CN115725204A - Nano printing and dyeing ink and processing device thereof - Google Patents
Nano printing and dyeing ink and processing device thereof Download PDFInfo
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- CN115725204A CN115725204A CN202211507142.8A CN202211507142A CN115725204A CN 115725204 A CN115725204 A CN 115725204A CN 202211507142 A CN202211507142 A CN 202211507142A CN 115725204 A CN115725204 A CN 115725204A
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- 238000007639 printing Methods 0.000 title claims abstract description 68
- 238000004043 dyeing Methods 0.000 title claims abstract description 58
- 239000012860 organic pigment Substances 0.000 claims abstract description 28
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 26
- 239000007788 liquid Substances 0.000 claims abstract description 24
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 19
- 229910021389 graphene Inorganic materials 0.000 claims abstract description 19
- 239000002994 raw material Substances 0.000 claims abstract description 19
- 229910000019 calcium carbonate Inorganic materials 0.000 claims abstract description 13
- 239000008367 deionised water Substances 0.000 claims abstract description 13
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 238000002360 preparation method Methods 0.000 claims abstract description 11
- 239000000654 additive Substances 0.000 claims abstract description 10
- 230000000996 additive effect Effects 0.000 claims abstract description 9
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000004831 Hot glue Substances 0.000 claims abstract description 7
- 238000004519 manufacturing process Methods 0.000 claims abstract description 4
- 239000011230 binding agent Substances 0.000 claims abstract description 3
- 238000003756 stirring Methods 0.000 claims description 71
- 239000000049 pigment Substances 0.000 claims description 46
- 238000009434 installation Methods 0.000 claims description 27
- 238000000227 grinding Methods 0.000 claims description 24
- 239000000203 mixture Substances 0.000 claims description 23
- 238000001914 filtration Methods 0.000 claims description 15
- 239000000463 material Substances 0.000 claims description 14
- 239000000945 filler Substances 0.000 claims description 10
- 238000011049 filling Methods 0.000 claims description 9
- 238000010438 heat treatment Methods 0.000 claims description 9
- 239000006185 dispersion Substances 0.000 claims description 6
- 238000010008 shearing Methods 0.000 claims description 6
- 238000007873 sieving Methods 0.000 claims description 6
- 238000007790 scraping Methods 0.000 claims description 5
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 5
- 239000008158 vegetable oil Substances 0.000 claims description 5
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- 235000019498 Walnut oil Nutrition 0.000 claims description 3
- 239000002518 antifoaming agent Substances 0.000 claims description 3
- 238000009924 canning Methods 0.000 claims description 3
- 238000001514 detection method Methods 0.000 claims description 3
- 239000002270 dispersing agent Substances 0.000 claims description 3
- 239000007970 homogeneous dispersion Substances 0.000 claims description 3
- 235000021388 linseed oil Nutrition 0.000 claims description 3
- 239000000944 linseed oil Substances 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- IEQIEDJGQAUEQZ-UHFFFAOYSA-N phthalocyanine Chemical compound N1C(N=C2C3=CC=CC=C3C(N=C3C4=CC=CC=C4C(=N4)N3)=N2)=C(C=CC=C2)C2=C1N=C1C2=CC=CC=C2C4=N1 IEQIEDJGQAUEQZ-UHFFFAOYSA-N 0.000 claims description 3
- 125000003367 polycyclic group Chemical group 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- 238000005070 sampling Methods 0.000 claims description 3
- 239000003381 stabilizer Substances 0.000 claims description 3
- 239000011550 stock solution Substances 0.000 claims description 3
- 239000008170 walnut oil Substances 0.000 claims description 3
- 238000000498 ball milling Methods 0.000 claims description 2
- 239000002245 particle Substances 0.000 abstract description 5
- 240000007594 Oryza sativa Species 0.000 abstract description 2
- 235000007164 Oryza sativa Nutrition 0.000 abstract description 2
- 235000009566 rice Nutrition 0.000 abstract description 2
- 239000000976 ink Substances 0.000 description 47
- 230000000694 effects Effects 0.000 description 9
- 101100298225 Caenorhabditis elegans pot-2 gene Proteins 0.000 description 5
- 239000000975 dye Substances 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 238000005054 agglomeration Methods 0.000 description 3
- 230000002776 aggregation Effects 0.000 description 3
- 239000001023 inorganic pigment Substances 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 230000004075 alteration Effects 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000005984 hydrogenation reaction Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000010865 sewage Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
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- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a nano printing and dyeing ink and a processing device thereof, and relates to the technical field of nano printing and dyeing ink production. The nano printing and dyeing ink comprises the following formula raw materials in parts by weight: 50-80 parts of organic pigment, 20-30 parts of binder, 10-20 parts of nano calcium carbonate, 5-8 parts of viscosity regulator, 10-20 parts of additive, 100-150 parts of deionized water, 3-5 parts of hot melt adhesive, 2-3 parts of gold powder and 20-30 parts of graphene. According to the invention, through the matched use of the feeding hopper, the shell, the filter box, the mounting seat and the collecting box, the organic pigment liquid can be filtered, the fineness of the organic pigment liquid is increased, the raw materials and the processed nano printing and dyeing ink are screened in the preparation aspect, the probability of raw material caking or larger particles is reduced, and the quality of the rice printing and dyeing ink is further improved.
Description
Technical Field
The invention relates to the technical field of nano printing and dyeing ink production, in particular to nano printing and dyeing ink and a processing device thereof.
Background
Many properties of nano-inks are related to pigments, for example, relative density, transparency, light resistance, and resistance to chemicals of the inks are related to pigments. Natural pigments are less colorful, while dyes are colorful, and the dyes are usually modified to have the pigment properties and used in inks.
A nanometer printing and dyeing ink with the publication number of CN105585900A and a use method thereof belong to the field of preparation of printing and dyeing ink, and particularly relate to the nanometer printing and dyeing ink and the use method thereof. The raw materials are calculated according to the mass fraction: 15% of organic dye, 62.7% of deionized water, 18% of polar monomer, 0.8% of polymer synthesis auxiliary agent, 2% of fatty acid hydrogenation catalyst and 2% of formaldehyde-free color fixing agent. The nano printing and dyeing ink can replace the traditional dye ink, greatly reduce the traditional printing and dyeing cost and the process flow, save energy, reduce consumption, have zero sewage discharge, is ecological and environment-friendly, and is favorable for sustainable development
According to the nano printing and dyeing ink and the processing device thereof, the raw materials and the processed nano printing and dyeing ink are not sieved, so that the condition of raw material agglomeration or large particles is easy to occur, and the quality of the prepared nano printing and dyeing ink is further influenced.
Disclosure of Invention
The invention aims to provide a nano printing and dyeing ink and a processing device thereof, which are used for solving the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme: the nano printing and dyeing ink comprises the following formula raw materials in parts by weight: 50-80 parts of organic pigment, 20-30 parts of connecting material, 10-20 parts of nano calcium carbonate, 5-8 parts of viscosity regulator, 10-20 parts of additive, 100-150 parts of deionized water, 3-5 parts of hot melt adhesive, 2-3 parts of gold powder and 20-30 parts of graphene; the preparation method of the nano printing and dyeing ink comprises the following steps:
s1, pigment preparation: putting the organic pigment in a corresponding part into a wall breaking machine for crushing, then pouring the organic pigment into a grinding machine for grinding, wherein the rotating speed of a grinding roller in the grinding machine is controlled to be 560-580r/min, then pouring the ground pigment and the deionized water in a corresponding part into a pot, then stirring by using a stirrer, the rotating speed of a stirring paddle of the stirrer is 360-500r/min, the stirring time is 15-18min, then collecting the obtained mixed pigment liquid, putting the mixed pigment liquid into a filter for filtering, and then collecting the stock solution to prepare the pigment liquid;
s2, processing of the filler: pouring the nano calcium carbonate with the corresponding parts into a grinder for grinding treatment, wherein the rotating speed of a grinding roller in the grinder is controlled to be 560-580r/min, then pouring the ground nano calcium carbonate into a sieving device for sieving for 1-3 times, then pouring the sieved nano calcium carbonate and the corresponding parts of connecting materials into a pot, then stirring by using a stirrer, the rotating speed of the stirrer is 360-500r/min, the stirring time is 5-9min, and then pouring into a container to obtain the filler required by the nano printing and dyeing ink;
s3, processing graphene: pouring the corresponding parts of graphene into a wall breaking machine for breaking for 10-20S, then pouring the wall-broken graphene powder into a high-speed homogenizing dispersion machine, stirring at a rotating speed of 400r/min for 11-15min, adjusting the rotating speed to 1000r/min, and shearing, dispersing and grinding at a high speed for 20-30min to obtain a graphene base material;
s4, stirring and mixing: pouring the prepared pigment liquid, the filler and the graphene-based material into a heating pot body, controlling the heating pot body to be heated to 30-50 ℃, stirring the mixture by a stirrer for 5-10 minutes, then pouring the viscosity regulator, the additive, the hot melt adhesive, the deionized water and the gold powder in corresponding parts into the heating pot body, continuously increasing the temperature to 70-80 ℃, stirring the mixture by the stirrer for 10-15 minutes, pouring the mixture into a high-speed homogeneous dispersion machine after the mixture is finished, stirring the mixture for 11-15 minutes at a rotating speed of 400r/min, adjusting the rotating speed to 1000r/min, carrying out high-speed shearing dispersion grinding for 20-30 minutes, then pouring the mixture into a ball mill for ball milling for 2-3 hours, wherein the rotating speed of the ball mill is 370-520 r/min, collecting the obtained mixed ink, and putting the mixed ink into a filter for filtering to obtain the nano printing and dyeing ink;
s5, inspecting and canning: and (4) sampling and detecting the sterilized nano printing and dyeing ink in the step (S4), adding the nano printing and dyeing ink into a specified filling machine after detection, and quantitatively filling the nano printing and dyeing ink by using the filling machine.
Preferably, the organic pigment is any one of azo pigments, phthalocyanine pigments, triarylmethane pigments, special pigments and polycyclic pigments.
Preferably, the binder is dry vegetable oil, and the dry vegetable oil is any one of linseed oil and walnut oil.
Preferably, the additives comprise the following raw materials in parts by weight: 3-5 parts of modified defoaming agent, 2-5 parts of dispersing agent, 3-5 parts of formaldehyde-free color fixing agent and 2-5 parts of PH stabilizing agent.
A production device of nano printing and dyeing ink comprises:
the pot comprises a support, wherein the top of the support is fixedly connected with two groups of transverse plates, a pot is arranged above the support, the two groups of transverse plates are fixedly arranged on the outer wall of the pot and symmetrically arranged, a circular sliding rail is arranged at the top of the pot, a circular cover plate is arranged at the top of the pot, pulleys are fixedly connected to the bottom of the circular cover plate, and the pulleys are slidably arranged in the circular sliding rail;
the lifting assembly is arranged on the transverse plate and comprises an L-shaped top plate, and the L-shaped top plate is positioned above the circular cover plate;
the stirring assembly is arranged on the pot and the L-shaped top plate and comprises a motor, a rotating square rod, an installation column, a circular cover plate, a stirring column, an installation block, an inclined rod, a scraping plate, a screw rod and a blade, the rotating square rod and the installation column are driven to rotate by starting the motor, and the installation column drives the installation block, the inclined rod, the scraping plate, the screw rod and the blade to rotate and stir and mix the pigment;
the blanking assembly is arranged on the pot and comprises a frame body, an opening is formed in the bottom of the pot, and the frame body is located in the opening;
and the filtering component is arranged on the bracket and used for filtering the mixed pigment.
Preferably, the lifting assembly further comprises a hydraulic rod A, a sliding sleeve and a sliding column, the hydraulic rod A is fixedly installed at the top of one of the group of transverse plates, the free end of the hydraulic rod A is fixedly connected with the bottom of the L-shaped top plate, the sliding sleeve is fixedly connected to one side of the L-shaped top plate, the sliding column is fixedly installed at the top of the other group of transverse plates, a circular opening is formed in the sliding sleeve, the sliding sleeve is slidably installed on the sliding column, a limiting disc is fixedly connected to the outer wall of the sliding column, and the limiting disc is in contact with the bottom of the sliding sleeve.
Preferably, the motor is fixedly installed at the top of the L-shaped top plate, the rotating square rod is rotatably installed at the bottom of the L-shaped top plate, the output shaft of the motor is fixedly connected with the rotating square rod, the top of the circular cover plate is rotatably installed with the installation column, the top of the installation column is provided with the square clamping groove, the rotating square rod can be clamped and installed in the square clamping groove, the bottom of the circular cover plate is rotatably installed with the stirring column, one end of the stirring column is fixedly connected with one end of the installation column, the outer wall of the stirring column is fixedly sleeved with two sets of installation blocks, the bottom of the circular cover plate is rotatably installed with two sets of lead screws, one end of each lead screw extends to the top of the circular cover plate and is sleeved with a rotating button, the two sets of lead screws are uniformly and threadedly connected with moving blocks, the inclined rods are respectively and hinged to the front sides of the installation blocks on the stirring column and the moving blocks on the lead screws, the number of the inclined rods is also two sets, one end of one set of inclined rods is fixedly connected with a scraper, and the stirring column is far away from the circular cover plate and is provided with a blade.
Preferably, the unloading subassembly is still including swash plate, hydraulic stem B and telescopic link, and the setting around the two sets of baffles of top fixedly connected with of framework just are, and the inboard bottom fixedly connected with swash plate of framework, swash plate are the slope setting, and hydraulic stem B fixed mounting are on the support, and the free end of hydraulic stem B and the bottom fixed connection of framework, telescopic link fixed mounting are on the support, the one end of telescopic link and the bottom fixed connection of framework.
Preferably, filtering component is including the casing, the filter cartridge, mount pad and collection box, casing fixed mounting is in one side of support, hopper under fixedly connected with on the support, open-ended A has been seted up on the casing, the one end of hopper is passed open-ended A and is communicated with each other with the casing is inside down, circular internal thread mouth has been seted up at the top of casing, the outer wall of mount pad is provided with the external screw thread, mount pad threaded mounting is in circular internal thread mouth, the bottom fixedly connected with filter cartridge of mount pad, open-ended B has been seted up to the opposite side of filter cartridge, open-ended B is greater than open-ended A, the front side of casing has been seted up the rectangle opening, the inboard bottom of casing has been seted up the spout and has been collected the box through spout slidable mounting, the front side fixedly connected with handle of collecting the box, the articulated feeding apron of installing of outer wall of pot.
Compared with the prior art, the invention has the beneficial effects that:
(1) The nano printing and dyeing ink and the processing device thereof have the advantages that the organic pigment is added in the aspect of raw materials, compared with the inorganic pigment, the organic pigment also has much higher tinting strength than the inorganic pigment, the variety with high tinting strength and high transparency can be prepared, the requirements of high-grade paint and printing ink are met, and the nano printing and dyeing ink is more suitable for printing and dyeing clothes patterns.
(2) According to the nano printing and dyeing ink and the processing device thereof, the raw materials and the processed nano printing and dyeing ink are screened in the preparation aspect, the probability of raw material agglomeration or large particle is reduced, and the quality of the nano printing and dyeing ink is improved.
() This apparatus for producing of five dimension amino acid oral liquid, pass through the motor, the square pole rotates, the erection column, circular apron, the stirring post, the installation piece, the down tube, the scraper blade, the cooperation of lead screw and blade is used, can mix the stirring with deionized water to organic pigment, make organic pigment liquid, the follow-up of being convenient for mixes, the processing of filler also can be regarded as to this equipment, inclination through the adjustment down tube, make its stirring more even, and the inner wall of adjustable scraper blade and support is laminated mutually, play the effect of scraping the material.
() This nanometer printing and dyeing printing ink and processingequipment, through the swash plate, the cooperation of hydraulic stem B and telescopic link is used, can adjust the position of framework, when framework and support are laminated mutually, play confined effect, after the framework downstream, can flow one side of the organic pigment liquid through the framework of good preparation, play the effect of unloading, also be convenient for clear up the framework, through hopper down, a housing, the filter box, the mount pad is used with the cooperation of collecting the box, can carry out filtration treatment to organic pigment liquid, increase the fineness of this organic pigment liquid.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a front view of the present invention;
FIG. 3 is an enlarged view of portion A of the present invention;
FIG. 4 is an enlarged view of section B of the present invention;
FIG. 5 is an enlarged view of section C of the present invention;
fig. 6 is a top view of the mounting post of the present invention.
In the figure: 1. a support; 2. cooking; 3. a transverse plate; 4. a hydraulic rod A; 5. an L-shaped top plate; 6. a sliding sleeve; 7. a traveler; 8. a motor; 9. rotating the square rod; 10. mounting a column; 11. a circular cover plate; 12. stirring the column; 13. mounting blocks; 14. a diagonal bar; 15. a squeegee; 16. a screw rod; 17. a blade; 18. a frame body; 19. a sloping plate; 20. a hydraulic rod B; 21. a telescopic rod; 22. a feeding hopper; 23. a housing; 24. a filter box; 25. a mounting seat; 26. and (4) collecting the box.
Detailed Description
Referring to fig. 1-6, the present invention provides a technical solution: the utility model provides a apparatus for producing of nanometer printing and dyeing printing ink, includes support 1, lifting unit, stirring subassembly, unloading subassembly and filtering component: the top of the support 1 is fixedly connected with two groups of transverse plates 3, a pan 2 is arranged above the support 1, the two groups of transverse plates 3 are fixedly mounted on the outer wall of the pan 2 and symmetrically arranged, a circular slide rail is arranged at the top of the pan 2, a circular cover plate 11 is arranged at the top of the pan 2, a pulley is fixedly connected to the bottom of the circular cover plate 11, and the pulley is slidably mounted in the circular slide rail; the lifting assembly is arranged on the transverse plate 3 and comprises an L-shaped top plate 5, and the L-shaped top plate 5 is positioned above the circular cover plate 11; the stirring assembly is arranged on the pot 2 and the L-shaped top plate 5 and comprises a motor 8, a rotating square rod 9, an installation column 10, a circular cover plate 11, a stirring column 12, an installation block 13, an inclined rod 14, a scraper 15, a screw rod 16 and a blade 17, the rotating square rod 9 and the installation column 10 are driven to rotate by starting the motor 8, and the installation column 10 drives the installation block 13, the inclined rod 14, the scraper 15, the screw rod 16 and the blade 17 to rotate and stir and mix the pigment;
the blanking assembly is arranged on the pot 2 and comprises a frame body 18, an opening is formed in the bottom of the pot 2, and the frame body 18 is located in the opening; the filter assembly is arranged on the bracket 1 and used for filtering the mixed pigment.
Lifting unit is still including hydraulic stem A4, sliding sleeve 6 and traveller 7, hydraulic stem A4 fixed mounting is in the top of one of them a set of diaphragm 3, hydraulic stem A4's free end and the bottom fixed connection of L shape roof 5, one side fixedly connected with sliding sleeve 6 of L shape roof 5, traveller 7 fixed mounting is in the top of another set of diaphragm 3, set up circular opening on the sliding sleeve 6, sliding sleeve 6 and traveller 7 slidable mounting, the outer wall fixedly connected with spacing dish of traveller 7, spacing dish contacts with the bottom of sliding sleeve 6.
Motor 8 fixed mounting is in the top of L shape roof 5, it installs in the bottom of L shape roof 5 to rotate square bar 9, motor 8's output shaft and rotation square bar 9 fixed connection, the top of circular apron 11 is rotated and is installed erection column 10, square draw-in groove has been seted up at the top of erection column 10, but rotate square bar 9 joint and install in square draw-in groove, the bottom of circular apron 11 is rotated and is installed stirring post 12, the one end of stirring post 12 and the one end fixed connection of erection column 10, the outer wall fixed cover of stirring post 12 is equipped with two sets of installation piece 13, the bottom of circular apron 11 is rotated and is installed two sets of lead screw 16, the one end of lead screw 16 extends to the top of circular apron 11 and the cover is equipped with the turn button, equal threaded connection has the movable block on two sets of lead screw 16, be located the front side of installation piece 13 on stirring post 12 and be located the movable block on lead screw 16 the articulated down tube 14 of installing the down tube, the quantity of down tube 14 is also two sets of down tube, wherein the one end fixed connection has scraper blade 15 of a set of down tube 14, the one end fixed connection of stirring post 12 is equipped with fixed cover plate 17 blade, it can carry out the mixed effect of the mixed pigment through the adjustable scraper blade of stirring post 12 and the follow-up stirring blade of stirring post, it and the mixed scraper blade of stirring post, it is convenient for the mixed pigment through stirring blade and the mixed scraper blade of stirring rod, the mixed scraper blade of stirring post, it, the mixed blade of stirring post, it is carried out the mixed blade of stirring post, the mixed blade of stirring rod 14, it and the mixed blade of stirring post, it is carried out the mixed blade of stirring post, it is more.
The blanking assembly further comprises an inclined plate 19, a hydraulic rod B20 and an expansion rod 21, two groups of baffles are fixedly connected to the top of the frame 18 and are arranged in the front and back directions, the inclined plate 19 is fixedly connected to the bottom of the inner side of the frame 18, the inclined plate 19 is arranged in an inclined manner, the hydraulic rod B20 is fixedly installed on the support 1, the free end of the hydraulic rod B20 is fixedly connected to the bottom of the frame 18, the expansion rod 21 is fixedly installed on the support 1, one end of the expansion rod 21 is fixedly connected to the bottom of the frame 18, the hydraulic rod B20 and the expansion rod 21 are matched for use, the position of the frame 18 can be adjusted, when the frame 18 is attached to the support 1, a closed effect is achieved, after the frame 18 moves downwards, manufactured organic pigment liquid can flow out through one side of the frame 18, a blanking effect is achieved, and the frame 18 is convenient to clean.
The filter assembly comprises a shell 23, a filter box 24, a mounting seat 25 and a collecting box 26, the shell 23 is fixedly installed on one side of a support 1, a hopper 22 is fixedly connected to the support 1, an opening A is formed in the shell 23, one end of the hopper 22 penetrates through the opening A to be communicated with the inside of the shell 23, a circular internal threaded opening is formed in the top of the shell 23, external threads are arranged on the outer wall of the mounting seat 25, the mounting seat 25 is installed in the circular internal threaded opening in a threaded mode, the filter box 24 is fixedly connected to the bottom of the mounting seat 25, an opening B is formed in the other side of the filter box 24 and is larger than the opening A, a rectangular opening is formed in the front side of the shell 23, a sliding groove is formed in the bottom of the inner side of the shell 23, a collecting box 26 is installed in a sliding mode through the sliding groove, a handle is fixedly connected to the front side of the collecting box 26, a feeding cover plate is installed on the outer wall of a pot 2 in a hinged mode, the shell 23, the filter box 24 is matched with the mounting seat 25 and the collecting box 26, organic pigment liquid can be filtered, and the fineness of the organic pigment liquid is increased.
The nano printing and dyeing ink comprises the following formula raw materials in parts by weight: 50-80 parts of organic pigment, 20-30 parts of connecting material, 10-20 parts of nano calcium carbonate, 5-8 parts of viscosity regulator, 10-20 parts of additive, 100-150 parts of deionized water, 3-5 parts of hot melt adhesive, 2-3 parts of gold powder and 20-30 parts of graphene; the preparation method of the nano printing and dyeing ink comprises the following steps of S1, pigment preparation: putting a corresponding part of organic pigment into a wall breaking machine for crushing treatment, then pouring the organic pigment into a grinding machine for grinding treatment, wherein the rotating speed of a grinding roller in the grinding machine is controlled to be 560-580r/min, then pouring the ground pigment and a corresponding part of deionized water into a pot, then stirring by using a stirrer, the rotating speed of a stirring paddle of the stirrer is 360-500r/min, and the stirring time is 15-18min, then collecting the obtained mixed pigment liquid, putting the mixed pigment liquid into a filter for filtering, and then collecting the stock solution to prepare the pigment liquid, wherein the organic pigment is any one of azo pigment, phthalocyanine pigment, triarylmethane pigment, special pigment and polycyclic pigment;
s2, processing of the filler: pouring the nano calcium carbonate with the corresponding parts into a grinder for grinding treatment, wherein the rotating speed of a grinding roller in the grinder is controlled to be 560-580r/min, then pouring the ground nano calcium carbonate into a sieving device for sieving for 1-3 times, then pouring the sieved nano calcium carbonate and the corresponding parts of connecting materials into a pot, then stirring by using a stirrer with the rotating speed of 360-500r/min for 5-9min, and then pouring into a container to obtain the filler required by the nano printing and dyeing ink, wherein the connecting materials are dry vegetable oil which is any one of linseed oil and walnut oil;
s3, processing graphene: pouring the corresponding parts of graphene into a wall breaking machine for breaking for 10-20S, then pouring the wall-broken graphene powder into a high-speed homogenizing dispersion machine, stirring at a rotating speed of 400r/min for 11-15min, adjusting the rotating speed to 1000r/min, and shearing, dispersing and grinding at a high speed for 20-30min to obtain a graphene base material;
s4, stirring and mixing: pouring the prepared pigment liquid, the filler and the graphene-based material into a heating pot body, controlling the heating pot body to be heated to 30-50 ℃, stirring the mixture by a stirrer for 5-10 minutes, then pouring the viscosity regulator, the additive, the hot melt adhesive, the deionized water and the gold powder in corresponding parts into the heating pot body, continuously increasing the temperature to 70-80 ℃, stirring the mixture by the stirrer for 10-15 minutes, pouring the mixture into a high-speed homogeneous dispersion machine after the mixture is finished, stirring the mixture for 11-15 minutes at a rotating speed of 400r/min, adjusting the rotating speed to 1000r/min, carrying out high-speed shearing dispersion grinding for 20-30 minutes, then pouring the mixture into a ball mill for 2-3 hours, and collecting the obtained mixed ink, putting the mixed ink into a filter for filtering, thus obtaining the nano printing and dyeing ink, wherein the additive comprises the following raw materials in parts by weight: 3-5 parts of a modified defoaming agent, 2-5 parts of a dispersing agent, 3-5 parts of an aldehyde-free color fixing agent and 2-5 parts of a PH stabilizing agent; s5, inspecting and canning: and (4) sampling and detecting the sterilized nano printing and dyeing ink in the step (S4), adding the nano printing and dyeing ink into a specified filling machine after detection, and quantitatively filling the nano printing and dyeing ink by using the filling machine.
The working principle is as follows: pour organic pigment and deionized water into pot 2 through the feeding apron in, control motor 8's start-up, it rotates square pole 9 and erection column 10 to drive to rotate, erection column 10 drives installation piece 13, down tube 14, scraper 15, lead screw 16 and blade 17 rotate and stir the mixture to pigment, the accessible rotates knob drive lead screw 16 and rotates, drive installation piece 13 vertical motion on the lead screw 16, and then adjust the angle of down tube 14, after the stirring, control hydraulic stem B20 downstream, hydraulic stem B20 drives behind the framework 18 downstream, can flow out one side of the organic pigment liquid of making through framework 18, then flow into filter box 24 through hopper 22 down, can carry out filtration to organic pigment liquid, then flow into in collecting box 26.
It can be seen from this that: the nano printing and dyeing ink and the processing device thereof do not sieve raw materials and processed nano printing and dyeing ink, the raw materials are easy to agglomerate or have larger particles, and further the quality of the prepared nano printing and dyeing ink is influenced. The printing process has the advantages that a good printing effect is provided, the printing color is uniform, the textile patterns are clear, the gold powder is added, the effect of increasing decoration in the printing and dyeing effect can be achieved, the raw materials and the processed nano printing and dyeing ink are screened in the preparation aspect, the probability of raw material agglomeration or large particle size is reduced, and the quality of the rice printing and dyeing ink is improved.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (9)
1. A nanometer printing and dyeing ink is characterized in that: the formula comprises the following raw materials in parts by weight: 50-80 parts of organic pigment, 20-30 parts of connecting material, 10-20 parts of nano calcium carbonate, 5-8 parts of viscosity regulator, 10-20 parts of additive, 100-150 parts of deionized water, 3-5 parts of hot melt adhesive, 2-3 parts of gold powder and 20-30 parts of graphene; the preparation method of the nano printing and dyeing ink comprises the following steps:
s1, pigment preparation: putting the organic pigment in a corresponding part into a wall breaking machine for crushing, then pouring the organic pigment into a grinding machine for grinding, wherein the rotating speed of a grinding roller in the grinding machine is controlled to be 560-580r/min, then pouring the ground pigment and the deionized water in a corresponding part into a pot, then stirring by using a stirrer, the rotating speed of a stirring paddle of the stirrer is 360-500r/min, the stirring time is 15-18min, then collecting the obtained mixed pigment liquid, putting the mixed pigment liquid into a filter for filtering, and then collecting the stock solution to prepare the pigment liquid;
s2, processing of the filler: pouring the nano calcium carbonate with the corresponding parts into a grinder for grinding treatment, wherein the rotating speed of a grinding roller in the grinder is controlled to be 560-580r/min, then pouring the ground nano calcium carbonate into a sieving device for sieving for 1-3 times, then pouring the sieved nano calcium carbonate and the corresponding parts of connecting materials into a pot, then stirring by using a stirrer, the rotating speed of the stirrer is 360-500r/min, the stirring time is 5-9min, and then pouring into a container to obtain the filler required by the nano printing and dyeing ink;
s3, processing graphene: pouring the corresponding parts of graphene into a wall breaking machine for breaking for 10-20S, then pouring the wall-broken graphene powder into a high-speed homogenizing dispersion machine, stirring at a rotating speed of 400r/min for 11-15min, adjusting the rotating speed to 1000r/min, and shearing, dispersing and grinding at a high speed for 20-30min to obtain a graphene base material;
s4, stirring and mixing: pouring the prepared pigment liquid, the filler and the graphene-based material into a heating pot body, controlling the heating pot body to be heated to 30-50 ℃, stirring the mixture by a stirrer for 5-10 minutes, then pouring the viscosity regulator, the additive, the hot melt adhesive, the deionized water and the gold powder in corresponding parts into the heating pot body, continuously increasing the temperature to 70-80 ℃, stirring the mixture by the stirrer for 10-15 minutes, pouring the mixture into a high-speed homogeneous dispersion machine after the mixture is finished, stirring the mixture for 11-15 minutes at a rotating speed of 400r/min, adjusting the rotating speed to 1000r/min, carrying out high-speed shearing dispersion grinding for 20-30 minutes, then pouring the mixture into a ball mill for ball milling for 2-3 hours, wherein the rotating speed of the ball mill is 370-520 r/min, collecting the obtained mixed ink, and putting the mixed ink into a filter for filtering to obtain the nano printing and dyeing ink;
s5, inspecting and canning: and (4) sampling and detecting the sterilized nano printing and dyeing ink in the step (S4), adding the nano printing and dyeing ink into a specified filling machine after detection, and quantitatively filling the nano printing and dyeing ink by using the filling machine.
2. The nano printing and dyeing ink as claimed in claim 1, wherein: the organic pigment is any one of azo pigment, phthalocyanine pigment, triarylmethane pigment, special pigment and polycyclic pigment.
3. The nano printing and dyeing ink as claimed in claim 2, wherein: the binder is dry vegetable oil, and the dry vegetable oil is any one of linseed oil and walnut oil.
4. The nano printing and dyeing ink as claimed in claim 3, wherein: the additive comprises the following raw materials in parts by weight: 3-5 parts of modified defoaming agent, 2-5 parts of dispersing agent, 3-5 parts of formaldehyde-free color fixing agent and 2-5 parts of PH stabilizing agent.
5. A production device of nano printing and dyeing ink is characterized by comprising:
the pot comprises a support (1), wherein transverse plates (3) are fixedly connected to the top of the support (1), the number of the transverse plates (3) is two, a pot (2) is arranged above the support (1), the two groups of transverse plates (3) are fixedly arranged on the outer wall of the pot (2) and symmetrically arranged, a circular sliding rail is arranged at the top of the pot (2), a circular cover plate (11) is arranged at the top of the pot (2), pulleys are fixedly connected to the bottom of the circular cover plate (11), and the pulleys are slidably arranged in the circular sliding rail;
the lifting assembly is arranged on the transverse plate (3) and comprises an L-shaped top plate (5), and the L-shaped top plate (5) is positioned above the circular cover plate (11);
the stirring assembly is arranged on the pot (2) and the L-shaped top plate (5) and comprises a motor (8), a rotating square rod (9), an installation column (10), a circular cover plate (11), a stirring column (12), an installation block (13), an inclined rod (14), a scraping plate (15), a screw rod (16) and a blade (17), the rotating square rod (9) and the installation column (10) are driven to rotate by starting the motor (8), and the installation column (10) drives the installation block (13), the inclined rod (14), the scraping plate (15), the screw rod (16) and the blade (17) to rotate and stir and mix pigments;
the blanking assembly is arranged on the pot (2) and comprises a frame body (18), an opening is formed in the bottom of the pot (2), and the frame body (18) is located in the opening;
and the filtering component is arranged on the bracket (1) and is used for filtering the mixed pigment.
6. The apparatus for producing a nano printing ink according to claim 5, wherein: the lifting assembly is characterized by further comprising a hydraulic rod A (4), a sliding sleeve (6) and a sliding column (7), wherein the hydraulic rod A (4) is fixedly installed at the top of one group of transverse plates (3), the free end of the hydraulic rod A (4) is fixedly connected with the bottom of the L-shaped top plate (5), the sliding sleeve (6) is fixedly connected with one side of the L-shaped top plate (5), the sliding column (7) is fixedly installed at the top of the other group of transverse plates (3), a circular opening is formed in the sliding sleeve (6), the sliding sleeve (6) is slidably installed with the sliding column (7), a limiting disc is fixedly connected to the outer wall of the sliding column (7), and the limiting disc is in contact with the bottom of the sliding sleeve (6).
7. The apparatus for producing a nano printing ink according to claim 6, wherein: motor (8) fixed mounting is in the top of L shape roof (5), it installs in the bottom of L shape roof (5) to rotate square bar (9), the output shaft and the rotation square bar (9) fixed connection of motor (8), the top of circular apron (11) is rotated and is installed erection column (10), square clamping groove has been seted up at the top of erection column (10), but rotation square bar (9) joint is installed in square clamping groove, the bottom of circular apron (11) is rotated and is installed stirring post (12), the one end of stirring post (12) and the one end fixed connection of erection column (10), the outer wall fixed cover of stirring post (12) is equipped with two sets of installation piece (13), the bottom of circular apron (11) is rotated and is installed two sets of lead screw (16), the one end of lead screw (16) extends to the top of circular apron (11) and is equipped with the turn button, equal threaded connection has the movable block on two sets of lead screw (16), the front side of installation piece (13) that is located stirring post (12) and the front side of the movable block that is located on circular apron (16) all articulate and install down tube (14), the quantity of a set of fixed post (14) is equipped with the fixed set of fixed bolster (14) one end (17) wherein, fixed set of fixed post (12) is equipped with the fixed cover plate (11) and is equipped with the fixed set of scraper blade (17).
8. The apparatus for producing a nano printing ink according to claim 7, wherein: unloading subassembly is still including swash plate (19), hydraulic stem B (20) and telescopic link (21), the setting around the two sets of baffles of top fixedly connected with of framework (18) just are, inboard bottom fixedly connected with swash plate (19) of framework (18), swash plate (19) are the slope and set up, hydraulic stem B (20) fixed mounting is on support (1), the free end of hydraulic stem B (20) and the bottom fixed connection of framework (18), telescopic link (21) fixed mounting is on support (1), the one end of telescopic link (21) and the bottom fixed connection of framework (18).
9. The apparatus for producing a nano printing ink according to claim 8, wherein: the utility model discloses a filter assembly, including casing (23), filter box (24), mount pad (25) and collection box (26), casing (23) fixed mounting is in one side of support (1), hopper (22) under fixedly connected with on support (1), open-ended A has been seted up on casing (23), the one end of hopper (22) is passed open-ended A and is communicated with each other with casing (23) inside down, circular internal thread mouth has been seted up at the top of casing (23), the outer wall of mount pad (25) is provided with the external screw thread, mount pad (25) threaded mounting is in circular internal thread mouth, the bottom fixedly connected with filter box (24) of mount pad (25), open-ended B has been seted up to the opposite side of filter box (24), open-ended B is greater than open-ended A, the front side of casing (23) has been seted up the rectangle opening, the inboard bottom of casing (23) has seted up the spout and has through spout slidable mounting and has collection box (26), the front side fixedly connected with handle of collection box (26), the articulated feeding apron of installing of pot (2) of outer wall.
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Application publication date: 20230303 |