CN115997836A - Composite protein tablet candy and preparation method thereof - Google Patents
Composite protein tablet candy and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a composite protein tablet candy and a preparation method thereof, wherein the composite protein tablet candy comprises composite protein particles, sugar alcohol, flavoring agent, sweetener, adhesive, lubricant and essence, and the components are calculated according to parts by weight: 10-60 parts of composite protein particles, 30-85 parts of sugar alcohol, 0.1-5 parts of flavoring agent, 0.01-5 parts of sweetener, 0.1-2 parts of adhesive, 0.2-4 parts of lubricant and 0.2-4 parts of essence; the composite protein particles comprise composite protein and an adhesive, wherein the composite protein particles comprise the following components in parts by weight: 90-99 parts of composite protein and 0.1-10 parts of adhesive. The invention optimizes the fluidity and compressibility of the composite protein composition, and is not easy to crack in the tabletting process.
Description
Technical Field
The invention relates to the field of protein products, in particular to a composite protein tablet candy and a preparation method thereof.
Background
With the rapid development of the food health industry, nutrient supplement products are of various types so as to meet the diversified demands of different people. The protein is the material foundation of life, can provide energy, improve immunity and participate in the composition of various tissues of human bodies. Because of the unique nutritional value and function of the protein, the sales share of the protein in the commercial nutrition products is listed as fescue, and the characteristics of the protein are widely applied to food production.
The edible protein products in the market are mainly protein powder in the form of solid beverage, are powder formed by combining animal-derived protein and plant-derived protein, are slightly soluble in water, have the problems of poor solubility and dispersibility, cohesive mass and adhesion and difficult stirring, and bring bad experience to consumers. The drinking mode determines that the drinking scene of the protein powder is not suitable for the open air, the use scene is limited, and the development of the dosage form is more considered how to provide various portable choices for consumers nowadays.
The protein-supplementing food material can be hundreds of kinds, and conventional animal-derived and plant-derived high-quality proteins, such as whey protein, milk protein, casein, soybean protein, pea protein and the like, are less applied in tablets. Even if the protein is applied occasionally, the protein raw material of the product has low proportion and the total protein content of the finished product is low. The main reasons are loose structure, poor fluidity and cohesiveness of the raw materials, easy cracking in the preparation process, low hardness of the finished product and large friability, and the product cost is correspondingly increased due to serious loss in the packaging and transportation process.
The formula of the compound plant protein tablet candy disclosed in the China patent with the prior publication number of CN201810680894.1 contains various plant-derived proteins, the application of animal-derived proteins is not involved, the types and the proportions of amino acids contained in the plant-derived proteins have a certain gap with the nutrition requirements of human bodies, and the absorption of the plant-derived proteins is difficult relative to the animal-derived proteins.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides a composite protein tabletting candy and a preparation method thereof, which not only optimize the fluidity of a composite protein composition, but also solve the problem of easy cracking in the tabletting process.
The invention is realized by the following technical scheme:
a composite protein tablet candy comprises composite protein particles, sugar alcohol, a flavoring agent, a sweetener, an adhesive A and a lubricant, wherein the composite protein particles comprise composite protein and an adhesive B, the composite protein comprises animal protein and plant protein, the animal protein comprises separated whey protein, and the ratio of the separated whey protein is 60% or more of the total components of the composite protein.
Further, the composite protein tablet candy comprises the following components in parts by weight: 10-60 parts of composite protein particles, 30-85 parts of sugar alcohol, 0.1-5 parts of flavoring agent, 0.01-5 parts of sweetener, 0.1-2 parts of adhesive A and 0.2-4 parts of lubricant;
further, the composite protein particles comprise the following components in parts by weight: 90-99 parts of composite protein and 0.1-10 parts of adhesive B.
Further, the composite protein tablet tabletting candy also comprises auxiliary materials, wherein the auxiliary materials are essence, and the weight parts of the auxiliary materials are as follows: 0.2 to 4 portions of essence.
Further, the composite protein is one or more of isolated whey protein, concentrated whey protein, soy isolated protein, wheat protein, pea protein, rice protein, milk protein and casein.
Further, the adhesive B is one or more of maltodextrin, povidone K30, acacia, xanthan gum, sodium carboxymethylcellulose and hydroxypropyl methylcellulose.
Further, the sugar alcohol is one or more of mannitol, sorbitol, erythritol, maltitol and isomalt.
Further, the flavoring agent is one or a combination of more of citric acid, DL-malic acid, fruit and vegetable powder and sodium citrate.
Further, the adhesive A is one or more of sodium carboxymethyl cellulose, povidone K30, acacia, xanthan gum, maltodextrin and hydroxypropyl methyl cellulose.
Further, the sweetener is one or more of aspartame, neotame, stevioside, sucralose and mogroside.
Further, the lubricant is one or more of magnesium stearate, stearic acid, leucine, polyethylene glycol 4000, polyethylene glycol 6000 and sodium chloride.
Further, the preparation method of the composite protein tablet candy comprises the following steps:
step S1: preparation of composite protein particles:
step a: weighing compound protein with the formula amount, mixing for 10-35 minutes by a three-dimensional mixer to obtain compound protein premix, until the product is uniformly mixed, and then putting into a boiling drying granulator;
step b: preparing slurry: dispersing the adhesive B with the formula amount in purified water to prepare a solution with the concentration of 20% -45%, and filtering to obtain uniform slurry;
step c: the adhesive B slurry is slowly and uniformly sprayed on the surface of the composite protein powder in the fluidization chamber through a peristaltic pump, so that the powder is coagulated into soft particles;
step d: and (3) drying: and (3) boiling and drying the soft particles for 20-45 minutes by hot air, and sieving the soft particles with a 20-mesh sieve to obtain the composite protein particles.
Step S2: weighing: weighing compound protein particles, sugar alcohol, flavoring agent, sweetener, adhesive A and essence according to the formula amount, and sieving with 20 mesh sieve for standby;
step S3: mixing: and (3) adding the prepared materials into a three-dimensional mixing tank for mixing for 20-30 minutes, and adding the lubricant for total mixing for 3 minutes to obtain a total mixed material.
Further, the preparation method of the composite protein tablet candy further comprises the following steps:
step S4: and (3) tabletting: putting the total mixed material into a tablet press for tabletting, and discharging tablets;
step S5: and (3) packaging: the pressed candy is packed by HDPE bottles, and a drying agent is arranged in the pressed candy.
In the step d, when the hot air is boiled and dried, the air inlet temperature is controlled to be 40-65 ℃, and the water content is controlled to be less than or equal to 5% at the detection temperature of 105 ℃.
Furthermore, the tabletting temperature is 18-26 ℃ and the humidity is less than or equal to 45% in the step S4 of tabletting.
Compared with the prior art, the invention has the advantages that:
1. the animal protein is added on the basis of the plant protein, the animal protein contains the separated whey protein, the ratio of the separated whey protein to the total components of the compound protein is more than or equal to 60 percent, on one hand, the animal protein is relatively consistent with the nutrition structure of human beings, the animal protein contains 8 amino acids necessary for the human body, the animal protein and the plant protein are combined in the compound protein, the protein types are rich, the protein content is high, and the nutrition demands of different people can be obtained through scientific proportioning; on the other hand, the ratio of the isolated whey protein is limited, so that the compound has obviously better adhesive force than other compound protein combinations after granulating, is not easy to split during tabletting, and has good compressibility and fluidity.
2. According to the invention, the composite protein particles are prepared by wet granulation, and the adhesive B slurry is slowly and uniformly sprayed on the surface of the composite protein powder through a peristaltic pump, so that the powder is bonded into soft particles, and then the soft particles are obtained by drying, so that the fluidity and compressibility of the composite protein particles are improved, the particle size after granulation processing is uniform, moisture absorption is not easy, the chip forming friability is low, the preparation process is simple, the cost is low, the operability is strong, and the industrial production is easy.
3. The composite protein tablet candy prepared by the invention has smooth surface and good chewiness, is suitable for various taste requirements of the market on protein tablets, has outstanding product flavor, is suitable for any scene, is convenient to carry, avoids the risk of easy tablet cracking caused by high protein content, improves the production efficiency of the protein tablets, and saves the labor cost for picking unqualified products.
Drawings
FIG. 1 is a schematic diagram of composite protein particles of inventive example 1, comparative example 1-1, and a schematic diagram of a common mixed protein powder of comparative example 1-2;
FIG. 2 is a schematic diagram of a composite protein tablet candy of inventive example 1, comparative example 1-1, and comparative example 1-2.
Detailed Description
The present invention will be described in further detail with reference to the following examples in order to make the objects, technical solutions and advantages of the present invention more apparent, so that those skilled in the art can fully understand the technical contents of the present invention. It is to be understood that the following examples are given by way of illustration of the present invention and are not to be construed as limiting the scope of the present invention, since various modifications and alterations of no particular nature will fall within the scope of the invention as defined by the appended claims. The specific manufacturing process parameters and the like described below are also only one example of suitable ranges, i.e., a person skilled in the art can select from the description herein without limiting to the specific values described below.
A composite protein tablet candy comprises composite protein particles, sugar alcohol, a flavoring agent, a sweetener, an adhesive A and a lubricant, wherein the composite protein particles comprise composite proteins and an adhesive B, the composite proteins comprise animal proteins and plant proteins, the animal proteins comprise separated whey proteins, and the separated whey proteins account for 60% or more of the total components of the composite proteins.
The composite protein tablet candy comprises the following components in parts by weight: 10-60 parts of composite protein particles, 30-85 parts of sugar alcohol, 0.1-5 parts of flavoring agent, 0.01-5 parts of sweetener, 0.1-2 parts of adhesive A and 0.2-4 parts of lubricant;
the composite protein particles comprise the following components in parts by weight: 90-99 parts of composite protein and 0.1-10 parts of adhesive B.
The composite protein tablet tabletting candy also comprises auxiliary materials, wherein the auxiliary materials are essence, and the weight parts of the auxiliary materials are as follows: 0.2 to 4 portions of essence.
The composite protein is one or more of isolated whey protein, concentrated whey protein, soybean isolated protein, wheat protein, pea protein, rice protein, milk protein, and casein.
The adhesive B is one or more of maltodextrin, povidone K30, acacia, xanthan gum, sodium carboxymethylcellulose and hydroxypropyl methylcellulose.
The sugar alcohol is one or more of mannitol, sorbitol, erythritol, maltitol, and isomalt.
The correctant is one or more of citric acid, DL-malic acid, fruit and vegetable powder, and sodium citrate.
The adhesive A is one or more of sodium carboxymethyl cellulose, povidone K30, acacia, xanthan gum, maltodextrin and hydroxypropyl methyl cellulose.
The sweetener is one or more of aspartame, neotame, stevioside, sucralose and mogroside.
The lubricant is one or more of magnesium stearate, stearic acid, leucine, polyethylene glycol 4000, polyethylene glycol 6000 and sodium chloride.
The preparation method of the composite protein tablet candy comprises the following steps:
step S1: preparation of composite protein particles:
step a: weighing compound protein with the formula amount, mixing for 10-35 minutes by a three-dimensional mixer to obtain compound protein premix, until the product is uniformly mixed, and then putting into a boiling drying granulator;
step b: preparing slurry: dispersing the adhesive B with the formula amount in purified water to prepare a solution with the concentration of 20% -45%, and filtering to obtain uniform slurry;
step c: the adhesive B slurry is slowly and uniformly sprayed on the surface of the composite protein powder in the fluidization chamber through a peristaltic pump, so that the powder is coagulated into soft particles;
step d: and (3) drying: and (3) boiling and drying the soft particles for 20-45 minutes by hot air, and sieving the soft particles with a 20-mesh sieve to obtain the composite protein particles.
Step S2: weighing: weighing compound protein particles, sugar alcohol, flavoring agent, sweetener, adhesive A and essence according to the formula amount, and sieving with 20 mesh sieve for standby;
step S3: mixing: and (3) adding the prepared materials into a three-dimensional mixing tank for mixing for 20-30 minutes, and adding the lubricant for total mixing for 3 minutes to obtain a total mixed material.
The preparation method of the composite protein tablet candy further comprises the following steps:
step S4: and (3) tabletting: putting the total mixed material into a tablet press for tabletting, and discharging tablets;
step S5: and (3) packaging: the pressed candy is packed by HDPE bottles, and a drying agent is arranged in the pressed candy.
In the step d, when the hot air is boiled and dried, the inlet air temperature is controlled to be 40-65 ℃, and the water content is controlled to be less than or equal to 5% at the detection temperature of 105 ℃.
And step S4, tabletting at the tabletting temperature of 18-26 ℃ and humidity of less than or equal to 45%.
The composite protein in the composite protein particles is one or a plurality of combinations of separated whey protein, concentrated whey protein, soybean separated protein, wheat protein, pea protein, rice protein, milk protein and casein. The compound protein formula contains the separated whey protein, the ratio of the separated whey protein is more than or equal to 60% of the total components of the compound protein, and the combination of the example 1 and the comparative example 1-1 shows that the ratio of the separated whey protein is limited, the adhesive force of the compound protein is improved, the compound protein is not easy to absorb moisture, the tablet weight difference is small, and the friability is low.
The composite protein is prepared by adding animal protein based on plant protein, wherein the animal protein is relatively consistent with the nutrition structure of human beings, and contains 8 amino acids necessary for the human body. Animal and plant proteins are combined, the protein is rich in variety and high in protein content, and the nutrition requirements of different people can be obtained through scientific proportioning.
The slurry prepared by the invention adopts purified water as a processing aid, has simple production process, simple equipment, easy operation, low cost and high safety. The adhesive B slurry is sprayed on the surface of the composite protein powder uniformly by peristaltic pump to bond the powder into soft particles, and then the soft particles are dried to obtain the composite protein particles, so that the fluidity and the compressibility of the composite protein particles are improved.
The binding agent B in the composite protein particles is one or more of maltodextrin, povidone K30, acacia, xanthan gum, sodium carboxymethylcellulose and hydroxypropyl methylcellulose. The maltodextrin is used in dairy products, so that the volume of the products is expanded, the products are not easy to agglomerate, are instant, have good brewing property, are easy to digest and absorb, prolong the shelf life of the products, reduce the cost and improve the economic benefit; when the anti-sand candy is used for candy, the toughness of the candy can be increased, sand return and melting are prevented, and the structure is improved. Reducing sweetness of candy, reducing odontopathy, reducing tooth sticking phenomenon, improving flavor, preventing deliquescence, and prolonging shelf life. The acacia is light yellow block or white powder, and has strong adhesive force.
The protein tablet candy prepared by the method disclosed by the invention is good in chewiness, suitable for various demands on protein tablets in the market, simple in production process, strong in operability, sufficient in nutrient components, capable of solving the problems of poor flowability and easiness in splitting of different protein candies, capable of effectively improving the production efficiency of the protein tablets and saving production cost of picking unqualified products and the like.
The following is a description of the concepts of the invention in conjunction with specific embodiments, but is not intended to limit the invention to the specific embodiments described below. Any particular value within the scope of the invention as described herein may be practiced.
Example 1
A composite protein tablet candy comprises the following components in percentage by weight: 60% of composite protein particles, 35.41% of sorbitol, 0.8% of sodium carboxymethyl cellulose, 1.8% of juicy peach juice powder, 0.04% of sucralose, 0.15% of DL-malic acid, 1.1% of edible essence and 0.7% of magnesium stearate.
The preparation method of the composite protein tablet candy comprises the following steps:
step S1: preparation of composite protein particles:
the compound protein granule comprises 75% of separated whey protein, 15% of soybean protein isolate, 5% of wheat protein and 5% of maltodextrin.
The preparation method of the composite protein particles comprises the following steps:
step a: weighing: weighing the formula amount of the isolated whey protein, the soybean isolated protein and the wheat protein according to the weight percentage, mixing for 20 minutes by a three-dimensional mixer to obtain a compound protein premix, and putting into a boiling drying granulator;
step b: preparing slurry: dispersing the maltodextrin with the formula amount into purified water to prepare a 35% solution, and filtering to obtain uniform slurry;
step c: the maltodextrin slurry is slowly and uniformly sprayed on the surface of the compound protein premix powder through a peristaltic pump, so that the powder is coagulated into soft particles;
step d: and (3) drying: the soft particles are boiled and dried for 25 minutes by hot air at the inlet air temperature of 50-65 ℃, the water content is controlled to be less than or equal to 5% at the detection temperature of 105 ℃, and the soft particles are sieved by a 20-mesh sieve to obtain composite protein particles;
step S2: weighing compound protein particles, sorbitol, sodium carboxymethylcellulose, juicy peach juice powder, sucralose and DL-malic acid according to the formula amount, and sieving the edible essence with a 20-mesh sieve for later use;
step S3: mixing: the preparation materials are put into a mixing tank for mixing for 20 to 30 minutes, and then added with magnesium stearate for total mixing for 3 minutes to obtain a total mixed material;
step S4: tabletting: adding the total mixed materials into a tablet press, controlling the temperature of the tablet press to be 18-26 ℃, controlling the humidity to be less than or equal to 45%, discharging tablets, measuring the weight difference of the tablets to be 0.8 g/tablet, and measuring the hardness and friability;
step S5: and (3) packaging: the pressed candy is packaged by HDPE bottle, and a drying agent is arranged in the pressed candy.
The composite protein granule product is shown in figure 1, and the composite protein tablet candy is shown in figure 2, and the composite protein granule is prepared by limiting the proportion of the separated whey protein in the composite protein and adopting wet granulation, so that the obtained composite protein tablet candy has smooth and clean surface, regular edge and no split.
Comparative example 1-1
A composite protein tablet candy comprises the following components in percentage by weight: 60% of composite protein particles, 35.41% of sorbitol, 0.8% of sodium carboxymethyl cellulose, 1.8% of juicy peach juice powder, 0.04% of sucralose, 0.15% of DL-malic acid, 1.1% of edible essence and 0.7% of magnesium stearate.
The preparation method of the composite protein tablet candy comprises the following steps:
step S1: preparation of composite protein particles:
the composite protein particles comprise the following components in percentage by weight: separating whey protein 40%, soybean protein 50%, wheat protein 5% and maltodextrin 5%;
the preparation method of the composite protein particles comprises the following steps:
step a: weighing: weighing the formula amount of the isolated whey protein, the soybean isolated protein and the wheat protein according to the weight percentage, mixing for 20 minutes by a three-dimensional mixer to obtain a compound protein premix, and putting into a boiling drying granulator;
step b: preparing slurry: dispersing the maltodextrin with the formula amount into purified water to prepare a 35% solution, and filtering to obtain uniform slurry;
step c: the maltodextrin slurry is slowly and uniformly sprayed on the surface of the compound protein premix powder through a peristaltic pump, so that the powder is coagulated into soft particles;
step d: and (3) drying: the soft particles are boiled and dried for 25 minutes by hot air at the inlet air temperature of 50-65 ℃, the water content is controlled to be less than or equal to 5% at the detection temperature of 105 ℃, and the soft particles are sieved by a 20-mesh sieve to obtain composite protein particles;
step S2: weighing compound protein particles, sorbitol, sodium carboxymethylcellulose, juicy peach juice powder, sucralose and DL-malic acid according to the formula amount, and sieving the edible essence with a 20-mesh sieve for later use;
step S3: mixing: the preparation materials are put into a mixing tank for mixing for 20 to 30 minutes, and then added with magnesium stearate for total mixing for 3 minutes to obtain a total mixed material;
step S4: tabletting: adding the total mixed materials into a tablet press, controlling the temperature of the tablet press to be 18-26 ℃, controlling the humidity to be less than or equal to 45%, discharging tablets, measuring the weight difference of the tablets to be 0.8 g/tablet, and measuring the hardness and friability;
step S5: and (3) packaging: the pressed candy is packaged by HDPE bottle, and a drying agent is arranged in the pressed candy.
The composite protein pellet product is shown in fig. 1, the composite protein pellet candy is shown in fig. 2, and the comparative example 1-1 is compared with example 1 to modify the isolated whey protein ratio of the composite protein formulation in the composite protein pellet, defining an isolated whey protein ratio of less than 60%. It can be seen that the obtained composite protein tablet candy has smooth and clean surface, rough edge and split appearance.
Comparative examples 1 to 2
The preparation method of the composite protein powder comprises the following steps: weighing the formula amount of the separated whey protein, the soybean protein isolate, the wheat protein and the maltodextrin, and mixing for 20 minutes by a three-dimensional mixer to obtain the composite protein powder.
The composite protein powder product is shown in figure 1;
a composite protein tablet candy (composite protein components are not granulated and are mixed in common) comprises the following components in percentage by weight: 45% of isolated whey protein, 9% of soybean isolated protein, 3% of wheat protein, 3% of maltodextrin, 35.41% of sorbitol, 0.8% of sodium carboxymethylcellulose, 1.8% of juicy peach juice powder, 0.04% of sucralose, 0.15% of DL-malic acid, 1.1% of edible essence and 0.7% of magnesium stearate.
The preparation method of the composite protein tablet candy comprises the following steps:
step S1: weighing the formula amount of the isolated whey protein, the soybean isolated protein, the wheat protein, the maltodextrin, the sorbitol, the sodium carboxymethyl cellulose, the juicy peach juice powder, the sucralose, the DL-malic acid and the edible essence, and screening by 20 meshes for later use;
step S2: mixing: the preparation materials are put into a mixing tank for mixing for 20 to 30 minutes, and then added with magnesium stearate for total mixing for 3 minutes to obtain a total mixed material;
step S3: tabletting: adding the total mixed materials into a tablet press, controlling the temperature of the tablet press to be 18-26 ℃, controlling the humidity to be less than or equal to 45%, discharging tablets, measuring the weight difference of the tablets to be 0.8 g/tablet, and measuring the hardness and friability;
step S4: and (3) packaging: the pressed candy is packaged by HDPE bottles, and a drying agent is arranged in the pressed candy;
the common mixed protein powder product is shown in fig. 1, the composite protein tablet candy product is shown in fig. 2, the preparation method of composite protein particles is modified in comparison with the preparation method of composite protein particles in comparative examples 1-2, the composite protein particles are not subjected to wet granulation, only common mixing is adopted, and the obtained composite protein tablet candy has rough surface, knocked edges and serious cracks.
Example 2
A composite protein tablet candy comprises the following components in percentage by weight: 10% of composite protein particles, 82.6% of isomalt, 0.5% of xanthan gum, 5% of corn flour, 0.1% of stevioside, 1.1% of edible essence, 0.3% of stearic acid and 0.4% of magnesium stearate.
The preparation method of the composite protein tablet candy comprises the following steps:
step S1: preparation of composite protein particles:
the composite protein particles comprise the following components in percentage by weight: 60% of isolated whey protein, 15% of concentrated whey protein, 15% of soybean isolated protein, 5% of rice protein, 4.5% of pea protein and 0.5% of Arabic gum.
The preparation method of the composite protein particles comprises the following steps:
step a: weighing: weighing the formula amount of the isolated whey protein, the soybean isolated protein and the wheat protein according to the weight percentage, mixing for 20 minutes by a three-dimensional mixer to obtain a compound protein premix, and putting into a boiling drying granulator;
step b: preparing slurry: dispersing the maltodextrin with the formula amount into purified water to prepare a 35% solution, and filtering to obtain uniform slurry;
step c: the maltodextrin slurry is slowly and uniformly sprayed on the surface of the compound protein premix powder through a peristaltic pump, so that the powder is coagulated into soft particles;
step d: and (3) drying: the soft particles are boiled and dried for 25 minutes by hot air at the inlet air temperature of 50-65 ℃, the water content is controlled to be less than or equal to 5% at the detection temperature of 105 ℃, and the soft particles are sieved by a 20-mesh sieve to obtain composite protein particles;
step S2: weighing compound protein particles, isomalt, xanthan gum, corn flour, stevioside and edible essence according to the formula amount, and sieving the mixture with a 20-mesh sieve for later use;
step S3: mixing: mixing the prepared materials in a mixing tank for 20-30 minutes, and adding stearic acid and magnesium stearate to mix for 3 minutes to obtain a total mixed material;
step S4: tabletting: adding the total mixed materials into a tablet press, controlling the temperature of the tablet press to be 18-26 ℃, controlling the humidity to be less than or equal to 45%, discharging tablets, measuring the weight difference of the tablets to be 0.8 g/tablet, and measuring the hardness and friability;
step S5: and (3) packaging: the pressed candy is packaged by HDPE bottle, and a drying agent is arranged in the pressed candy.
Comparative example 2-1
The preparation method of the composite protein powder comprises the following steps: weighing the formula amount of the separated whey protein, the soybean protein isolate, the wheat protein and the maltodextrin, and mixing for 20 minutes by a three-dimensional mixer to obtain the composite protein powder.
A composite protein tablet candy (composite protein components are not granulated and are mixed in common) comprises the following components in percentage by weight: 6% of isolated whey protein, 1.5% of concentrated whey protein, 1.5% of soybean isolated protein, 0.5% of rice protein, 4.5% of pea protein, 0.05% of acacia, 82.6% of isomalt, 0.5% of xanthan gum, 5% of corn flour, 0.1% of stevioside, 1.1% of edible essence, 0.3% of stearic acid and 0.4% of magnesium stearate.
The preparation method of the composite protein tablet candy comprises the following steps:
step S1: weighing the formula amount of the isolated whey protein, the concentrated whey protein, the soybean isolated protein, the rice protein, the pea protein, the Arabic gum, the isomalt, the xanthan gum, the corn flour, the stevioside and the edible essence, and screening by 20 meshes for standby;
step S2: mixing: mixing the prepared materials in a mixing tank for 20-30 minutes, and adding stearic acid and magnesium stearate to mix for 3 minutes to obtain a total mixed material;
step S3: tabletting: adding the total mixed materials into a tablet press, controlling the temperature of the tablet press to be 18-26 ℃, controlling the humidity to be less than or equal to 45%, discharging tablets, measuring the weight difference of the tablets to be 0.8 g/tablet, and measuring the hardness and friability;
step S4: and (3) packaging: the pressed candy is packaged by HDPE bottle, and a drying agent is arranged in the pressed candy.
Test results
1. The composite protein particles in the above example 1, comparative example 1-2, example 2 and example 2-1 were subjected to performance test, respectively, and each of the powder parameters of the composite protein particles and the common mixed protein powder was tested with reference to the pharmacopoeia method.
Angle of repose: the maximum angle formed by the free inclined plane of the powder accumulation layer and the horizontal plane. The smaller the repose angle, the smaller the friction force, the better the fluidity, and the fluidity is considered to be good when the theta is less than or equal to 30 degrees, and the fluidity requirement in the production process can be met when the theta is less than or equal to 40 degrees. The fluidity of the powder has great influence on the weight difference of preparations such as granules, capsules, tablets and the like and normal operation.
Particle size: the size of the particles, also known as "particle size" or "diameter". Belongs to the key preparation process parameters, and the particle size can influence the material mixing uniformity of the product and the dissolution behavior and stability of the preparation.
Bulk density: the density of the powder is obtained by dividing the powder by the volume V of the container occupied by the powder. Bulk density has a critical impact on the choice of tableting film tool in tablet production.
The test results are shown in Table 1 below
TABLE 1 comparison of composite protein particles and parameters of common Mixed protein powder
As can be seen from table 1:
(1) By combining the embodiment 1 with the comparative embodiment 1-2 and the embodiment 2 with the comparative embodiment 2-1, the wet granulation scheme can effectively unify the particle size distribution of the powder, 70% of the particles are concentrated in the range of 40-65 meshes after granulation, and the particle size difference of the composite protein powder after common mixing is large and the particles are unevenly distributed.
(2) The ratio of the isolated whey protein in the composite protein is less than 60% as shown in the combination of the example 1 and the comparative example 1-1, and the wet granulation scheme can effectively unify the particle size distribution of the powder, and the particle distribution is relatively uniform.
(3) By combining the examples with Table 1, it is known that the powder surface repose angle is reduced from 55 DEG to 36 DEG after granulation by adopting the wet granulation scheme, and the flowability requirement in the production process can be met.
2. Observation of the production of tablets in the above examples was performed separately:
and (3) carrying out production operation under the condition that the relative humidity is less than or equal to 45%, and recording abnormal production conditions and parameter indexes of the preparation by production staff.
The test results are shown in Table 2 below
Table 2 observations of the production tableting conditions for example 1 to comparative example 2-1.
As can be seen from table 2:
1) The wet granulated composite protein tablet candy combining the example 1 with the comparative example 1-2 and the example 2 with the comparative example 2-1 is not easy to crack in the production process, has the chip friability lower than 0.4%, smooth chip surface and neat edge, and has various key indexes superior to those of the composite protein tablet candy prepared by common mixing.
2) As can be seen from the combination of example 1 and comparative example 1-1, when the fraction of the isolated whey protein in the composite protein is less than 60% of the total protein, the composite protein is easily cracked during tabletting even through wet granulation, and has low flaking rate, high friability, rough flaky surface and collision at the edges, and cannot meet the requirement of tabletting quality.
3) It can be seen from a combination of examples 1 and 2 that the lower the ratio of the composite protein particles in the composite protein tablet confectionery composition, the more excellent the tablet shape, hardness, friability of the tablet.
It should be noted that the foregoing description of the preferred embodiments is merely illustrative of the technical concept and features of the present invention, and is not intended to limit the scope of the invention, as long as the scope of the invention is defined by the claims and their equivalents. All equivalent changes or modifications made in accordance with the spirit of the present invention should be construed to be included in the scope of the present invention.
Claims (10)
1. The composite protein tablet candy is characterized by comprising composite protein particles, sugar alcohol, a flavoring agent, a sweetener, a binding agent A and a lubricant, wherein the composite protein particles comprise composite protein and a binding agent B, the composite protein comprises animal protein and plant protein, the animal protein comprises separated whey protein, and the separated whey protein accounts for 60% or more of the total components of the composite protein.
2. The composite protein pellet candy of claim 1, wherein the:
the composite protein tablet candy comprises the following components in parts by weight: 10-60 parts of composite protein particles, 30-85 parts of sugar alcohol, 0.1-5 parts of flavoring agent, 0.01-5 parts of sweetener, 0.1-2 parts of adhesive A and 0.2-4 parts of lubricant;
the composite protein particles comprise the following components in parts by weight: 90-99 parts of composite protein and 0.1-10 parts of adhesive B.
3. The composite protein tablet candy of claim 1, further comprising an auxiliary material, wherein the auxiliary material is essence, and the auxiliary material is calculated according to parts by weight: 0.2 to 4 portions of essence.
4. The composite protein pellet candy of claim 1, wherein the:
the composite protein is one or more of separated whey protein, concentrated whey protein, soybean protein isolate, wheat protein, pea protein, rice protein, milk protein and casein;
the adhesive B is one or more of maltodextrin, povidone K30, acacia, xanthan gum, sodium carboxymethylcellulose and hydroxypropyl methylcellulose.
5. The composite protein pellet candy of claim 1, wherein the:
the sugar alcohol is one or more of mannitol, sorbitol, erythritol, maltitol and isomaltulose alcohol;
the flavoring agent is one or a combination of more of citric acid, DL-malic acid, fruit and vegetable powder and sodium citrate;
the adhesive A is one or a combination of more of sodium carboxymethyl cellulose, povidone K30, acacia, xanthan gum, maltodextrin and hydroxypropyl methyl cellulose.
6. The composite protein pellet candy of claim 1, wherein the:
the sweetener is one or more of aspartame, neotame, stevioside, sucralose and mogroside;
the lubricant is one or more of magnesium stearate, stearic acid, leucine, polyethylene glycol 4000, polyethylene glycol 6000 and sodium chloride.
7. The method for preparing the composite protein tablet candy according to any one of claims 1 to 6, comprising the steps of:
step S1: preparation of composite protein particles:
step a: weighing compound protein with the formula amount, mixing for 10-35 minutes by a three-dimensional mixer to obtain compound protein premix, uniformly mixing the product, and then putting the mixture into a boiling drying granulator;
step b: preparing slurry: dispersing the adhesive B with the formula amount in purified water to prepare a solution with the concentration of 20% -45%, and filtering to obtain uniform slurry;
step c: the slurry of the adhesive B is slowly and uniformly sprayed on the surface of the composite protein powder in the fluidization chamber through a peristaltic pump, so that the powder is coagulated into soft particles;
step d: and (3) drying: boiling and drying the soft particles for 20-45 minutes by hot air, and sieving the soft particles with a 20-mesh sieve to obtain composite protein particles;
step S2: weighing: weighing compound protein particles, sugar alcohol, flavoring agent, sweetener, adhesive A and essence according to the formula amount, and sieving with 20 mesh sieve for standby;
step S3: mixing: and (3) adding the prepared materials into a three-dimensional mixing tank for mixing for 20-30 minutes, and adding the lubricant for total mixing for 3 minutes to obtain a total mixed material.
8. The method for preparing a composite protein tablet candy according to claim 7, further comprising the steps of:
step S4: and (3) tabletting: putting the total mixed material into a tablet press for tabletting, and discharging tablets;
step S5: and (3) packaging: the pressed candy is packed by HDPE bottles, and a drying agent is arranged in the pressed candy.
9. The method for preparing the composite protein tablet candy according to claim 7, wherein:
in the step d, when the hot air is boiled and dried, the air inlet temperature is controlled to be 40-65 ℃, and the water content is controlled to be less than or equal to 5% at the detection temperature of 105 ℃.
10. The method for preparing the composite protein tablet candy according to claim 8, wherein the tablet pressing temperature in the step S4 is 18-26 ℃ and the humidity is less than or equal to 45%.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202211428870.XA CN115997836A (en) | 2022-11-15 | 2022-11-15 | Composite protein tablet candy and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202211428870.XA CN115997836A (en) | 2022-11-15 | 2022-11-15 | Composite protein tablet candy and preparation method thereof |
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| Publication Number | Publication Date |
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| CN115997836A true CN115997836A (en) | 2023-04-25 |
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| CN202211428870.XA Pending CN115997836A (en) | 2022-11-15 | 2022-11-15 | Composite protein tablet candy and preparation method thereof |
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| Country | Link |
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| CN (1) | CN115997836A (en) |
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- 2022-11-15 CN CN202211428870.XA patent/CN115997836A/en active Pending
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