CN115634499B - Rotational flow shearing slag-removing type solid-liquid separation device and use method thereof - Google Patents

Rotational flow shearing slag-removing type solid-liquid separation device and use method thereof Download PDF

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Publication number
CN115634499B
CN115634499B CN202211287344.6A CN202211287344A CN115634499B CN 115634499 B CN115634499 B CN 115634499B CN 202211287344 A CN202211287344 A CN 202211287344A CN 115634499 B CN115634499 B CN 115634499B
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filter
guide pipe
flow guide
filter assembly
cavity
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CN115634499A (en
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罗会清
孟新乐
李博瀚
白志山
胡思祥
田胡东
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Sichuan University of Science and Engineering
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Sichuan University of Science and Engineering
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Abstract

The invention discloses a rotational flow shearing slag-removing type solid-liquid separation device and a use method thereof, belonging to the technical field of solid-liquid separation equipment, and comprising a tank body, a filtering component, a flow guide pipe, a partition board, fluid conveying equipment and power equipment, wherein the partition board is positioned in the tank body and divides the tank body into two chambers, the filtering component is positioned in one chamber, the flow guide pipe penetrates through the partition board and is in rotary sealing connection with the partition board, one end of the flow guide pipe is communicated with the filtering component, and the other end of the flow guide pipe is communicated with a buffer cavity; the power equipment drives the honeycomb duct to rotate, and the fluid conveying equipment provides backwash fluid for the buffer cavity. The filter assembly of the invention continuously rotates, fluid can continuously impact and clean the outer wall of the filter element in the back flushing process, and simultaneously, the fluid distribution amount of each filter hole on the filter element can be changed, so that the instantaneous flow of part of the filter holes is increased, and the cleaning effect of the whole device is better.

Description

Rotational flow shearing slag-removing type solid-liquid separation device and use method thereof
Technical Field
The invention relates to the technical field of solid-liquid separation equipment, also belongs to the technical field of filtering equipment, and particularly relates to a rotational flow shearing slag-cleaning type solid-liquid separation device and a use method thereof.
Background
At present, the domestic chlorination method for preparing titanium dioxide has the problems of low product quality, large waste discharge and the like. Titanium dioxide is a multi-component or less-component coated ultrafine particle material which takes titanium dioxide as a main component, is processed into a particle size of 200 nm-350 nm by a chemical method, and is coated with other inorganic matters and organic matters. The acidic mother liquor used for acidolysis in the production process of preparing titanium dioxide by the chlorination method can be polluted by impurities such as particles generated in the preparation engineering, and becomes acidic waste liquor after the acidolysis process is finished. The waste liquid contains high-concentration hydrochloric acid waste liquid and extremely fine titanium dioxide, colloid and other particles, if the waste liquid is directly discharged without treatment, the environment is seriously polluted, and unnecessary resource waste is caused. In the production process of titanium dioxide by the chlorination method, after three-stage condensation and liquefaction are carried out on crude titanium tetrachloride generated by a chlorination furnace, the residual tail gas contains a large amount of N 2、TiCl4、HCl、CO、CO2 and the like, and a treatment process of washing with water and then alkaline washing is generally adopted in industry, and most TiCl 4, HCl and the like are absorbed in the water washing process, so that byproduct hydrochloric acid is generated. At present, the concentration of byproduct hydrochloric acid with 20-27% is about 0.4t when titanium dioxide is produced every 1t of titanium dioxide. Because the water absorbs the SiCl 4、TiCl4 and a small amount of other metal chlorides in the tail gas during spray water washing, the substances are hydrolyzed when meeting water, so that the byproduct hydrochloric acid contains 0.1-1% of colloid impurities, including silicic acid, orthosilicic acid, tiO2 and the like, which makes the byproduct acid system contain white colloid, is difficult for downstream customers to accept, is difficult for marketing, and affects the normal production of titanium dioxide for a long time. Therefore, it is necessary to perform solid-liquid separation.
The existing solid-liquid separation equipment is many, impurity content is high in this trade, the filter screen is easy to block up, consequently, usually adopt back flush filter, it is fixed the filter screen in the container with the filter screen, solution passes the filter screen in order to obtain purifying, in the operation with the pressure differential of filter screen front and back, start back flush when pressure differential is high and clear away impurity, it has realized dismantling-free cleaning, but the cleaning performance is not good, usually longer cleaning time is required, impurity washs incompletely, for example often appear impurity break away from behind the filter screen and hang in the condition of filter screen outer wall, the impurity that hangs after the liquid feed once more gets into the filter screen very fast again under the disturbance of fluid and leads to the jam.
Disclosure of Invention
In order to solve at least one of the problems, the invention provides a rotational flow shearing slag-removing type solid-liquid separation device and a use method thereof, wherein a filtering component is continuously rotated so that fluid continuously impacts the outer wall of a filtering element, thereby cleaning impurities on the outer wall of a filter element.
The specific scheme of the invention is as follows:
the utility model provides a whirl shearing scarfing cinder formula solid-liquid separation device, includes the jar body and is located the filter equipment in jar body, and filter equipment includes at least one filter element, its characterized in that still includes
The baffle plate is positioned in the tank body and divides the tank body into two chambers, and the two chambers are a filter cavity and a buffer cavity respectively; the filter assembly is positioned in the filter cavity, a first interface and a first valve for opening and closing the first interface are arranged on the filter cavity, a second interface and a second valve for opening and closing the second interface are arranged on the buffer cavity, and a third interface and a third valve for opening and closing the third interface are arranged at the bottom of the filter cavity;
A flow guide pipe which penetrates through the partition plate and is in rotary sealing connection with the partition plate, wherein one end of the flow guide pipe extends into the filter cavity and is communicated with the filter assembly, and the other end of the flow guide pipe is communicated with the buffer cavity;
The power equipment is used for driving the flow guide pipe to rotate;
a fluid delivery device for providing fluid to the buffer chamber.
As a specific embodiment of the invention, the filter element is a filter element, and the filter element is radially distributed along the honeycomb duct.
Further, the filter assembly comprises at least two groups of filter elements, wherein each group of filter elements is arranged along the circumference of the flow guide pipe, and the filter elements in two adjacent groups of filter elements are axially and alternately arranged along the flow guide pipe.
As a specific embodiment of the present invention, the filter element is a filter disc, and the upper side or the lower side of the filter disc is provided with a filter hole.
Further, an included angle between the filter disc and the central line of the flow guide pipe is an acute angle.
Further, the filter disc is spiral.
The application method of the cyclone shearing slag-removing type solid-liquid separation device comprises the following steps of: the synchronous rotation filter assembly in the back flushing process or the synchronous rotation filter assembly in the back flushing later stage. Impurities on the surface of the filter assembly are removed by the rotation action.
Further, the rotating process includes both forward rotating the filter assembly and reverse rotating the filter assembly, which allows for a full flushing of the outer walls of the filter assembly.
Still further, the filter assembly is rotated in a reciprocating forward and reverse direction.
Compared with the prior art, the invention has the following advantages:
(1) The filter assembly of the invention continuously rotates, and fluid continuously impacts the outer wall of the filter element in the back flushing process, thereby cleaning impurities on the outer wall of the filter element, avoiding the impurities from adhering around the filter hole, and leading the pressure difference of the filter assembly to be rapidly increased when the fluid is disturbed and enters the filter hole in the later stage of filtering.
(2) The fluid distribution amount of each filter hole on the filter element can be changed when the filter assembly rotates, so that the instantaneous flow of part of the filter holes is increased (the more the flow distributed by the filter holes far away from the flow guide pipe is), the cleaning of the part of the holes is more thorough, and the cleaning effect of the whole device is better.
Drawings
FIG. 1 is a schematic of the overall result of example 1 of the present invention;
FIG. 2 is a schematic view showing the structure of a filter assembly according to embodiment 1 of the present invention;
FIG. 3 is a schematic view showing the structure of a filter assembly according to embodiment 2 of the present invention;
FIG. 4 is a schematic view showing the structure of a filter assembly according to embodiment 3 of the present invention;
FIG. 5 is a schematic view showing the structure of a filter assembly according to embodiment 4 of the present invention;
FIG. 6 is a schematic view showing the structure of a filter assembly according to embodiment 5 of the present invention;
in the figure, a tank body 1, a filter assembly 2, a baffle plate 3, a flow guide pipe 4, a power device 5,
Filter chamber 11, buffer chamber 12, filter element 21, first through hole 41,
A first interface 111, a second interface 112, a third interface 113, a fourth interface 114,
A first valve 121, a second valve 122, a third valve 123, a fourth valve 124.
Detailed Description
The present invention will be described in detail below with reference to the drawings and the detailed description thereof, so that the above objects, features and advantages of the present invention can be more clearly understood. In the following description, numerous specific details are set forth in order to provide a thorough understanding of the present invention
In the description of the present embodiment, the terms "first," "second," "third," and the like are used for descriptive purposes only and are not to be construed as indicating or implying relative importance or implicitly indicating the number of technical features indicated. Thus, a feature defining "a first", "a second", and "a third" may explicitly or implicitly include at least one such feature.
Moreover, those of ordinary skill in the art will appreciate that the drawings are provided herein for illustrative purposes and that the drawings are not necessarily drawn to scale.
In this embodiment, unless explicitly specified and limited otherwise, the terms "mounted," "connected," "secured," and the like are to be construed broadly and include, for example, either permanently connected, removably connected, or integrally formed; can be mechanically or electrically connected; either directly or indirectly, through intermediaries, or both, may be in communication with each other or in interaction with each other, unless expressly defined otherwise. The specific meaning of the above terms in the present invention can be understood by those of ordinary skill in the art according to the specific circumstances.
Example 1
Referring to fig. 1, fig. 1 is a schematic diagram of the overall result of the present invention. The rotational flow shearing slag-removing type solid-liquid separation device comprises a tank body 1, a filtering component 2, a partition plate 3, a flow guide pipe 4 and power equipment 5. The partition plate 3 is arranged in the tank body 1 and divides the tank body 1 into an upper independent cavity and a lower independent cavity, namely a filter cavity 11 and a buffer cavity 12; the filter component 2 is arranged in the filter cavity 11, the guide pipe 4 is vertically arranged, the lower end of the guide pipe 4 penetrates through the partition board 3 and is rotationally connected with the partition board 3, the upper end of the guide pipe 4 penetrates through the filter cavity 11 and is rotationally connected with the wall surface of the filter cavity 11, meanwhile, two ends of the guide pipe 4 are closed, a section of the guide pipe 4 positioned in the filter cavity 11 is communicated with the filter component 2, a section of the guide pipe 4 positioned in the buffer cavity 12 is provided with a first through hole 41 penetrating through the body, and therefore, the filter cavity 11 is communicated with the buffer cavity 12 through the filter component 2 and the guide pipe 4, and fluid of the two cavities can flow in a penetrating manner. The side wall of the filter cavity 11 is provided with a first interface 111 and a first valve 121 for opening and closing the first interface 111, which is mainly used for controlling the raw material solution to enter the filter cavity 11; the bottom of the filter cavity 11 is provided with a third interface 113 and a third valve 123 for opening and closing the third interface 113, which is mainly used for discharging waste liquid containing high-concentration impurities during back flushing; the buffer cavity 12 is provided with a second interface 112 and a second valve 122 for opening and closing the second interface 112, and the interface is mainly used for flowing filtered clear liquid out of the buffer cavity 12; the buffer cavity 12 is provided with a fourth interface 114 and a fourth valve 124 for opening and closing the fourth interface 114; the fourth port 114 is connected to a fluid delivery device (not shown) for providing backwash liquid, here backwash liquid, filtered clear liquid (liquid free of impurities) to the buffer chamber 12. In addition, the upper end of the flow guiding pipe 4 extends out of the filter cavity 11 and is coaxially connected with the power equipment 5, and the power equipment is a variable speed motor and is used for driving the flow guiding pipe 4 to rotate so as to drive the filter assembly 2 to rotate together.
Specifically, referring to fig. 2, fig. 2 is a schematic structural diagram of a filtering component in the present embodiment. The filter assembly 2 in this embodiment comprises four sets of filter elements 21 arranged circumferentially along the flow conduit 3, each set of filter elements 21 having 16 cylindrical filter elements, each filter element being arranged radially along the flow conduit.
The normal filtering flow of this embodiment is: the first valve 121, the second valve 122 are opened, the third valve 123, the fourth valve 124 are closed, the fluid enters the filter cavity 11 from the first port 111, then the filter element 21 and the flow guide tube 3 enter the buffer cavity 12, and finally the fluid flows out from the second port 112.
The backwash flow of this embodiment is: the first valve 121 and the second valve 122 are closed, the third valve 123 and the fourth valve 124 are opened, filtered clear liquid is filled into the buffer cavity 12 by using the fluid conveying device, and fluid enters the filter cavity 11 along the flow guide pipe 3 and the filter element 21 and finally flows out of the third interface 113.
In the back flushing process, the fluid reversely passes through the filter element to flush out impurities in the filter hole, part of the impurities are directly discharged from the third interface along with the fluid, part of the impurities are adhered beside the filter hole, the power equipment 5 is started to reciprocally rotate the guide pipe 3 forwards and reversely, in the rotating process, the drainage surface of the filter element is contacted with the fluid, the impurities on the outer wall of the filter element are flushed out by the fluid, and the water fluid is discharged from the third interface. The method avoids the phenomenon that the cleaned impurities adhere to the periphery of the filter hole, and the impurities rapidly enter the filter hole again under the disturbance of fluid in the later stage of filtering, so that the pressure difference of the filter assembly is rapidly increased; meanwhile, the fluid distribution amount of each filter hole on the filter element can be changed in the rotation process of the filter element, so that the instantaneous flow of part of the filter holes is increased (the more the flow distributed by the filter holes far away from the guide pipe), the part of holes are cleaned more thoroughly, the filter assembly can be cleaned more thoroughly in both aspects, the single use time of the filter assembly is prolonged, and the backwash frequency is reduced.
Example 2
Embodiment 2 differs from embodiment 1 in the arrangement of the filter element 21 (filter element), and please refer to fig. 3, fig. 3 is a schematic structural diagram of the filter assembly of this embodiment. In this embodiment, the filter assembly 2 also includes four sets of filter elements 21, where the four sets of filter elements are disposed along the circumference of the flow guide 3, each set of filter elements 21 has 16 cylindrical filter elements, and each filter element is disposed radially along the flow guide, but the filter elements in two adjacent sets of filter elements are disposed at intervals along the axial direction of the flow guide, i.e. are staggered from each other, so as to be beneficial to disturbance effect on fluid when the filter elements rotate. Thus, the time for rotating the whole filter element can be further shortened, and impurities on the outer wall of the filter element can be removed more quickly.
Example 3
Embodiment 3 is different from embodiment 1 in that the filter assembly is different from embodiment 1, please refer to fig. 4, fig. 4 is a schematic structural diagram of the filter assembly of this embodiment, in this embodiment, the filter element 21 is a disc-shaped filter disc, and the upper side and the lower side of the filter disc are both provided with filter holes.
Example 4
Embodiment 4 differs from embodiment 3 in the arrangement manner of the filter assembly, and please refer to fig. 5, fig. 5 is a schematic structural diagram of the filter assembly according to the present embodiment, in which an included angle between the center line of the filter disc and the center line of the guide tube is an acute angle, specifically 3 °.
Example 5
The filter element in example 5 was also a filter disc, but the filter disc was spiral, as shown in fig. 6.
Testing
Impact of rotational speed on cleaning Effect
The device of example 1 was used for testing, the device was used for filtering titanium white by-product waste acid, the feeding rate was 1m 3/h, and back flushing was performed when the pressure difference between the inlet and outlet of the filter assembly reached 0.25MPa after a period of time. The clear liquid after filtration is used as a back flushing medium in back flushing, the flow is 3.6m 3/h, the flushing time is 2min, and the working period of the motor in the back flushing process is 1min (forward rotation 15s, pause 15s, reverse rotation 15s and pause 15 s). After washing, the clear liquid after filtration is used as a medium for filtration, the filtration flow rate is (1 m 3/h), the filtration is carried out for 0min, and the pressure difference at the inlet and the outlet of the filter assembly is measured after 30 min. The above steps were repeated using the motor rotation speed as a variable, and the influence of the unnecessary rotation speed on the cleaning effect was determined, and the results are shown in table 1.
TABLE 1 differential pressure statistics for example 1 backwashed filter assemblies at different rotational speeds
As can be seen from Table 1, during the secondary filtration, the differential pressure of test cases 1-1 and 1-2 is the same at the initial time and is larger than that of test cases 1-3 and 1-4, which means that impurities still exist in the filter holes after the back flushing in test cases 1-1 and 1-2, and impurities in the filter holes are further cleaned after the rotation speed of test cases 1-3 and 1-4 is increased, because the rotation results in uneven distribution of flow in the filter holes, part of the filter holes are cleaned more quantitatively, and impurities which cannot be flushed out under the condition of partial low impact flow are cleaned, which means that the cleaning effect of the filter assembly can be improved from the rotation speed.
In comparison with the above test cases, the pressure difference at 0min and 30min was significantly increased in test case 1-1, and less in test cases 1-2 and 1-3, and no increase in 1-4. As the secondary filtration adopts the filtered clear liquid as the filter medium, no solid particles which can be intercepted exist in the raw materials, so that no solid impurities which can be intercepted exist on the outer wall of the filter element, the obvious increase of the test example 1 shows that more filter impurities which can be intercepted are adsorbed on the outer wall of the filter element, and the impurities are sucked into the filter holes again in the later stage, so that the filtration period is shortened. This also illustrates that rotating the filter assembly advantageously increases the effectiveness of the backwash.
(II) Effect of Filter Assembly arrangement on cleaning Effect
The devices in the embodiment 1 and the embodiment 2 are adopted for experiments, the sizes and the number of filter holes (the filter areas are the same) of the filter components in the two devices are the same, the titanium dioxide byproduct waste acid is filtered by the devices, the feeding rate is 1m 3/h, and the titanium dioxide byproduct waste acid is backwashed after a period of time when the pressure difference between the inlet and the outlet of the filter components reaches 0.25 MPa. During back flushing, the filtered clear liquid is used as a back flushing medium, the flow is 3.6m 3/h, and different flushing times are selected. After washing, the clear liquid after filtration is used as a medium for filtration, the filtration flow rate is (1 m 3/h), the filtration is carried out for 0min, and the pressure difference at the inlet and the outlet of the filter assembly is measured after 30min. The above steps were repeated using the motor rotation speed as a variable, and the influence of the unnecessary rotation speed on the cleaning effect was determined, and the results are shown in table 2.
Table 2 statistics of differential pressure after different flushing times of filter assemblies
As can be seen from Table 2, when the back flushing time is 1min, the initial pressure difference of the secondary filtration in the embodiment 1 and the embodiment 2 is the same, which indicates that the arrangement mode has no obvious influence on the removal of impurities in the filter holes; comparing test example 2-1 with test example 2-3 and test example 2-2 with test example 2-4, it was found that the difference between the pressure difference after 30min of secondary filtration of test examples 2-3, 2-4 and the initial pressure difference was unchanged, which indicated that the impurities of the filter element were completely cleaned, while the slight increase in test examples 2-1, 2-2 indicated that the impurities of the filter element which could be intercepted still remained, which indicated that the arrangement of example 2 was more advantageous for causing fluid turbulence to remove the impurities of the filter element outer wall.
The foregoing is only a preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any changes or substitutions easily contemplated by those skilled in the art within the technical scope of the present invention disclosed in the embodiments of the present invention should be covered by the present invention. Therefore, the protection scope of the present invention should be subject to the protection scope of the claims.

Claims (4)

1. The utility model provides a whirl shearing scarfing cinder formula solid-liquid separation device, includes the jar body and is located the filter equipment in the jar body, and filter equipment includes at least one filter element, its characterized in that still includes:
The baffle plate is positioned in the tank body and divides the tank body into two chambers, and the two chambers are a filter cavity and a buffer cavity respectively; the filter assembly is positioned in the filter cavity, a first interface and a first valve for opening and closing the first interface are arranged on the filter cavity, a second interface and a second valve for opening and closing the second interface are arranged on the buffer cavity, and a third interface and a third valve for opening and closing the third interface are arranged at the bottom of the filter cavity;
A flow guide pipe which penetrates through the partition plate and is in rotary sealing connection with the partition plate, wherein one end of the flow guide pipe extends into the filter cavity and is communicated with the filter assembly, and the other end of the flow guide pipe is communicated with the buffer cavity;
The power equipment is used for driving the flow guide pipe to rotate;
a fluid delivery device for providing fluid to the buffer chamber;
The filter element is a filter element, and the filter element is radially distributed along the guide pipe;
the filter assembly at least comprises two groups of filter elements, each group of filter elements are arranged along the circumference of the flow guide pipe, and two adjacent groups of filter elements are axially arranged at intervals along the flow guide pipe and are staggered with each other.
2. A method of using the cyclone shear slag-cleaning type solid-liquid separation device of claim 1, comprising a back-flushing stage, the back-flushing stage comprising rotating the filter assembly during flushing.
3. The method of using a cyclonic shear slag-cleaning type solid-liquid separation apparatus as claimed in claim 2, wherein the rotating the filter assembly comprises rotating the filter assembly in a forward direction and rotating the filter assembly in a reverse direction.
4. A method of using a cyclonic shear slag-cleaning type solid-liquid separation apparatus as claimed in claim 3, wherein the rotating the filter assembly comprises circulating a forward rotating filter assembly, a reverse rotating filter assembly.
CN202211287344.6A 2022-10-20 2022-10-20 Rotational flow shearing slag-removing type solid-liquid separation device and use method thereof Active CN115634499B (en)

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