CN115786044A - Shaddock peel essence handmade soap and preparation method thereof - Google Patents
Shaddock peel essence handmade soap and preparation method thereof Download PDFInfo
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- CN115786044A CN115786044A CN202211542260.2A CN202211542260A CN115786044A CN 115786044 A CN115786044 A CN 115786044A CN 202211542260 A CN202211542260 A CN 202211542260A CN 115786044 A CN115786044 A CN 115786044A
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- handmade soap
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- shaddock
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- 239000000344 soap Substances 0.000 title claims abstract description 38
- 244000276331 Citrus maxima Species 0.000 title claims abstract description 32
- 235000001759 Citrus maxima Nutrition 0.000 title claims abstract description 26
- 238000002360 preparation method Methods 0.000 title description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 36
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000012153 distilled water Substances 0.000 claims abstract description 10
- 235000005979 Citrus limon Nutrition 0.000 claims abstract description 9
- 244000131522 Citrus pyriformis Species 0.000 claims abstract description 9
- 235000019482 Palm oil Nutrition 0.000 claims abstract description 9
- 239000002540 palm oil Substances 0.000 claims abstract description 9
- 239000000341 volatile oil Substances 0.000 claims abstract description 9
- 239000004359 castor oil Substances 0.000 claims abstract description 8
- 235000019438 castor oil Nutrition 0.000 claims abstract description 8
- 239000003240 coconut oil Substances 0.000 claims abstract description 8
- 235000019864 coconut oil Nutrition 0.000 claims abstract description 8
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims abstract description 8
- 239000004006 olive oil Substances 0.000 claims abstract description 8
- 235000008390 olive oil Nutrition 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 238000007127 saponification reaction Methods 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 5
- 238000005520 cutting process Methods 0.000 claims description 3
- 238000002844 melting Methods 0.000 claims description 3
- 230000008018 melting Effects 0.000 claims description 3
- 238000009835 boiling Methods 0.000 claims description 2
- 238000001914 filtration Methods 0.000 claims description 2
- 238000000034 method Methods 0.000 claims 2
- 230000000694 effects Effects 0.000 abstract description 10
- 238000004140 cleaning Methods 0.000 abstract description 9
- 230000007613 environmental effect Effects 0.000 abstract description 5
- 230000003020 moisturizing effect Effects 0.000 abstract description 5
- 230000006378 damage Effects 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 239000002585 base Substances 0.000 description 4
- 238000005187 foaming Methods 0.000 description 4
- 239000000047 product Substances 0.000 description 3
- 235000015112 vegetable and seed oil Nutrition 0.000 description 3
- 239000008158 vegetable oil Substances 0.000 description 3
- 241000193830 Bacillus <bacterium> Species 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 230000007794 irritation Effects 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- ZEMPKEQAKRGZGQ-AAKVHIHISA-N 2,3-bis[[(z)-12-hydroxyoctadec-9-enoyl]oxy]propyl (z)-12-hydroxyoctadec-9-enoate Chemical compound CCCCCCC(O)C\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CC(O)CCCCCC)COC(=O)CCCCCCC\C=C/CC(O)CCCCCC ZEMPKEQAKRGZGQ-AAKVHIHISA-N 0.000 description 1
- 239000001606 7-[(2S,3R,4S,5S,6R)-4,5-dihydroxy-6-(hydroxymethyl)-3-[(2S,3R,4R,5R,6S)-3,4,5-trihydroxy-6-methyloxan-2-yl]oxyoxan-2-yl]oxy-5-hydroxy-2-(4-hydroxyphenyl)chroman-4-one Substances 0.000 description 1
- 241000588724 Escherichia coli Species 0.000 description 1
- 241000191967 Staphylococcus aureus Species 0.000 description 1
- 208000037386 Typhoid Diseases 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative effect Effects 0.000 description 1
- 208000001848 dysentery Diseases 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000686 essence Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000002480 mineral oil Substances 0.000 description 1
- 235000010446 mineral oil Nutrition 0.000 description 1
- 239000004570 mortar (masonry) Substances 0.000 description 1
- DFPMSGMNTNDNHN-ZPHOTFPESA-N naringin Chemical compound O[C@@H]1[C@H](O)[C@@H](O)[C@H](C)O[C@H]1O[C@H]1[C@H](OC=2C=C3O[C@@H](CC(=O)C3=C(O)C=2)C=2C=CC(O)=CC=2)O[C@H](CO)[C@@H](O)[C@@H]1O DFPMSGMNTNDNHN-ZPHOTFPESA-N 0.000 description 1
- 229940052490 naringin Drugs 0.000 description 1
- 229930019673 naringin Natural products 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 238000000967 suction filtration Methods 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 239000008399 tap water Substances 0.000 description 1
- 235000020679 tap water Nutrition 0.000 description 1
- 201000008297 typhoid fever Diseases 0.000 description 1
Images
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention discloses a shaddock ped essence handmade soap which is prepared from the following raw materials in parts by mass: 4-6 parts of shaddock peel, 70-75 parts of white palm oil, 20-25 parts of coconut oil, 15-20 parts of olive oil, 5-8 parts of castor oil, 15-17 parts of sodium hydroxide, 1-3 parts of lemon essential oil and 170-180 parts of distilled water. The shaddock ped essence handmade soap provided by the invention has strong moistening, moisturizing and cleaning effects. Simple manufacture, low cost and no damage to human skin. Meets the requirements of environmental protection and does not cause pollution to the environment.
Description
Technical Field
The invention relates to a cleaning product, in particular to a shaddock peel essence handmade soap and a preparation method thereof.
Background
With the continuous development of the times, people pay more and more attention to the quality of life, and the fancy soap from the prior fancy soap to the current handmade soap is more and more popular. The handmade soap has the performances of natural safety, moistening, moisturizing, environmental protection and the like. The shaddock peel has the effects of beautifying, refreshing air, nourishing stomach, moistening throat and the like, and the shaddock peel also contains naringin which has the effect of inhibiting staphylococcus aureus, escherichia coli, dysentery bacillus, typhoid bacillus and the like.
In daily skin care products on the market, more and more chemical reagents such as synthetic essence and pigment, preservatives, mineral oil and the like are used. The long-term use may damage our skin, so the handmade soap 3
The handmade soap is a good choice of skin care products, is purely natural and purely manual, does not contain any chemical reagent, has no burden on the skin, and has moisturizing effect.
Under the large background, the handmade soap industry is gradually developed, the production technology of handmade soap on the market is gradually mature, and the handmade soap is developed into a novel industry. With the continuous expansion of market demands, the handmade soap with high efficiency, environmental protection, low price, convenient implementation, good cleaning capability, good efficacy and high safety is urgently needed to be developed.
Disclosure of Invention
The pomelo peel essence handmade soap and the preparation method thereof provided by the invention have the advantages of simplicity in preparation, low cost, low irritation, high environmental friendliness, no harm to human skin, moistening, moisturizing, high-efficiency cleaning and the like.
In order to achieve the above object, the present invention provides the following technical solutions: the pomelo peel essence handmade soap is prepared from the following raw materials in parts by mass: 4-6 parts of shaddock peel, 70-75 parts of white palm oil, 20-25 parts of coconut oil, 15-20 parts of olive oil, 5-8 parts of castor oil, 15-17 parts of sodium hydroxide, 1-3 parts of lemon essential oil and 170-180 parts of distilled water.
Further, the invention is prepared from the following raw materials in parts by mass: 5 parts of shaddock peel, 72 parts of white palm oil, 24 parts of coconut oil, 18 parts of olive oil, 6 parts of castor oil, 16.1 parts of sodium hydroxide, 2 parts of lemon essential oil and 175.8 parts of distilled water.
The preparation method of the shaddock peel essence handmade soap comprises the following steps:
(1) Cutting pericarpium Citri Grandis into pieces, boiling with part of distilled water, decocting for 1.5-2 hr, and filtering to obtain pericarpium Citri Grandis extractive solution;
(2) Melting white palm oil, coconut oil, olive oil and castor oil, and adding sodium hydroxide solution for saponification to obtain soap base;
(3) Adding pericarpium Citri Grandis extract and lemon essential oil into soap base, stirring, pouring into mold, solidifying, and demolding.
The saponification is carried out at 45-50 ℃ in the step (2).
Advantageous effects
The shaddock ped essence handmade soap provided by the invention has strong moistening, moisturizing and cleaning effects. Simple manufacture, low cost and no damage to human skin. Meets the requirements of green environmental protection and does not cause pollution to the environment.
Drawings
FIG. 1 is a schematic representation of a stain prior to cleaning;
FIG. 2 is a schematic representation of a soil after cleaning;
1: washing with tap water 2: cleaning with a novel shaddock peel essence handmade soap 3: washing with market soap; visible cleaning ability: 2> < 3> < 1 >.
Detailed Description
The inventor adopts an orthogonal experimental method to optimize and determine formula combination, so that the raw materials are matched with each other, and a better synergistic effect is achieved. According to the invention, the shaddock peel essence handmade soap which is natural, safe, natural, environment-friendly and capable of moistening skin is prepared by utilizing shaddock peel and mainly taking shaddock peel extracting solution as a main additive. The handmade soap has the functions of strong dirt-removing power, weak irritation, moistening and skin-care, and the like. Thereby meeting the requirements of people on handmade soap and forming environment-friendly recycling.
The experimental conditions were as follows:
table 1 explores the effect of saponification temperature on bubble force and pH of handmade soap
From the above table data: the second set of temperatures (47 ℃) works better for the pH and the foaming capacity of the hand soap.
Table 2 explores the effect of alkaline water on handmade soap bubble force and pH
From the above data it follows: the optimum condition is that the water/alkali requirement multiple is 2.6 times.
Table 3 explores the effect of the addition of the shaddock peel extract on foaming power and pH
TABLE 4 orthogonal experimental factors and horizontal design
TABLE 5 orthogonal experimental results and analysis
The range analysis showed that factor a had a significant effect on PH and factor C had a significant effect on foaming. The most preferred combination is A2B2C3, i.e. saponification temperature is 50 ℃, alkali water ratio is 1:2.6, when the addition amount of the shaddock peel extracting solution is 1.5mL, the prepared handmade soap has the highest foaming power and the lowest pH value.
Decontamination capability: the results are shown in FIGS. 1-2.
Example one
Raw materials: 5.0 parts of shaddock peel, 175.8 parts of distilled water, 72.0 parts of white palm oil, 24.0 parts of coconut oil, 18.0 parts of olive oil, 6.0 parts of castor oil, 16.1 parts of sodium hydroxide and 2.0 parts of lemon essential oil.
(1) The pericarpium Citri Grandis is yellow peel of fresh Shatian pomelo. Gently kneading the shaddock peel with edible salt, removing the wax layer on the surface, and cutting into fine pieces. Putting into a beaker, adding 150.0 parts of distilled water, decocting for 1.5h, taking out the shaddock peel, grinding with a mortar, putting back into the shaddock peel solution, decocting for 10min, and performing suction filtration with a Buchner funnel to obtain a yellow shaddock peel extracting solution for later use.
(2) Mixing white palm oil, oleum Cocois, oleum Olivarum, and oleum ricini, and melting to obtain mixed natural vegetable oil; the sodium hydroxide was dissolved in 25.8 parts of distilled water to obtain a sodium hydroxide solution. Mixing natural vegetable oil and sodium hydroxide solution at 45-50 deg.C, adding sodium hydroxide solution into the melted natural vegetable oil, stirring while adding, and stirring to moderate consistency to obtain soap base.
(3) Adding pericarpium Citri Grandis extract and lemon essential oil into soap base, stirring, pouring into mold, standing for 1-2 days, demolding, and placing in shade and dry place for 5-6 weeks to obtain the final product.
Claims (4)
1. The shaddock ped essence handmade soap is characterized by being prepared from the following raw materials in parts by mass: 4-6 parts of shaddock peel, 70-75 parts of white palm oil, 20-25 parts of coconut oil, 15-20 parts of olive oil, 5-8 parts of castor oil, 15-17 parts of sodium hydroxide, 1-3 parts of lemon essential oil and 170-180 parts of distilled water.
2. The pomelo peel essence handmade soap according to claim 1 is characterized by being prepared from the following raw materials in parts by mass: 5 parts of shaddock peel, 72 parts of white palm oil, 24 parts of coconut oil, 18 parts of olive oil, 6 parts of castor oil, 16.1 parts of sodium hydroxide, 2 parts of lemon essential oil and 175.8 parts of distilled water.
3. The method for preparing the pomelo peel essence handmade soap of claim 1 or 2, which is characterized by comprising the steps of:
(1) Cutting pericarpium Citri Grandis into pieces, boiling with part of distilled water, decocting for 1.5-2 hr, and filtering to obtain pericarpium Citri Grandis extractive solution;
(2) Melting white palm oil, coconut oil, olive oil and castor oil, and adding sodium hydroxide solution for saponification to obtain soap base;
(3) Adding pericarpium Citri Grandis extract and lemon essential oil into soap base, stirring, pouring into mold, solidifying, and demolding.
4. The method for preparing the pomelo peel essence handmade soap according to claim 3, wherein the saponification in the step (2) is performed at 45-50 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211542260.2A CN115786044A (en) | 2022-12-02 | 2022-12-02 | Shaddock peel essence handmade soap and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211542260.2A CN115786044A (en) | 2022-12-02 | 2022-12-02 | Shaddock peel essence handmade soap and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN115786044A true CN115786044A (en) | 2023-03-14 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202211542260.2A Pending CN115786044A (en) | 2022-12-02 | 2022-12-02 | Shaddock peel essence handmade soap and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN115786044A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104629950A (en) * | 2015-02-13 | 2015-05-20 | 陕西理工学院 | Moisturizing and whitening handmade soap and production method thereof |
| KR20160112865A (en) * | 2015-03-20 | 2016-09-28 | 전금옥 | Weak acidic soap powder composition, method for manufacturing weak acidic soap using the composition, and weak acidic soap manufacured by the method |
| CN108102824A (en) * | 2017-12-18 | 2018-06-01 | 郭舒洋 | A kind of preparation method of Multifunctional fancy soap |
| CN109294771A (en) * | 2018-11-30 | 2019-02-01 | 薛冰寒 | Handmade soap and handmade soap prepare mold |
-
2022
- 2022-12-02 CN CN202211542260.2A patent/CN115786044A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104629950A (en) * | 2015-02-13 | 2015-05-20 | 陕西理工学院 | Moisturizing and whitening handmade soap and production method thereof |
| KR20160112865A (en) * | 2015-03-20 | 2016-09-28 | 전금옥 | Weak acidic soap powder composition, method for manufacturing weak acidic soap using the composition, and weak acidic soap manufacured by the method |
| CN108102824A (en) * | 2017-12-18 | 2018-06-01 | 郭舒洋 | A kind of preparation method of Multifunctional fancy soap |
| CN109294771A (en) * | 2018-11-30 | 2019-02-01 | 薛冰寒 | Handmade soap and handmade soap prepare mold |
Non-Patent Citations (1)
| Title |
|---|
| 糖亚: "百万网友最常问 手工皂不败秘技", 河南科学技术出版社, pages: 21 * |
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