CN115703676A - Preparation method of high-permeability cement slurry for plugging - Google Patents
Preparation method of high-permeability cement slurry for plugging Download PDFInfo
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- CN115703676A CN115703676A CN202110935265.0A CN202110935265A CN115703676A CN 115703676 A CN115703676 A CN 115703676A CN 202110935265 A CN202110935265 A CN 202110935265A CN 115703676 A CN115703676 A CN 115703676A
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- 239000004568 cement Substances 0.000 title claims abstract description 42
- 239000002002 slurry Substances 0.000 title claims abstract description 32
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000000843 powder Substances 0.000 claims abstract description 19
- 239000011398 Portland cement Substances 0.000 claims abstract description 10
- 239000004570 mortar (masonry) Substances 0.000 claims abstract description 10
- 239000000835 fiber Substances 0.000 claims abstract description 9
- 239000002994 raw material Substances 0.000 claims abstract description 9
- 239000012744 reinforcing agent Substances 0.000 claims abstract description 9
- 239000004576 sand Substances 0.000 claims abstract description 7
- 239000010881 fly ash Substances 0.000 claims abstract description 6
- -1 polypropylene Polymers 0.000 claims abstract description 6
- 229920000049 Carbon (fiber) Polymers 0.000 claims abstract description 5
- 239000004743 Polypropylene Substances 0.000 claims abstract description 5
- 239000004917 carbon fiber Substances 0.000 claims abstract description 5
- 239000000017 hydrogel Substances 0.000 claims abstract description 5
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 5
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000011707 mineral Substances 0.000 claims abstract description 5
- 229920001778 nylon Polymers 0.000 claims abstract description 5
- 229920001155 polypropylene Polymers 0.000 claims abstract description 5
- 238000003756 stirring Methods 0.000 claims description 84
- 238000010438 heat treatment Methods 0.000 claims description 14
- 238000007599 discharging Methods 0.000 claims description 10
- 238000006243 chemical reaction Methods 0.000 claims description 9
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 6
- 230000005540 biological transmission Effects 0.000 claims description 6
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 5
- 239000003638 chemical reducing agent Substances 0.000 claims description 5
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 4
- 239000000378 calcium silicate Substances 0.000 claims description 4
- 229910052918 calcium silicate Inorganic materials 0.000 claims description 4
- OYACROKNLOSFPA-UHFFFAOYSA-N calcium;dioxido(oxo)silane Chemical compound [Ca+2].[O-][Si]([O-])=O OYACROKNLOSFPA-UHFFFAOYSA-N 0.000 claims description 4
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 claims description 4
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims description 4
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 claims description 4
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 claims description 4
- 229920002401 polyacrylamide Polymers 0.000 claims description 4
- LLHKCFNBLRBOGN-UHFFFAOYSA-N propylene glycol methyl ether acetate Chemical compound COCC(C)OC(C)=O LLHKCFNBLRBOGN-UHFFFAOYSA-N 0.000 claims description 4
- 239000005871 repellent Substances 0.000 claims description 4
- 230000002940 repellent Effects 0.000 claims description 4
- 125000001181 organosilyl group Chemical group [SiH3]* 0.000 claims description 3
- 239000004816 latex Substances 0.000 claims description 2
- 229920000126 latex Polymers 0.000 claims description 2
- 239000004567 concrete Substances 0.000 abstract description 14
- 230000035699 permeability Effects 0.000 abstract description 12
- 230000000694 effects Effects 0.000 abstract description 8
- 230000008901 benefit Effects 0.000 abstract description 7
- 238000010276 construction Methods 0.000 abstract description 6
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 230000002035 prolonged effect Effects 0.000 abstract description 3
- 239000002956 ash Substances 0.000 abstract description 2
- 239000000463 material Substances 0.000 description 9
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 8
- 238000002156 mixing Methods 0.000 description 8
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 239000003795 chemical substances by application Substances 0.000 description 6
- 239000000499 gel Substances 0.000 description 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 4
- 239000003822 epoxy resin Substances 0.000 description 4
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000011812 mixed powder Substances 0.000 description 4
- 229920000647 polyepoxide Polymers 0.000 description 4
- 239000011347 resin Substances 0.000 description 4
- 229920005989 resin Polymers 0.000 description 4
- 239000003570 air Substances 0.000 description 3
- 239000008367 deionised water Substances 0.000 description 3
- 229910021641 deionized water Inorganic materials 0.000 description 3
- 239000011159 matrix material Substances 0.000 description 3
- 239000011380 pervious concrete Substances 0.000 description 3
- WIEXMPDBTYDSQF-UHFFFAOYSA-N 1,3-bis(furan-2-yl)propan-2-one Chemical compound C=1C=COC=1CC(=O)CC1=CC=CO1 WIEXMPDBTYDSQF-UHFFFAOYSA-N 0.000 description 2
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 description 2
- QZPSOSOOLFHYRR-UHFFFAOYSA-N 3-hydroxypropyl prop-2-enoate Chemical compound OCCCOC(=O)C=C QZPSOSOOLFHYRR-UHFFFAOYSA-N 0.000 description 2
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- 108010010803 Gelatin Proteins 0.000 description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- 208000012886 Vertigo Diseases 0.000 description 2
- ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 description 2
- 239000002518 antifoaming agent Substances 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 description 2
- 229920003086 cellulose ether Polymers 0.000 description 2
- 239000007822 coupling agent Substances 0.000 description 2
- 238000005336 cracking Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- GVGUFUZHNYFZLC-UHFFFAOYSA-N dodecyl benzenesulfonate;sodium Chemical compound [Na].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 GVGUFUZHNYFZLC-UHFFFAOYSA-N 0.000 description 2
- 238000010041 electrostatic spinning Methods 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 239000013305 flexible fiber Substances 0.000 description 2
- 229920000159 gelatin Polymers 0.000 description 2
- 239000008273 gelatin Substances 0.000 description 2
- 235000019322 gelatine Nutrition 0.000 description 2
- 235000011852 gelatine desserts Nutrition 0.000 description 2
- GVALZJMUIHGIMD-UHFFFAOYSA-H magnesium phosphate Chemical compound [Mg+2].[Mg+2].[Mg+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O GVALZJMUIHGIMD-UHFFFAOYSA-H 0.000 description 2
- 239000004137 magnesium phosphate Substances 0.000 description 2
- 229960002261 magnesium phosphate Drugs 0.000 description 2
- 229910000157 magnesium phosphate Inorganic materials 0.000 description 2
- 235000010994 magnesium phosphates Nutrition 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- SDVVLIIVFBKBMG-UHFFFAOYSA-N penta-2,4-dienoic acid Chemical compound OC(=O)C=CC=C SDVVLIIVFBKBMG-UHFFFAOYSA-N 0.000 description 2
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 2
- 229920001568 phenolic resin Polymers 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 238000004321 preservation Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 description 2
- 238000009987 spinning Methods 0.000 description 2
- 239000012745 toughening agent Substances 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 description 1
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 1
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 description 1
- FDLQZKYLHJJBHD-UHFFFAOYSA-N [3-(aminomethyl)phenyl]methanamine Chemical compound NCC1=CC=CC(CN)=C1 FDLQZKYLHJJBHD-UHFFFAOYSA-N 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000012615 aggregate Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910001870 ammonium persulfate Inorganic materials 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000012295 chemical reaction liquid Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000005007 epoxy-phenolic resin Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- ZIUHHBKFKCYYJD-UHFFFAOYSA-N n,n'-methylenebisacrylamide Chemical compound C=CC(=O)NCNC(=O)C=C ZIUHHBKFKCYYJD-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000005011 phenolic resin Substances 0.000 description 1
- 229920000768 polyamine Polymers 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 235000019353 potassium silicate Nutrition 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 229910000077 silane Inorganic materials 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 description 1
- 238000001132 ultrasonic dispersion Methods 0.000 description 1
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/91—Use of waste materials as fillers for mortars or concrete
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- Curing Cements, Concrete, And Artificial Stone (AREA)
Abstract
The invention belongs to the technical field of concrete processing and manufacturing, and particularly relates to a preparation method of cement slurry for high-permeability plugging, which comprises the following raw materials in parts by weight: 70-85 parts of volcanic ash portland cement, 17-33 parts of S95 grade mineral powder, 75-90 parts of fly ash, 70-90 parts of 70-100 mesh fine sand, 15-20 parts of polypropylene fiber or nylon fiber, 10-15 parts of carbon fiber, 13-25 parts of hydrogel, 18-27 parts of mortar reinforcing agent and 60-110 parts of clear water; the prepared cement slurry has the advantages of scientific and reasonable formula, strong product permeability, high bonding strength, strong cohesive force, stable performance and the like, is fully stirred in a vacuum environment, and all raw materials are uniformly mixed together, so that the using effect of the cement slurry is improved, the plugging effect of cracks of a building is improved, the impermeability and durability of concrete are effectively improved, the construction quality is improved, the production cost and the construction cost are reduced, the service life of the building is prolonged, and the cement slurry has good economic benefit and social benefit.
Description
The technical field is as follows:
the invention belongs to the technical field of concrete processing and manufacturing, and particularly relates to a preparation method of cement slurry for high-permeability plugging.
Background art:
the concrete is a heterogeneous brittle material formed by mixing sand aggregate, cement, water and other additional materials, because of a series of problems of concrete construction, deformation and constraint of the concrete, pores, air pockets, microcracks and the like exist in the hardened and formed concrete, the concrete is influenced by external conditions, the surface moisture loss is too fast, the deformation is larger, the change of internal humidity is smaller, the larger surface drying shrinkage deformation is restrained by the concrete, the crack is generated due to larger tensile stress, and the concrete needs to be stopped in time, so that the integrity of the surface of a building is realized, and the service life of the building is prolonged; chinese patent 2013104439865 discloses a high permeability pervious concrete cementing agent and a preparation method and application thereof, wherein the high permeability pervious concrete cementing agent comprises 2-3 parts by weight of furfuryl ketone resin, 100 parts by weight of cement, 4-6 parts by weight of epoxy resin, 1-2 parts by weight of a curing agent and 2-4 parts by weight of a toughening agent, the furfuryl ketone resin consists of furfural and acetone, the weight ratio of the furfural to the acetone is 2:1-4:1, under the action of diluted alkali NaOH, an initial polymer is obtained by heating at 110-180 ℃ for 2 hours, the cement is 42.5-grade ordinary portland cement, the epoxy resin is commercially available E-44, the molecular weight is 450, the shrinkage is 1-2%, the thermal expansion coefficient is 6-10.5%, the curing agent is mixed polyamine of m-xylylenediamine and epichlorohydrin of 1:1, and the toughening agent is polyurethane synthesized by utilizing water-soluble 2,4-tolylene diisocyanate and trimethylolpropane; chinese patent 2017102644651 discloses a high permeability cement grouting mortar and a preparation method thereof, which is prepared from cement, an additive, an admixture, sand and water in a mass ratio of 51-61%, 0.06-0.12%, 3-5%, 6.5-12.5% and 28-32%, wherein the cement is portland cement, ordinary portland cement or portland cement blended with a mixture, the admixture is a polycarboxylic acid high efficiency powder water reducer synthesized from methacrylic acid and methacrylic acid-polyethylene glycol ester, the mass ratio of the two is 1.5; chinese patent 201810996758.3 discloses a preparation method of a high-permeability anti-seepage plugging material, wherein 45-50 parts of sodium hydroxide solution, 10-15 parts of enzymolysis rice bran and 0.1-0.2 part of hydrogen peroxide are respectively weighed and placed in a three-neck flask, stirred, mixed and reacted in a heat preservation way, reaction liquid is collected and kept stand and cooled to room temperature, the pH value is adjusted to 5.0, and the filtrate is filtered, collected and dried under reduced pressure to obtain a dry substance; then respectively weighing 45-50 parts of deionized water, 10-15 parts of acrylic acid, 0.5-1.0 part of N, N' -methylene bisacrylamide, 3-5 parts of dry matter and 0.1-0.2 part of ammonium persulfate according to parts by weight, placing the materials in a three-neck flask, adjusting the pH value to 7.0, introducing nitrogen to remove air, after the introduction is finished, carrying out heat preservation reaction, standing and cooling to room temperature, and collecting mixed gel liquid; placing the mixed gel liquid into an injector of an electrostatic spinning device, carrying out electrostatic spinning treatment, collecting spinning fibers, cutting the spinning fibers, and collecting modified cut fibers; respectively weighing 45-50 parts by weight of deionized water, 10-15 parts by weight of portland cement, 6-8 parts by weight of fly ash, 3-5 parts by weight of blast furnace slag and 3-5 parts by weight of modified cut fiber, placing the materials into a beaker, stirring and mixing the materials, and collecting mixed powder; according to the mass ratio of 1:3, stirring and mixing the mixed powder with deionized water, placing the mixture into a cement paste stirrer, stirring and mixing, collecting matrix gel slurry, and then mixing the matrix gel slurry according to the volume ratio of 1:1, adding water glass into the matrix gel slurry prepared by the invention, stirring and mixing, and performing ultrasonic dispersion to prepare the high-permeability anti-seepage plugging material; chinese patent 2019104455032 discloses a high permeability pervious concrete cementing agent, which comprises 100 parts of magnesium phosphate cement, 15-20 parts of polyorganosiloxane, 25-35 parts of epoxy resin, 12-15 parts of phenolic resin, 13-18 parts of hydroxypropyl acrylate, 3-6 parts of acrylamide, 8-10 parts of cellulose ether, 6-8 parts of active silica powder, 3-4 parts of gelatin, 8-10 parts of polyvinyl alcohol, 6-9 parts of pentaerythritol, 4-7 parts of calcium sulfoaluminate hydrate, 10-12 parts of calcium carbonate whisker, 3-4 parts of sodium dodecyl benzene sulfonate, 1-2 parts of 2,4-zinc pentadienoate, 3-4 parts of coupling agent, 4-5 parts of defoaming agent and 45-55 parts of water, the preparation method comprises the steps of uniformly mixing magnesium phosphate cement, active silicon dioxide powder and hydrated calcium sulphoaluminate according to the formula ratio to obtain mixed powder for later use, dissolving gelatin, polyvinyl alcohol, hydroxypropyl acrylate, acrylamide, cellulose ether, pentaerythritol and sodium dodecyl benzene sulfonate according to the formula ratio in water to obtain mixed liquid for later use, mixing polyorganosiloxane, epoxy resin and phenolic resin according to the formula ratio to obtain mixed resin for later use, adding the mixed powder and the mixed resin into a concrete stirrer, stirring for 2-3 minutes, sequentially adding calcium carbonate whisker, 2,4-zinc pentadienoate, a coupling agent, a defoaming agent and the mixed liquid according to the formula ratio, and stirring for 5-6 minutes to obtain the cementing agent; the cement slurry for leaking stoppage in the prior art and the products of the patents has a complex processing and preparation process, and the prepared cement slurry still has air pockets, pores and the like, so that the strength of the filled slurry is not high, even secondary cracking occurs, particularly, the use requirement cannot be met in an outdoor complex environment, the factors causing cracking in the cement slurry cannot be fully eliminated due to the fact that uniform stirring cannot be achieved, the quality is difficult to guarantee, the service life of a building is influenced, repeated construction can be caused, and the workload of constructors is increased; therefore, the invention designs the high-permeability cement slurry for leaking stoppage, which enhances the viscosity of the cement slurry, increases the binding power, improves the binding strength and enhances the permeability of concrete by adding the flexible fibers into the cement slurry, improves the using effect of the cement slurry, promotes the plugging effect of cracks of a building and prolongs the service life of the building by fully stirring in a vacuum environment, and has good social value and economic benefit.
The invention content is as follows:
the invention aims to overcome the defects in the prior art and provide the high-permeability cement paste for plugging, the viscosity of the cement paste is enhanced, the cohesive force is increased, the cohesive strength is improved, the permeability of concrete is enhanced by adding the flexible fibers into the cement paste, the use effect of the cement paste is improved by fully stirring in a vacuum environment, the plugging effect of cracks of a building is improved, and the service life of the building is prolonged.
In order to realize the aim, the high-permeability cement slurry for plugging comprises the following raw materials in parts by weight: 70-85 parts of pozzolanic portland cement, 17-33 parts of S95 grade mineral powder, 75-90 parts of fly ash, 70-90 parts of 70-100 mesh fine sand, 15-20 parts of polypropylene fiber or nylon fiber, 10-15 parts of carbon fiber, 13-25 parts of hydrogel, 18-27 parts of mortar reinforcing agent and 60-110 parts of clear water.
The invention relates to a mortar reinforcing agent which comprises the following components in parts by weight: 5 to 11 parts of polycarboxylic acid water reducing agent, 8 to 12 parts of hydroxypropyl methyl cellulose, 11 to 13 parts of propylene glycol methyl ether acetate, 3 to 4 parts of polyacrylamide, 3 to 4 parts of polyvinyl alcohol powder, 1 to 3 parts of silyl water repellent, 2 to 3 parts of sodium dodecyl sulfate, 3 to 15 parts of latex powder and 7 to 10 parts of calcium silicate powder.
The preparation of the cement slurry for high permeability plugging is completed in a reaction kettle, and the main structure of the reaction kettle comprises: the device comprises a kettle body, a vacuumizing motor, a sealed feeding hole, a stirring shaft driving motor, a stirring shaft, stirring blades, a discharging hole, a discharging valve, a heating pipe and a controller; a vacuumizing motor is fixedly arranged on the central axis position of the top end of the kettle body in a sealed mode, two groups of stirring shaft driving motors are symmetrically arranged on two sides of the vacuumizing motor, and a sealed feeding hole capable of being opened and closed is further formed in one side of the top end of the kettle body; two groups of stirring shafts which respectively correspond to the two groups of stirring shaft driving motors are arranged in the kettle body in parallel, the stirring shafts are in transmission connection with the stirring shaft driving motors, stirring blades are fixedly arranged at the bottom ends of the stirring shafts, the top ends of upper shaft levers of the stirring shafts are in transmission connection with the stirring shaft driving motors, a plurality of groups of stirring blades which are uniformly distributed are fixedly arranged on lower shaft levers of the stirring shafts, and upper shaft levers and the lower shaft levers of the stirring shafts are fixedly connected through springs; the heating pipe is also arranged in the kettle body and is provided with an inlet, a spiral pipe body and an outlet, the inlet and the outlet are all penetrated through the side wall of the kettle body, and the spiral pipe body is spirally provided with a plurality of layers from top to bottom along the inner wall of the kettle body, so that the heating in the kettle body is realized; a discharge hole is formed in the bottom end of the kettle body, and a discharge valve is arranged on the discharge hole; the kettle body is externally provided with a controller which is respectively electrically connected with the vacuumizing motor and the stirring shaft driving motor to respectively realize the control of the vacuumizing motor and the stirring shaft driving motor.
When the cement slurry for high permeability plugging is prepared, raw materials of various weight components are poured into a kettle body of a reaction kettle through a feeding hole of the kettle body, a stirring shaft driving motor is started through a controller and drives a stirring shaft to rotate, stirring of the materials in the kettle body is achieved through stirring blades on the stirring shaft, the kettle body is heated through a heating pipe, constant-temperature stirring is carried out at the temperature of 35-40 ℃, the vacuumizing motor is controlled through the controller to carry out vacuumizing treatment on the kettle body while stirring, stirring is continued for 15-20 minutes after the vacuumizing motor is turned off, stirring is more uniform, and after stirring is completed, the stirring shaft driving motor is turned off, a discharging valve is turned on, and the mixed cement slurry is discharged through a discharging hole.
Compared with the prior art, the invention has the advantages of scientific and reasonable formula, strong product permeability, high bonding strength, strong cohesive force, stable performance and the like, is convenient to use and operate, fully stirs the cement slurry in a vacuum environment, mixes all raw materials more uniformly, improves the use effect of the cement slurry, improves the plugging effect of the cracks of the building, more effectively improves the impermeability and durability of the concrete, can improve the construction quality, reduces the production cost and the construction cost, prolongs the service life of the building, and generates good economic benefit and social benefit.
Description of the drawings:
FIG. 1 is a schematic diagram of the principle of the main structure of a reaction kettle related to the invention;
FIG. 2 is a schematic diagram of the connection structure of the electric principle of the reaction kettle according to the present invention.
Detailed Description
The invention is further illustrated by the following examples in connection with the accompanying drawings.
Example 1:
the high-permeability cement slurry for plugging comprises the following raw materials in parts by weight: 70 parts of volcanic ash portland cement, 33 parts of S95 grade mineral powder, 90 parts of fly ash, 70 parts of 70-100 mesh fine sand, 15 parts of polypropylene fiber or nylon fiber, 10 parts of carbon fiber, 13 parts of hydrogel, 27 parts of mortar reinforcing agent and 60 parts of clear water.
The invention relates to a mortar reinforcing agent which comprises the following components in parts by weight: 11 parts of polycarboxylic acid water reducing agent, 8 parts of hydroxypropyl methyl cellulose, 11 parts of propylene glycol methyl ether acetate, 3 parts of polyacrylamide, 3 parts of polyvinyl alcohol powder, 3 parts of silane-based water repellent, 3 parts of sodium dodecyl sulfate, 3 parts of emulsion powder and 7 parts of calcium silicate powder.
When the high-permeability cement slurry for plugging is prepared, the main structure of the reactor comprises: the device comprises a kettle body 1, a vacuumizing motor 2, a sealed feeding hole 3, a stirring shaft driving motor 4, a stirring shaft 5, stirring blades 6, a discharging hole 7, a discharging valve 8, a heating pipe 9 and a controller 10; a vacuumizing motor 2 is fixedly arranged on the central axis position of the top end of the kettle body 1 in a sealed mode, two groups of stirring shaft driving motors 4 are symmetrically arranged on two sides of the vacuumizing motor 2, and a sealed feeding hole 3 capable of being opened and closed is further formed in one side of the top end of the kettle body 1; two groups of stirring shafts 5 which respectively correspond to the two groups of stirring shaft driving motors 4 are arranged in the kettle body 1 in parallel, the stirring shafts 5 are in transmission connection with the stirring shaft driving motors 4, the bottom ends of the stirring shafts 5 are fixedly provided with stirring blades 6, the top ends of upper shaft levers 501 of the stirring shafts are in transmission connection with the stirring shaft driving motors 4, a plurality of groups of uniformly distributed stirring blades 6 are fixedly arranged on lower shaft levers 502 of the stirring shafts, and the upper shaft levers 501 and the lower shaft levers 502 of the stirring shafts are fixedly connected through springs 503; a heating pipe 9 is further arranged in the kettle body 1, the heating pipe 9 is provided with an inlet 901, a spiral pipe body 902 and an outlet 903, the inlet 901 and the outlet 903 both penetrate through the side wall of the kettle body 1, and the spiral pipe body 902 is spirally provided with multiple layers from top to bottom along the inner wall of the kettle body 1, so that heating in the kettle body 1 is realized; a discharge port 7 is arranged at the bottom end of the kettle body 1, and a discharge valve 8 is arranged on the discharge port 7; the controller 10 is arranged outside the kettle body 1, and the controller 10 is respectively electrically connected with the vacuumizing motor 2 and the stirring shaft driving motor 4 to respectively realize the control of the vacuumizing motor 2 and the stirring shaft driving motor 4.
The invention relates to a preparation method of cement slurry for high permeability plugging, which comprises the steps of firstly pouring raw materials of various weight components into a kettle body 1 of a reaction kettle through a feed inlet of the kettle body 1, starting a stirring shaft driving motor 4 through a controller 10, driving a stirring shaft 5 to rotate by the stirring shaft driving motor 4, stirring materials in the kettle body 1 through stirring blades 6 on the stirring shaft 5, heating the kettle body 1 through a heating pipe 9, controlling the temperature to be 35-40 ℃ for stirring at constant temperature, controlling a vacuumizing motor 2 to perform vacuumizing treatment on the kettle body 1 through the controller 10 while stirring, continuing stirring for 15-20 minutes after the vacuumizing motor 2 is closed, enabling stirring to be more uniform, closing the stirring shaft driving motor 4 after stirring is completed, opening a discharging valve 8, and discharging mixed cement slurry through a discharge outlet 7.
Example 2:
the preparation process of this example is the same as that of example 1, except that the raw materials used are different in weight components, wherein: 85 parts of pozzolanic portland cement, 17 parts of S95 grade mineral powder, 75 parts of fly ash, 90 parts of 70-100 mesh fine sand, 20 parts of polypropylene fiber or nylon fiber, 15 parts of carbon fiber, 25 parts of hydrogel, 18 parts of mortar reinforcing agent and 110 parts of clear water.
The mortar reinforcing agent related to the embodiment comprises the following components in parts by weight: 5 parts of polycarboxylic acid water reducing agent, 12 parts of hydroxypropyl methyl cellulose, 13 parts of propylene glycol methyl ether acetate, 4 parts of polyacrylamide, 4 parts of polyvinyl alcohol powder, 1 part of silyl water repellent, 2 parts of sodium dodecyl sulfate, 15 parts of emulsion powder and 10 parts of calcium silicate powder.
The cement slurry prepared by the embodiment has strong permeability and is suitable for leakage repairing in severe environment.
Claims (3)
1. The preparation method of the cement slurry for high-permeability plugging is characterized by comprising the following raw materials in parts by weight: 70-85 parts of pozzolanic portland cement, 17-33 parts of S95 grade mineral powder, 75-90 parts of fly ash, 70-90 parts of 70-100 mesh fine sand, 15-20 parts of polypropylene fiber or nylon fiber, 10-15 parts of carbon fiber, 13-25 parts of hydrogel, 18-27 parts of mortar reinforcing agent and 60-110 parts of clear water.
2. The preparation method of the cement slurry for high-permeability plugging according to claim 1, characterized by comprising the following steps: the mortar reinforcing agent comprises the following components in parts by weight: 5 to 11 parts of polycarboxylic acid water reducing agent, 8 to 12 parts of hydroxypropyl methyl cellulose, 11 to 13 parts of propylene glycol methyl ether acetate, 3 to 4 parts of polyacrylamide, 3 to 4 parts of polyvinyl alcohol powder, 1 to 3 parts of silyl water repellent, 2 to 3 parts of sodium dodecyl sulfate, 3 to 15 parts of latex powder and 7 to 10 parts of calcium silicate powder.
3. The preparation method of the cement paste for high-permeability plugging according to claim 1 or 2, characterized by comprising the following steps: the preparation of the cement slurry for high-permeability plugging is completed in a reaction kettle, and the main structure of the reaction kettle comprises: the device comprises a kettle body, a vacuumizing motor, a sealed feeding hole, a stirring shaft driving motor, a stirring shaft, stirring blades, a discharging hole, a discharging valve, a heating pipe and a controller; a vacuumizing motor is fixedly arranged on the central axis position of the top end of the kettle body in a sealed mode, two groups of stirring shaft driving motors are symmetrically arranged on two sides of the vacuumizing motor, and a sealed feeding hole capable of being opened and closed is further formed in one side of the top end of the kettle body; two groups of stirring shafts which respectively correspond to the two groups of stirring shaft driving motors are arranged in the kettle body in parallel, the stirring shafts are in transmission connection with the stirring shaft driving motors, stirring blades are fixedly arranged at the bottom ends of the stirring shafts, the top ends of upper shaft levers of the stirring shafts are in transmission connection with the stirring shaft driving motors, a plurality of groups of stirring blades which are uniformly distributed are fixedly arranged on lower shaft levers of the stirring shafts, and upper shaft levers and the lower shaft levers of the stirring shafts are fixedly connected through springs; the heating pipe is also arranged in the kettle body and is provided with an inlet, a spiral pipe body and an outlet, the inlet and the outlet are all penetrated through the side wall of the kettle body, and the spiral pipe body is spirally provided with a plurality of layers from top to bottom along the inner wall of the kettle body, so that the heating in the kettle body is realized; a discharge hole is formed in the bottom end of the kettle body, and a discharge valve is arranged on the discharge hole; the kettle body is externally provided with a controller which is respectively electrically connected with the vacuumizing motor and the stirring shaft driving motor to respectively realize the control of the vacuumizing motor and the stirring shaft driving motor.
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1217096A (en) * | 1968-04-05 | 1970-12-23 | Brooks Instr N V | Mixing device |
| CN108484045A (en) * | 2018-04-23 | 2018-09-04 | 青岛环秀涂料有限公司 | A kind of high intensity dry-mixed mortar |
| CN108483981A (en) * | 2018-04-23 | 2018-09-04 | 青岛环秀涂料有限公司 | A kind of mortar reinforcing agent and preparation method thereof |
| CN208975806U (en) * | 2018-09-27 | 2019-06-14 | 青岛科润生物科技有限公司 | A kind of stirring apparatus for reaction kettle with elevating hopper |
| CN209005737U (en) * | 2018-09-27 | 2019-06-21 | 青岛科润生物科技有限公司 | A kind of reaction kettle cleaning device |
| CN112851276A (en) * | 2021-02-23 | 2021-05-28 | 中建商品混凝土有限公司 | Light underwater undispersed plugging concrete and preparation method thereof |
-
2021
- 2021-08-16 CN CN202110935265.0A patent/CN115703676A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1217096A (en) * | 1968-04-05 | 1970-12-23 | Brooks Instr N V | Mixing device |
| CN108484045A (en) * | 2018-04-23 | 2018-09-04 | 青岛环秀涂料有限公司 | A kind of high intensity dry-mixed mortar |
| CN108483981A (en) * | 2018-04-23 | 2018-09-04 | 青岛环秀涂料有限公司 | A kind of mortar reinforcing agent and preparation method thereof |
| CN208975806U (en) * | 2018-09-27 | 2019-06-14 | 青岛科润生物科技有限公司 | A kind of stirring apparatus for reaction kettle with elevating hopper |
| CN209005737U (en) * | 2018-09-27 | 2019-06-21 | 青岛科润生物科技有限公司 | A kind of reaction kettle cleaning device |
| CN112851276A (en) * | 2021-02-23 | 2021-05-28 | 中建商品混凝土有限公司 | Light underwater undispersed plugging concrete and preparation method thereof |
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