CN115852461A - Acid bright copper plating electroplating method - Google Patents

Acid bright copper plating electroplating method Download PDF

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Publication number
CN115852461A
CN115852461A CN202211609045.XA CN202211609045A CN115852461A CN 115852461 A CN115852461 A CN 115852461A CN 202211609045 A CN202211609045 A CN 202211609045A CN 115852461 A CN115852461 A CN 115852461A
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China
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plate
copper plating
hollow shaft
trigger
spring
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Chinese (zh)
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舒平
严东华
李洪斌
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Jiangxi Boquan Chemical Co ltd
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Jiangxi Boquan Chemical Co ltd
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Priority to CN202211609045.XA priority Critical patent/CN115852461A/en
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Abstract

The invention discloses an acid bright copper plating electroplating method, which relates to the technical field of electroplating and is realized by using acid bright copper plating electroplating equipment, wherein the acid bright copper plating electroplating equipment comprises a pre-used mixing tank, the bottom of the pre-used mixing tank is fixedly provided with an electroplating bath, the top of the pre-used mixing tank is fixedly nested with an activated carbon powder discharging tank, and a partition plate and a filter plate are sequentially and fixedly arranged in the pre-used mixing tank from top to bottom; the fixed actuating mechanism that is provided with in advance mixing tank, actuating mechanism outside transmission is connected with triggers formula shutoff mechanism, division board and trigger formula shutoff mechanism go up to be provided with a plurality of regulation formula rabbling mechanisms jointly. The electroplating solution transfer device saves manpower, has higher automation degree, can effectively reduce the floating generated in the active carbon adding process, can also quickly finish the transfer of the electroplating solution, and improves the preparation efficiency of the electroplating solution.

Description

Acid bright copper plating electroplating method
Technical Field
The invention relates to the technical field of electroplating, in particular to an acid bright copper plating electroplating method.
Background
The acid copper plating has high current efficiency and simple components, and a full-bright plating layer with good toughness can be obtained after adding the brightener, so that the acid copper plating is the plating seed with the most excellent leveling property and brightness at present.
The invention patent of the publication No. CN103320820B discloses an acid bright copper plating electroplating process, which comprises the steps of preparation of a copper plating solution, pretreatment of a workpiece, acid bright copper plating and the like. By adopting the process, the copper plating layer with the thickness of a few millimeters can be continuously plated on the surface of the metal matrix, and the electroplating is not required to be divided for multiple times; the electroplating cast copper has good bonding force with a matrix and can bear the external forces of machines such as turning, milling, stretching, external polishing and the like; the plating solution has good stability and uniform surface.
When the copper plating solution is prepared in the electroplating process, the mixing of deionized water, sulfuric acid and copper sulfate is completed in a pre-used tank, then activated carbon is uniformly scattered into the mixed solution, the clarification of the solution in the pre-used tank is waited, then the filtering is carried out, and the filtrate is transferred into an electroplating tank.
But the technical staff in this field discovers when practical application, in order to make the active carbon can evenly spill into, consequently when carrying out this operation, often by artifical manual operation, when extravagant manpower, the active carbon still can produce in unrestrained in-process and drift, still can cause the influence to operational environment when extravagant raw materials, in addition because the solution volume of waiting to filter in the groove in advance is great, adopt traditional filterable mode can consume longer time, there is great influence to plating solution preparation efficiency.
Therefore, it is necessary to develop an acid bright copper plating method to solve the above problems.
Disclosure of Invention
The invention aims to provide an acid bright copper plating electroplating method to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme: the acid bright copper plating electroplating method is realized by using acid bright copper plating electroplating equipment, the acid bright copper plating electroplating equipment comprises a pre-used mixing tank, the bottom of the pre-used mixing tank is fixedly provided with an electroplating bath, the top of the pre-used mixing tank is fixedly nested with an active carbon powder discharging tank, and a partition plate and a filter plate are sequentially and fixedly arranged in the pre-used mixing tank from top to bottom;
a driving mechanism is fixedly arranged in the pre-use mixing tank, a triggering type plugging mechanism is connected to the outer side of the driving mechanism in a transmission mode, a plurality of adjusting type stirring mechanisms are jointly arranged on the partition plate and the triggering type plugging mechanism, and a triggering type mixing feeding mechanism is jointly arranged on the right side of the pre-use mixing tank and the driving mechanism;
the driving mechanism comprises a mounting frame, a hollow shaft, a driving motor, a driving gear and a throwing disc;
the mounting rack is fixedly arranged at the bottom of the inner side of the pre-used mixing tank, the hollow shaft penetrates through the mounting rack and is rotatably connected with the mounting rack through a bearing, the driving motors are fixedly arranged on the right side of the bottom of the mounting rack, two driving gears are arranged, the hollow shaft is in transmission connection with the driving motors through the two driving gears, and the throwing disc is fixedly arranged at the top end of the hollow shaft;
the trigger type plugging mechanism comprises a trigger plate, a first spring, an upper closing plate, a connecting rod and a lower closing plate;
trigger plate, first spring, go up the shut and down the shut from top to bottom cup joints in proper order and sets up in the hollow shaft outside, trigger plate and hollow shaft threaded connection, go up the shut all with hollow shaft sliding connection with lower shut, first spring one end with trigger plate fixed connection and the other end and last shut fixed connection, the connecting rod is provided with four, four the connecting rod is fixed respectively and sets up in last shut bottom four corners, and all with shut fixed connection down.
Preferably, the adjustable stirring mechanism comprises a screw, a first stirring rod, a longitudinal sliding groove, a sliding column, a sliding sleeve, a second stirring rod and a second spring.
Preferably, the screw rod runs through the division board and is connected with the division board rotation through the bearing, the screw rod run through the trigger board and with trigger board threaded connection, first puddler, slip post, slip sleeve pipe, second puddler and second spring all are provided with a plurality ofly, and are a plurality of first puddler is even fixed to be set up in screw rod both sides bottom, vertical spout is seted up in the screw rod openly.
Preferably, it is a plurality of the slip post slides along vertical direction and sets up in vertical spout inboard, and is a plurality of slip sleeve pipe slides to cup joint and sets up in the screw rod outside, and respectively with a plurality of slip post fixed connection, it is a plurality of the second puddler is fixed respectively and sets up in a plurality of slip sleeve pipe both sides, and is a plurality of the second spring evenly cup joints and sets up in the screw rod outside, and arbitrary one second spring is located between two adjacent slip sleeve pipes.
Preferably, trigger formula mixes feed mechanism includes brightener storage jar, first valve, intake pipe, air pump, discharging pipe, second valve, T shape shutoff pole and third spring.
Preferably, brightener storage jar is fixed to be set up in the blending tank right side of using in advance, the fixed nestification of first valve sets up in brightener storage jar right side top, the intake pipe is fixed to run through and to set up in brightener storage jar right side and be connected with the output of air pump, the discharging pipe is fixed to run through and to set up in brightener storage jar bottom and be connected with the hollow shaft bottom through rotary joint.
Preferably, the second valve is provided with a plurality of, and is a plurality of the even fixed nestification of second valve sets up in hollow shaft outside bottom, the T shape shutoff pole slides along vertical direction nestedly and sets up in the hollow shaft inboard, third spring one end and hollow shaft inner wall fixed connection and the other end and T shape shutoff pole fixed connection.
Preferably, the method specifically comprises the following steps:
s1, adding deionized water into a pre-used mixing tank, starting a driving motor, driving a hollow shaft to rotate through a driving gear by the driving motor, driving a trigger plate to ascend when the hollow shaft rotates, driving a screw to rotate when the trigger plate ascends, driving a plurality of second stirring rods to stir the deionized water by the screw, sequentially adding sulfuric acid and copper sulfate, uniformly mixing the sulfuric acid and the deionized water to form a mixed solution under the continuous stirring of the second stirring rods, and dissolving the copper sulfate in the mixed solution;
s2, the trigger plate drives the compressed first spring to gradually reset when rising, at the moment, the activated carbon powder is added into the activated carbon powder feeding tank, the activated carbon powder continuously falls onto the top of the throwing disc from a discharge hole in the bottom of the activated carbon powder feeding tank, the throwing disc continuously rotates to uniformly throw the activated carbon powder falling onto the top of the throwing disc, and the activated carbon powder uniformly falls into the mixed solution;
s3, the plurality of second stirring rods continue to stir the mixed solution, when the rising distance of the trigger plate reaches a first threshold value, the driving motor is stopped, the mixed solution is clarified, then the driving motor is started again, and at the moment, along with the continuous rising of the trigger plate, the trigger plate pulls the upper sealing plate through the first spring;
s4, when the ascending distance of the trigger plate reaches a second threshold value, the upper sealing plate releases the blockage of the partition plate, meanwhile, the T-shaped sealing rod ascends under the pushing of the trigger plate, the blockage of a second valve is further released from the interior of the hollow shaft, and the clarified mixed solution passes through a channel on the partition plate and falls into the top of the filter plate to be filtered by the filter plate;
s5, after the second valves are unblocked, the air flow input into the brightener storage tank through the air inlet pipe by the air pump pushes the brightener in the brightener storage tank, the brightener enters the hollow shaft through the discharge pipe, and is sprayed out through the second valves to be mixed with the mixed solution to be filtered to form a copper plating solution;
s6, when the rising distance of the trigger plate reaches a third threshold value, the mixed solution at the top of the partition plate completely passes through a channel on the partition plate and falls into the top of the filter plate, the lower closing plate is driven by the connecting rod to block the channel on the partition plate from the lower part, then the driving motor is stopped, the brightener continuously enters a cavity formed between the partition plate and the filter plate through a second valve, and the mixed solution rapidly passes through the filter plate due to pressure and falls into the plating bath under the condition that the pressure between the partition plate and the filter plate is enhanced because the partition plate is closed until the transfer of the copper plating solution is completed;
s7, pre-plating copper on the workpiece by adopting a conventional alkaline copper plating process, and then placing the workpiece subjected to pre-plating copper into a plating bath containing a copper plating solution for electroplating treatment.
The invention has the technical effects and advantages that:
the invention is provided with the driving mechanism, the triggering type plugging mechanism, the adjusting type stirring mechanism and the triggering type mixed feeding mechanism, so that the driving mechanism drives the adjusting type stirring mechanism to realize material mixing, the triggering type plugging mechanism can be driven to further enable the triggering type plugging mechanism to remove plugging of the partition plate, and quick output of mixed solution is realized.
Drawings
Fig. 1 is an overall front sectional structural view of the present invention.
Fig. 2 is a partial front sectional structural schematic view of the driving mechanism of the present invention.
Fig. 3 is a partial front sectional structural schematic view of the triggered plugging mechanism and the triggered hybrid feeding mechanism according to the present invention.
Fig. 4 is a schematic sectional front view of an adjustable stirring mechanism according to the present invention.
Fig. 5 is a partial front cross-sectional structural schematic view of the trigger type mixing and feeding mechanism of the present invention.
In the figure: 1. a pre-use mixing tank; 2. an electroplating bath; 3. feeding the activated carbon powder into a material tank; 4. a partition plate; 5. filtering a plate; 6. a drive mechanism; 61. a mounting frame; 62. a hollow shaft; 63. a drive motor; 64. a drive gear; 65. a throwing disc; 7. a trigger type plugging mechanism; 71. a trigger plate; 72. a first spring; 73. an upper closing plate; 74. a connecting rod; 75. a lower closing plate; 8. an adjustable stirring mechanism; 81. a screw; 82. a first stirring rod; 83. a longitudinal chute; 84. a sliding post; 85. a sliding sleeve; 86. a second stirring rod; 87. a second spring; 9. a trigger type mixing feeding mechanism; 91. a brightener storage tank; 92. a first valve; 93. an air inlet pipe; 94. an air pump; 95. a discharge pipe; 96. a second valve; 97. a T-shaped plugging rod; 98. a third spring.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be obtained by a person skilled in the art without making any creative effort based on the embodiments in the present invention, belong to the protection scope of the present invention.
Example 1
The invention provides an acid bright copper plating electroplating method as shown in figures 1-5, which is realized by using acid bright copper plating electroplating equipment, wherein the acid bright copper plating electroplating equipment comprises a pre-used mixing tank 1, the bottom of the pre-used mixing tank 1 is fixedly provided with an electroplating bath 2, the top of the pre-used mixing tank 1 is fixedly nested with an activated carbon powder discharging tank 3, and a partition plate 4 and a filter plate 5 are sequentially and fixedly arranged in the pre-used mixing tank 1 from top to bottom;
it is provided with actuating mechanism 6 to use 1 inside fixed of blending tank in advance, 6 outside transmissions of actuating mechanism are connected with and trigger formula shutoff mechanism 7, division board 4 and trigger formula shutoff mechanism 7 go up and be provided with a plurality of regulation formula rabbling mechanisms 8 jointly, it triggers formula mixed feeding mechanism 9 to be provided with jointly on 1 right side of blending tank in advance and the actuating mechanism 6.
As shown in fig. 2 and 3, the driving mechanism 6 includes a mounting bracket 61, a hollow shaft 62, a driving motor 63, a driving gear 64 and a throwing disk 65, wherein the mounting bracket 61 is fixedly arranged at the bottom inside the pre-mixing tank 1, the hollow shaft 62 penetrates through the mounting bracket 61 and is rotatably connected with the mounting bracket 61 through a bearing, the driving motor 63 is fixedly arranged at the right side of the bottom of the mounting bracket 61, the two driving gears 64 are arranged, the hollow shaft 62 is in transmission connection with the driving motor 63 through the two driving gears 64, and the throwing disk 65 is fixedly arranged at the top end of the hollow shaft 62.
Through setting up above-mentioned structure to drive hollow shaft 62 through drive gear 64 and rotate after driving motor 63 starts, hollow shaft 62 then continuously drives throwing dish 65 and rotates, and active carbon powder is constantly fallen on throwing dish 65 top back by the discharge gate of active carbon powder unloading jar 3 bottom, and the active carbon powder that falls on its top is evenly thrown and is flown by the throwing dish 65 of continuous rotation, and active carbon powder evenly falls into the mixed solution.
As shown in fig. 3, the triggered plugging mechanism 7 includes a trigger plate 71, a first spring 72, an upper closing plate 73, a connecting rod 74 and a lower closing plate 75, wherein the trigger plate 71, the first spring 72, the upper closing plate 73 and the lower closing plate 75 are sequentially sleeved and arranged on the outer side of the hollow shaft 62 from top to bottom, the trigger plate 71 is in threaded connection with the hollow shaft 62, the upper closing plate 73 and the lower closing plate 75 are both in sliding connection with the hollow shaft 62, one end of the first spring 72 is fixedly connected with the trigger plate 71, the other end of the first spring is fixedly connected with the upper closing plate 73, the connecting rods 74 are four, and the four connecting rods 74 are respectively and fixedly arranged at four corners of the bottom of the upper closing plate 73 and are both fixedly connected with the lower closing plate 75.
By adopting the structure, the compressed first spring 72 is driven to gradually return when the trigger plate 71 rises, when the rising distance of the trigger plate 71 reaches a second threshold value, the upper sealing plate 73 unblocks the partition plate 4, and the clarified mixed solution passes through the passage on the partition plate 4 and falls onto the top of the filter plate 5 to be filtered by the filter plate 5.
As shown in fig. 4, the adjustable stirring mechanism 8 includes a screw 81, a first stirring rod 82, a longitudinal sliding groove 83, sliding columns 84, sliding sleeves 85, a second stirring rod 86 and a second spring 87, wherein the screw 81 penetrates through the partition plate 4 and is rotatably connected with the partition plate 4 through a bearing, the screw 81 penetrates through the trigger plate 71 and is in threaded connection with the trigger plate 71, the first stirring rod 82, the sliding columns 84, the sliding sleeves 85, the second stirring rod 86 and the second spring 87 are all provided with a plurality of first stirring rods 82, the plurality of first stirring rods 82 are uniformly fixed and arranged at the bottoms of the two sides of the screw 81, the longitudinal sliding groove 83 is arranged on the front surface of the screw 81, the plurality of sliding columns 84 are slidably arranged on the inner side of the longitudinal sliding groove 83 along the vertical direction, the plurality of sliding sleeves 85 are slidably arranged on the outer side of the screw 81 and are respectively fixedly connected with the plurality of sliding columns 84, the plurality of second stirring rods 86 are respectively fixedly arranged on two sides of the plurality of sliding sleeves 85, the plurality of second springs 87 are uniformly arranged on the outer side of the screw 81, and any one second spring 87 is located between two adjacent sliding sleeves 85.
Through setting up above-mentioned structure, so that it rotates to drive screw rod 81 when trigger plate 71 rises, screw rod 81 then drives a plurality of second puddlers 86 and stirs the material, and then make the material homogeneous mixing or dissolve with higher speed, simultaneously when trigger plate 71 rises, the second spring 87 of compressed can promote sliding sleeve 85, and then make sliding sleeve 85 drive second puddler 86 and rise, and then adjust the height-to-stir, screw rod 81 can also treat filterable mixed solution and brightener through first puddler 82 and stir the mixing simultaneously.
As shown in fig. 3 and 5, trigger type mixed feeding mechanism 9 includes brightener storage tank 91, first valve 92, intake pipe 93, air pump 94, discharging pipe 95, second valve 96, T-shaped plugging rod 97 and third spring 98, wherein brightener storage tank 91 is fixed to be set up in pre-use mixing tank 1 right side, first valve 92 is fixed nested to be set up in brightener storage tank 91 right side top, intake pipe 93 is fixed to run through to be set up in brightener storage tank 91 right side and be connected with the output of air pump 94, discharging pipe 95 is fixed to run through to be set up in brightener storage tank 91 bottom and be connected with hollow shaft 62 bottom through rotary joint, second valve 96 is provided with a plurality ofly, and is a plurality of second valve 96 is even fixed nested to be set up in hollow shaft 62 outside bottom, T-shaped plugging rod 97 slides along vertical direction and nestedly to be set up in hollow shaft 62 inboard, third spring 98 one end and hollow shaft 62 inner wall fixed connection and the other end and T-shaped plugging rod 97 fixed connection.
Through setting up above-mentioned structure, so that T shape shutoff pole 97 rises under the promotion of trigger plate 71, and then remove the shutoff to second valve 96 by hollow shaft 62 is inside, the mixed solution after the clarification passes the passageway on the division board 4 and falls into the filter plate 5 top and is filtered by filter plate 5 this moment, second valve 96 removes the shutoff back simultaneously, air pump 94 promotes the inside brightener of brightener storage jar 91 through the inside air current of intake pipe 93 input brightener storage jar 91, the brightener enters into inside hollow shaft 62 through discharging pipe 95, then spout through a plurality of second valves 96, and then mix with the mixed solution that treats filtration, form copper-plating solution.
In addition, when the passage on the partition plate 4 is blocked again, the brightener continuously enters the chamber formed between the partition plate 4 and the filter plate 5 through the second valve 96, and the partition plate 4 is closed, so that the mixed solution can penetrate through the filter plate 5 and fall into the plating tank 2 more quickly due to the pressure under the condition that the pressure between the partition plate 4 and the filter plate 5 is increased.
Example 2
The method specifically comprises the following steps:
s1, adding deionized water into a pre-used mixing tank 1, then starting a driving motor 63, driving the hollow shaft 62 to rotate by the driving motor 63 through a driving gear 64, driving a trigger plate 71 to ascend when the hollow shaft 62 rotates, driving a screw 81 to rotate when the trigger plate 71 ascends, driving a plurality of second stirring rods 86 to stir the deionized water by the screw 81, sequentially adding sulfuric acid and copper sulfate, uniformly mixing the sulfuric acid and the deionized water to form a mixed solution under the continuous stirring of the second stirring rods 86, and dissolving the copper sulfate in the mixed solution;
s2, the trigger plate 71 drives the compressed first spring 72 to gradually reset when rising, at the moment, the activated carbon powder is added into the activated carbon powder feeding tank 3, the activated carbon powder continuously falls on the top of the throwing disc 65 from a discharge hole in the bottom of the activated carbon powder feeding tank 3, the throwing disc 65 which continuously rotates uniformly throws the activated carbon powder falling on the top of the throwing disc, and the activated carbon powder uniformly falls into the mixed solution;
s3, the plurality of second stirring rods 86 continue to stir the mixed solution, when the rising distance of the trigger plate 71 reaches a first threshold value, the driving motor 63 is stopped, the mixed solution is clarified, then the driving motor 63 is started again, and at the moment, along with the continuous rising of the trigger plate 71, the trigger plate 71 pulls the upper closing plate 73 through the first spring 72;
s4, when the ascending distance of the trigger plate 71 reaches a second threshold value, the upper closing plate 73 removes the blockage of the partition plate 4, meanwhile, the T-shaped blocking rod 97 ascends under the pushing of the trigger plate 71, and further removes the blockage of the second valve 96 from the interior of the hollow shaft 62, and at the moment, the clarified mixed solution passes through a channel on the partition plate 4 and falls onto the top of the filter plate 5 to be filtered by the filter plate 5;
s5, after the second valves 96 are unblocked, air flow input into the brightener storage tank 91 through the air inlet pipe 93 by the air pump 94 pushes the brightener in the brightener storage tank 91, the brightener enters the hollow shaft 62 through the discharge pipe 95 and is sprayed out through the second valves 96 to be mixed with a mixed solution to be filtered to form a copper plating solution;
s6, when the rising distance of the trigger plate 71 reaches a third threshold value, the mixed solution at the top of the partition plate 4 completely passes through a channel on the partition plate 4 and falls onto the top of the filter plate 5, the lower closing plate 75 is driven by the connecting rod 74 to block the channel on the partition plate 4 from the lower part, then the driving motor 63 is stopped, and at the moment, the brightener continuously enters a cavity formed between the partition plate 4 and the filter plate 5 through the second valve 96, and because the partition plate 4 is closed, under the condition that the pressure between the partition plate 4 and the filter plate 5 is enhanced, the mixed solution rapidly passes through the filter plate 5 due to the pressure and falls into the electroplating bath 2 until the transfer of the copper plating solution is completed;
s7, pre-plating copper on the workpiece by adopting a conventional alkaline copper plating process, and then putting the pre-plated copper workpiece into a plating bath containing a copper plating solution for electroplating treatment.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, those skilled in the art can still make modifications to the technical solutions described in the foregoing embodiments, or make equivalent substitutions and improvements to part of the technical features of the foregoing embodiments, and any modifications, equivalent substitutions and improvements made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims (8)

1. An acid bright copper plating electroplating method is characterized in that: the acid bright copper plating electroplating method is realized by using acid bright copper plating electroplating equipment, the acid bright copper plating electroplating equipment comprises a pre-used mixing tank (1), an electroplating bath (2) is fixedly arranged at the bottom of the pre-used mixing tank (1), an activated carbon powder discharging tank (3) is fixedly nested at the top of the pre-used mixing tank (1), and a partition plate (4) and a filter plate (5) are fixedly arranged in the pre-used mixing tank (1) from top to bottom in sequence;
a driving mechanism (6) is fixedly arranged in the pre-use mixing tank (1), the outer side of the driving mechanism (6) is in transmission connection with a trigger type plugging mechanism (7), a plurality of adjusting type stirring mechanisms (8) are jointly arranged on the partition plate (4) and the trigger type plugging mechanism (7), and a trigger type mixing and feeding mechanism (9) is jointly arranged on the right side of the pre-use mixing tank (1) and the driving mechanism (6);
the driving mechanism (6) comprises a mounting frame (61), a hollow shaft (62), a driving motor (63), a driving gear (64) and a throwing disc (65);
the mounting rack (61) is fixedly arranged at the bottom of the inner side of the pre-used mixing tank (1), the hollow shaft (62) penetrates through the mounting rack (61) and is rotatably connected with the mounting rack (61) through a bearing, the driving motor (63) is fixedly arranged on the right side of the bottom of the mounting rack (61), two driving gears (64) are arranged, the hollow shaft (62) is in transmission connection with the driving motor (63) through the two driving gears (64), and the sprinkling plate (65) is fixedly arranged at the top end of the hollow shaft (62);
the trigger type plugging mechanism (7) comprises a trigger plate (71), a first spring (72), an upper closing plate (73), a connecting rod (74) and a lower closing plate (75);
trigger plate (71), first spring (72), go up closing plate (73) and lower closing plate (75) from top to bottom cup joint in proper order and set up in the hollow shaft (62) outside, trigger plate (71) and hollow shaft (62) threaded connection, go up closing plate (73) and lower closing plate (75) all with hollow shaft (62) sliding connection, first spring (72) one end with trigger plate (71) fixed connection and the other end and last closing plate (73) fixed connection, connecting rod (74) are provided with four, four connecting rod (74) are fixed respectively and set up in last closing plate (73) bottom four corners, and all with lower closing plate (75) fixed connection.
2. The method of acid bright copper plating according to claim 1, characterized in that: the adjustable stirring mechanism (8) comprises a screw rod (81), a first stirring rod (82), a longitudinal sliding groove (83), a sliding column (84), a sliding sleeve (85), a second stirring rod (86) and a second spring (87).
3. The method of acid bright copper plating according to claim 2, characterized in that: screw rod (81) run through division board (4) and rotate with division board (4) through the bearing and be connected, screw rod (81) run through trigger plate (71) and with trigger plate (71) threaded connection, first puddler (82), slip post (84), slip sleeve (85), second puddler (86) and second spring (87) all are provided with a plurality ofly, and are a plurality of first puddler (82) are even fixed to be set up in screw rod (81) both sides bottom, screw rod (81) are openly seted up in vertical spout (83).
4. The method according to claim 3, wherein the plating solution comprises: it is a plurality of slip post (84) slide along vertical direction and set up in vertical spout (83) inboard, it is a plurality of slip sleeve pipe (85) slide to cup joint and set up in screw rod (81) outside, and respectively with a plurality of slip post (84) fixed connection, it is a plurality of second puddler (86) are fixed respectively and set up in a plurality of slip sleeve pipe (85) both sides, and are a plurality of second spring (87) evenly cup joint and set up in the screw rod (81) outside, and arbitrary one second spring (87) are located between two adjacent slip sleeve pipes (85).
5. The method of acid bright copper plating according to claim 4, wherein: trigger formula mixes feed mechanism (9) includes brightener storage jar (91), first valve (92), intake pipe (93), air pump (94), discharging pipe (95), second valve (96), T shape shutoff pole (97) and third spring (98).
6. The method of acid bright copper plating according to claim 5, wherein: brightener storage jar (91) is fixed to be set up in mixing tank (1) right side for use in advance, first valve (92) are fixed nested to be set up in brightener storage jar (91) right side top, intake pipe (93) are fixed to run through to be set up in brightener storage jar (91) right side and be connected with the output of air pump (94), discharging pipe (95) are fixed to run through to be set up in brightener storage jar (91) bottom and through rotary joint and hollow shaft (62) bottom connection.
7. The method of acid bright copper plating according to claim 6, wherein: the second valve (96) is provided with a plurality of, a plurality of second valve (96) are evenly fixed and nested and are arranged at the bottom of the outer side of the hollow shaft (62), the T-shaped plugging rod (97) is arranged at the inner side of the hollow shaft (62) in a sliding and nesting mode along the vertical direction, one end of the third spring (98) is fixedly connected with the inner wall of the hollow shaft (62) and the other end of the third spring is fixedly connected with the T-shaped plugging rod (97).
8. The acid bright copper plating electroplating method according to claim 7, characterized in that the method specifically comprises the following steps:
s1, adding deionized water into a pre-used mixing tank (1), then starting a driving motor (63), wherein the driving motor (63) drives a hollow shaft (62) to rotate through a driving gear (64), the hollow shaft (62) drives a trigger plate (71) to ascend when rotating, the trigger plate (71) drives a screw rod (81) to rotate when ascending, the screw rod (81) drives a plurality of second stirring rods (86) to stir the deionized water, sequentially adding sulfuric acid and copper sulfate, and under the continuous stirring of the second stirring rods (86), uniformly mixing the sulfuric acid and the deionized water to form a mixed solution, wherein the copper sulfate is dissolved in the mixed solution;
s2, the trigger plate (71) drives the compressed first spring (72) to gradually reset when rising, at the moment, the activated carbon powder is added into the activated carbon powder discharging tank (3), the activated carbon powder is continuously dropped on the top of the throwing disc (65) from a discharging port at the bottom of the activated carbon powder discharging tank (3), the continuously rotating throwing disc (65) uniformly throws the activated carbon powder dropped on the top of the throwing disc, and the activated carbon powder uniformly drops into the mixed solution;
s3, continuously stirring the mixed solution by a plurality of second stirring rods (86), stopping the driving motor (63) when the ascending distance of the trigger plate (71) reaches a first threshold value, waiting for clarification of the mixed solution, and then starting the driving motor (63) again, wherein the trigger plate (71) pulls the upper closing plate (73) through the first spring (72) along with continuous ascending of the trigger plate (71);
s4, when the ascending distance of the trigger plate (71) reaches a second threshold value, the upper closing plate (73) removes the blockage of the partition plate (4), meanwhile, the T-shaped blocking rod (97) ascends under the pushing of the trigger plate (71), and then the blockage of the second valve (96) is removed from the interior of the hollow shaft (62), and at the moment, the clarified mixed solution passes through a channel on the partition plate (4) and falls onto the top of the filter plate (5) to be filtered by the filter plate (5);
s5, after the second valves (96) are unblocked, the air pump (94) inputs air flow inside the brightener storage tank (91) through the air inlet pipe (93) to push the brightener inside the brightener storage tank (91), the brightener enters the hollow shaft (62) through the discharge pipe (95), is sprayed out through the second valves (96) and is mixed with a mixed solution to be filtered to form a copper plating solution;
s6, when the rising distance of the trigger plate (71) reaches a third threshold value, the mixed solution at the top of the partition plate (4) completely passes through a channel on the partition plate (4) and falls into the top of the filter plate (5), the lower closing plate (75) is driven by the connecting rod (74) to block the channel on the partition plate (4) from below, then the driving motor (63) is stopped, the brightener continuously enters a cavity formed between the partition plate (4) and the filter plate (5) through a second valve (96), and the partition plate (4) is closed, so that the mixed solution rapidly passes through the filter plate (5) due to pressure and falls into the electroplating bath (2) under the condition that the pressure between the partition plate (4) and the filter plate (5) is enhanced until the copper plating solution is transferred;
s7, pre-plating copper on the workpiece by adopting a conventional alkaline copper plating process, and then putting the pre-plated copper workpiece into a plating bath containing a copper plating solution for electroplating treatment.
CN202211609045.XA 2022-12-14 2022-12-14 Acid bright copper plating electroplating method Pending CN115852461A (en)

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Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR980009120A (en) * 1996-07-05 1998-04-30 박계향 Activated carbon supply method and supply device for water purification plant
KR200303104Y1 (en) * 2002-10-31 2003-02-06 주식회사 동양고속건설 Apparatus for casting an activated charcoal with high water content rate
CN102312270A (en) * 2010-07-06 2012-01-11 富葵精密组件(深圳)有限公司 Electroplating system and application method thereof
JP2017141503A (en) * 2016-02-10 2017-08-17 株式会社荏原製作所 Apparatus and method for feeding plating solution to plating tank, plating system, powder container, and plating method
KR101781781B1 (en) * 2017-04-07 2017-09-25 이근백 Activated carbon powder auto dissolving unit
CN208618004U (en) * 2018-07-11 2019-03-19 深圳市好天机械设备有限公司 A kind of Automatic Dosing dispensation apparatus efficiently mixed
KR20210015989A (en) * 2019-03-18 2021-02-10 티티앤에스 주식회사 Coating apparatus for coating a substrate with a coating solution containing mixed powder
CN212895068U (en) * 2020-05-29 2021-04-06 洛阳吉瓦新材料科技有限公司 Purification treatment device for thickened plating solution for electroplating diamond wire production
CN215352424U (en) * 2021-06-28 2021-12-31 南京天印电镀有限公司 Electroplating solution filtering device
CN114525574A (en) * 2020-11-23 2022-05-24 余姚市爱迪升电镀科技有限公司 Plating solution circulating device and plating solution filtering method
CN116216764A (en) * 2022-12-08 2023-06-06 江西博泉化学有限公司 Method for producing easily soluble copper oxide by using acidic etching waste liquid

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR980009120A (en) * 1996-07-05 1998-04-30 박계향 Activated carbon supply method and supply device for water purification plant
KR200303104Y1 (en) * 2002-10-31 2003-02-06 주식회사 동양고속건설 Apparatus for casting an activated charcoal with high water content rate
CN102312270A (en) * 2010-07-06 2012-01-11 富葵精密组件(深圳)有限公司 Electroplating system and application method thereof
JP2017141503A (en) * 2016-02-10 2017-08-17 株式会社荏原製作所 Apparatus and method for feeding plating solution to plating tank, plating system, powder container, and plating method
KR101781781B1 (en) * 2017-04-07 2017-09-25 이근백 Activated carbon powder auto dissolving unit
CN208618004U (en) * 2018-07-11 2019-03-19 深圳市好天机械设备有限公司 A kind of Automatic Dosing dispensation apparatus efficiently mixed
KR20210015989A (en) * 2019-03-18 2021-02-10 티티앤에스 주식회사 Coating apparatus for coating a substrate with a coating solution containing mixed powder
CN212895068U (en) * 2020-05-29 2021-04-06 洛阳吉瓦新材料科技有限公司 Purification treatment device for thickened plating solution for electroplating diamond wire production
CN114525574A (en) * 2020-11-23 2022-05-24 余姚市爱迪升电镀科技有限公司 Plating solution circulating device and plating solution filtering method
CN215352424U (en) * 2021-06-28 2021-12-31 南京天印电镀有限公司 Electroplating solution filtering device
CN116216764A (en) * 2022-12-08 2023-06-06 江西博泉化学有限公司 Method for producing easily soluble copper oxide by using acidic etching waste liquid

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
袁诗璞;: "光亮酸性镀铜的设备配置", 涂装与电镀, no. 03, 15 June 2010 (2010-06-15), pages 15 - 22 *

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