CN115804375B - Foam disinfectant for farms and preparation method thereof - Google Patents

Foam disinfectant for farms and preparation method thereof Download PDF

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Publication number
CN115804375B
CN115804375B CN202211501534.3A CN202211501534A CN115804375B CN 115804375 B CN115804375 B CN 115804375B CN 202211501534 A CN202211501534 A CN 202211501534A CN 115804375 B CN115804375 B CN 115804375B
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disinfectant
foam
agent
disinfection
quaternary ammonium
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CN115804375A (en
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周衡
崔小七
申金艳
陈盟
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Zhengzhou Bary Animal Pharmaceutical Co ltd
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Zhengzhou Bary Animal Pharmaceutical Co ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/70Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in livestock or poultry

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Abstract

The invention belongs to the technical field of disinfection in the breeding industry, and discloses a foam disinfectant for a breeding farm, which comprises the following components in percentage by mass: 10-20% of quaternary ammonium salt disinfectant, 5-10% of glutaraldehyde disinfectant, 2-10% of foaming agent, 1-5% of foam stabilizer, 5-10% of builder, 1-3% of emulsifier, 1-5% of humectant, 10-15% of antifreezing agent, 0.2-2% of flavoring agent, 0.1-0.3% of pH regulator and the balance of water; the foaming agent is a mixture of alpha-olefin sodium sulfonate and glyceroglycosides; the foam stabilizer is lauryl dimethyl ammonium oxide. The disinfectant disclosed by the invention has the advantages that the foaming auxiliary agent is added while the quality of the disinfectant is ensured, so that the foam is fine and rich, the foam is not easy to foam, the adhesion force is strong, the contact time of the disinfectant with a target interface and pathogenic microorganisms is prolonged, and the more efficient and thorough disinfection effect is realized.

Description

Foam disinfectant for farms and preparation method thereof
Technical Field
The invention belongs to the technical field of disinfection in the breeding industry, and relates to a foam disinfectant for a breeding farm and a preparation method thereof.
Background
The livestock and poultry farming industry needs to take various measures for controlling the occurrence and the epidemic of livestock and poultry infectious diseases, wherein disinfection is an important measure. The disinfection of the farm can stop the epidemic disease from spreading continuously by killing pathogenic microorganisms in the environment and cutting off the transmission path. The farm should establish a practical disinfection system to disinfect the farm housing, the farm equipment, the chicken coops, the slaughter houses and the like regularly.
The traditional cleaning and disinfecting method has the defects of high labor intensity, long cleaning time and low disinfectant utilization rate, and can not effectively remove diarrhea excreted adhesion, grease, biological films and the like in a hurdle; the foam type cleaning disinfectant has high removal rate for the refractory adherends, has the advantages of good adhesion and permeability, high cleaning and disinfecting efficiency, good observability and operability and the like, and is a novel product with increasingly wide application at present. The foam disinfectant is adhered to the surface of an object in a mode of converting liquid disinfectant into gas-phase foam through the foam generating device, and biological films on the surface of the object are removed through the actions of wetting, emulsifying, penetrating, dispersing and solubilizing after the foam disinfectant contacts with the surface to be disinfected, so that the aim of deep cleaning and disinfection is fulfilled.
The foam can be covered on the surface of an object for a long time, and an operator can completely and clearly know which parts are cleaned and disinfected (foam-beating areas) and which parts are not cleaned and disinfected (foam-beating areas) in the house according to the covering condition of the foam, so that the situation that the process of the traditional method cannot be judged after the traditional method is used for disinfection is effectively improved. Meanwhile, foam multiple overlapping can be formed on the edges, the trough, the corners and other parts of the fence according to the foam thickness, key cleaning and disinfection are carried out, quantitative and controllable indexes are provided for cleaning and disinfection, the intuitiveness is stronger, and the aim of visual disinfection is fulfilled.
The invention patent with the publication number of CN 105925395B discloses a foam cleaning agent for animals, which has good foaming effect, rich and fine foam, strong adhesiveness and long adhesion time; meanwhile, the detergent has excellent decontamination effect, and can effectively remove various intractable stains such as dry feces, grease, blood, biological films and the like. However, the foam cleaning agent for animals is a foam cleaning disinfectant with strong alkalinity, is easy to burn the skin of a user, does not contain active ingredients of the disinfectant, and does not have the effect of visual disinfection.
The invention patent with the application publication number of CN 106135202A discloses a foam disinfectant, which comprises the following components in percentage by weight: 10-30% of trimethoprim, 0.5-1% of high-efficiency penetrating agent, 40-60% of foaming agent, 1-1.5% of nonionic surfactant and 100% of purified water, and has broad-spectrum, high-efficiency and rapid sterilization and disinfection effects, but the requirements of stable foam are not fully considered in the prescription, and the effective contact time of the disinfectant and the surface to be disinfected is insufficient.
In recent years, more and more farms have chosen to boost the resistance of farms to pathogenic microorganisms through biosafety measures. In the construction of a plant biosafety system, two operation steps of cleaning and sterilizing are indispensable. The cleaning can remove dirt and organic matters in the culture environment and equipment and facilities to different degrees, thereby improving the contact degree of the disinfectant and pathogens and achieving the aim of disinfection.
Therefore, the foam disinfectant which has good disinfection effect, good foam stability, fine foam and no skin irritation to users is developed, and has important significance in production practice of the breeding industry.
Disclosure of Invention
Aiming at the problem that the sterilization effect is poor due to the fact that the prior art disinfectant is not provided with foaming capacity or poor foam stabilizing capacity, the invention provides the foam disinfectant for the farm and the preparation method thereof, and the foaming auxiliary agent is added while the quality of the disinfectant is ensured, so that the foam is fine and rich, foam is not easy to foam, the adhesion force is strong, the contact time of the disinfectant with a target interface and pathogenic microorganisms is increased, and the more efficient and thorough sterilization effect is realized.
In order to achieve the above purpose, the present invention adopts the following technical scheme:
The invention provides a foam disinfectant for farms, which comprises the following components in percentage by mass: 10-20% of quaternary ammonium salt disinfectant, 5-10% of glutaraldehyde disinfectant, 2-10% of foaming agent, 1-5% of foam stabilizer, 5-10% of builder, 1-3% of emulsifier, 1-5% of humectant, 10-15% of antifreezing agent, 0.2-2% of flavoring agent, 0.1-0.3% of pH regulator and the balance of water; the foaming agent is a mixture of alpha-olefin sodium sulfonate and glyceroglycosides; the foam stabilizer is lauryl dimethyl ammonium oxide.
In one technical scheme, the quaternary ammonium salt disinfectant is a mixture of benzalkonium chloride and decamethyiammonium bromide.
In one embodiment, the builder is ethylene glycol butyl ether.
In one embodiment, the emulsifying agent is poloxamer 407.
In one embodiment, the humectant is polyethylene glycol-6.
In one embodiment, the antifreeze is glycerol.
In one technical scheme, the flavoring agent is a floral type essence.
In one embodiment, the pH adjuster is phosphoric acid.
The invention also provides a preparation method of the foam disinfectant for the farm, which comprises the following steps:
Step 1: weighing the components according to the mass fraction, taking 30-40% of the total mass of the purified water, adding the components into a material melting kettle, adding quaternary ammonium salt disinfectant and glutaraldehyde disinfectant into the material melting kettle respectively, and uniformly stirring;
step 2: respectively adding foaming agent, builder, emulsifier, humectant, antifreezing agent, flavoring agent and the rest purified water, and stirring uniformly;
step 3: adding a pH regulator, regulating the pH value to be 2.0-4.0, and uniformly stirring to obtain the foam disinfectant for visual disinfection.
Compared with the prior art, the invention has the beneficial effects that:
1. The disinfectant disclosed by the invention comprises a quaternary ammonium disinfectant and an aldehyde disinfectant, wherein the quaternary ammonium disinfectant is benzalkonium chloride and decamethylene bromide; the aldehyde disinfectant is glutaraldehyde. The quaternary ammonium salt disinfectant has the advantages of outstanding advantages, no skin irritation, no corrosiveness, no strong oxidizing property, good water solubility, strong surface activity, convenient use, stable property, light resistance, heat resistance and storage resistance. Glutaraldehyde belongs to a broad-spectrum and high-efficiency disinfectant and has the advantages of small irritation, low corrosiveness, safety, low toxicity, small influence by organic matters and the like. The quaternary ammonium salt disinfectant and the aldehyde disinfectant are compounded, so that the disinfectant has strong sterilization and disinfection capability, and can kill pathogenic microorganisms in the environment, thereby cutting off the transmission of the pathogens and achieving the purpose of guaranteeing the safety and health of the livestock and poultry cultivation environment.
2. The foaming agent, foam stabilizer, builder, emulsifier, humectant, antifreezing agent, flavoring agent, pH regulator and purified water in the disinfectant can lead the foam to be fine and rich, and the disinfectant is difficult to foam, strong in adhesive force, double in permeation and strong in decontamination. The foaming auxiliary agent is added while the quality of the disinfectant is ensured, and the special foaming gun is used for disinfection, so that the contact time of the disinfectant with a target interface and pathogenic microorganisms can be increased, and the more efficient and thorough disinfection effect is realized.
3. The foam disinfectant disclosed by the invention meets three elements of effective disinfection: the disinfectant has the advantages of effective disinfectant, effective concentration, full contact, good disinfection effect, high disinfectant utilization rate, strong decontamination and sterilization capability, strong practicability, convenience, quickness, low cost and the like.
Drawings
FIG. 1 shows the results of the foaming force and foam stability test of the present invention.
Detailed Description
The following examples are illustrative of the present invention and are not intended to limit the scope of the invention. The technical means used in the examples are conventional means well known to those skilled in the art unless otherwise indicated. The test methods in the following examples are conventional methods unless otherwise specified. The chemical reagents used in the examples described below are all commercially available. The floral essence in the following examples is lemon essence, purchased from Shenzhen city, yaxiang House essence and perfume Co.
Example 1
Taking 50kg of disinfectant as an example, the foam disinfectant for the farm in the embodiment comprises the following components in percentage by mass:
the preparation method of the foam disinfectant comprises the following steps:
Step 1: weighing the components according to the mass fraction, adding 30-40% of the total mass of the purified water into a material melting kettle, adding benzalkonium chloride, decamethylene bromide and glutaraldehyde into the material melting kettle respectively, and uniformly stirring;
step 2: respectively adding alpha-olefin sodium sulfonate, glyceroglycosides, ethylene glycol butyl ether, poloxamer 407, polyethylene glycol-6, glycerol, floral essence and the rest purified water, and stirring uniformly;
Step 3: adding phosphoric acid, regulating the pH value to 2.0-4.0, and uniformly stirring to obtain the foam disinfectant for visual disinfection.
And (3) detecting the foam disinfectant for visual disinfection, and filling, labeling and boxing the foam disinfectant after the foam disinfectant is qualified.
Example two
Taking 50kg of disinfectant as an example, the foam disinfectant for the farm in the embodiment comprises the following components in percentage by mass:
the disinfectant of this example was prepared in the same manner as in example 1.
Example III
Taking 50kg of disinfectant as an example, the foam disinfectant for the farm in the embodiment comprises the following components in percentage by mass:
the disinfectant of this example was prepared in the same manner as in example 1.
Example IV
Taking 50kg of disinfectant as an example, the foam disinfectant for the farm in the embodiment comprises the following components in percentage by mass:
the disinfectant of this example was prepared in the same manner as in example 1.
Comparative example 1
Compared with example 4, the mass percent of benzalkonium chloride is reduced from 7% to 1%, and the other steps are the same as those of example 4.
Comparative example 2
The glutaraldehyde mass percentage was reduced from 8% to 1% compared to example 4, otherwise the same as in example 4.
Comparative example 3
The mass percent of lauryl dimethyl ammonium oxide was reduced from 2% to 0.1% compared to example 4, otherwise the same as example 4.
Comparative example 4
The mass percent of glycerin was reduced from 15% to 1% as compared to example 4, otherwise the same as in example 4.
Experimental example 1: the ATP content can clearly indicate the residual amount of microorganisms and other organisms in the sample for judging the sanitary condition by comparing ATP detection data before and after washing with the ATP content in all living cells.
The foam disinfectant products of examples 1 to 4 and comparative examples 1 to 4 were diluted 200 times to the use concentration, and ATP detection data before and after washing were compared, and the results are shown in Table 1. As can be seen from Table 1, the cleaning rates of examples 1 to 4 were not very different; the cleaning rate of comparative examples 1 to 4 was significantly lowered. Therefore, reasonable proportion of each component in the invention has important influence on the cleaning rate.
TABLE 1 comparison of ATP detection data (Unit: RLU)
Experimental example 2: foaming force and foam stabilizing performance test
After foam formation, the surface is adhered, and organic biological films on the surface of the object are decomposed through complex physical and chemical actions such as wetting, infiltration, emulsification, suspension, deflocculation, dispersion and solubilization and the like, and the adhesion force between objects and the surface tension between solid and liquid are reduced; meanwhile, bacteria and viruses on the surface and in the gaps are killed and disinfected by the disinfecting component. The foaming power of the foam disinfectant plays a key role in sterilizing effect.
Foam disinfectant products of examples 1 to 4 and comparative examples 1 to 4 were diluted 200 times to use concentrations, and foaming force test was performed according to the surfactant detergent test method (GB/T13173-2021), and the results are shown in FIG. 1.
As can be seen from fig. 1, the foaming forces and foam stabilizing properties of examples 1 to 4 are not greatly different; the foaming power and foam stabilizing performance of comparative examples 1 to 4 were significantly lowered. Therefore, the reasonable proportion of each component in the invention has important influence on the foaming force and the foam stabilizing performance.
Experimental example 3: anti-freezing effect test
The winter climate in northern China is cold, especially northwest and northeast, such as Heilongjiang, inner Mongolian autonomous region, xinjiang and the like, and the winter is long. The disinfectant can be inconvenient to use due to icing.
100ML of each of the foam disinfectant products for visual disinfection of examples 1 to 4 and comparative examples 1 to 4 was taken, placed in a reagent bottle, capped and screwed up, placed in an ultralow temperature refrigerator, the refrigerator was started, the temperature was gradually lowered from room temperature, and the anti-freezing effect was recorded as shown in Table 2.
As can be seen from table 2, the antifreeze effects of examples 1 to 4 differ considerably; the antifreeze effect of the comparative examples 1 to 3 is lower than the antifreeze effect of the examples 1 to 4; the antifreeze effect of the comparative example 4 is significantly reduced. Therefore, reasonable proportion of each component in the invention has important influence on the antifreezing effect.
TABLE 2 antifreeze temperature of foam disinfectants for visual disinfection
The above-mentioned embodiments are merely preferred embodiments of the present invention, which are not intended to limit the scope of the present invention, and other embodiments can be easily made by those skilled in the art through substitution or modification according to the technical disclosure in the present specification, so that all changes and modifications made in the principle of the present invention shall be included in the scope of the present invention.

Claims (4)

1. The foam disinfectant for the farm is characterized by comprising the following components in percentage by mass: 10-20% of quaternary ammonium salt disinfectant, 5-10% of glutaraldehyde disinfectant, 2-10% of foaming agent, 1-5% of foam stabilizer, 5-10% of ethylene glycol butyl ether, 407-3% of poloxamer, 6-5% of polyethylene glycol, 10-15% of glycerin, 0.2-2% of flavoring agent, 0.1-0.3% of pH regulator and the balance of water; the foaming agent is a mixture of alpha-olefin sodium sulfonate and glyceroglycosides; the foam stabilizer is lauryl dimethyl ammonium oxide; the quaternary ammonium salt disinfectant is a mixture of benzalkonium chloride and decamethenamine bromide.
2. A foam disinfectant for farms according to claim 1, wherein the fragrance is a floral type essence.
3. A foam disinfectant for farms according to claim 1, wherein the pH adjuster is phosphoric acid.
4. A method for preparing a foam disinfectant for farms according to any one of claims 1 to 3, comprising the steps of:
Step 1: weighing the components according to the mass percent of claim 1, taking 30-40% of the total mass of the purified water, adding the components into a material melting kettle, adding quaternary ammonium salt disinfectant and glutaraldehyde disinfectant into the material melting kettle respectively, and uniformly stirring;
Step 2: respectively adding foaming agent, ethylene glycol butyl ether, poloxamer 407, polyethylene glycol-6, glycerol, flavoring agent and the rest purified water, and stirring uniformly;
step 3: adding a pH regulator, regulating the pH value to be 2.0-4.0, and uniformly stirring to obtain the foam disinfectant for visual disinfection.
CN202211501534.3A 2022-11-28 2022-11-28 Foam disinfectant for farms and preparation method thereof Active CN115804375B (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20200041494A (en) * 2018-10-12 2020-04-22 농업회사법인 주식회사 과농 Sterilization and cleansing agent of antifreezing for cattle shed
CN112913847A (en) * 2021-01-18 2021-06-08 海韵一剑大卫生科技有限公司 Chlorine-containing disinfectant for low-temperature environment and preparation method thereof
CN114246180A (en) * 2020-09-24 2022-03-29 湖南五指峰生化有限公司 Foam cleaning disinfectant and preparation method thereof
CN114916544A (en) * 2022-05-10 2022-08-19 中国农业科学院饲料研究所 Compound foam type long-acting disinfectant containing citric acid and preparation method and application thereof
CN115052578A (en) * 2021-10-13 2022-09-13 振德医疗用品股份有限公司 Moisturizing and non-irritating foam type hand-washing-free antibacterial liquid and preparation method thereof

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9357771B2 (en) * 2012-12-17 2016-06-07 Kimberly-Clark Worldwide, Inc. Foaming sanitizing formulations and products including a quaternary ammonium compound

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20200041494A (en) * 2018-10-12 2020-04-22 농업회사법인 주식회사 과농 Sterilization and cleansing agent of antifreezing for cattle shed
CN114246180A (en) * 2020-09-24 2022-03-29 湖南五指峰生化有限公司 Foam cleaning disinfectant and preparation method thereof
CN112913847A (en) * 2021-01-18 2021-06-08 海韵一剑大卫生科技有限公司 Chlorine-containing disinfectant for low-temperature environment and preparation method thereof
CN115052578A (en) * 2021-10-13 2022-09-13 振德医疗用品股份有限公司 Moisturizing and non-irritating foam type hand-washing-free antibacterial liquid and preparation method thereof
CN114916544A (en) * 2022-05-10 2022-08-19 中国农业科学院饲料研究所 Compound foam type long-acting disinfectant containing citric acid and preparation method and application thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
泡沫型清洁消毒剂在畜禽养殖业上的应用;卓曲;李英;张军;武力;陈宝妮;;养猪(第06期);全文 *

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