=CC=CC=C1C(O)=O BZSXEZOLBIJVQK-UHFFFAOYSA-N 0.000 title claims abstract description 17
- 239000012452 mother liquor Substances 0.000 title claims description 35
- 238000003756 stirring Methods 0.000 claims abstract description 18
- 239000007788 liquid Substances 0.000 claims description 25
- 244000309464 bull Species 0.000 claims description 16
- 239000010413 mother solution Substances 0.000 abstract description 7
- 238000006243 chemical reaction Methods 0.000 description 8
- 230000000694 effects Effects 0.000 description 8
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 6
- 239000001110 calcium chloride Substances 0.000 description 6
- 229910001628 calcium chloride Inorganic materials 0.000 description 6
- 238000000746 purification Methods 0.000 description 5
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 238000001728 nano-filtration Methods 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- JHWIEAWILPSRMU-UHFFFAOYSA-N 2-methyl-3-pyrimidin-4-ylpropanoic acid Chemical compound OC(=O)C(C)CC1=CC=NC=N1 JHWIEAWILPSRMU-UHFFFAOYSA-N 0.000 description 2
- 241000883990 Flabellum Species 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- 238000002955 isolation Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 239000013049 sediment Substances 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L sodium carbonate Substances [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910001424 calcium ion Inorganic materials 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 230000005389 magnetism Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000036632 reaction speed Effects 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model relates to the technical field of purifying devices and discloses a sodium chlorate mother solution purifying device which effectively solves the problems that the existing stirring fan blade is fixedly arranged on a stirring shaft, the stirring area is smaller, and the purifying efficiency is affected.
Description
Technical Field
The utility model belongs to the technical field of purifying devices, and particularly relates to a sodium chlorate mother solution purifying device.
Background
According to the patent document with the publication number of CN208087364U, the utility model name of sodium chlorate production mother liquor treatment device is described in the specification: adding calcium chloride into a feed inlet of a first filter to generate calcium sulfate precipitate in the first filter and filter, enabling a stirring device to accelerate the reaction rate, enabling the treated solution to enter a second filter, adding sodium hydroxide and sodium carbonate into the feed inlet of the second filter to remove excessive calcium ions, and finally enabling the solution to enter a nanofiltration device, wherein the nanofiltration device can separate sodium dichromate, a first outlet of the nanofiltration device is a water outlet, and a second outlet is an interception outlet, so that the second outlet is connected to a recovery tank, and sodium dichromate with higher purity is stored in the recovery tank for recycling; the following drawbacks still remain:
the general agitating unit has (mixing) shaft, stirring flabellum and agitator motor to constitute, and wherein the fixed setting of stirring flabellum is on the (mixing) shaft to make the stirring region less, thereby make reaction rate slower, thereby influence purification efficiency.
Disclosure of Invention
Aiming at the situation, in order to overcome the defects of the prior art, the utility model provides the sodium chlorate mother solution purifying device, which effectively solves the problems that the stirring fan blade is fixedly arranged on the stirring shaft, the stirring area is smaller, and the purifying efficiency is influenced.
In order to achieve the above purpose, the present utility model provides the following technical solutions: the sodium chlorate mother solution purifying device comprises a machine body, wherein a top cover is arranged above the machine body, a fixing seat is arranged at the bottom end of one side of the machine body, a connecting seat is arranged at one side of the top cover, a first air cylinder is arranged at the top end of the fixing seat, the output end of the first air cylinder is fixedly connected with the connecting seat, a feeding pipe is arranged at the top end of the top cover, and a mother solution purifying component is arranged in the machine body;
the mother liquor purifying component comprises a liquid discharge pipe arranged at the bottom end of the machine body, the top end of the liquid discharge pipe is positioned in the machine body, the top end of the liquid discharge pipe is closed, liquid discharge holes are formed in the outer wall of the liquid discharge pipe at equal angles, and the liquid discharge holes are formed in the machine body.
Preferably, the outside cover of fluid-discharge tube is equipped with the isolated cover, and the inner wall of isolated cover is hugged closely with the outer wall of fluid-discharge tube, and the filter is installed in the bottom outside of isolated cover, and the outer wall of filter hugs closely with the inner wall of organism, and the diapire of filter hugs closely with the interior bottom wall of organism.
Preferably, the inside rotation of top cap is connected with the bull stick, and spacing commentaries on classics piece is installed to the bottom of bull stick, and spacing commentaries on classics piece rotates to be connected in the inside of spacing commentaries on classics groove, and spacing commentaries on classics groove is offered in the top of isolated cover.
Preferably, the outer wall of the rotating rod is symmetrically provided with sliding grooves, the outer side of the rotating rod is sleeved with a rotating ring, stirring blades are arranged at equal angles on the outer side of the rotating ring, and the rotating ring is in sliding connection with the sliding grooves.
Preferably, a magnetic ring is arranged at the top end of the swivel, an electromagnet is arranged on the bottom wall of the top cover, the electromagnet is externally connected with a power supply, and the electromagnet is magnetically connected with the magnetic ring.
Preferably, the top end of the top cover is provided with a fixed sleeve, the fixed sleeve is sleeved on the outer side of the rotating rod, the top end of the fixed sleeve is rotationally connected with a toothed ring, the toothed ring is in sliding connection with the sliding chute, one side of the toothed ring is connected with a gear in a meshed manner, the gear is fixedly connected with an output shaft of the motor, and the motor is fixedly arranged on the top end of the top cover.
Preferably, the top board is installed on the top of bull stick, and the bottom of top board is fixed connection with the output of second cylinder, and second cylinder fixed mounting is on the top cap, and the supporting leg is installed to the bottom equiangular degree of organism.
Compared with the prior art, the utility model has the beneficial effects that:
(1) According to the utility model, the filter plates are positioned on the bottom wall of the machine body, so that mother liquor is prevented from entering the lower part of the filter plates through the filter plates, the subsequent filtering effect is improved, the limiting rotating blocks at the bottom ends of the rotating rods are rotationally clamped in the limiting rotating grooves of the isolation sleeve, and after the rotating rods move upwards, the filter plates are driven to move to the upper part of the liquid discharge pipe, so that the mother liquor and sediment are conveniently separated, and the mother liquor is conveniently purified;
(2) This is novel through opening the motor for the gear rotates, drives the ring gear and rotates then, drives the bull stick and rotates, drives the swivel and rotates, stirs mother liquor and calcium chloride, improves the reaction effect, and electro-magnet discontinuity on the top cap diapire is on-off simultaneously, makes the swivel vertically reciprocating motion under magnetic force and gravity effect, conveniently stirs the mother liquor of co-altitude not, improves reaction rate, increases stirring region, improves purification efficiency.
Drawings
The accompanying drawings are included to provide a further understanding of the utility model and are incorporated in and constitute a part of this specification, illustrate the utility model and together with the embodiments of the utility model, serve to explain the utility model.
In the drawings:
FIG. 1 is a schematic diagram of a sodium chlorate mother liquor purifying device;
FIG. 2 is a schematic diagram of a mother liquor purifying assembly according to the present utility model;
FIG. 3 is a schematic view of the structure of the toothed ring of the present utility model;
FIG. 4 is a schematic view of a drain pipe according to the present utility model;
FIG. 5 is a schematic view of a filter plate structure according to the present utility model;
in the figure: 1. a body; 2. support legs; 3. a top cover; 4. a fixing seat; 5. a connecting seat; 6. a first cylinder; 7. a feed pipe; 8. a mother liquor purification assembly; 801. a rotating rod; 802. a chute; 803. a fixed sleeve; 804. a toothed ring; 805. a motor; 806. a gear; 807. a top plate; 808. a second cylinder; 809. a liquid discharge pipe; 810. a liquid discharge hole; 811. an isolation sleeve; 812. a filter plate; 813. limiting rotating grooves; 814. limiting rotating blocks; 815. a swivel; 816. stirring the leaves; 817. and a magnetic ring.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and fully with reference to the accompanying drawings, in which it is evident that the embodiments described are only some, but not all embodiments of the utility model; all other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
1-5, the utility model comprises a machine body 1, wherein a supporting leg 2 is arranged at equal angles at the bottom end of the machine body 1, a top cover 3 is arranged above the machine body 1, a fixed seat 4 is arranged at the bottom end of one side of the machine body 1, a connecting seat 5 is arranged at one side of the top cover 3, a first cylinder 6 is arranged at the top end of the fixed seat 4, the output end of the first cylinder 6 is fixedly connected with the connecting seat 5, a feeding pipe 7 is arranged at the top end of the top cover 3, and a mother liquor purifying component 8 is arranged in the machine body 1;
the mother liquor purifying component 8 comprises a liquid discharge pipe 809 arranged at the bottom end of the machine body 1, the top end of the liquid discharge pipe 809 is positioned in the machine body 1, the top end of the liquid discharge pipe 809 is closed, a liquid discharge hole 810 is formed in the outer wall of the liquid discharge pipe 809 at equal angles, the liquid discharge hole 810 is positioned in the machine body 1, an insulating sleeve 811 is sleeved outside the liquid discharge pipe 809, the inner wall of the insulating sleeve 811 is tightly attached to the outer wall of the liquid discharge pipe 809, a filter plate 812 is arranged at the outer side of the bottom end of the insulating sleeve 811, the outer wall of the filter plate 812 is tightly attached to the inner wall of the machine body 1, the bottom wall of the filter plate 812 is tightly attached to the inner bottom wall of the machine body 1, a rotating rod 801 is rotatably connected to the inner part of the top cover 3, a limiting rotating block 814 is rotatably connected to the inner part of the limiting rotating groove 813, the limiting rotating groove 813 is formed in the top end of the insulating sleeve 811, a sliding groove 802 is symmetrically formed in the outer wall of the rotating rod 801, the outside cover of bull stick 801 is equipped with swivel 815, agitating vane 816 is installed to the equiangular outside of swivel 815, swivel 815 and spout 802 sliding connection, magnetic ring 817 is installed on the top of swivel 815, install the electro-magnet on the diapire of top cap 3, the electro-magnet external power supply, the electro-magnet is connected with magnetic ring 817 magnetism, fixed cover 803 is installed on the top of top cap 3, the outside of bull stick 801 is located to fixed cover 803, the top of fixed cover 803 rotates and is connected with ring gear 804, ring gear 804 and spout 802 sliding connection, one side meshing of ring gear 804 is connected with gear 806, gear 806 and the output shaft fixed connection of motor 805, motor 805 fixed mounting is in the top of top cap 3, top board 807 is installed on the top of bull stick 801, the bottom of top board 807 and the output fixed connection of second cylinder 808, second cylinder 808 fixed mounting is on top cap 3, filter 812 is located the diapire of organism 1, thereby avoid entering into filter 812 below through filter 812 between the mother liquor to improve subsequent filter effect, and the spacing commentaries on classics piece 814 rotation joint in the spacing groove 813 of isolated cover 811 of bull stick 801 bottom, the bull stick 801 upwards moves the back, drive the filter 812 and remove to the top of fluid-discharge tube 809, conveniently carry out the separation of mother liquor and deposit, conveniently carry out the mother liquor purification, open motor 805, make gear 806 rotate, drive ring gear 804 rotation then, drive bull stick 801 rotation, drive swivel 815 rotation, stir mother liquor and calcium chloride, improve the reaction effect, electro-magnet intermittent type on the top cap 3 diapire is cut off the electricity simultaneously, make swivel 815 vertically reciprocating motion under magnetic force and gravity effect, the convenience stirs the mother liquor of different co-altitude, improve reaction rate.
Working principle: when the filter plate 812 is used, firstly, sodium chlorate mother liquor is introduced into the machine body 1 from the feed pipe 7, at the moment, the filter plate 812 is positioned on the inner bottom wall of the machine body 1, the liquid discharge hole 810 on the liquid discharge pipe 809 is closed by the isolating sleeve 811, and then, calcium chloride is added into the machine body 1 from the feed pipe 7, so that the calcium chloride reacts with sodium sulfate possibly existing in the sodium chlorate mother liquor, and calcium sulfate precipitation is produced, so that the mother liquor is purified, and the filter plate 812 is positioned on the bottom wall of the machine body 1, so that the mother liquor is prevented from entering the lower part of the filter plate 812 through the filter plate 812, and the subsequent filtering effect is improved;
the motor 805 is started to enable the gear 806 to rotate, and as the gear 806 is meshed with the toothed ring 804, the toothed ring 804 is driven to rotate, and the toothed ring 804 is clamped with the rotating rod 801, so that the rotating rod 801 is driven to rotate, and then the rotating ring 815 is driven to rotate, so that the mother solution and the calcium chloride are stirred, and the reaction effect is improved;
the electromagnet on the bottom wall of the top cover 3 is intermittently powered on and off, when the electromagnet is powered on, attractive force is generated to the magnetic ring 817 on the rotating ring 815 to drive the rotating ring 815 to move upwards, after the electromagnet is powered off, the rotating ring 815 moves back, and rotates along with the rotating rod 801 in the moving and rotating process of the rotating ring 815, so that mother solutions with different heights are conveniently stirred, and the reaction speed is improved;
because the spacing commentaries on classics piece 814 of bull stick 801 bottom rotates the joint in the spacing groove 813 that changes of insulating cover 811 to after the reaction, open second cylinder 808, drive bull stick 801 and upwards move, then drive filter 812 upwards move to the top of fluid-discharge tube 809, thereby make things convenient for the mother liquor to follow filter 812, fluid-discharge hole 810 department and discharge, conveniently carry out the separation of mother liquor and sediment, conveniently carry out the mother liquor purification.
Claims (7)
1. The utility model provides a sodium chlorate mother liquor purifier, includes organism (1), its characterized in that: a top cover (3) is arranged above the machine body (1), a fixed seat (4) is arranged at the bottom end of one side of the machine body (1), a connecting seat (5) is arranged at one side of the top cover (3), a first air cylinder (6) is arranged at the top end of the fixed seat (4), the output end of the first air cylinder (6) is fixedly connected with the connecting seat (5), a feeding pipe (7) is arranged at the top end of the top cover (3), and a mother liquor purifying component (8) is arranged in the machine body (1);
the mother liquor purifying component (8) comprises a liquid discharge pipe (809) arranged at the bottom end of the machine body (1), the top end of the liquid discharge pipe (809) is located in the machine body (1), the top end of the liquid discharge pipe (809) is closed, liquid discharge holes (810) are formed in the outer wall of the liquid discharge pipe (809) at equal angles, and the liquid discharge holes (810) are located in the machine body (1).
2. The sodium chlorate mother liquor purifying device according to claim 1, wherein: the outside cover of fluid-discharge tube (809) is equipped with isolated cover (811), and the inner wall of isolated cover (811) is hugged closely with the outer wall of fluid-discharge tube (809), and filter (812) are installed in the bottom outside of isolated cover (811), and the outer wall of filter (812) is hugged closely with the inner wall of organism (1), and the diapire of filter (812) is hugged closely with the interior bottom wall of organism (1).
3. A sodium chlorate mother liquor purifying device according to claim 2, wherein: the inside rotation of top cap (3) is connected with bull stick (801), and spacing commentaries on classics piece (814) are installed to the bottom of bull stick (801), and spacing commentaries on classics piece (814) rotate to connect in the inside of spacing commentaries on classics groove (813), and spacing commentaries on classics groove (813) are seted up on the top of isolated cover (811).
4. A sodium chlorate mother liquor purifying device according to claim 3, wherein: the outer wall of the rotating rod (801) is symmetrically provided with a sliding groove (802), a rotating ring (815) is sleeved on the outer side of the rotating rod (801), stirring blades (816) are arranged on the outer side of the rotating ring (815) at equal angles, and the rotating ring (815) is in sliding connection with the sliding groove (802).
5. The sodium chlorate mother liquor purifying device according to claim 4, wherein: the top end of the swivel (815) is provided with a magnetic ring (817), the bottom wall of the top cover (3) is provided with an electromagnet, the electromagnet is externally connected with a power supply, and the electromagnet is magnetically connected with the magnetic ring (817).
6. A sodium chlorate mother liquor purifying device according to claim 3, wherein: the top of top cap (3) is installed fixed cover (803), and the outside of bull stick (801) is located to fixed cover (803) cover, and the top of fixed cover (803) rotates and is connected with ring gear (804), ring gear (804) and spout (802) sliding connection, and one side meshing of ring gear (804) is connected with gear (806), and gear (806) and motor (805) output shaft fixed connection, motor (805) fixed mounting in top of top cap (3).
7. A sodium chlorate mother liquor purifying device according to claim 3, wherein: the top board (807) is installed on top of bull stick (801), and the bottom of top board (807) is fixed connection with the output of second cylinder (808), and second cylinder (808) fixed mounting is on top cap (3), and supporting leg (2) are installed to the bottom equiangular degree of organism (1).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321839662.9U CN220558645U (en) | 2023-07-13 | 2023-07-13 | Sodium chlorate mother liquor purifier |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321839662.9U CN220558645U (en) | 2023-07-13 | 2023-07-13 | Sodium chlorate mother liquor purifier |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220558645U true CN220558645U (en) | 2024-03-08 |
Family
ID=90095860
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202321839662.9U Active CN220558645U (en) | 2023-07-13 | 2023-07-13 | Sodium chlorate mother liquor purifier |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220558645U (en) |
-
2023
- 2023-07-13 CN CN202321839662.9U patent/CN220558645U/en active Active
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