CN115594731A - Glutathione decoloring processing technology - Google Patents
Glutathione decoloring processing technology Download PDFInfo
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- CN115594731A CN115594731A CN202211346140.5A CN202211346140A CN115594731A CN 115594731 A CN115594731 A CN 115594731A CN 202211346140 A CN202211346140 A CN 202211346140A CN 115594731 A CN115594731 A CN 115594731A
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- C07—ORGANIC CHEMISTRY
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- C07K5/00—Peptides containing up to four amino acids in a fully defined sequence; Derivatives thereof
- C07K5/02—Peptides containing up to four amino acids in a fully defined sequence; Derivatives thereof containing at least one abnormal peptide link
- C07K5/0215—Peptides containing up to four amino acids in a fully defined sequence; Derivatives thereof containing at least one abnormal peptide link containing natural amino acids, forming a peptide bond via their side chain functional group, e.g. epsilon-Lys, gamma-Glu
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- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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- C12P21/02—Preparation of peptides or proteins having a known sequence of two or more amino acids, e.g. glutathione
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Abstract
The invention relates to the technical field of material decoloration, in particular to a glutathione decoloration processing technology which comprises an installation plate, wherein a decoloration barrel is installed at the upper end of the installation plate through a support rod, a decoloration device is in threaded connection with the upper end of the decoloration barrel, and an air inlet device is installed on the outer surface of the decoloration barrel. When the existing trapped liquid is decolorized, the trapped liquid is usually directly poured into a decolorizing kettle for decolorization, the decolorizing kettle is effective in decolorizing the trapped liquid and is simple and convenient to operate, but activated carbon in the decolorizing kettle is accumulated at the bottom and is not easy to contact with the trapped liquid, so that the efficiency of decolorizing the trapped liquid is reduced. The secondary decolorizing mechanism adopted by the glutathione decolorizing processing technology provided by the invention can disperse the trapped fluid into a plurality of round cylinders for decolorizing treatment, thereby avoiding the active carbon from decolorizing a large amount of trapped fluid at one time and improving the decolorizing rate of the trapped fluid.
Description
Technical Field
The invention relates to the technical field of material decoloration, in particular to a glutathione decoloration processing technology.
Background
Glutathione is a tripeptide compound formed by condensing glutamic acid, cysteine and glycine through peptide bonds, contains gamma-glutamyl and active sulfhydryl in molecules, is a structural basis of a plurality of important physiological functions, and has wide application prospects in the fields of clinical medicine, food processing, cosmetics and the like.
Glutathione need carry out decoloration processing when synthesizing through the enzyme process, current trapped liquid is carrying out decoloration processing, to intercept liquid and directly pour into the decoloration cauldron and carry out the decoloration processing usually, the decoloration cauldron can control its inside pressure and temperature, thereby effectual carry out decoloration processing and easy operation convenience to trapped liquid, nevertheless decoloration cauldron inner structure is single, activated carbon can pile up in the bottom in putting into the decoloration cauldron, after trapped liquid pours into the decoloration cauldron, lie in inside activated carbon difficult with hold back the liquid contact, thereby the efficiency of trapped liquid decoloration has been reduced.
Disclosure of Invention
The invention provides a glutathione decoloration processing technology, which can solve the problems existing in the process of carrying out the decoloration processing on the glutathione.
The technical scheme is as follows: in order to achieve the purpose, the invention adopts the following technical scheme that a glutathione decoloration processing technology uses a glutathione decoloration processing device, the glutathione decoloration processing device comprises a mounting plate, and the specific method when the glutathione decoloration processing device is used for decoloring trapped fluid is as follows:
s1, preparing raw materials: adding raw materials such as L-glutamic acid, L-cysteine, glycine, purified water and the like into a material tank of ultrafiltration membrane equipment for circular dissolution, and adding a dilute alkali solution buffer solution to maintain the pH value of the system.
S2, synthesizing materials: and adding bifunctional enzyme for synthesizing glutathione into the material tank, and carrying out catalytic reaction.
S3, decoloring treatment: and (3) washing the trapped fluid generated in the step (S2) by pure water, and placing the trapped fluid into a decoloring barrel from a decoloring device, wherein the decoloring device performs a decoloring reaction on the trapped fluid.
S4, completing decoloring: and (4) opening the decoloring barrel, separating decolored trapped fluid from activated carbon, and finishing decoloring.
The decolouring bucket is installed through the bracing piece in the mounting panel upper end, and threaded connection has the discoloring device on the decolouring bucket, and the outer surface mounting of decoloring bucket has air inlet unit.
The decolouring device comprises a cover plate which is connected with the upper end of the decolouring barrel through a plurality of bolts in a threaded manner, the middle part of the cover plate is rotatably connected with a rotating pipe through a bearing, the upper wall of the rotating pipe is slidably and penetratingly connected with a pushing rod, a spacing mechanism is installed at the lower end of the rotating pipe, a primary decolouring mechanism is slidably connected in the spacing mechanism, and a secondary decolouring mechanism is connected at the lower end of the spacing mechanism.
Preferably, the spacing mechanism comprises a connecting circular plate arranged at the lower end of the rotating pipe, a water falling hole is formed in the middle of the connecting circular plate, two cylindrical rods are symmetrically arranged at the lower end of the connecting circular plate along the axis of the connecting circular plate, a spacing plate is jointly arranged at the lower end of the cylindrical rods, a sealing sleeve is arranged on the outer annular surface of the spacing plate, a plurality of arc-shaped through holes which are uniformly distributed in the circumferential direction are formed in the spacing plate, a guide block is arranged at the lower end of the connecting circular plate, a limiting rod is arranged between the cylindrical rods, the limiting rod and the connecting circular plate are in through sliding fit, and two spacing rings are symmetrically inserted into the upper end of the spacing plate.
Preferably, the primary decoloring mechanism comprises a circular frame which is connected between the connecting circular plate and the spacing plate in a sliding manner, a water through hole is formed in the middle of the upper wall of the circular frame, two guide openings are symmetrically formed in the upper end of the circular frame along the axis of the circular frame, a guide block is in sliding fit with any one of the guide openings, a plurality of water outlets which are uniformly distributed in the circumferential direction are formed in the upper side and the lower side of the annular wall of the circular frame, a corrugated pipe is mounted on the inner end face of the upper wall of the circular frame, a water passing frame is mounted at the lower end of the corrugated pipe and provided with a circular hole, a lower pressing rod is mounted on the inner end face of the lower wall of the water passing frame, a bearing plate is connected to the lower end of the water passing frame through a screw thread, a rubber sleeve is arranged on the outer annular face of the bearing plate, a plurality of activated carbons are placed on the upper end of the bearing plate, and the bearing plate is of a disc-shaped structure.
Preferably, the secondary decolorization mechanism is including installing the toper arc plate of space bar lower extreme, the installation plectane is installed to toper arc plate lower extreme, set up a plurality of circumference evenly distributed's screw hole on the installation plectane, screw hole female connection has a circular section of thick bamboo, a plurality of evenly distributed's weeping hole is seted up to the circular section of thick bamboo lower extreme, the slip through connection has the lifter in the middle part of the installation plectane, the circular plate is installed to the lifter lower extreme, install the reset spring that the cover was established on the lifter between circular plate upper end and the installation plectane, a plurality of circumference evenly distributed's connecting plate is installed to the outer anchor ring of circular plate, the one end that the circular plate was kept away from to the connecting plate upper end is installed and is separated the baffle, separate the baffle upper end and install a plurality of plugging heads, plugging head and circular section of thick bamboo lower extreme weeping hole sliding fit.
Preferably, a plurality of air inlets which are uniformly distributed in the circumferential direction are formed in the wall of the decoloring barrel, a drain pipe is installed at the lower end of the decoloring barrel, a control valve is arranged on the drain pipe, and a support ring for supporting the partition plate is installed on the inner wall of the decoloring barrel.
Preferably, the air inlet device comprises an air inlet frame arranged on the outer surface of the decoloring barrel, the air inlet frame is communicated with the plurality of air inlets, and an air pump is arranged at the left end of the air inlet frame.
Preferably, a water inlet pipe is installed on the pipe wall of the rotating pipe, and a sealing cover is connected to one end, far away from the rotating pipe, of the water inlet pipe in a threaded mode.
Preferably, the upper end of the mounting circular plate is provided with a conical protruding block, and the middle part of the conical protruding block is in sliding through fit with the lifting rod.
Preferably, a filter screen is arranged in the liquid leakage hole at the lower end of the circular cylinder.
(III) the beneficial effects are as follows: 1. the primary decolorizing mechanism and the secondary decolorizing mechanism adopted by the processing technology for decolorizing the glutathione provided by the invention act together, so that the trapped fluid can be decolorized twice, and the decolorizing effect of the trapped fluid is improved.
2. The primary decolorizing mechanism and the secondary decolorizing mechanism adopted by the glutathione decolorizing processing technology provided by the invention can fully contact trapped fluid with active carbon, thereby ensuring that the trapped fluid can be fully decolorized.
3. The secondary decolorizing mechanism adopted by the glutathione decolorizing processing technology provided by the invention can disperse the trapped fluid into a plurality of round cylinders for decolorizing treatment, thereby avoiding the active carbon from decolorizing a large amount of trapped fluid at one time and improving the decolorizing rate of the trapped fluid.
4. The decoloring device and the decoloring barrel adopted by the glutathione decoloring processing technology provided by the invention are detachably connected, the circular frame is detachably connected with the bearing plate, and the circular cylinder is detachably connected with the mounting circular plate, so that the replacement of the activated carbon is facilitated, the activated carbon can be effectively separated from trapped liquid, and the operation steps of separating the activated carbon from the trapped liquid are reduced.
Drawings
The invention is further illustrated with reference to the following figures and examples.
FIG. 1 is a process flow diagram of the present invention.
Fig. 2 is a schematic perspective view of a first perspective structure according to the present invention.
Fig. 3 is a front view of the present invention.
Fig. 4 is a left side view of the present invention.
Fig. 5 is a first perspective view of the decoloring apparatus according to the present invention.
FIG. 6 is a perspective view of a second perspective of the decolorization device of the present invention.
Fig. 7 isbase:Sub>A cross-sectional viewbase:Sub>A-base:Sub>A of fig. 4 in accordance with the present invention.
Fig. 8 is an enlarged view of the invention at N in fig. 7.
Fig. 9 is an enlarged view at X in fig. 7 of the present invention.
In the figure: 1. mounting a plate; 2. a decolorizing barrel; 21. a support ring; 3. a decolorizing device; 31. a cover plate; 32. rotating the tube; 321. a water inlet pipe; 322. a sealing cover; 33. a pushing rod; 34. a spacing mechanism; 341. connecting the circular plate; 3411. a water falling hole; 342. a cylindrical rod; 343. a limiting rod; 344. a guide block; 345. a partition plate; 3451. an arc-shaped through hole; 346. a baffle ring; 35. a primary decolorizing mechanism; 351. a circular frame; 3511. a water through hole; 3512. a water outlet hole; 352. a bellows; 353. a water passing frame; 354. a lower pressure lever; 355. a carrying plate; 36. a secondary decolorization mechanism; 361. a tapered arc plate; 362. mounting a circular plate; 363. a circular cylinder; 364. a lifting rod; 365. a circular plate; 366. a return spring; 367. a connecting plate; 368. a baffle plate; 369. plugging the head; 4. an air intake device; 41. an air intake frame; 42. an air pump.
Detailed Description
Embodiments of the invention will be described in detail below with reference to the drawings, but the invention can be implemented in many different ways as defined and covered by the claims.
In order to achieve the purpose, the invention adopts the following technical scheme, referring to fig. 1 and fig. 2, a glutathione decoloration processing technology uses a glutathione decoloration processing device, the glutathione decoloration processing device comprises a mounting plate 1, and the specific method when the glutathione decoloration processing device is used for decoloring trapped fluid is as follows:
s1, preparing raw materials: adding raw materials such as L-glutamic acid, L-cysteine, glycine, purified water and the like into a material tank of ultrafiltration membrane equipment for circular dissolution, and adding a dilute alkali solution slow solution to maintain the pH value of the system.
S2, synthesizing materials: and adding bifunctional enzyme for synthesizing glutathione into the material tank, and carrying out catalytic reaction.
S3, decoloring treatment: washing the trapped fluid generated in the step S2 by pure water, and putting the trapped fluid into a decoloring barrel 2 from a decoloring device 3, wherein the decoloring device 3 performs a decoloring reaction on the trapped fluid.
S4, decoloring is completed: and (4) opening the decoloring barrel 2, separating decolored trapped fluid from activated carbon, and finishing decoloring.
Referring to fig. 2-4, the upper end of the mounting plate 1 is provided with a decoloring barrel 2 through a support rod, the upper end of the decoloring barrel 2 is connected with a decoloring device 3 through a thread, and the outer surface of the decoloring barrel 2 is provided with an air inlet device 4.
Referring to fig. 5 and 6, the decoloring device 3 includes a cover plate 31 screwed to the upper end of the decoloring barrel 2 through a plurality of bolts, the middle of the cover plate 31 is rotatably connected to a rotating pipe 32 through a bearing, the upper wall of the rotating pipe 32 is slidably connected to a pushing rod 33 in a penetrating manner, a spacing mechanism 34 is installed at the lower end of the rotating pipe 32, a primary decoloring mechanism 35 is slidably connected to the spacing mechanism 34, and a secondary decoloring mechanism 36 is connected to the lower end of the spacing mechanism 34.
Referring to fig. 5 and 7, the spacing mechanism 34 includes a connecting circular plate 341 mounted at the lower end of the rotating pipe 32, a water falling hole 3411 is disposed in the middle of the connecting circular plate 341, two cylindrical rods 342 are symmetrically mounted at the lower end of the connecting circular plate 341 along the axis of the connecting circular plate 341, a spacing plate 345 is mounted at the lower ends of the two cylindrical rods 342 together, a sealing sleeve is mounted on the outer ring surface of the spacing plate 345, a plurality of arc-shaped through holes 3451 uniformly distributed in the circumferential direction are formed in the spacing plate 345, a guide block 344 is mounted at the lower end of the connecting circular plate 341, a limiting rod 343 is disposed between the two cylindrical rods 342, the limiting rod 343 is in penetrating and sliding fit with the connecting circular plate 341, and two spacing rings 346 are symmetrically inserted at the upper end of the spacing plate 345.
Referring to fig. 4-7, in specific operation, activated carbon is manually placed in the primary decoloring mechanism 35 and the secondary decoloring mechanism 36, the primary decoloring mechanism 35 is then placed between the connection circular plate 341 and the partition plate 345, the two limiting rods 343 are inserted into the connection circular plate 341, the two limiting rods 343 and the two cylindrical rods 342 limit the primary decoloring mechanism 35, the two barrier rings 346 are then inserted into the partition plate 345, the cover plate 31 is manually or mechanically moved to the upper end of the decoloring barrel 2, the cover plate 31 moves the partition mechanism 34, the primary decoloring mechanism 35 and the secondary decoloring mechanism 36 into the decoloring barrel 2 through the rotating pipe 32, and the cover plate 31 is fixed to the upper end of the decoloring barrel 2 through bolts.
Referring to fig. 7, a plurality of air inlets are uniformly distributed in the circumferential direction on the wall of the decoloring barrel 2, a drain pipe is installed at the lower end of the decoloring barrel 2, a control valve is disposed on the drain pipe, and a support ring 21 for supporting a partition 345 is installed on the inner wall of the decoloring barrel 2.
Referring to fig. 7, the air inlet device 4 includes an air inlet frame 41 installed on an outer surface of the decoloring barrel 2, the air inlet frame 41 is communicated with a plurality of air inlet holes, and an air pump 42 is installed at a left end of the air inlet frame 41.
Referring to fig. 7, in operation, the air pump 42 is connected to an external nitrogen storage tank, the air pump 42 is started, the air pump 42 pumps nitrogen into the decoloring barrel 2 through the air inlet holes on the air inlet frame 41 and the decoloring barrel 2, the nitrogen exhausts the air in the decoloring barrel 2, and then the control valve and the air pump 42 are closed.
Referring to fig. 7, a water inlet pipe 321 is installed on the wall of the rotating pipe 32, and a sealing cover 322 is screwed to an end of the water inlet pipe 321 away from the rotating pipe 32.
Referring to fig. 7 and 8, the primary decoloring mechanism 35 includes a circular frame 351 slidably connected between the connecting circular plate 341 and the partition plate 345, a water through hole 3511 is formed in the middle of the upper wall of the circular frame 351, two guide openings are symmetrically formed in the upper end of the circular frame 351 along the axis thereof, the guide block 344 is slidably matched with any one of the guide openings, a plurality of circumferentially and uniformly distributed water outlet holes 3512 are formed in both the upper and lower sides of the annular wall of the circular frame 351, a corrugated pipe 352 is installed on the inner end surface of the upper wall of the circular frame 351, a water passing frame 353 is installed at the lower end of the corrugated pipe 352, a circular hole 3531 is formed in the annular wall of the water passing frame 353, a lower pressing rod 354 is installed on the inner end surface of the lower wall of the water passing frame 353, a receiving plate 355 is connected to the lower end of the water passing frame 353 through a screw thread, a rubber sleeve is arranged on the outer circumferential surface of the receiving plate 355, a plurality of activated carbons are placed on the upper end of the receiving plate 355, and the receiving plate 355 is of a disc-shaped structure.
Referring to fig. 5, 7 and 8, in an initial state, a plurality of activated carbons are manually placed in the circular frame 351, the receiving plate 355 is inserted into the circular frame 351 to support the activated carbons, the receiving plate 355 blocks the water outlet holes 3512 located at the lower side of the circular frame 351, the receiving plate 355 is fixed at the lower end of the water passing frame 353 through screws, the circular frame 351 is manually placed between the connecting circular plate 341 and the spacing plate 345, the guide opening is slidably engaged with the guide block 344 to guide the placement of the circular frame 351, after the placement of the circular frame 351 is finished, the sealing cover 322 is opened, then the trapped liquid is injected into the rotating pipe 32 through the water inlet pipe 321, the trapped liquid in the rotating pipe 32 falls onto the water passing frame 353 through the water falling holes 3411 and the water passing holes 3511, and then flows onto the receiving plate 355 from the circular hole 3531, and along with the injection of the trapped liquid, the liquid level of trapped liquid in the circular frame 351 slowly rises, the active carbon performs primary decoloration treatment on the trapped liquid, the retention time of the trapped liquid in the active carbon is prolonged, the trapped liquid can be ensured to be in full contact with the active carbon, the trapped liquid subjected to primary decoloration is discharged onto the partition plate 345 through the water outlet holes 3512 above the circular frame 351, the trapped liquid subjected to primary decoloration falls into the secondary decoloration mechanism 36 through the arc-shaped through holes 3451, the two partition rings 346 partition the trapped liquid subjected to primary decoloration, the pushing rod 33 is pressed downwards, the pushing rod 33 pushes the lower pressing rod 354, the lower pressing rod 354 drives the bearing plate 355 to move downwards through the water passing frame 353 and exposes the water outlet holes 3512 on the lower side of the circular frame 351, the residual trapped liquid in the circular frame 351 flows out through the water outlet holes 3512 on the lower side of the circular frame 351 and falls into the secondary decoloration mechanism 36 through the arc-shaped through holes 3451, and the residual of the trapped liquid is avoided.
Referring to fig. 6, 7 and 9, the secondary decoloring mechanism 36 includes a conical arc plate 361 installed at the lower end of the partition plate 345, an installation circular plate 362 is installed at the lower end of the conical arc plate 361, a plurality of threaded holes uniformly distributed in the circumferential direction are formed in the installation circular plate 362, a circular tube 363 is connected to the threaded hole in a threaded manner, a plurality of weep holes uniformly distributed are formed in the lower end of the circular tube 363, a lifting rod 364 is connected to the middle of the installation circular plate 362 in a sliding and penetrating manner, a conical protruding block is installed at the upper end of the installation circular plate 362, the middle of the conical protruding block is matched with the lifting rod 364 in a sliding and penetrating manner, a circular plate 365 is installed at the lower end of the lifting rod 364, a return spring 366 sleeved on the lifting rod 364 is installed between the upper end of the circular plate 365 and the installation circular plate 362, a plurality of connecting plates 367 uniformly distributed in the circumferential direction are installed on the outer annular surface of the circular plate 365, a partition plate 368 is installed at the end of the connecting plate 367, a plurality of plug 369 is installed at the end far away from the circular plate 365, a plurality of the plug 369 is installed at the upper end of the partition plate 368, the plug is matched with the plug at the lower end of the plug, the plug 369 and the plug at the lower end of the circular tube 363, and the plug are installed in a filter screen is installed in the weep hole at the lower end of the circular tube 363, and installed in the weep hole at the lower end of the circular tube 363.
Referring to fig. 6, 7 and 9, in a specific operation, in an initial state, the circular cylinder 363 filled with activated carbon is manually screwed into the threaded hole of the installation circular plate 362, the multiple circular cylinders 363 can effectively disperse the trapped fluid into multiple parts, which is convenient for decoloring the trapped fluid, the trapped fluid with primary decoloring falls onto the installation circular plate 362 through the tapered arc plate 361, the trapped fluid on the installation circular plate 362 falls into the multiple circular cylinders 363, so as to ensure that the trapped fluid can be completely contacted with the activated carbon, the activated carbon in the circular cylinders 363 performs secondary decoloring treatment on the trapped fluid, thereby improving the decoloring effect of the trapped fluid, after decoloring for a period of time, the pushing rod 33 is continuously pressed downwards, the pushing rod 33 pushes the lower pressing rod 354, the lower pressing rod 354 drives the carrying plate 355 and the corresponding screw to move downwards through the water frame 353, the screw pushes the lifting rod 364, the lifting rod 364 drives the plug 369 on the partition plate 368 through the circular plate 365 and the connecting plate 367 to be removed from the hole of the leaked fluid, thereby facilitating outflow of the trapped fluid, opening the control valve, and manually controlling the drainage pipe for collecting and draining the trapped fluid.
When in decolorization: s1: the activated carbon is manually placed in the primary decoloring mechanism 35 and the secondary decoloring mechanism 36, respectively, and then the primary decoloring mechanism 35 is placed in the spacing mechanism 34.
S2: the cover plate 31 is manually or mechanically moved to the upper end of the decoloring barrel 2, the cover plate 31 moves the spacing mechanism 34, the primary decoloring mechanism 35 and the secondary decoloring mechanism 36 into the decoloring barrel 2 through the rotating pipe 32, and the cover plate 31 is fixed to the upper end of the decoloring barrel 2 through bolts.
S3: the sealing cover 322 is opened, then the trapped fluid is injected into the rotating pipe 32 through the water inlet pipe 321, the trapped fluid in the rotating pipe 32 passes through the primary decolorizing mechanism 35 and the secondary decolorizing mechanism 36, and the primary decolorizing mechanism 35 and the secondary decolorizing mechanism 36 decolorize the trapped fluid.
S4: the trapped liquid falls into the decoloring barrel 2 through the primary decoloring mechanism 35 and the secondary decoloring mechanism 36, the control valve is opened, the trapped liquid is discharged through the drain pipe, the discharged control valve is manually collected, and the decoloring is completed.
The above description is only a preferred embodiment of the present invention and is not intended to limit the present invention, and various modifications and changes may be made by those skilled in the art. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (9)
1. The utility model provides a glutathione decoloration processing technology, it has used a glutathione decoloration processing equipment, this glutathione decoloration processing equipment includes mounting panel (1), its characterized in that: the specific method for decoloring trapped fluid by adopting the glutathione decoloring processing equipment is as follows:
s1, preparing raw materials: adding raw materials such as L-glutamic acid, L-cysteine, glycine, purified water and the like into a material tank of ultrafiltration membrane equipment for circular dissolution, and adding a dilute alkali liquor slow-dissolving solution to maintain the pH value of a system;
s2, synthesizing materials: adding bifunctional enzyme for synthesizing glutathione into the material tank, and carrying out catalytic reaction;
s3, decoloring treatment: washing the trapped fluid generated in the step S2 by pure water, and placing the trapped fluid into a decoloring barrel (2) from a decoloring device (3), wherein the decoloring device (3) performs a decoloring reaction on the trapped fluid;
s4, completing decoloring: opening the decoloring barrel (2), separating decolored trapped fluid from activated carbon, and finishing decoloring;
the upper end of the mounting plate (1) is provided with a decoloring barrel (2) through a support rod, the upper end of the decoloring barrel (2) is in threaded connection with a decoloring device (3), and the outer surface of the decoloring barrel (2) is provided with an air inlet device (4);
decoloration device (3) include through a plurality of bolt threaded connection apron (31) of decoloration bucket (2) upper end, apron (31) middle part is rotated through the bearing and is connected with rotating tube (32), and rotating tube (32) upper wall sliding through connection has a pole (33) of pushing, and spacer mechanism (34) are installed to rotating tube (32) lower extreme, and sliding connection has primary decoloration mechanism (35) in spacer mechanism (34), and spacer mechanism (34) lower extreme is connected with secondary decoloration mechanism (36).
2. The glutathione decoloring processing technology according to claim 1, characterized in that: the spacing mechanism (34) comprises a connecting circular plate (341) installed at the lower end of the rotating pipe (32), a water falling hole (3411) is formed in the middle of the connecting circular plate (341), two cylindrical rods (342) are symmetrically installed at the lower end of the connecting circular plate (341) along the axis of the connecting circular plate (341), a spacing plate (345) is installed at the lower ends of the two cylindrical rods (342) together, a sealing sleeve is installed on the outer annular surface of the spacing plate (345), a plurality of arc-shaped through holes (3451) which are uniformly distributed in the circumferential direction are formed in the spacing plate (345), a guide block (344) is installed at the lower end of the connecting circular plate (341), a limiting rod (343) is arranged between the two cylindrical rods (342), the limiting rod (343) penetrates through and is in sliding fit with the connecting circular plate (341), and two spacing rings (346) are symmetrically inserted at the upper end of the spacing plate (345).
3. The glutathione decoloration processing technique according to claim 2, which is characterized in that: the primary decoloring mechanism (35) comprises a circular frame (351) which is slidably connected between a connecting circular plate (341) and a spacing plate (345), a water through hole (3511) is formed in the middle of the upper wall of the circular frame (351), two guide openings are symmetrically formed in the upper end of the circular frame (351) along the axis of the circular frame, a guide block (344) is in sliding fit with any one of the guide openings, a plurality of circumferentially and uniformly distributed water outlets (3512) are formed in the upper side and the lower side of the annular wall of the circular frame (351), a corrugated pipe (352) is installed on the inner end face of the upper wall of the circular frame (351), a water passing frame (353) is installed at the lower end of the lower wall of the water passing frame (353), a lower pressing rod (354) is installed on the inner end face of the lower wall of the water passing frame (353), a bearing plate (355) is connected to the lower end of the water passing frame (353) through a screw thread, a rubber sleeve is arranged on the outer annular face of the bearing plate (355), and a plurality of activated carbons are placed on the upper end of the bearing plate (355).
4. The glutathione decoloration processing technique according to claim 2, which is characterized in that: the secondary decoloring mechanism (36) comprises a conical arc plate (361) installed at the lower end of a partition plate (345), an installation circular plate (362) is installed at the lower end of the conical arc plate (361), a plurality of threaded holes uniformly distributed in the circumferential direction are formed in the installation circular plate (362), a circular cylinder (363) is connected to the inner thread of each threaded hole, a plurality of leakage holes uniformly distributed are formed in the lower end of the circular cylinder (363), a lifting rod (364) is connected to the middle of the installation circular plate (362) in a sliding penetrating mode, a circular plate (365) is installed at the lower end of the lifting rod (364), a return spring (366) sleeved on the lifting rod (364) is installed between the upper end of the circular plate (365) and the installation circular plate (362), a plurality of connecting plates (367) uniformly distributed in the circumferential direction are installed on the outer circular plate (365), a partition plate (368) is installed at one end, far away from the circular plate (365) at the upper end of the connecting plate (367), a plurality of plugging heads (369) are installed at the upper end of the partition plate (368), and the leakage holes at the lower end of the circular cylinder (363) are in sliding fit.
5. The glutathione decoloring processing technology according to claim 2, characterized in that: the utility model discloses a decoloration barrel, including decoloration bucket (2), the drain pipe is installed to decoloration bucket (2) lower extreme, is provided with the control valve on the drain pipe, install support ring (21) that are used for supporting space bar (345) on decoloration bucket (2) inner wall.
6. The glutathione decoloration processing technique according to claim 5, which is characterized in that: the air inlet device (4) comprises an air inlet frame (41) arranged on the outer surface of the decoloring barrel (2), the air inlet frame (41) is communicated with a plurality of air inlets, and an air pump (42) is arranged at the left end of the air inlet frame (41).
7. The glutathione decoloration processing technique according to claim 1, which is characterized in that: a water inlet pipe (321) is installed on the pipe wall of the rotating pipe (32), and a sealing cover (322) is connected to one end, far away from the rotating pipe (32), of the water inlet pipe (321) in a threaded mode.
8. The glutathione decoloration processing technique according to claim 4, which is characterized in that: the upper end of the mounting circular plate (362) is provided with a conical protruding block, and the middle part of the conical protruding block is in sliding through fit with the lifting rod (364).
9. The glutathione decoloring processing technology according to claim 4, characterized in that: a filter screen is arranged in the liquid leakage hole at the lower end of the round cylinder (363).
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN116159337A (en) * | 2023-04-23 | 2023-05-26 | 山东金力王实业有限公司 | High-efficient equipment of leaching of aluminium sulfate preparation |
Citations (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20010009756A1 (en) * | 1998-01-06 | 2001-07-26 | Derek Hei | Flow devices for the reduction of compounds from biological compositions and methods of use |
| JP2008220208A (en) * | 2007-03-09 | 2008-09-25 | Nippon Kayaku Co Ltd | Method for producing low-molecular collagen |
| KR20100086186A (en) * | 2009-01-22 | 2010-07-30 | (주)해림파메틱 | A method of producing l-cystine |
| CN101863959A (en) * | 2010-05-28 | 2010-10-20 | 食品行业生产力促进中心 | Technique for separating and purifying glutathione from fresh yeast |
| US8232105B1 (en) * | 2010-09-30 | 2012-07-31 | Magellan Biosciences Point-of-Care, Inc. | Reagents and methods and systems using them |
| CN105906688A (en) * | 2016-05-01 | 2016-08-31 | 江苏诚信药业有限公司 | Technological system and technological method for extracting glutathione |
| CN106086126A (en) * | 2016-08-29 | 2016-11-09 | 开平牵牛生化制药有限公司 | A kind of method of Enzyme catalyzed synthesis glutathion |
| CN106366159A (en) * | 2016-08-31 | 2017-02-01 | 精晶药业股份有限公司 | Carnosine extracting and purifying method |
| CN109134594A (en) * | 2017-06-15 | 2019-01-04 | 深圳市古特新生生物科技有限公司 | A kind of method that enzyme process prepares glutathione |
| WO2019239340A1 (en) * | 2018-06-14 | 2019-12-19 | Gnosis S.P.A. | Reduced glutathione in a highly soluble, amorphous solid form, and process for the preparation thereof |
| JP2020023420A (en) * | 2018-08-08 | 2020-02-13 | 株式会社サンワ | Active carbon and manufacturing method of active carbon, and decoloration method |
| CN111321189A (en) * | 2020-03-19 | 2020-06-23 | 成都六然医疗科技有限公司 | Cordyceps militaris polypeptide and preparation method thereof |
| CN211885724U (en) * | 2019-11-29 | 2020-11-10 | 湖北省天星现代农业有限公司 | Decoloration device that production ferulic acid was used |
| CN112608266A (en) * | 2020-12-30 | 2021-04-06 | 南通紫琅生物医药科技有限公司 | Preparation method of L-proline |
-
2022
- 2022-10-31 CN CN202211346140.5A patent/CN115594731B/en active Active
Patent Citations (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20010009756A1 (en) * | 1998-01-06 | 2001-07-26 | Derek Hei | Flow devices for the reduction of compounds from biological compositions and methods of use |
| JP2008220208A (en) * | 2007-03-09 | 2008-09-25 | Nippon Kayaku Co Ltd | Method for producing low-molecular collagen |
| KR20100086186A (en) * | 2009-01-22 | 2010-07-30 | (주)해림파메틱 | A method of producing l-cystine |
| CN101863959A (en) * | 2010-05-28 | 2010-10-20 | 食品行业生产力促进中心 | Technique for separating and purifying glutathione from fresh yeast |
| US8232105B1 (en) * | 2010-09-30 | 2012-07-31 | Magellan Biosciences Point-of-Care, Inc. | Reagents and methods and systems using them |
| CN105906688A (en) * | 2016-05-01 | 2016-08-31 | 江苏诚信药业有限公司 | Technological system and technological method for extracting glutathione |
| CN106086126A (en) * | 2016-08-29 | 2016-11-09 | 开平牵牛生化制药有限公司 | A kind of method of Enzyme catalyzed synthesis glutathion |
| CN106366159A (en) * | 2016-08-31 | 2017-02-01 | 精晶药业股份有限公司 | Carnosine extracting and purifying method |
| CN109134594A (en) * | 2017-06-15 | 2019-01-04 | 深圳市古特新生生物科技有限公司 | A kind of method that enzyme process prepares glutathione |
| WO2019239340A1 (en) * | 2018-06-14 | 2019-12-19 | Gnosis S.P.A. | Reduced glutathione in a highly soluble, amorphous solid form, and process for the preparation thereof |
| JP2020023420A (en) * | 2018-08-08 | 2020-02-13 | 株式会社サンワ | Active carbon and manufacturing method of active carbon, and decoloration method |
| CN211885724U (en) * | 2019-11-29 | 2020-11-10 | 湖北省天星现代农业有限公司 | Decoloration device that production ferulic acid was used |
| CN111321189A (en) * | 2020-03-19 | 2020-06-23 | 成都六然医疗科技有限公司 | Cordyceps militaris polypeptide and preparation method thereof |
| CN112608266A (en) * | 2020-12-30 | 2021-04-06 | 南通紫琅生物医药科技有限公司 | Preparation method of L-proline |
Non-Patent Citations (7)
| Title |
|---|
| BOYU SHEN等: "Activated charcoal significantly improved the reliability of methods for quantitative analysis of endogenous substances in biological specimens: Glutathione and cysteine as cases", 《JOURNAL OF CHROMATOGRAPHY B》, vol. 1095, pages 241 - 250 * |
| CHANG SU等: "Glutathione enables full utilization of wool wastes for keratin production and wastewater decolorization", 《JOURNAL OF CLEANER PRODUCTION》, vol. 270, no. 12, pages 1 - 11 * |
| 张冰: "酿酒酵母中分离提取谷胱甘肽(GSH)和S-腺苷-L-甲硫氨酸(SAM)", 《中国优秀硕士学位论文全文数据库》, no. 2016 * |
| 张雪等: "响应面法优化鱿鱼(Ommastrephes bartrami)皮胶原蛋白提取液脱色工艺", 《海洋与湖沼》, vol. 46, no. 01, pages 01 * |
| 林志兴等: "从酿酒酵母中分离纯化谷胱甘肽", 《生物加工过程》, vol. 05, no. 04, pages 60 - 64 * |
| 王晓菊、傅力、王纯利: "从巴斯德毕赤酵母中分离纯化还原型谷胱甘肽", 《食品科技》, vol. 34, no. 01, pages 183 - 186 * |
| 陈丽娜、石矛、王大为: "玉米胚谷胱甘肽提取及纯化技术的研究", 《食品科技》, vol. 34, no. 02, pages 160 - 166 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116159337A (en) * | 2023-04-23 | 2023-05-26 | 山东金力王实业有限公司 | High-efficient equipment of leaching of aluminium sulfate preparation |
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