CN115670981B - Hair care composition with color locking, brightening, softening and repairing effects and preparation method thereof - Google Patents
Hair care composition with color locking, brightening, softening and repairing effects and preparation method thereof Download PDFInfo
- Publication number
- CN115670981B CN115670981B CN202211459179.8A CN202211459179A CN115670981B CN 115670981 B CN115670981 B CN 115670981B CN 202211459179 A CN202211459179 A CN 202211459179A CN 115670981 B CN115670981 B CN 115670981B
- Authority
- CN
- China
- Prior art keywords
- parts
- weight
- stirring
- hair
- oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 85
- 230000000694 effects Effects 0.000 title claims abstract description 14
- 238000005282 brightening Methods 0.000 title claims abstract description 6
- 238000002360 preparation method Methods 0.000 title abstract description 19
- 239000002904 solvent Substances 0.000 claims abstract description 41
- 102000011782 Keratins Human genes 0.000 claims abstract description 33
- 108010076876 Keratins Proteins 0.000 claims abstract description 33
- 102000004169 proteins and genes Human genes 0.000 claims abstract description 31
- 108090000623 proteins and genes Proteins 0.000 claims abstract description 31
- 241000209140 Triticum Species 0.000 claims abstract description 30
- 235000021307 Triticum Nutrition 0.000 claims abstract description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 30
- SNPLKNRPJHDVJA-ZETCQYMHSA-N D-panthenol Chemical compound OCC(C)(C)[C@@H](O)C(=O)NCCCO SNPLKNRPJHDVJA-ZETCQYMHSA-N 0.000 claims abstract description 28
- 229940101267 panthenol Drugs 0.000 claims abstract description 28
- 235000020957 pantothenol Nutrition 0.000 claims abstract description 28
- 239000011619 pantothenol Substances 0.000 claims abstract description 28
- 244000068988 Glycine max Species 0.000 claims abstract description 26
- 235000010469 Glycine max Nutrition 0.000 claims abstract description 26
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000000284 extract Substances 0.000 claims abstract description 26
- 241000226555 Leontopodium Species 0.000 claims abstract description 25
- 235000019774 Rice Bran oil Nutrition 0.000 claims abstract description 24
- WHMDKBIGKVEYHS-IYEMJOQQSA-L Zinc gluconate Chemical compound [Zn+2].OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O WHMDKBIGKVEYHS-IYEMJOQQSA-L 0.000 claims abstract description 24
- 239000008165 rice bran oil Substances 0.000 claims abstract description 24
- 229930003799 tocopherol Natural products 0.000 claims abstract description 24
- 235000010384 tocopherol Nutrition 0.000 claims abstract description 24
- 239000011732 tocopherol Substances 0.000 claims abstract description 24
- 229960001295 tocopherol Drugs 0.000 claims abstract description 24
- 229960000306 zinc gluconate Drugs 0.000 claims abstract description 24
- 235000011478 zinc gluconate Nutrition 0.000 claims abstract description 24
- 239000011670 zinc gluconate Substances 0.000 claims abstract description 24
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 claims abstract description 24
- 235000013868 candelilla wax Nutrition 0.000 claims abstract description 23
- 239000004204 candelilla wax Substances 0.000 claims abstract description 23
- 229940073532 candelilla wax Drugs 0.000 claims abstract description 23
- 239000008367 deionised water Substances 0.000 claims abstract description 23
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 23
- IUJAMGNYPWYUPM-UHFFFAOYSA-N hentriacontane Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCC IUJAMGNYPWYUPM-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000003549 soybean oil Substances 0.000 claims abstract description 23
- 239000004519 grease Substances 0.000 claims abstract description 14
- 206010020649 Hyperkeratosis Diseases 0.000 claims abstract description 13
- 239000003906 humectant Substances 0.000 claims abstract description 12
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 11
- 150000002191 fatty alcohols Chemical class 0.000 claims abstract description 10
- 238000000034 method Methods 0.000 claims abstract description 10
- 239000003755 preservative agent Substances 0.000 claims abstract description 9
- 230000002335 preservative effect Effects 0.000 claims abstract description 9
- 239000002562 thickening agent Substances 0.000 claims abstract description 9
- 238000003756 stirring Methods 0.000 claims description 145
- 230000001804 emulsifying effect Effects 0.000 claims description 84
- 239000003921 oil Substances 0.000 claims description 59
- 235000019198 oils Nutrition 0.000 claims description 59
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical group CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 51
- 238000001816 cooling Methods 0.000 claims description 34
- 238000002156 mixing Methods 0.000 claims description 34
- 229940082500 cetostearyl alcohol Drugs 0.000 claims description 20
- OULAJFUGPPVRBK-UHFFFAOYSA-N tetratriacontyl alcohol Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCO OULAJFUGPPVRBK-UHFFFAOYSA-N 0.000 claims description 20
- 239000002245 particle Substances 0.000 claims description 19
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 18
- 229910019142 PO4 Inorganic materials 0.000 claims description 18
- 239000001341 hydroxy propyl starch Substances 0.000 claims description 18
- 235000013828 hydroxypropyl starch Nutrition 0.000 claims description 18
- 229960005323 phenoxyethanol Drugs 0.000 claims description 18
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 18
- 239000010452 phosphate Substances 0.000 claims description 18
- 125000001453 quaternary ammonium group Chemical class 0.000 claims description 18
- ANZUDYZHSVGBRF-UHFFFAOYSA-N 3-ethylnonane-1,2,3-triol Chemical compound CCCCCCC(O)(CC)C(O)CO ANZUDYZHSVGBRF-UHFFFAOYSA-N 0.000 claims description 17
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 claims description 17
- 229930182478 glucoside Natural products 0.000 claims description 17
- 150000008131 glucosides Chemical class 0.000 claims description 17
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 claims description 17
- 239000000811 xylitol Substances 0.000 claims description 17
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical group OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 claims description 17
- 235000010447 xylitol Nutrition 0.000 claims description 17
- 229960002675 xylitol Drugs 0.000 claims description 17
- NWGKJDSIEKMTRX-AAZCQSIUSA-N Sorbitan monooleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O NWGKJDSIEKMTRX-AAZCQSIUSA-N 0.000 claims description 16
- 239000003240 coconut oil Substances 0.000 claims description 16
- 235000019864 coconut oil Nutrition 0.000 claims description 16
- 229950004959 sorbitan oleate Drugs 0.000 claims description 16
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 8
- 235000016108 Argania sideroxylon Nutrition 0.000 claims description 5
- 244000125300 Argania sideroxylon Species 0.000 claims description 5
- 235000007164 Oryza sativa Nutrition 0.000 claims description 4
- 235000021302 avocado oil Nutrition 0.000 claims description 4
- 239000008163 avocado oil Substances 0.000 claims description 4
- YSJGOMATDFSEED-UHFFFAOYSA-M behentrimonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCCCCCCCC[N+](C)(C)C YSJGOMATDFSEED-UHFFFAOYSA-M 0.000 claims description 4
- 229940095081 c13-16 isoparaffin Drugs 0.000 claims description 3
- 235000011187 glycerol Nutrition 0.000 claims description 3
- KUVMKLCGXIYSNH-UHFFFAOYSA-N isopentadecane Chemical compound CCCCCCCCCCCCC(C)C KUVMKLCGXIYSNH-UHFFFAOYSA-N 0.000 claims description 3
- 235000009566 rice Nutrition 0.000 claims description 3
- XFRVVPUIAFSTFO-UHFFFAOYSA-N 1-Tridecanol Chemical compound CCCCCCCCCCCCCO XFRVVPUIAFSTFO-UHFFFAOYSA-N 0.000 claims description 2
- 240000007594 Oryza sativa Species 0.000 claims description 2
- LWZFANDGMFTDAV-BURFUSLBSA-N [(2r)-2-[(2r,3r,4s)-3,4-dihydroxyoxolan-2-yl]-2-hydroxyethyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O LWZFANDGMFTDAV-BURFUSLBSA-N 0.000 claims description 2
- 229920002553 poly(2-methacrylolyloxyethyltrimethylammonium chloride) polymer Polymers 0.000 claims description 2
- 229950006451 sorbitan laurate Drugs 0.000 claims description 2
- 235000011067 sorbitan monolaureate Nutrition 0.000 claims description 2
- 229940087291 tridecyl alcohol Drugs 0.000 claims description 2
- 239000010497 wheat germ oil Substances 0.000 claims description 2
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 claims 2
- 238000005406 washing Methods 0.000 abstract description 10
- 230000009286 beneficial effect Effects 0.000 abstract description 3
- 230000008901 benefit Effects 0.000 abstract description 3
- 238000005562 fading Methods 0.000 abstract description 3
- 235000016709 nutrition Nutrition 0.000 abstract description 3
- 230000035764 nutrition Effects 0.000 abstract description 3
- 239000000049 pigment Substances 0.000 abstract description 3
- 239000013589 supplement Substances 0.000 abstract description 3
- -1 hair conditioner Substances 0.000 abstract description 2
- 238000009776 industrial production Methods 0.000 abstract description 2
- 230000014759 maintenance of location Effects 0.000 abstract description 2
- 230000008569 process Effects 0.000 abstract description 2
- 241001249542 Leonia <angiosperm> Species 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 68
- 239000000463 material Substances 0.000 description 36
- 238000005303 weighing Methods 0.000 description 23
- UBHWBODXJBSFLH-UHFFFAOYSA-N hexadecan-1-ol;octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO.CCCCCCCCCCCCCCCCCCO UBHWBODXJBSFLH-UHFFFAOYSA-N 0.000 description 18
- 238000007599 discharging Methods 0.000 description 16
- 238000012360 testing method Methods 0.000 description 12
- 239000000047 product Substances 0.000 description 9
- 238000010438 heat treatment Methods 0.000 description 7
- 230000006872 improvement Effects 0.000 description 7
- 238000002474 experimental method Methods 0.000 description 6
- 230000006378 damage Effects 0.000 description 5
- 230000001953 sensory effect Effects 0.000 description 4
- 238000009960 carding Methods 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
- 238000011056 performance test Methods 0.000 description 3
- 230000008439 repair process Effects 0.000 description 3
- 210000004761 scalp Anatomy 0.000 description 3
- 210000003491 skin Anatomy 0.000 description 3
- 241000894006 Bacteria Species 0.000 description 2
- 241001553290 Euphorbia antisyphilitica Species 0.000 description 2
- 241000209094 Oryza Species 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 238000005119 centrifugation Methods 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 229920001184 polypeptide Polymers 0.000 description 2
- 102000004196 processed proteins & peptides Human genes 0.000 description 2
- 108090000765 processed proteins & peptides Proteins 0.000 description 2
- 239000002453 shampoo Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 201000004384 Alopecia Diseases 0.000 description 1
- 238000012935 Averaging Methods 0.000 description 1
- GHOKWGTUZJEAQD-UHFFFAOYSA-N Chick antidermatitis factor Natural products OCC(C)(C)C(O)C(=O)NCCC(O)=O GHOKWGTUZJEAQD-UHFFFAOYSA-N 0.000 description 1
- 241001391944 Commicarpus scandens Species 0.000 description 1
- LEVWYRKDKASIDU-QWWZWVQMSA-N D-cystine Chemical compound OC(=O)[C@H](N)CSSC[C@@H](N)C(O)=O LEVWYRKDKASIDU-QWWZWVQMSA-N 0.000 description 1
- 102000016942 Elastin Human genes 0.000 description 1
- 108010014258 Elastin Proteins 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 206010019030 Hair colour changes Diseases 0.000 description 1
- 206010019049 Hair texture abnormal Diseases 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- 241000226556 Leontopodium alpinum Species 0.000 description 1
- 108091005804 Peptidases Proteins 0.000 description 1
- 239000004365 Protease Substances 0.000 description 1
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 description 1
- 244000098338 Triticum aestivum Species 0.000 description 1
- 229930003571 Vitamin B5 Natural products 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- HVYLDJKDVOOTHV-UHFFFAOYSA-N acetic acid;2-iminoethanethiol Chemical compound CC(O)=O.CC(O)=O.SCC=N HVYLDJKDVOOTHV-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003570 air Substances 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 238000000861 blow drying Methods 0.000 description 1
- FAPWYRCQGJNNSJ-UBKPKTQASA-L calcium D-pantothenic acid Chemical compound [Ca+2].OCC(C)(C)[C@@H](O)C(=O)NCCC([O-])=O.OCC(C)(C)[C@@H](O)C(=O)NCCC([O-])=O FAPWYRCQGJNNSJ-UBKPKTQASA-L 0.000 description 1
- 229960002079 calcium pantothenate Drugs 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 239000003093 cationic surfactant Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 229960003067 cystine Drugs 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000032798 delamination Effects 0.000 description 1
- 230000003467 diminishing effect Effects 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 230000003670 easy-to-clean Effects 0.000 description 1
- 229920002549 elastin Polymers 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 210000002615 epidermis Anatomy 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 239000003102 growth factor Substances 0.000 description 1
- 230000037308 hair color Effects 0.000 description 1
- 239000000118 hair dye Substances 0.000 description 1
- 208000024963 hair loss Diseases 0.000 description 1
- 230000003676 hair loss Effects 0.000 description 1
- 230000017525 heat dissipation Effects 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000010369 molecular cloning Methods 0.000 description 1
- 229920005615 natural polymer Polymers 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 235000014593 oils and fats Nutrition 0.000 description 1
- 238000001543 one-way ANOVA Methods 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 239000003223 protective agent Substances 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 230000007480 spreading Effects 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 235000009492 vitamin B5 Nutrition 0.000 description 1
- 239000011675 vitamin B5 Substances 0.000 description 1
- 235000021470 vitamin B5 (pantothenic acid) Nutrition 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
Abstract
The invention provides a hair care composition with color locking, brightening, softening and repairing effects and a preparation method thereof, wherein the hair care composition comprises the following components: zinc gluconate, fatty alcohol, hair conditioner, solvent, thickener, candelilla wax, tocopherol, wild soybean oil, rice bran oil, panthenol, hydrolyzed wheat protein, functional grease, alpine leonia herb callus extract, humectant, emulsifier, keratin, preservative and deionized water. The hair care composition provided by the invention can supplement hair nutrition, smooth hair scales and slow down fading through the cooperation of rice bran oil, functional grease, panthenol, hydrolyzed wheat protein, alpine leontopodium callus extract, keratin and other components, and can improve pigment loss caused by frequent hair washing and prolong color retention time. The preparation method provided by the invention has the advantages of simple process, mild condition and short time consumption, and is beneficial to industrial production.
Description
Technical Field
The invention relates to the field of daily chemicals, in particular to a hair care composition with the effects of color locking, brightening, softening and repairing and a preparation method thereof.
Background
The hair is natural polymer keratin fiber, and is covered on scalp to prevent scalp heat dissipation, protect scalp from damage and beautify. The hair keratin fibers are inert in nature, but light, hot air, acid, alkali, oxidizing agents, and reducing agents can damage the hair. Hair is often dyed, straightened, curled, hair-dryer, etc. in life, which can cause different degrees of damage to hair. The main manifestations are: on the one hand, the hair scales on the surface of the hair are damaged and tilted, so that the hair is difficult to comb and has dull and matt luster; on the other hand, after the keratin fiber structure is destroyed, the toughness and strength of the hair are obviously reduced, and the hair is fragile and easy to break.
In the existing hair repair technology, products such as shampoo, hair conditioner, hair film and the like repair damaged hair through the electrostatic attraction of a cationic conditioner to hair. The hair conditioner is compounded by taking the cationic surfactant as a main body, so that tangled hair is taken smoothly, and the effect of easy carding is achieved. However, the existing hair conditioner products have poor repairing effect on rough hair and cannot effectively prevent hair from being fragile and broken; in addition, hair conditioner products are rarely available on the market which can maintain a bright and shiny hair color.
Disclosure of Invention
In view of this, the present invention provides a hair care composition and a method for preparing the same.
The technical scheme of the invention is as follows:
a hair care composition with color locking, brightening, softening and repairing effects comprises the following components in parts by weight: 0.5 to 2 parts of zinc gluconate, 2 to 5 parts of fatty alcohol, 0.3 to 1 part of hair conditioner, 1 to 3 parts of solvent, 0.3 to 1 part of thickener, 1 to 3 parts of candelilla wax, 0.5 to 2 parts of tocopherol, 3 to 7 parts of wild soybean oil, 3 to 7 parts of rice bran oil, 2 to 5 parts of panthenol, 2 to 5 parts of hydrolyzed wheat protein, 0.5 to 2 parts of functional grease, 0.5 to 2 parts of alpine leontopodium herb callus extract, 0.3 to 1 part of humectant, 1 to 3 parts of emulsifier, 0.5 to 2 parts of keratin, 0.5 to 1.5 parts of preservative and 55 to 75 parts of deionized water.
Further, the hair care composition comprises the following components in parts by weight: 1 part of zinc gluconate, 3 parts of fatty alcohol, 0.5 part of hair conditioner, 2 parts of solvent, 0.5 part of thickener, 2 parts of candelilla wax, 1 part of tocopherol, 5 parts of wild soybean oil, 5 parts of rice bran oil, 3 parts of panthenol, 3 parts of hydrolyzed wheat protein, 1 part of functional grease, 1 part of alpine leontopodium herb callus extract, 0.5 part of humectant, 2 parts of emulsifier, 1 part of keratin, 0.8 part of preservative and 68 parts of deionized water.
Further, the hair care composition comprises a fatty alcohol, wherein the fatty alcohol is cetostearyl alcohol;
the hair conditioner is quaternary ammonium salt-87 and/or behenyl trimethyl ammonium chloride;
the solvent is propylene glycol and/or glycerol;
the thickener is hydroxypropyl starch phosphate and/or cetostearyl alcohol;
the functional grease is one or more of coconut oil, hydrogenated avocado oil, argania spinosa kernel oil and wheat germ oil;
the humectant is xylitol-based glucoside and/or sorbitan laurate;
the emulsifier is one or more of sorbitan oleate, polyquaternium-37, C13-16 isoparaffin and tridecyl alcohol polyether-6;
the preservative is one or more of phenoxyethanol and ethylhexyl glycerol.
The invention also provides a preparation method of the hair care composition, which comprises the following steps:
s1, adding an emulsifying agent, fatty alcohol, candelilla wax, tocopherol, wild soybean oil and rice chaff oil into an oil phase pot, stirring and dissolving uniformly, adding deionized water, stirring and homogenizing until all components are dispersed uniformly;
s2, adding the solvent, the panthenol, the hair conditioner, the humectant, the zinc gluconate and the thickener into an emulsifying pot, stirring and homogenizing until all the components are uniformly dispersed;
s3, putting the mixture obtained in the step S1 into an emulsifying pot, stirring and homogenizing the mixture with the mixture obtained in the step S2 until no particles exist, and preserving heat;
s4, continuously stirring the mixture obtained in the step S3, and when the temperature is reduced to 45 ℃, adding hydrolyzed wheat protein, functional grease, alpine leontopodium herb callus extract, keratin and preservative, and uniformly stirring and mixing;
s5, continuously stirring the mixture obtained in the step S4, and cooling to 35 ℃ to obtain the hair care composition.
Further, in the preparation method, in the step S1, the stirring homogenizing temperature is 80-90 ℃, the stirring rotating speed is 120 r/min, and the stirring time is 20 min.
Further, in the preparation method, in the step S2, the stirring homogenizing temperature is 80-90 ℃, the stirring rotating speed is 120 r/min, and the stirring time is 20 min.
Further, in the above preparation method, in step S3, the heat preservation period is 10 minutes.
The zinc gluconate adopted by the invention can stabilize pigment particles, improve color stability and delay fading.
The hair conditioner adopted by the invention is quaternary ammonium salt-87 and/or behenyl trimethyl ammonium chloride, and has certain cleaning, antibacterial and antistatic effects.
The tocopherol adopted by the invention, also called vitamin E, can protect the hair from being damaged by high temperature, and has the advantages of color locking, external isolation and beautiful hair.
The candelilla (EUPHORBIA CERIFERA) wax adopted by the invention can improve the brightness texture of the prepared hair care composition and maintain the soft and soft hair state.
The wild soybean (Glycine SOJA) oil adopted by the invention is grease extracted from wild soybeans, can be used as a growth factor of skin, contains fragrant components, can be used as essence and spice, and is mainly used as an antioxidant and a humectant in skin care products.
The rice (ORYZA SATIVA) furfuryl oil adopted by the invention can nourish and protect the hairline, and a protective film is formed on the surface of the hairline, so that the external injury is avoided.
The alpine leontopodium (LEONTOPODIUM ALPINUM) callus extract adopted by the invention can slow down the degradation of elastin, has a certain inhibition effect on some bacteria, and has the effects of resisting bacteria and diminishing inflammation.
The hydrolyzed wheat protein is protein extracted from wheat seeds, and the structure of the wheat protein is modified by adopting a hydrolysis technical means to obtain a polypeptide component. After the protein is hydrolyzed, the main products are various amino acids and polypeptides, and the hairline can be rapidly absorbed in multiple ways so as to supplement nutrition.
Panthenol used in the present invention is an alcohol derivative of vitamin B5 (pantothenic acid). It is an excellent hair protecting agent, and can make hair bright and oily by adding a certain amount of panthenol into hair care product, and its molecules can permeate into hair and quickly be reduced into vitamin B5 under the action of enzyme.
The effective oils and fats which can be used in the present invention include coconut oil, hydrogenated avocado oil, ARGANIA SPINOSA (ARGANIA SPINOSA) kernel oil, wheat (Triticum VULGARE) germ oil, which can nourish the water without greasiness and reduce hair loss.
The keratin adopted by the invention contains more cystine, the molecules of the keratin form a highly cross-linked three-dimensional network structure through disulfide bonds and hydrogen bonds and other actions, the chemical property is very stable, the keratin has higher mechanical strength, is insoluble in water and strong in decomposition resistance, cannot be decomposed by common protease, and is considered as a potential high-quality protein source with higher nutritive value. The keratin has high-resistance physicochemical characteristics and special biological effects, contains a large amount of amino, hydroxyl and other hydrophilic groups, plays a role in water retention, and plays an important role in maintaining normal physiological functions of epidermis.
The beneficial effects of the invention are as follows: the hair care composition disclosed by the invention can supplement hair nutrition, smooth hair scales and repair damage through the cooperation of rice bran oil, functional grease, panthenol, hydrolyzed wheat protein, alpine leontopodium callus extract, keratin and other components, and can improve pigment loss caused by frequent hair washing, slow down fading and prolong the color retention time. The preparation method provided by the invention has the advantages of simple process, mild condition and short time consumption, and is beneficial to industrial production.
Detailed Description
The experimental methods used in the following examples are all conventional methods unless otherwise specified; the reagents, materials and the like used in the following examples are commercially available or can be prepared by known methods unless otherwise specified. The experimental procedure, which does not address the specific conditions in the examples below, is generally followed by routine conditions such as Sambrook et al, molecular cloning: conditions described in the laboratory Manual (New York: cold SpringHarbor Laboratory Press, 1989) or as recommended by the manufacturer.
Example 1
(1) Dispersing an oil phase: 2 parts of sorbitan oleate, 3 parts of cetostearyl alcohol, 2 parts of candelilla wax, 1 part of tocopherol, 5 parts of wild soybean oil and 5 parts of rice bran oil are weighed, put into an oil phase pot, stirred and dissolved uniformly, 68 parts of deionized water is added, the temperature is raised to 90 ℃, and stirring and homogenizing are kept at 80 ℃ for 20 minutes until all components are dispersed uniformly, and the stirring speed is 120 revolutions per minute;
(2) Dispersing solvent: 2 parts by weight of propylene glycol, 3 parts by weight of panthenol, 0.5 part by weight of quaternary ammonium salt-87, 0.5 part by weight of xylitol-based glucoside, 1 part by weight of zinc gluconate and 0.5 part by weight of hydroxypropyl starch phosphate are weighed and put into an emulsifying pot, heated to 90 ℃, stirred and homogenized at 80 ℃ for 20 minutes until all components are uniformly dispersed, and the stirring speed is 120 revolutions per minute;
(3) Mixing and homogenizing: adding the dispersed oil phase into an emulsifying pot, stirring and homogenizing with the dispersed solvent for 5 minutes until no particles exist, preserving heat for 10 minutes, and then cooling;
(4) Adding the functional components: continuously stirring materials in an emulsifying pot, when the temperature is reduced to 45 ℃, weighing 3 parts by weight of hydrolyzed wheat protein, 1 part by weight of coconut oil, 1 part by weight of a calli extract of alpine leontopodium herb, 1 part by weight of keratin, 0.3 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerol, putting into the emulsifying pot, and stirring and mixing uniformly;
(5) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35deg.C to obtain hair care composition.
Example 2
(1) Dispersing an oil phase: weighing trideceth-6 3 parts by weight, cetostearyl alcohol 5 parts by weight, candelilla wax 3 parts by weight, tocopherol 2 parts by weight, wild soybean oil 7 parts by weight and rice bran oil 7 parts by weight, putting into an oil phase pot, stirring and dissolving uniformly, adding 75 parts of deionized water, heating to 90 ℃, and keeping stirring and homogenizing at 80 ℃ for 20 minutes until all the components are dispersed uniformly, wherein the stirring speed is 120 revolutions per minute;
(2) Dispersing solvent: weighing 1 part by weight of glycerin, 2 parts by weight of panthenol, 0.3 part by weight of behenyl trimethyl ammonium chloride, 0.3 part by weight of xylitol-based glucoside, 0.5 part by weight of zinc gluconate and 0.3 part by weight of hydroxypropyl starch phosphate, putting into an emulsifying pot, heating to 90 ℃, and stirring and homogenizing at 80 ℃ for 20 minutes until all components are uniformly dispersed, wherein the stirring speed is 120 revolutions per minute;
(3) Mixing and homogenizing: adding the dispersed oil phase into an emulsifying pot, stirring and homogenizing with the dispersed solvent for 5 minutes until no particles exist, preserving heat for 10 minutes, and then cooling;
(4) Adding the functional components: continuously stirring materials in an emulsifying pot, when the temperature is reduced to 45 ℃, weighing 5 parts by weight of hydrolyzed wheat protein, 2 parts by weight of argania spinosa kernel oil, 2 parts by weight of alpine leontopodium herb callus extract, 2 parts by weight of keratin and 1.5 parts by weight of phenoxyethanol, putting into the emulsifying pot, and stirring and mixing uniformly;
(5) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35deg.C to obtain hair care composition.
Example 3
(1) Dispersing an oil phase: weighing 2 parts by weight of C13-16 isoparaffin, 3 parts by weight of cetostearyl alcohol, 2 parts by weight of candelilla wax, 1 part by weight of tocopherol, 5 parts by weight of wild soybean oil and 5 parts by weight of rice bran oil, putting into an oil phase pot, stirring and dissolving uniformly, adding 68 parts of deionized water, heating to 90 ℃, and keeping stirring and homogenizing at 80 ℃ for 20 minutes until all the components are dispersed uniformly, wherein the stirring speed is 120 revolutions per minute;
(2) Dispersing solvent: 2 parts by weight of propylene glycol, 3 parts by weight of panthenol, 0.5 part by weight of quaternary ammonium salt-87, 0.5 part by weight of xylitol-based glucoside, 1 part by weight of zinc gluconate and 0.5 part by weight of hydroxypropyl starch phosphate are weighed and put into an emulsifying pot, heated to 90 ℃, stirred and homogenized at 80 ℃ for 20 minutes until all components are uniformly dispersed, and the stirring speed is 120 revolutions per minute;
(3) Mixing and homogenizing: adding the dispersed oil phase into an emulsifying pot, stirring and homogenizing with the dispersed solvent for 5 minutes until no particles exist, preserving heat for 10 minutes, and then cooling;
(4) Adding the functional components: continuously stirring materials in an emulsifying pot, when the temperature is reduced to 45 ℃, weighing 3 parts by weight of hydrolyzed wheat protein, 1 part by weight of hydrogenated avocado oil, 1 part by weight of alpine leontopodium herb callus extract, 1 part by weight of keratin, 0.3 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerol, putting into the emulsifying pot, and stirring and mixing uniformly;
(5) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35deg.C to obtain hair care composition.
Comparative example 1
(1) Dispersing an oil phase: 2 parts of sorbitan oleate, 1 part of cetostearyl alcohol, 0.5 part of candelilla wax, 1 part of tocopherol, 2 parts of wild soybean oil and 2 parts of rice bran oil are weighed, put into an oil phase pot, stirred and dissolved uniformly, 68 parts of deionized water is added, the temperature is raised to 90 ℃, and stirring and homogenizing are kept at 80 ℃ for 20 minutes until all components are dispersed uniformly, and the stirring speed is 120 revolutions per minute;
(2) Dispersing solvent: 2 parts by weight of propylene glycol, 3 parts by weight of panthenol, 0.5 part by weight of quaternary ammonium salt-87, 0.5 part by weight of xylitol-based glucoside, 1 part by weight of zinc gluconate and 0.5 part by weight of hydroxypropyl starch phosphate are weighed and put into an emulsifying pot, heated to 90 ℃, stirred and homogenized at 80 ℃ for 20 minutes until all components are uniformly dispersed, and the stirring speed is 120 revolutions per minute;
(3) Mixing and homogenizing: adding the dispersed oil phase into an emulsifying pot, stirring and homogenizing with the dispersed solvent for 5 minutes until no particles exist, preserving heat for 10 minutes, and then cooling;
(4) Adding the functional components: continuously stirring materials in an emulsifying pot, when the temperature is reduced to 45 ℃, weighing 3 parts by weight of hydrolyzed wheat protein, 1 part by weight of coconut oil, 1 part by weight of a calli extract of alpine leontopodium herb, 1 part by weight of keratin, 0.3 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerol, putting into the emulsifying pot, and stirring and mixing uniformly;
(5) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35deg.C to obtain hair care composition.
Comparative example 2
(1) Dispersing an oil phase: 2 parts of sorbitan oleate, 3 parts of cetostearyl alcohol, 2 parts of candelilla wax, 1 part of tocopherol, 5 parts of wild soybean oil and 5 parts of rice bran oil are weighed, put into an oil phase pot, stirred and dissolved uniformly, 90 parts of deionized water is added, the temperature is raised to 90 ℃, and stirring and homogenizing are kept at 80 ℃ for 20 minutes until all components are dispersed uniformly, and the stirring speed is 120 revolutions per minute;
(2) Dispersing solvent: weighing 5 parts by weight of propylene glycol, 3 parts by weight of panthenol, 0.5 part by weight of quaternary ammonium salt-87, 0.5 part by weight of xylitol-based glucoside, 1 part by weight of zinc gluconate and 0.5 part by weight of hydroxypropyl starch phosphate, putting into an emulsifying pot, heating to 90 ℃, and stirring and homogenizing at 80 ℃ for 20 minutes until all components are uniformly dispersed, wherein the stirring speed is 120 revolutions per minute;
(3) Mixing and homogenizing: adding the dispersed oil phase into an emulsifying pot, stirring and homogenizing with the dispersed solvent for 5 minutes until no particles exist, preserving heat for 10 minutes, and then cooling;
(4) Adding the functional components: continuously stirring materials in an emulsifying pot, when the temperature is reduced to 45 ℃, weighing 3 parts by weight of hydrolyzed wheat protein, 1 part by weight of coconut oil, 1 part by weight of a calli extract of alpine leontopodium herb, 1 part by weight of keratin, 0.3 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerol, putting into the emulsifying pot, and stirring and mixing uniformly;
(5) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35deg.C to obtain hair care composition.
Comparative example 3
(1) Dispersing an oil phase: 2 parts of sorbitan oleate, 7 parts of cetostearyl alcohol, 5 parts of candelilla wax, 1 part of tocopherol, 10 parts of wild soybean oil and 10 parts of rice bran oil are weighed, put into an oil phase pot, stirred and dissolved uniformly, 68 parts of deionized water is added, the temperature is raised to 90 ℃, and stirring and homogenizing are kept at 80 ℃ for 20 minutes until all components are dispersed uniformly, and the stirring speed is 120 revolutions per minute;
(2) Dispersing solvent: 2 parts by weight of propylene glycol, 3 parts by weight of panthenol, 0.5 part by weight of quaternary ammonium salt-87, 0.5 part by weight of xylitol-based glucoside, 1 part by weight of zinc gluconate and 0.5 part by weight of hydroxypropyl starch phosphate are weighed and put into an emulsifying pot, heated to 90 ℃, stirred and homogenized at 80 ℃ for 20 minutes until all components are uniformly dispersed, and the stirring speed is 120 revolutions per minute;
(3) Mixing and homogenizing: adding the dispersed oil phase into an emulsifying pot, stirring and homogenizing with the dispersed solvent for 5 minutes until no particles exist, preserving heat for 10 minutes, and then cooling;
(4) Adding the functional components: continuously stirring materials in an emulsifying pot, when the temperature is reduced to 45 ℃, weighing 3 parts by weight of hydrolyzed wheat protein, 1 part by weight of coconut oil, 1 part by weight of a calli extract of alpine leontopodium herb, 1 part by weight of keratin, 0.3 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerol, putting into the emulsifying pot, and stirring and mixing uniformly;
(5) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35deg.C to obtain hair care composition.
Comparative example 4
(1) Dispersing an oil phase: 2 parts of sorbitan oleate, 3 parts of cetostearyl alcohol, 2 parts of candelilla wax, 1 part of tocopherol, 5 parts of wild soybean oil and 5 parts of rice bran oil are weighed, put into an oil phase pot, stirred and dissolved uniformly, 45 parts of deionized water are added, the temperature is raised to 90 ℃, and stirring and homogenizing are kept at 80 ℃ for 20 minutes until all components are dispersed uniformly, and the stirring speed is 120 revolutions per minute;
(2) Dispersing solvent: weighing 0.5 part by weight of propylene glycol, 3 parts by weight of panthenol, 0.5 part by weight of quaternary ammonium salt-87, 0.5 part by weight of xylitol-based glucoside, 1 part by weight of zinc gluconate and 0.5 part by weight of hydroxypropyl starch phosphate, putting into an emulsifying pot, heating to 90 ℃, and stirring and homogenizing at 80 ℃ for 20 minutes until all components are uniformly dispersed, wherein the stirring speed is 120 revolutions per minute;
(3) Mixing and homogenizing: adding the dispersed oil phase into an emulsifying pot, stirring and homogenizing with the dispersed solvent for 5 minutes until no particles exist, preserving heat for 10 minutes, and then cooling;
(4) Adding the functional components: continuously stirring materials in an emulsifying pot, when the temperature is reduced to 45 ℃, weighing 3 parts by weight of hydrolyzed wheat protein, 1 part by weight of coconut oil, 1 part by weight of a calli extract of alpine leontopodium herb, 1 part by weight of keratin, 0.3 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerol, putting into the emulsifying pot, and stirring and mixing uniformly;
(5) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35deg.C to obtain hair care composition.
Comparative example 5
(1) Dispersing an oil phase: weighing 5 parts by weight of sorbitan oleate, 3 parts by weight of cetostearyl alcohol, 2 parts by weight of candelilla wax, 1 part by weight of tocopherol, 5 parts by weight of wild soybean oil and 5 parts by weight of rice bran oil, putting into an oil phase pot, stirring and dissolving uniformly, adding 68 parts of deionized water, heating to 90 ℃, and keeping stirring and homogenizing at 80 ℃ for 20 minutes until all components are dispersed uniformly, wherein the stirring speed is 120 revolutions per minute;
(2) Dispersing solvent: 2 parts by weight of propylene glycol, 3 parts by weight of panthenol, 0.5 part by weight of quaternary ammonium salt-87, 0.5 part by weight of xylitol-based glucoside, 1 part by weight of zinc gluconate and 0.5 part by weight of hydroxypropyl starch phosphate are weighed and put into an emulsifying pot, heated to 90 ℃, stirred and homogenized at 80 ℃ for 20 minutes until all components are uniformly dispersed, and the stirring speed is 120 revolutions per minute;
(3) Mixing and homogenizing: adding the dispersed oil phase into an emulsifying pot, stirring and homogenizing with the dispersed solvent for 5 minutes until no particles exist, preserving heat for 10 minutes, and then cooling;
(4) Adding the functional components: continuously stirring materials in an emulsifying pot, when the temperature is reduced to 45 ℃, weighing 3 parts by weight of hydrolyzed wheat protein, 1 part by weight of coconut oil, 1 part by weight of a calli extract of alpine leontopodium herb, 1 part by weight of keratin, 0.3 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerol, putting into the emulsifying pot, and stirring and mixing uniformly;
(5) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35deg.C to obtain hair care composition.
Comparative example 6
(1) Dispersing an oil phase: weighing 0.5 part by weight of sorbitan oleate, 3 parts by weight of cetostearyl alcohol, 2 parts by weight of candelilla wax, 1 part by weight of tocopherol, 5 parts by weight of wild soybean oil and 5 parts by weight of rice bran oil, putting into an oil phase pot, stirring and dissolving uniformly, adding 68 parts of deionized water, heating to 90 ℃, and keeping stirring and homogenizing at 80 ℃ for 20 minutes until all components are dispersed uniformly, wherein the stirring speed is 120 revolutions per minute;
(2) Dispersing solvent: 2 parts by weight of propylene glycol, 3 parts by weight of panthenol, 0.5 part by weight of quaternary ammonium salt-87, 0.5 part by weight of xylitol-based glucoside, 1 part by weight of zinc gluconate and 0.5 part by weight of hydroxypropyl starch phosphate are weighed and put into an emulsifying pot, heated to 90 ℃, stirred and homogenized at 80 ℃ for 20 minutes until all components are uniformly dispersed, and the stirring speed is 120 revolutions per minute;
(3) Mixing and homogenizing: adding the dispersed oil phase into an emulsifying pot, stirring and homogenizing with the dispersed solvent for 5 minutes until no particles exist, preserving heat for 10 minutes, and then cooling;
(4) Adding the functional components: continuously stirring materials in an emulsifying pot, when the temperature is reduced to 45 ℃, weighing 3 parts by weight of hydrolyzed wheat protein, 1 part by weight of coconut oil, 1 part by weight of a calli extract of alpine leontopodium herb, 1 part by weight of keratin, 0.3 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerol, putting into the emulsifying pot, and stirring and mixing uniformly;
(5) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35deg.C to obtain hair care composition.
Comparative example 7
(1) Dispersing an oil phase: 2 parts of sorbitan oleate, 3 parts of cetostearyl alcohol, 2 parts of candelilla wax, 1 part of tocopherol, 5 parts of wild soybean oil and 5 parts of rice bran oil are weighed, put into an oil phase pot, stirred and dissolved uniformly, 68 parts of deionized water is added, the temperature is raised to 90 ℃, and stirring and homogenizing are kept at 80 ℃ for 20 minutes until all components are dispersed uniformly, and the stirring speed is 120 revolutions per minute;
(2) Dispersing solvent: 2 parts by weight of propylene glycol, 3 parts by weight of panthenol, 0.5 part by weight of quaternary ammonium salt-87, 0.5 part by weight of xylitol-based glucoside, 1 part by weight of zinc gluconate and 0.5 part by weight of hydroxypropyl starch phosphate are weighed and put into an emulsifying pot, heated to 90 ℃, stirred and homogenized at 80 ℃ for 20 minutes until all components are uniformly dispersed, and the stirring speed is 120 revolutions per minute;
(3) Mixing and homogenizing: adding the dispersed oil phase into an emulsifying pot, stirring and homogenizing with the dispersed solvent for 5 minutes until no particles exist, preserving heat for 10 minutes, and then cooling;
(4) Adding the functional components: continuously stirring materials in an emulsifying pot, when the temperature is reduced to 45 ℃, weighing 4 parts by weight of hydrolyzed wheat protein, 1 part by weight of coconut oil, 1 part by weight of a calli extract of alpine leontopodium herb, 0.3 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerol, putting into the emulsifying pot, and uniformly stirring and mixing, wherein the formula has no keratin;
(5) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35deg.C to obtain hair care composition.
Comparative example 8
(1) Dispersing an oil phase: 2 parts of sorbitan oleate, 3 parts of cetostearyl alcohol, 2 parts of candelilla wax, 1 part of tocopherol and 10 parts of wild soybean oil are weighed, put into an oil phase pot, stirred and dissolved uniformly, 68 parts of deionized water is added, the temperature is raised to 90 ℃, stirring and homogenizing are kept at 80 ℃ for 20 minutes until all components are dispersed uniformly, and the stirring speed is 120 r/min, so that the formula has no rice bran oil;
(2) Dispersing solvent: 2 parts by weight of propylene glycol, 3 parts by weight of panthenol, 0.5 part by weight of quaternary ammonium salt-87, 0.5 part by weight of xylitol-based glucoside, 1 part by weight of zinc gluconate and 0.5 part by weight of hydroxypropyl starch phosphate are weighed and put into an emulsifying pot, heated to 90 ℃, stirred and homogenized at 80 ℃ for 20 minutes until all components are uniformly dispersed, and the stirring speed is 120 revolutions per minute;
(3) Mixing and homogenizing: adding the dispersed oil phase into an emulsifying pot, stirring and homogenizing with the dispersed solvent for 5 minutes until no particles exist, preserving heat for 10 minutes, and then cooling;
(4) Adding the functional components: continuously stirring materials in an emulsifying pot, when the temperature is reduced to 45 ℃, weighing 3 parts by weight of hydrolyzed wheat protein, 1 part by weight of coconut oil, 1 part by weight of a calli extract of alpine leontopodium herb, 1 part by weight of keratin, 0.3 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerol, putting into the emulsifying pot, and stirring and mixing uniformly;
(5) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35deg.C to obtain hair care composition.
Comparative example 9
(1) Dispersing an oil phase: 2 parts of sorbitan oleate, 3 parts of cetostearyl alcohol, 2 parts of candelilla wax, 1 part of tocopherol, 5 parts of wild soybean oil and 5 parts of rice bran oil are weighed, put into an oil phase pot, stirred and dissolved uniformly, 68 parts of deionized water is added, the temperature is raised to 90 ℃, and stirring and homogenizing are kept at 80 ℃ for 20 minutes until all components are dispersed uniformly, and the stirring speed is 120 revolutions per minute;
(2) Dispersing solvent: 2 parts by weight of propylene glycol, 0.5 part by weight of quaternary ammonium salt-87, 0.5 part by weight of xylitol-based glucoside, 1 part by weight of zinc gluconate and 0.5 part by weight of hydroxypropyl starch phosphate are weighed and put into an emulsifying pot, the temperature is raised to 90 ℃, stirring and homogenizing are kept at 80 ℃ for 20 minutes until all components are uniformly dispersed, and the stirring rotation speed is 120 r/min, so that the formula has no panthenol;
(3) Mixing and homogenizing: adding the dispersed oil phase into an emulsifying pot, stirring and homogenizing with the dispersed solvent for 5 minutes until no particles exist, preserving heat for 10 minutes, and then cooling;
(4) Adding the functional components: continuously stirring materials in an emulsifying pot, when the temperature is reduced to 45 ℃, weighing 3 parts by weight of hydrolyzed wheat protein, 1 part by weight of coconut oil, 1 part by weight of a calli extract of alpine leontopodium herb, 1 part by weight of keratin, 0.3 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerol, putting into the emulsifying pot, and stirring and mixing uniformly;
(5) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35deg.C to obtain hair care composition.
Comparative example 10
(1) Dispersing an oil phase: 2 parts of sorbitan oleate, 3 parts of cetostearyl alcohol, 2 parts of candelilla wax, 1 part of tocopherol, 5 parts of wild soybean oil and 5 parts of rice bran oil are weighed, put into an oil phase pot, stirred and dissolved uniformly, 68 parts of deionized water is added, the temperature is raised to 90 ℃, and stirring and homogenizing are kept at 80 ℃ for 20 minutes until all components are dispersed uniformly, and the stirring speed is 120 revolutions per minute;
(2) Dispersing solvent: 2 parts by weight of propylene glycol, 3 parts by weight of panthenol, 0.5 part by weight of quaternary ammonium salt-87, 0.5 part by weight of xylitol-based glucoside, 1 part by weight of zinc gluconate and 0.5 part by weight of hydroxypropyl starch phosphate are weighed and put into an emulsifying pot, heated to 90 ℃, stirred and homogenized at 80 ℃ for 20 minutes until all components are uniformly dispersed, and the stirring speed is 120 revolutions per minute;
(3) Mixing and homogenizing: adding the dispersed oil phase into an emulsifying pot, stirring and homogenizing with the dispersed solvent for 5 minutes until no particles exist, preserving heat for 10 minutes, and then cooling;
(4) Adding the functional components: continuously stirring materials in an emulsifying pot, and when the temperature is reduced to 45 ℃, weighing 1 part by weight of coconut oil, 1 part by weight of a calli extract of alpine leontopodium herb, 4 parts by weight of keratin, 0.3 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerol, putting the materials into the emulsifying pot, and stirring and mixing the materials uniformly, wherein the formula has no hydrolyzed wheat protein;
(5) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35deg.C to obtain hair care composition.
Comparative example 11
(1) Dispersing an oil phase: 2 parts of sorbitan oleate, 3 parts of cetostearyl alcohol, 2 parts of candelilla wax, 1 part of tocopherol, 5 parts of wild soybean oil and 5 parts of rice bran oil are weighed, put into an oil phase pot, stirred and dissolved uniformly, 68 parts of deionized water is added, the temperature is raised to 90 ℃, and stirring and homogenizing are kept at 80 ℃ for 20 minutes until all components are dispersed uniformly, and the stirring speed is 120 revolutions per minute;
(2) Dispersing solvent: 2 parts by weight of propylene glycol, 3 parts by weight of panthenol, 0.5 part by weight of quaternary ammonium salt-87, 0.5 part by weight of xylitol-based glucoside, 1 part by weight of zinc gluconate and 0.5 part by weight of hydroxypropyl starch phosphate are weighed and put into an emulsifying pot, heated to 90 ℃, stirred and homogenized at 80 ℃ for 20 minutes until all components are uniformly dispersed, and the stirring speed is 120 revolutions per minute;
(3) Mixing and homogenizing: adding the dispersed oil phase into an emulsifying pot, stirring and homogenizing with the dispersed solvent for 5 minutes until no particles exist, preserving heat for 10 minutes, and then cooling;
(4) Adding the functional components: continuously stirring materials in an emulsifying pot, and when the temperature is reduced to 45 ℃, weighing 3 parts by weight of hydrolyzed wheat protein, 1 part by weight of coconut oil, 1 part by weight of keratin, 0.3 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerol, putting the materials into the emulsifying pot, and stirring and mixing uniformly;
(5) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35deg.C to obtain hair care composition.
Comparative example 12
(1) Dispersing an oil phase: 2 parts of sorbitan oleate, 3 parts of cetostearyl alcohol, 2 parts of candelilla wax, 1 part of tocopherol, 5 parts of wild soybean oil and 5 parts of rice bran oil are weighed, put into an oil phase pot, stirred and dissolved uniformly, 68 parts of deionized water is added, the temperature is raised to 90 ℃, and stirring and homogenizing are kept at 80 ℃ for 20 minutes until all components are dispersed uniformly, and the stirring speed is 120 revolutions per minute;
(2) Dispersing solvent: 2 parts of propylene glycol, 3 parts of panthenol, 0.5 part of quaternary ammonium salt-87, 1 part of zinc gluconate and 0.5 part of hydroxypropyl starch phosphate are weighed and put into an emulsifying pot, the temperature is raised to 90 ℃, and stirring and homogenizing are kept at 80 ℃ for 20 minutes until all components are uniformly dispersed, and the stirring rotating speed is 120 revolutions per minute, so that the formula has no humectant;
(3) Mixing and homogenizing: adding the dispersed oil phase into an emulsifying pot, stirring and homogenizing with the dispersed solvent for 5 minutes until no particles exist, preserving heat for 10 minutes, and then cooling;
(4) Adding the functional components: continuously stirring materials in an emulsifying pot, when the temperature is reduced to 45 ℃, weighing 3 parts by weight of hydrolyzed wheat protein, 1 part by weight of coconut oil, 1 part by weight of a calli extract of alpine leontopodium herb, 1 part by weight of keratin, 0.3 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerol, putting into the emulsifying pot, and stirring and mixing uniformly;
(5) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35deg.C to obtain hair care composition.
Comparative example 13
(1) Dispersing an oil phase: 2 parts of sorbitan oleate, 3 parts of cetostearyl alcohol, 2 parts of candelilla wax, 1 part of tocopherol, 5 parts of wild soybean oil and 6 parts of rice bran oil are weighed, put into an oil phase pot, stirred and dissolved uniformly, 68 parts of deionized water is added, the temperature is raised to 90 ℃, and stirring and homogenizing are kept at 80 ℃ for 20 minutes until all components are dispersed uniformly, and the stirring speed is 120 revolutions per minute;
(2) Dispersing solvent: 2 parts by weight of propylene glycol, 3 parts by weight of panthenol, 0.5 part by weight of quaternary ammonium salt-87, 0.5 part by weight of xylitol-based glucoside, 1 part by weight of zinc gluconate and 0.5 part by weight of hydroxypropyl starch phosphate are weighed and put into an emulsifying pot, heated to 90 ℃, stirred and homogenized at 80 ℃ for 20 minutes until all components are uniformly dispersed, and the stirring speed is 120 revolutions per minute;
(3) Mixing and homogenizing: adding the dispersed oil phase into an emulsifying pot, stirring and homogenizing with the dispersed solvent for 5 minutes until no particles exist, preserving heat for 10 minutes, and then cooling;
(4) Adding the functional components: continuously stirring materials in an emulsifying pot, when the temperature is reduced to 45 ℃, weighing 3 parts by weight of hydrolyzed wheat protein, 1 part by weight of a calli extract of alpine leontopodium herb, 1 part by weight of keratin, 0.3 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerol, putting into the emulsifying pot, stirring and mixing uniformly, wherein the formula is free of reactive grease;
(5) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35deg.C to obtain hair care composition.
Performance testing
(1) Sensory index
The hair care compositions prepared in examples 1 to 3 and comparative examples 1 to 13 were subjected to sensory comparison with a standard at room temperature, visual appearance and color, and smell fragrance.
Table 1 sensory indices of hair care compositions obtained by the various preparation processes
As shown in the above table, the hair care compositions prepared in each example and comparative example have similar sensory indexes and are uniform white paste with floral fragrance.
(2) Stability of
The hair care compositions prepared in each example and comparative example were respectively placed in a constant temperature refrigerator of-18 to-10 ℃ and an electrothermal constant temperature blast drying oven of 48+ -1 ℃ and taken out after 48 hours, and the room temperature was restored and the layering condition was observed.
TABLE 2 stability of hair care compositions obtained by different preparation processes
Stability affects the shelf life of hair care compositions in different environments. As shown in the above table, the hair care compositions prepared in examples 1 to 3 and comparative examples 7 to 13 were not layered at high and low temperatures; comparative examples 1 to 6 show delamination after low temperature treatment and high temperature treatment. The reason is presumed to be that: the oil-water ratio of comparative examples 1 and 2 is lower; the oil-water ratio of comparative examples 3 and 4 is higher; comparative example 5 excessive emulsifier; comparative example 6 has too little emulsifier.
(3) Viscosity of the mixture
The viscosity of the hair care compositions prepared in each example and comparative example was measured at 25℃according to the specification of national standard GB/T15357, and 20000 to 30000 was defined as a pass interval.
TABLE 3 viscosity of hair care compositions obtained by different preparation processes
Viscosity affects the use feeling of the hair care composition, and the hair is not easy to adhere due to the small viscosity; the viscosity is too small, and the cleaning is difficult. As shown in the above table, the viscosity of the hair care compositions prepared in examples 1 to 3 and comparative examples 7 to 13 was 25000 to 27000, the viscosity of the hair care compositions prepared in comparative examples 1 and 2 was less than 20000, the viscosity of the hair care compositions prepared in comparative examples 3, 4 and 5 was more than 30000, and the viscosity of the hair care composition prepared in comparative example 6 was slightly more than 20000. The test results show that the hair care compositions prepared in comparative examples 1 and 2 are less likely to adhere to hair during use than other preparation processes; the hair care compositions prepared in comparative examples 3, 4 and 5 are not easy to clean in use; in a hair care composition of acceptable viscosity, the product of comparative example 6 is relatively thin.
(4) Centrifugal test
The hair care compositions prepared in each example and comparative example were subjected to centrifugal test according to the specification of national standard GB/T29665, and were not layered after rotating for 30 minutes at a speed of 3000r/min, and were regarded as acceptable.
Table 4 results of centrifugal test on hair care compositions obtained by different preparation processes
/>
The centrifugal separation experiment is a key means for checking the stability and the shelf life of the cream emulsion cosmetics. As shown in the above table, the hair care compositions prepared in examples 1 to 3 and comparative examples 7 to 13 were not layered after centrifugation, whereas the hair care compositions prepared in comparative examples 1 to 6 were layered after centrifugation. The above results demonstrate that the hair care compositions prepared in comparative examples 1-6 have poor stability and long shelf life.
(5) Gloss and smoothness Effect evaluation
The tresses of the human hair used in the experimental hair care products were taken, the single tresses of hair were 40 cm long and 30 gram weight. The hair tresses were tested for gloss (pre-application gloss) using a skin gloss test probe, then rinsed with water for 10 seconds to wet, and the hair care compositions prepared in each of the examples and comparative examples were applied at 0.4 gram of test product per 1 gram of hair. After standing for 10 seconds, washing for 30 seconds, and drying by a blower at 50 ℃; repeating for three times, filtering out more water by using a finger seam until no water drops drop at the hair tips before drying for the last time, and then performing a carding performance test (wet hair carding performance); after blow-drying, a combing performance test (dry combing performance) was performed in the same manner, the glossiness (glossiness after use) was measured, and the glossiness improvement percentage was calculated. The same tress without applying the hair care composition was also set to measure gloss and combing performance as a blank.
The combing performance of wet hair and dry hair is tested by a tension meter, and the whole hair bundle is fixed on the combing meter for combing performance test. Each hair strand was tested 6 times and the 3-strand hair strand test was repeated. The calculation formula of the percentage of gloss improvement is: (post-use gloss-before-use gloss)/pre-use gloss x 100%.
Data were statistically processed by SPSS26 software and differences between groups were compared using one-way anova with p < 0.05 as significant differences.
TABLE 5 combing work and percent gloss improvement (mean+ -SD) for hair care compositions prepared by different preparation processes
| Preparation process | Wet hair combing work/J | Comb work/J | Percent gloss improvement (%) |
| Blank group | 6.57±0.93 | 2.49±0.73 | -1.24±0.83 |
| Example 1 | 3.15±0.54* | 0.65±0.26* | 50.95±5.52* |
| Example 2 | 3.74±0.45* | 0.97±0.49* | 49.86±5.17* |
| Example 3 | 3.86±0.49* | 1.12±0.51* | 48.62±5.99* |
| Comparative example 1 | 4.26±0.76* | 1.25±0.33* | 42.21±4.83* |
| Comparative example 2 | 4.43±0.68 | 1.28±0.47* | 40.19±5.05* |
| Comparative example 3 | 4.35±0.62* | 1.32±0.38* | 41.32±6.22* |
| Comparative example 4 | 4.21±0.53* | 1.30±0.41* | 39.98±5.82* |
| Comparative example 5 | 4.30±0.59* | 1.34±0.36* | 40.56±6.45* |
| Comparative example 6 | 4.45±0.74 | 1.29±0.30* | 39.40±4.40* |
| Comparative example 7 | 3.83±0.61* | 1.39±0.45* | 22.19±3.94* |
| Comparative example 8 | 5.32±0.70 | 1.82±0.61 | 42.80±5.69* |
| Comparative example 9 | 3.66±0.57* | 1.36±0.42* | 39.09±6.01* |
| Comparative example 10 | 5.48±0.67 | 1.79±0.66 | 40.29±6.63* |
| Comparative example 11 | 3.71±0.73* | 1.40±0.59* | 40.78±6.32* |
| Comparative example 12 | 5.55±0.82 | 1.85±0.57 | 39.36±5.36* |
| Comparative example 13 | 3.94±0.68* | 1.38±0.43* | 42.10±5.90* |
". Times." indicates that p < 0.05 compared to the blank.
The combing test is the best method for judging the smooth effect of the hair care composition, and the smaller the combing work is, the smaller the acting force between the hair and the comb is, and the smoother the hair is. As shown in the above table, in the wet combing experiments, the combing work of each group of hair strands using the hair care composition was reduced compared with that of the blank group, and examples 1 to 3, comparative examples 1 to 5, 7, 9, 11, 13 were significantly different; in the dry combing experiments, the combing work was reduced for each group using the hair care composition compared to the blank group, and the remaining groups were significantly different from the blank group except for comparative examples 8, 10, and 12. In addition, in both wet and dry combing experiments, the combing work was less for each example group than for each control group. The above results demonstrate that the hair care compositions prepared in examples 1-3 provide better smoothness, which is achieved by the combination of rice bran oil, panthenol, hydrolyzed wheat protein, humectants and other ingredients.
The percent gloss improvement reflects the lightening effect of the hair care composition. As shown in the above table, the gloss of each group of hair strands using the hair care composition was significantly improved as compared to the blank group; the percent improvement in hair strand gloss for each comparative example group was less than for each experimental group, wherein the range of improvement in hair strand gloss for comparative example 7 group was significantly less than for the other examples and comparative example groups. The above results demonstrate that the hair care compositions prepared in examples 1-3 provide better lightening results, which are predominantly provided by keratin.
(6) Color protection performance
Pretreatment: selecting 17 hair bundles (effective hair length is 16.5 CM, effective hair width is 3.6 CM, and hair length is 4.7 g/hair bundle) of the same batch, dyeing the hair bundles by using the same hair dye, washing, naturally airing, balancing to be consistent with indoor temperature and humidity, spreading the hair bundles on a white board, ensuring the light tightness of the hair bundles, reading Lab values of the hair bundles by using a color difference meter (CM-2006 d, meida), selecting 15 points on different positions of each hair bundle, reading, and averaging L0, a0 and b0.
Washing: soaking each group of hair bundles with L0, a0 and b0 measured, washing by using clean shampoo, giving the hair care compositions prepared in each example and comparative example according to the condition that 0.4g of hair care composition is smeared on every 1g of hair after washing, standing for 10 seconds, washing for 30 seconds, circulating the washing-smeared hair care compositions for 8 times, naturally airing, balancing to be consistent with indoor temperature and humidity, testing Lab value, and calculating dE value; de=l0, a0, b0-L, a, b. The blank was subjected to only a dyeing-washing treatment without applying a hair care composition.
TABLE 6 results of Hair Condition test (mean+ -SD) of hair care compositions obtained by different preparation techniques
| Preparation process | dE value |
| Blank group | 12.24±0.43 |
| Example 1 | 6.06±0.21* |
| Example 2 | 6.28±0.31* |
| Example 3 | 6.15±0.28* |
| Comparative example 1 | 7.89±0.30* |
| Comparative example 2 | 8.85±0.38 |
| Comparative example 3 | 8.20±0.43 |
| Comparative example 4 | 8.47±0.35 |
| Comparative example 5 | 8.20±0.42 |
| Comparative example 6 | 8.70±0.41 |
| Comparative example 7 | 7.87±0.46* |
| Comparative example 8 | 8.12±0.32 |
| Comparative example 9 | 7.50±0.34* |
| Comparative example 10 | 8.96±0.48 |
| Comparative example 11 | 10.71±0.43 |
| Comparative example 12 | 8.65±0.32 |
| Comparative example 13 | 10.56±0.48 |
". Times." indicates that p < 0.05 compared to the blank.
The dE value (i.e., color difference before and after the test) reflects the degree of hair discoloration, the greater the dE value, the more severe the discoloration. As shown in the above table, the color of the blank hair bundles becomes obviously lighter after multiple times of washing; each group using the hair care composition had a reduced value of hair strand dE compared to the blank, wherein examples 1-3, comparative examples 1, 7, 9, and the blank had significant differences; in each group using the hair care composition, examples 1-3 had a dE value less than that of each control group. The results show that the hair care compositions prepared in examples 1-3 have better color protection performance, which is mainly brought by the combination of the alpine leontopodium herb callus extract, the functional grease and other components.
Although embodiments of the present application have been shown and described above, it is understood that the above embodiments are exemplary and not to be construed as limiting the application, and that variations, modifications, alternatives, and variations may be made to the above embodiments by one of ordinary skill in the art within the scope of the application.
Claims (6)
1. A hair care composition with color locking, brightening, softening and repairing effects comprises the following components in parts by weight: 0.5 to 2 parts of zinc gluconate, 2 to 5 parts of fatty alcohol, 0.3 to 1 part of hair conditioner, 1 to 3 parts of solvent, 0.3 to 1 part of thickener, 1 to 3 parts of candelilla wax, 0.5 to 2 parts of tocopherol, 3 to 7 parts of wild soybean oil, 3 to 7 parts of rice bran oil, 2 to 5 parts of panthenol, 2 to 5 parts of hydrolyzed wheat protein, 0.5 to 2 parts of functional grease, 0.5 to 2 parts of alpine leontopodium herb callus extract, 0.3 to 1 part of humectant, 1 to 3 parts of emulsifier, 0.5 to 2 parts of keratin, 0.5 to 1.5 parts of preservative and 55 to 75 parts of deionized water;
the fatty alcohol is cetostearyl alcohol;
the hair conditioner is quaternary ammonium salt-87 and/or behenyl trimethyl ammonium chloride;
the solvent is propylene glycol and/or glycerol;
the thickener is hydroxypropyl starch phosphate and/or cetostearyl alcohol;
the functional grease is one or more of coconut oil, hydrogenated avocado oil, argania spinosa kernel oil and wheat germ oil;
the humectant is xylitol-based glucoside and/or sorbitan laurate;
the emulsifier is one or more of sorbitan oleate, polyquaternium-37, C13-16 isoparaffin and tridecyl alcohol polyether-6;
the preservative is one or more of phenoxyethanol and ethylhexyl glycerol.
2. The hair care composition according to claim 1, comprising the following components in parts by weight: 1 part of zinc gluconate, 3 parts of fatty alcohol, 0.5 part of hair conditioner, 2 parts of solvent, 0.5 part of thickener, 2 parts of candelilla wax, 1 part of tocopherol, 5 parts of wild soybean oil, 5 parts of rice bran oil, 3 parts of panthenol, 3 parts of hydrolyzed wheat protein, 1 part of functional grease, 1 part of alpine leontopodium herb callus extract, 0.5 part of humectant, 2 parts of emulsifier, 1 part of keratin, 0.8 part of preservative and 68 parts of deionized water.
3. A method of preparing the hair care composition of claim 1 or 2, comprising the steps of:
s1, adding an emulsifying agent, fatty alcohol, candelilla wax, tocopherol, wild soybean oil and rice chaff oil into an oil phase pot, stirring and dissolving uniformly, adding deionized water, stirring and homogenizing until all components are dispersed uniformly;
s2, adding the solvent, the panthenol, the hair conditioner, the humectant, the zinc gluconate and the thickener into an emulsifying pot, stirring and homogenizing until all the components are uniformly dispersed;
s3, putting the mixture obtained in the step S1 into an emulsifying pot, stirring and homogenizing the mixture with the mixture obtained in the step S2 until no particles exist, and preserving heat;
s4, continuously stirring the mixture obtained in the step S3, and when the temperature is reduced to 45 ℃, adding hydrolyzed wheat protein, functional grease, alpine leontopodium herb callus extract, keratin and preservative, and uniformly stirring and mixing;
s5, continuously stirring the mixture obtained in the step S4, and cooling to 35 ℃ to obtain the hair care composition.
4. The method according to claim 3, wherein in the step S1, the homogenizing temperature is 80-90 ℃, the stirring speed is 120 rpm, and the stirring time is 20 minutes.
5. The method according to claim 3, wherein in the step S2, the homogenizing temperature is 80-90 ℃, the stirring speed is 120 rpm, and the stirring time is 20 minutes.
6. The method according to claim 3, wherein in the step S3, the heat-retaining period is 10 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211459179.8A CN115670981B (en) | 2022-11-17 | 2022-11-17 | Hair care composition with color locking, brightening, softening and repairing effects and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211459179.8A CN115670981B (en) | 2022-11-17 | 2022-11-17 | Hair care composition with color locking, brightening, softening and repairing effects and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN115670981A CN115670981A (en) | 2023-02-03 |
| CN115670981B true CN115670981B (en) | 2024-04-12 |
Family
ID=85054625
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202211459179.8A Active CN115670981B (en) | 2022-11-17 | 2022-11-17 | Hair care composition with color locking, brightening, softening and repairing effects and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN115670981B (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112587424A (en) * | 2020-12-18 | 2021-04-02 | 珠海伊斯佳科技股份有限公司 | A hair composition with effects of protecting color and hair, and its preparation method |
| CN113908095A (en) * | 2021-11-09 | 2022-01-11 | 上海蜂花日用品有限公司 | Oil-control moisturizing hair composition containing double proteins |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20220354768A1 (en) * | 2021-04-29 | 2022-11-10 | L’Oreal | Hair care compositions |
-
2022
- 2022-11-17 CN CN202211459179.8A patent/CN115670981B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112587424A (en) * | 2020-12-18 | 2021-04-02 | 珠海伊斯佳科技股份有限公司 | A hair composition with effects of protecting color and hair, and its preparation method |
| CN113908095A (en) * | 2021-11-09 | 2022-01-11 | 上海蜂花日用品有限公司 | Oil-control moisturizing hair composition containing double proteins |
Also Published As
| Publication number | Publication date |
|---|---|
| CN115670981A (en) | 2023-02-03 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN111529466B (en) | Washing-free protein nourishing hair-moistening cream and preparation method thereof | |
| JP5725653B2 (en) | Hair rinse composition | |
| JP6184708B2 (en) | Perm solution and hair conditioner | |
| CN111631983A (en) | Softening and repairing hair care composition and application thereof | |
| CN114376925A (en) | Plant loose powder and preparation method thereof | |
| EP0681826A2 (en) | Heat-safe hair preparation and method of using same | |
| CN115670981B (en) | Hair care composition with color locking, brightening, softening and repairing effects and preparation method thereof | |
| CN110876697A (en) | Hair care composition with heat protection effect and preparation method thereof | |
| JP2014043426A (en) | Hair cosmetics | |
| CN111449991B (en) | Hair repair composition, preparation method and application thereof | |
| KR20120042281A (en) | Hair cosmetic composition | |
| KR20150146011A (en) | Cosmetic composition for preventing hair damage | |
| CN114224785A (en) | Organic silicon elastomer composition and preparation method and application thereof | |
| CN113876686A (en) | Moistening and repairing hair conditioner and preparation method thereof | |
| JP4136965B2 (en) | Hair cosmetics | |
| CN113693953A (en) | Acidic reverse-film hair-perming and hair-caring integrated hair perming cream and preparation method thereof | |
| CN109689025A (en) | Hair oil composition containing rose hip oil for hair care and its application | |
| CN112168732A (en) | Matte velvet lipstick and preparation method thereof | |
| KR101131706B1 (en) | Hair cosmetic composition | |
| JP2009161519A (en) | Cosmetic base material and hair cosmetic | |
| KR101145589B1 (en) | Hair Cosmetic Composition | |
| CN114028276B (en) | Hair care composition with multiple-effect repairing effect and application thereof | |
| CN109091435A (en) | Raw shining face frost of member and preparation method thereof | |
| CN116196236B (en) | Hairline toughening agent capable of resisting washing and application thereof | |
| KR101664333B1 (en) | Cosmetic composition for hair styling using reducing substance and marine collagen peptide |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |