CN115465887B - Charging system for chlorination furnace - Google Patents
Charging system for chlorination furnace Download PDFInfo
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- CN115465887B CN115465887B CN202211114313.0A CN202211114313A CN115465887B CN 115465887 B CN115465887 B CN 115465887B CN 202211114313 A CN202211114313 A CN 202211114313A CN 115465887 B CN115465887 B CN 115465887B
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- 238000005660 chlorination reaction Methods 0.000 title claims abstract description 62
- 238000005303 weighing Methods 0.000 claims abstract description 122
- 238000007789 sealing Methods 0.000 claims abstract description 68
- 239000000463 material Substances 0.000 claims abstract description 41
- 239000002994 raw material Substances 0.000 claims abstract description 20
- 238000010926 purge Methods 0.000 claims description 7
- 239000011261 inert gas Substances 0.000 claims description 5
- 230000008859 change Effects 0.000 claims description 4
- 239000002893 slag Substances 0.000 description 78
- 239000007789 gas Substances 0.000 description 24
- 238000009835 boiling Methods 0.000 description 9
- 238000000034 method Methods 0.000 description 9
- 238000003763 carbonization Methods 0.000 description 5
- 239000000460 chlorine Substances 0.000 description 5
- 230000008569 process Effects 0.000 description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 description 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 3
- 229910052801 chlorine Inorganic materials 0.000 description 3
- 230000007797 corrosion Effects 0.000 description 3
- 238000005260 corrosion Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 238000005192 partition Methods 0.000 description 3
- 230000003068 static effect Effects 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000013585 weight reducing agent Substances 0.000 description 2
- 230000009471 action Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000010828 elution Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000014509 gene expression Effects 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- SZVJSHCCFOBDDC-UHFFFAOYSA-N iron(II,III) oxide Inorganic materials O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 description 1
- 230000007257 malfunction Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 208000026438 poor feeding Diseases 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000010959 steel Chemical group 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- GFNGCDBZVSLSFT-UHFFFAOYSA-N titanium vanadium Chemical compound [Ti].[V] GFNGCDBZVSLSFT-UHFFFAOYSA-N 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/02—Halides of titanium
- C01G23/022—Titanium tetrachloride
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65G—TRANSPORT OR STORAGE DEVICES, e.g. CONVEYORS FOR LOADING OR TIPPING, SHOP CONVEYOR SYSTEMS OR PNEUMATIC TUBE CONVEYORS
- B65G53/00—Conveying materials in bulk through troughs, pipes or tubes by floating the materials or by flow of gas, liquid or foam
- B65G53/34—Details
- B65G53/36—Arrangements of containers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65G—TRANSPORT OR STORAGE DEVICES, e.g. CONVEYORS FOR LOADING OR TIPPING, SHOP CONVEYOR SYSTEMS OR PNEUMATIC TUBE CONVEYORS
- B65G53/00—Conveying materials in bulk through troughs, pipes or tubes by floating the materials or by flow of gas, liquid or foam
- B65G53/34—Details
- B65G53/66—Use of indicator or control devices, e.g. for controlling gas pressure, for controlling proportions of material and gas, for indicating or preventing jamming of material
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Furnace Details (AREA)
- Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
Abstract
本发明公开了一种用于氯化炉的加料系统。所述系统包括:原料仓;两个称重料仓、两个第一切断阀,两个所述称重料仓分别通过两个所述第一切断阀与所述原料仓连接;输送泵,配置为驱动所述原料仓内的物料进入所述称重料仓;两个缓存料仓、两个第二切断阀、两个第一气动密封阀,两个所述缓存料仓分别依次通过两个所述第一气动密封阀、两个所述第二切断阀与两个所述称重料仓连接,两个所述缓存料仓分别位于两个所述称重料仓下方;U型阀、两个第二气动密封阀,两个所述缓存料仓分别通过两个所述第二气动密封阀与所述U型阀连接,所述U型阀用于与氯化炉连接。本发明能够实现精准、稳定、连续加料,并且能够防止氯化炉内气体返窜至加料系统。
The invention discloses a feeding system for a chlorination furnace. The system includes: a raw material bin; two weighing bins and two first cut-off valves; the two weighing bins are respectively connected to the raw material bin through the two first cut-off valves; a delivery pump, It is configured to drive the materials in the raw material bin into the weighing bin; two cache bins, two second cut-off valves, two first pneumatic sealing valves, and the two cache bins pass through two One of the first pneumatic sealing valves and two of the second cut-off valves are connected to the two weighing silos, and the two buffer silos are respectively located below the two weighing silos; U-shaped valve , two second pneumatic sealing valves, the two cache silos are respectively connected to the U-shaped valve through the two second pneumatic sealing valves, and the U-shaped valve is used to connect with the chlorination furnace. The invention can realize accurate, stable and continuous feeding, and can prevent gas in the chlorination furnace from returning to the feeding system.
Description
技术领域Technical field
本发明涉及化工技术领域,具体涉及一种用于氯化炉的加料系统。The invention relates to the technical field of chemical industry, and in particular to a feeding system for a chlorination furnace.
背景技术Background technique
钒钛磁铁矿通过高炉冶炼得到含钛高炉渣,高炉渣经过高温碳化预处理后获得碳化渣,碳化渣经过氯化获得用于制备钛白粉的TiCl4。碳化渣在氯化炉内进行沸腾氯化,由于碳化渣中有效成分偏低,加入原料量大,为提升氯化效率,需要对碳化渣进行连续稳定准确加料,使碳化渣用量与氯气用量有效匹配。Vanadium-titanium magnetite is smelted in a blast furnace to obtain titanium-containing blast furnace slag. The blast furnace slag is subjected to high-temperature carbonization pretreatment to obtain carbonized slag. The carbonized slag is chlorinated to obtain TiCl 4 used to prepare titanium dioxide. The carbonized slag is boiling chlorinated in the chlorination furnace. Since the effective components in the carbonized slag are low and the amount of raw materials added is large, in order to improve the chlorination efficiency, it is necessary to continuously, stably and accurately feed the carbonized slag so that the amount of carbonized slag and the amount of chlorine are effective. match.
现有技术中存在采用“原料仓+仓式泵+高位料仓+皮带秤计量+中间缓存料仓+星型给料器+U型阀”形式的氯化炉加料系统。该加料系统存在以下几方面的问题:In the existing technology, there is a chlorination furnace feeding system in the form of "raw material bin + bin pump + high level bin + belt scale metering + intermediate cache bin + star feeder + U-shaped valve". This feeding system has the following problems:
第一方面,碳化渣用量仅由皮带秤动态计量,加料量偏差通常在±10%以上,最大达到±50%,且两条皮带秤交替作业,稳定性均较差,故障率高,切换频繁;碳化渣加料量波动大,不能实现精准、稳定、连续加料,导致碳化渣加入量和循环氯气不匹配,对系统连续稳定运行和碳化渣氯化效率产生较大影响。First, the amount of carbonized slag is only dynamically measured by the belt scale. The deviation of the feeding amount is usually more than ±10%, and the maximum reaches ±50%. Moreover, the two belt scales operate alternately, with poor stability, high failure rate, and frequent switching. ; The amount of carbonized slag added fluctuates greatly, and accurate, stable, and continuous feeding cannot be achieved, resulting in a mismatch between the amount of carbonized slag added and the circulating chlorine gas, which has a great impact on the continuous and stable operation of the system and the chlorination efficiency of the carbonized slag.
第二方面,进料系统密封性差,仅依靠U型阀及缓存料仓中碳化渣形成料封,当皮带秤下料不畅,缓存料仓和U型阀碳化渣较少时,易造成炉内Cl2、TiCl4及HCl等气体返窜,导致U型阀、中间料仓碳化渣进料不畅,且炉内气体泄漏会造成环境污染和设备腐蚀。Secondly, the feeding system has poor sealing performance and only relies on the U-shaped valve and the carbonized slag in the cache silo to form a material seal. When the belt scale does not unload smoothly and there is less carbonized slag in the cache silo and U-shaped valve, it is easy to cause the furnace to malfunction. Gases such as Cl 2 , TiCl 4 and HCl will flow back inside, causing the U-shaped valve and intermediate silo to be fed carbonized slag unsmoothly, and gas leakage in the furnace will cause environmental pollution and equipment corrosion.
第三方面,加料系统设备故障率高,检修劳动强度大,保供能力差。皮带秤不仅计量精度不高,波动较大,校准困难,且易出现跑偏、堆料、漏料问题,同时星型给料器也易出现卡阻,且受TiCl4及冷凝堵塞影响,进料系统两套装置不能形成一用一备,导致加料系统保供能力较差,检修任务重。Thirdly, the equipment failure rate of the feeding system is high, the maintenance labor intensity is high, and the ability to ensure supply is poor. Belt scales not only have low measurement accuracy, large fluctuations, difficult calibration, and are prone to problems such as deviation, material stacking, and material leakage, but the star feeder is also prone to jamming and is affected by TiCl 4 and condensation blockage. The two sets of devices in the feeding system cannot form one for use and one for standby, resulting in poor supply capacity of the feeding system and heavy maintenance tasks.
发明内容Contents of the invention
本发明的主要目的在于提供一种用于氯化炉的加料系统,以解决上述技术问题的至少一个方面。The main purpose of the present invention is to provide a charging system for a chlorination furnace to solve at least one aspect of the above technical problems.
根据本发明的一个方面,提出一种用于氯化炉的加料系统,包括:原料仓;两个称重料仓、两个第一切断阀,两个所述称重料仓分别通过两个所述第一切断阀与所述原料仓连接;输送泵,配置为驱动所述原料仓内的物料进入所述称重料仓;两个缓存料仓、两个第二切断阀、两个第一气动密封阀,两个所述缓存料仓分别依次通过两个所述第一气动密封阀、两个所述第二切断阀与两个所述称重料仓连接,两个所述缓存料仓分别位于两个所述称重料仓下方;U型阀、两个第二气动密封阀,两个所述缓存料仓分别通过两个所述第二气动密封阀与所述U型阀连接,所述U型阀用于与氯化炉连接。According to one aspect of the present invention, a feeding system for a chlorination furnace is proposed, including: a raw material bin; two weighing bins, and two first cut-off valves. The two weighing bins pass through two The first cut-off valve is connected to the raw material bin; a delivery pump is configured to drive the materials in the raw material bin into the weighing bin; two buffer bins, two second cut-off valves, two third A pneumatic sealing valve, and the two cache silos are connected to the two weighing silos through the two first pneumatic sealing valves and the two second cut-off valves respectively. The two cache silos are The bins are respectively located under the two weighing bins; a U-shaped valve and two second pneumatic sealing valves. The two buffer bins are respectively connected to the U-shaped valve through two second pneumatic sealing valves. , the U-shaped valve is used to connect with the chlorination furnace.
根据本发明的一个实施例,所述系统还包括多个软连接件,两个所述称重料仓分别通过多个所述软连接件安装在所述系统中。According to an embodiment of the present invention, the system further includes a plurality of soft connectors, and the two weighing bins are respectively installed in the system through a plurality of the soft connectors.
根据本发明的一个实施例,所述软连接件包括弹性部件和/或柔性部件。According to an embodiment of the present invention, the soft connection includes elastic components and/or flexible components.
根据本发明的一个实施例,所述缓存料仓配置有料位计。According to an embodiment of the present invention, the buffer silo is equipped with a material level meter.
根据本发明的一个实施例,所述缓存料仓配置有惰性气体吹扫装置以及料仓振打装置。According to one embodiment of the present invention, the cache silo is equipped with an inert gas purging device and a silo rapping device.
根据本发明的一个实施例,所述U型阀的松动气量控制在10~15m3/h,所述U型阀的输送气量控制在20~30m3/h。According to an embodiment of the present invention, the loose air volume of the U-shaped valve is controlled at 10-15 m 3 /h, and the delivered air volume of the U-shaped valve is controlled at 20-30 m 3 /h.
根据本发明的一个实施例,所述系统还包括:控制装置,配置为:基于所述称重料仓检测的重量值达到第一预设值,以及与所述称重料仓相对应的所述第二切断阀处于关闭状态,控制与所述称重料仓相对应的所述第一切断阀打开,以向所述称重料仓加料。According to an embodiment of the present invention, the system further includes: a control device configured to: based on the weight value detected by the weighing bin reach the first preset value, and all the weight values corresponding to the weighing bin The second cut-off valve is in a closed state, and the first cut-off valve corresponding to the weighing silo is controlled to open to add materials to the weighing silo.
根据本发明的一个实施例,所述控制装置配置为:基于所述称重料仓检测的重量值达到第二预设值,控制与所述称重料仓相对应的所述第一切断阀关闭。According to an embodiment of the present invention, the control device is configured to: based on the weight value detected by the weighing bin reaching a second preset value, control the first cut-off valve corresponding to the weighing bin. closure.
根据本发明的一个实施例,所述控制装置配置为:基于所述称重料仓检测的重量值的变化值达到期望值,关闭与所述称重料仓相对应的所述第二切断阀和所述第一气动密封阀。According to an embodiment of the present invention, the control device is configured to: based on the change value of the weight value detected by the weighing bin reaching a desired value, close the second cut-off valve corresponding to the weighing bin and The first pneumatic sealing valve.
根据本发明的一个实施例,所述控制装置还配置为:基于任一第二气动密封阀的打开时间达到预设时间,控制所述任一第二气动密封阀关闭,并控制另一第二气动密封阀打开,以及控制与所述任一第二气动密封阀相对应的第二切断阀以及第一气动密封阀打开。According to an embodiment of the present invention, the control device is further configured to: based on the opening time of any second pneumatic sealing valve reaching a preset time, control the closing of any second pneumatic sealing valve, and control the other second pneumatic sealing valve to close. The pneumatic sealing valve opens, and the second cut-off valve and the first pneumatic sealing valve corresponding to any second pneumatic sealing valve are controlled to open.
根据本发明实施例的用于氯化炉的加料系统,利用称重料仓实现对物料的称重,称重料仓采用静态称重方式,准确性好,可以避免由皮带秤动态计量导致的准确度低、稳定性不好的问题。称重料仓、缓存料仓以及相关的切断阀和气动密封阀均设置两套,可以实现交替连续加料,保证加料的连续性和稳定性,并能提升保供能力。在缓存料仓的进出料端均设置气动密封阀,可以防止氯化炉中的气体向称重料仓返窜而对相关设备造成污染和腐蚀。According to the feeding system for the chlorination furnace according to the embodiment of the present invention, the weighing silo is used to weigh the materials. The weighing silo adopts a static weighing method, which has good accuracy and can avoid problems caused by dynamic weighing of the belt scale. Problems of low accuracy and poor stability. There are two sets of weighing silos, cache silos and related cut-off valves and pneumatic sealing valves, which can realize alternate and continuous feeding, ensure the continuity and stability of feeding, and improve the supply capacity. Pneumatic sealing valves are installed at the inlet and outlet ends of the buffer silo to prevent gas in the chlorination furnace from flowing back to the weighing silo and causing pollution and corrosion to related equipment.
附图说明Description of the drawings
为了更清楚地说明本发明实施例或现有技术中的技术方案,下面将对实施例或现有技术描述中所需要使用的附图作简单地介绍,显而易见地,下面描述中的附图仅仅是本发明的一些实施例,对于本领域普通技术人员来讲,在不付出创造性劳动的前提下,还可以根据这些附图获得其他的附图。In order to explain the embodiments of the present invention or the technical solutions in the prior art more clearly, the drawings needed to be used in the description of the embodiments or the prior art will be briefly introduced below. Obviously, the drawings in the following description are only These are some embodiments of the present invention. For those of ordinary skill in the art, other drawings can be obtained based on these drawings without exerting creative efforts.
图1示出根据本发明实施例的用于氯化炉的加料系统的示意图。Figure 1 shows a schematic diagram of a charging system for a chlorination furnace according to an embodiment of the present invention.
具体实施方式Detailed ways
为使本发明的目的、技术方案和优点更加清楚明白,以下结合具体实施例,并参照附图,对本发明实施例进一步详细说明。In order to make the purpose, technical solutions and advantages of the present invention more clear, the embodiments of the present invention will be further described in detail below with reference to specific embodiments and the accompanying drawings.
需要说明的是,本发明实施例中所有使用“第一”和“第二”的表述均是为了区分两个相同名称非相同的实体或者非相同的参量,可见“第一”“第二”仅为了表述的方便,不应理解为对本发明实施例的限定,后续实施例对此不再一一说明。It should be noted that all expressions using "first" and "second" in the embodiments of the present invention are to distinguish two entities or parameters with the same name but not the same, so it can be seen that "first" and "second" It is only for the convenience of description and should not be understood as a limitation on the embodiments of the present invention, and subsequent embodiments will not describe this one by one.
针对碳化渣沸腾氯化加料系统存在的动态计量准确度低,波动大,稳定性均较差,故障率高,切换频繁,碳化渣加入量和循环氯气不匹配,进料系统密封性差,易造成炉内Cl2、TiCl4及HCl等气体返窜,导致碳化渣进料不畅,造成环境污染和设备腐蚀等问题,本申请提出如下将要描述的用于氯化炉的加料系统100,以期对上述问题提供解决方案。Regarding the carbonized slag boiling chlorination feeding system, the dynamic metering accuracy is low, the fluctuation is large, the stability is poor, the failure rate is high, the switching is frequent, the carbonized slag addition amount does not match the circulating chlorine gas, the feeding system has poor sealing, and it is easy to cause Gases such as Cl 2 , TiCl 4 and HCl flow back in the furnace, resulting in poor feeding of carbonized slag, causing environmental pollution, equipment corrosion and other problems. This application proposes a feeding system 100 for a chlorination furnace to be described as follows, in order to improve Solutions are provided for the above problems.
图1示出根据本发明实施例的用于氯化炉的加料系统100的示意图。如图1所示,系统100包括:原料仓10;两个称重料仓20,22、两个第一切断阀30,32,两个称重料仓20,22分别通过两个第一切断阀30,32与原料仓10连接;输送泵40,配置为驱动原料仓10内的物料进入称重料仓20,22;两个缓存料仓50,52、两个第二切断阀60,62、两个第一气动密封阀70,72,两个缓存料仓50,52分别依次通过两个第一气动密封阀70,72、两个第二切断阀60,62与两个称重料仓20,22连接,两个缓存料仓50,52分别位于两个称重料仓20,22下方;U型阀80、两个第二气动密封阀90,92,两个缓存料仓50,52分别通过两个第二气动密封阀90,92与U型阀80连接,U型阀80用于与氯化炉1连接。Figure 1 shows a schematic diagram of a charging system 100 for a chlorination furnace according to an embodiment of the present invention. As shown in Figure 1, the system 100 includes: a raw material bin 10; two weighing bins 20, 22, and two first cut-off valves 30, 32. The two weighing bins 20, 22 pass through two first cut-off valves respectively. Valves 30, 32 are connected to the raw material bin 10; the delivery pump 40 is configured to drive the materials in the raw material bin 10 into the weighing bin 20, 22; two buffer bins 50, 52, and two second cut-off valves 60, 62 , two first pneumatic sealing valves 70,72, two buffer silos 50,52 respectively pass through the two first pneumatic sealing valves 70,72, the two second cut-off valves 60,62 and the two weighing silos. 20,22 connection, two cache silos 50,52 are located below the two weighing silos 20,22 respectively; U-shaped valve 80, two second pneumatic sealing valves 90,92, two cache silos 50,52 They are respectively connected to the U-shaped valve 80 through two second pneumatic sealing valves 90 and 92, and the U-shaped valve 80 is used to connect to the chlorination furnace 1.
在本发明的实施例中,通过采用“静态称重+密闭料仓交替批次实现连续+U型阀高浓相低气量输送”复合加料模式,可以实现碳化渣连续稳定密闭精确加料,实现碳化渣准确计量,平稳加入氯化炉,在氯化炉内高效匹配、反应,提高碳化渣中TiC和氯气的利用效率。In the embodiment of the present invention, by adopting the composite feeding mode of "static weighing + closed silo alternating batches to achieve continuous + U-shaped valve high-density phase and low gas volume transportation", continuous, stable, sealed and precise feeding of carbonized slag can be achieved to achieve carbonization The slag is accurately measured, smoothly added to the chlorination furnace, and efficiently matched and reacted in the chlorination furnace to improve the utilization efficiency of TiC and chlorine in the carbonized slag.
系统100可以包括两套密闭称重装置,所述密闭称重装置由图1中的虚线框出。两套密闭称重装置彼此相同。第一套密闭称重装置包括:第一切断阀30、称重料仓20、第二切断阀60、第一气动密封阀70、缓存料仓50以及第二气动密封阀90。类似地,第二套密闭称重装置包括:第一切断阀32、称重料仓22、第二切断阀62、第一气动密封阀72、缓存料仓52以及第二气动密封阀92。原料仓10与两个第一切断阀30,32连接,在原料仓10与第一切断阀30,32的连接路径上设有输送泵40。两个第二气动密封阀90,92与U型阀80连接,U型阀80再与氯化炉1连接。缓存料仓50,52可以为小体积定容料仓,对于同种物料每次加入量恒定。System 100 may include two sets of closed weighing devices, which are outlined by the dashed lines in Figure 1 . The two sets of closed weighing devices are identical to each other. The first set of closed weighing devices includes: a first cut-off valve 30, a weighing bin 20, a second cut-off valve 60, a first pneumatic sealing valve 70, a buffer silo 50 and a second pneumatic sealing valve 90. Similarly, the second set of closed weighing devices includes: the first cut-off valve 32 , the weighing bin 22 , the second cut-off valve 62 , the first pneumatic sealing valve 72 , the buffer bin 52 and the second pneumatic sealing valve 92 . The raw material bin 10 is connected to the two first shut-off valves 30 and 32, and a delivery pump 40 is provided on the connection path between the raw material bin 10 and the first shut-off valves 30 and 32. The two second pneumatic sealing valves 90 and 92 are connected to the U-shaped valve 80, and the U-shaped valve 80 is connected to the chlorination furnace 1. The buffer silos 50 and 52 can be small-volume fixed-volume silos, with a constant amount of the same material added each time.
两套密闭称重装置的设计,使得系统100可以实现交替连续加料,并且在使用过程中,两套密闭称重装置一用一备,具有良好的保供能力。The design of two sets of sealed weighing devices enables the system 100 to achieve alternate and continuous feeding. During use, the two sets of sealed weighing devices are used, one in use and one in standby, with good supply capability.
称重料仓20/22可以为配置有称重传感器的料仓。称重料仓20/22采用静态称重的方式,计量的准确性和稳定性好。可根据加料精度要求选择相应的称重传感器,实现高精度准确称量,例如精度可达到公斤级。The weighing bin 20/22 may be a bin equipped with a weighing sensor. The weighing silo 20/22 adopts static weighing method, which has good measurement accuracy and stability. The corresponding weighing sensor can be selected according to the feeding accuracy requirements to achieve high-precision and accurate weighing. For example, the accuracy can reach kilogram level.
在本发明的实施例中,系统100还包括多个软连接件42,两个称重料仓20,22分别通过多个软连接件42安装在系统100中。称重料仓20/22可以通过软连接件42而从加料系统100中独立,实现准确称量。软连接件42可以包括弹性部件和/或柔性部件,例如绳、弹性条等。In the embodiment of the present invention, the system 100 further includes a plurality of soft connectors 42, and the two weighing bins 20 and 22 are respectively installed in the system 100 through the plurality of soft connectors 42. The weighing bin 20/22 can be independent from the feeding system 100 through the soft connection 42 to achieve accurate weighing. The soft connector 42 may include elastic components and/or flexible components, such as ropes, elastic strips, etc.
系统100在使用时,首先往称重料仓20/22中加入一定量的物料。然后由称重料仓20/22向缓存料仓50/52提供期望量的物料,可以通过控制称重料仓20/22检测的重量值的减少值来控制物料的加入量,实现精确加料。缓存料仓50/52设置在称重料仓20/22下方,在打开第二切断阀60/62和第一气动密封阀70/72之后,物料可以在重力作用下落入缓存料仓50/52。When the system 100 is in use, a certain amount of material is first added to the weighing bin 20/22. Then the weighing silo 20/22 provides the desired amount of material to the buffer silo 50/52. The amount of material added can be controlled by controlling the decrease in the weight value detected by the weighing silo 20/22 to achieve accurate feeding. The cache silo 50/52 is set below the weighing silo 20/22. After opening the second cut-off valve 60/62 and the first pneumatic sealing valve 70/72, the material can fall into the cache silo 50/52 under the action of gravity. .
在对称重料仓20进行加料时,第一切断阀30打开,第一切断阀32关闭。当称重料仓20完成加料之后,第一切断阀30关闭,此时可以打开第一切断阀32,完成对称重料仓22的加料。同时,当称重料仓20完成加料之后,可以打开第二切断阀60和第一气动密封阀70,进行对缓存料仓50的加料。相应地,当称重料仓22完成加料之后,可以打开第二切断阀62和第一气动密封阀72,进行对缓存料仓52的加料。When charging the weighing bin 20, the first shut-off valve 30 is opened and the first shut-off valve 32 is closed. After the filling of the weighing bin 20 is completed, the first shut-off valve 30 is closed. At this time, the first shut-off valve 32 can be opened to complete the feeding of the weighing bin 22 . At the same time, after the weighing silo 20 completes charging, the second cut-off valve 60 and the first pneumatic sealing valve 70 can be opened to feed the buffer silo 50 . Correspondingly, after the filling of the weighing bin 22 is completed, the second shut-off valve 62 and the first pneumatic sealing valve 72 can be opened to feed the buffer bin 52 .
当缓存料仓50中加入期望量的物料之后,打开第二气动密封阀90,在U型阀80的调节作用下,缓存料仓50中的物料可以稳定地加入氯化炉1中。当缓存料仓50中的物料用尽时,及时地关闭第二气动密封阀90,并打开第二气动密封阀92,切换为由缓存料仓52向氯化炉1加料。在缓存料仓52向氯化炉1加料的过程中,打开第二切断阀60和第一气动密封阀70,对缓存料仓50进行新一轮的加料,以待缓存料仓52的物料用尽之后再次由缓存料仓50向氯化炉1加料。如此通过两个缓存料仓50,52交替地向氯化炉1加料,保证加料的连续性。而缓存料仓50/52的物料量又可以通过称重料仓20/22精准地提供,从而实现向氯化炉1精准、稳定、持续地加料。After the desired amount of materials is added to the cache silo 50, the second pneumatic sealing valve 90 is opened. Under the adjustment of the U-shaped valve 80, the materials in the cache silo 50 can be stably added to the chlorination furnace 1. When the materials in the cache silo 50 are used up, the second pneumatic sealing valve 90 is closed in time, and the second pneumatic sealing valve 92 is opened to switch to feeding the chlorination furnace 1 from the cache silo 52 . During the process of charging the cache silo 52 to the chlorination furnace 1, the second cut-off valve 60 and the first pneumatic sealing valve 70 are opened, and a new round of feeding is performed to the cache silo 50, so that the materials in the cache silo 52 can be used. After that, the buffer silo 50 is used to feed the chlorination furnace 1 again. In this way, the chlorination furnace 1 is alternately fed with materials through the two buffer silos 50 and 52 to ensure the continuity of feeding. The amount of material in the cache silo 50/52 can be accurately provided by the weighing silo 20/22, thereby achieving accurate, stable and continuous feeding of materials to the chlorination furnace 1.
第二气动密封阀90/92设置在缓存料仓50/52与U型阀80之间,即设置在缓存料仓50/52的出料管路上,可以实现缓存料仓50/52与U型阀80之间的有效隔断,还能实现缓存料仓50/52与氯化炉1之间的有效隔断。第一气动密封阀70/72设置在缓存料仓50/52与称重料仓20/22之间,即设置在缓存料仓50/52的进料管路上,可实现缓存料仓50/52与称重料仓20/22的有效隔断。从而多重保障任何时刻氯化炉1与称重料仓50/52均能有效隔断,杜绝氯化炉1内有毒有害气体向称重料仓50/52返窜。当第二气动密封阀90/92打开以便向氯化炉1加料时,第一气动密封阀70/72能够起到隔断缓存料仓50/52与称重料仓20/22的作用,防止氯化炉内气体进入称重料仓20/22。The second pneumatic sealing valve 90/92 is disposed between the cache silo 50/52 and the U-shaped valve 80, that is, it is disposed on the discharge pipeline of the cache silo 50/52, which can realize the connection between the cache silo 50/52 and the U-shaped valve 80. The effective partition between the valves 80 can also realize the effective partition between the cache silo 50/52 and the chlorination furnace 1. The first pneumatic sealing valve 70/72 is set between the cache silo 50/52 and the weighing silo 20/22, that is, it is set on the feed pipeline of the cache silo 50/52, so that the cache silo 50/52 can be realized Effective partition with weighing silo 20/22. This provides multiple guarantees that the chlorination furnace 1 and the weighing silo 50/52 can be effectively isolated at any time to prevent toxic and harmful gases in the chlorination furnace 1 from returning to the weighing silo 50/52. When the second pneumatic sealing valve 90/92 is opened to feed the chlorination furnace 1, the first pneumatic sealing valve 70/72 can play the role of isolating the buffer silo 50/52 and the weighing silo 20/22 to prevent chlorine The gas in the furnace enters the weighing silo 20/22.
在一些实施例中,缓存料仓50,52配置有料位计。料位计可以准确反馈物料量、加料速度和进料稳定性等。可以根据料位计反馈结果调节U型阀80,使得物料稳定地进入氯化炉1内。In some embodiments, cache bins 50, 52 are configured with level gauges. The material level meter can accurately feedback the material amount, feeding speed and feeding stability. The U-shaped valve 80 can be adjusted according to the feedback result of the material level gauge, so that the material can enter the chlorination furnace 1 stably.
在一些实施例中,缓存料仓50,52配置有惰性气体吹扫装置以及料仓振打装置。在加料后期,物料加入量可能受影响,通过惰性气体吹扫装置以及料仓振打装置可以保持物料加入量稳定。吹扫气以不与原料和产品反应为原则选取,优选氮气。In some embodiments, the cache bins 50, 52 are configured with an inert gas purge device and a bin rapping device. In the later stage of feeding, the amount of material added may be affected. The inert gas purging device and bin vibration device can keep the material added amount stable. The purge gas is selected based on the principle that it does not react with the raw materials and products, preferably nitrogen.
U型阀80可以实现物料均衡稳定加入氯化炉1中,可以提供一定的密封作用,防止氯化炉1中气体向加料系统倒窜、泄漏。同时,U型阀80还可以实现很小气量(相比FK泵等气力输送设备可以降低1~2个数量级)下将物料加入氯化炉1内,大幅减轻气体对沸腾氯化、TiCl4收集及尾气处理系统造成压力,提升氯化炉、TiCl4收集及尾气处理系统运行稳定性。The U-shaped valve 80 can realize the balanced and stable feeding of materials into the chlorination furnace 1, and can provide a certain sealing effect to prevent the gas in the chlorination furnace 1 from flowing back and leaking into the feeding system. At the same time, the U-shaped valve 80 can also add materials into the chlorination furnace 1 with a very small gas volume (compared to pneumatic conveying equipment such as FK pumps, which can be reduced by 1 to 2 orders of magnitude), greatly reducing the impact of gas on boiling chlorination and TiCl 4 collection. and exhaust gas treatment system to create pressure, improving the operational stability of the chlorination furnace, TiCl 4 collection and exhaust gas treatment system.
本申请的发明人意识到,由于沸腾氯化炉对气体量要求高,当气量增大后不仅有大量的细颗粒碳化渣随气体带出氯化炉,给旋风和除尘带来较大负担,且影响碳化渣氯化效果。同时较大量的惰性气体冲淡TiCl4含量,给TiCl4淋洗捕集和尾气处理增加较大负荷,降低全流程经济性。因此气力输送设备FK泵、脉冲式仓式泵均不适合直接向氯化炉加碳化渣。本发明通过采用U型阀来避免输送气量较大的问题。The inventor of this application realized that since the boiling chlorination furnace has high gas volume requirements, when the gas volume increases, not only a large amount of fine-grained carbonized slag will be taken out of the chlorination furnace with the gas, which will bring a greater burden to the cyclone and dust removal, but also And affect the chlorination effect of carbonized slag. At the same time, a larger amount of inert gas dilutes the TiCl 4 content, adds a greater load to TiCl 4 elution capture and tail gas treatment, and reduces the economy of the entire process. Therefore, the pneumatic conveying equipment FK pump and pulse warehouse pump are not suitable for adding carbonized slag directly to the chlorination furnace. The present invention avoids the problem of large gas delivery volume by using a U-shaped valve.
在本发明的实施例中,U型阀80的松动气量控制在10~15m3/h,U型阀80的输送气量控制在20~30m3/h。一方面保证物料的流量,另一方面避免气量过大而对沸腾氯化、TiCl4收集及尾气处理系统造成压力。In the embodiment of the present invention, the loose air volume of the U-shaped valve 80 is controlled at 10 to 15 m 3 /h, and the delivered air volume of the U-shaped valve 80 is controlled at 20 to 30 m 3 /h. On the one hand, it ensures the flow of materials, and on the other hand, it avoids excessive gas volume causing pressure on the boiling chlorination, TiCl 4 collection and tail gas treatment systems.
系统100可以实现一定程度的自动化控制。在一些实施例中,系统100还包括:控制装置,配置为:基于称重料仓20/22检测的重量值达到第一预设值,以及与称重料仓20/22相对应的第二切断阀60/62处于关闭状态,控制与称重料仓20/22相对应的第一切断阀30/32打开,以向称重料仓20/22加料。System 100 can achieve a certain degree of automated control. In some embodiments, the system 100 further includes: a control device configured to: reach a first preset value based on the weight value detected by the weighing bin 20/22, and a second value corresponding to the weighing bin 20/22. The cut-off valve 60/62 is in a closed state, and the first cut-off valve 30/32 corresponding to the weighing silo 20/22 is controlled to open to add materials to the weighing silo 20/22.
当称重料仓20/22内的物料较少时,可以自动地进行对称重料仓20/22加料,并且在向称重料仓20/22加料时,确保称重料仓20/22未向相应的缓存料仓50/52加料,以防加料不准。所述第一预设值可以为30吨。When there is less material in the weighing bin 20/22, the weighing bin 20/22 can be automatically filled with materials, and when adding materials to the weighing bin 20/22, ensure that the weighing bin 20/22 is not Add materials to the corresponding buffer bin 50/52 to prevent inaccurate feeding. The first preset value may be 30 tons.
在一些实施例中,所述控制装置配置为:基于称重料仓20/22检测的重量值达到第二预设值,控制与称重料仓20/22相对应的第一切断阀30/32关闭。当称重料仓20/22加入足够量的物料后,可以自动地结束加料。所述第二预设值可以为80吨。In some embodiments, the control device is configured to: based on the weight value detected by the weighing bin 20/22 reaching the second preset value, control the first cut-off valve 30/ corresponding to the weighing bin 20/22. 32 off. When a sufficient amount of material is added to the weighing bin 20/22, the feeding can be ended automatically. The second preset value may be 80 tons.
在一些实施例中,所述控制装置配置为:基于称重料仓20/22检测的重量值的变化值达到期望值,关闭与称重料仓20/22相对应的第二切断阀60/62和第一气动密封阀70/72。从而根据称重料仓20/22检测的重量值的变化值来自动地向缓存料仓50/52加入期望量的物料,实现精准加料。In some embodiments, the control device is configured to close the second cut-off valve 60/62 corresponding to the weighing bin 20/22 based on the change value of the weight value detected by the weighing bin 20/22 reaching a desired value. and first pneumatic sealing valve 70/72. Thereby, the desired amount of material is automatically added to the buffer silo 50/52 according to the change value of the weight value detected by the weighing silo 20/22 to achieve accurate feeding.
在一些实施例中,所述控制装置还配置为:基于任一第二气动密封阀90/92的打开时间达到预设时间,控制任一第二气动密封阀90/92关闭,并控制另一第二气动密封阀90/92打开,以及控制与任一第二气动密封阀90/92相对应的第二切断阀60/62以及第一气动密封阀70/72打开。从而自动地实现交替、持续加料。对于每个缓存料仓50/52,其向氯化炉1加料的时间可以是预设的,当第二气动密封阀90/92的打开时间达到预设时间,即可确定缓存料仓50/52完成向氯化炉1加料。所述预设时间可以为35min。In some embodiments, the control device is further configured to: based on the opening time of any second pneumatic sealing valve 90/92 reaching a preset time, control any second pneumatic sealing valve 90/92 to close, and control the other The second pneumatic sealing valve 90/92 is opened, and the second shut-off valve 60/62 and the first pneumatic sealing valve 70/72 corresponding to any second pneumatic sealing valve 90/92 are controlled to be opened. Thus, alternating and continuous feeding can be realized automatically. For each cache silo 50/52, the time for feeding the chlorination furnace 1 can be preset. When the opening time of the second pneumatic sealing valve 90/92 reaches the preset time, the cache silo 50/52 can be determined. 52 Completes charging of chlorination furnace 1. The preset time may be 35 minutes.
根据以上描述,本发明实施例的加料系统100能够实现碳化渣沸腾氯化过程中的密闭、连续、稳定、准确加料,通过优化碳化渣计量方式和碳化渣进料设备结构,调整碳化渣输送工艺,实现氯化炉和主料仓有效隔断,碳化渣准确计量,在密闭体系下通过控制输送气量实现碳化渣连续稳定准确加入氯化炉中实现与氯气有效匹配,从而有效提高碳化渣中钛元素的综合氯化效果。本发明的加料系统100还具有简单可靠、连续稳定性好、效率高、占地面积小、能耗低、处理能力大等优点。According to the above description, the feeding system 100 of the embodiment of the present invention can realize sealed, continuous, stable and accurate feeding during the boiling chlorination process of carbonized slag, and adjust the carbonized slag transportation process by optimizing the carbonized slag metering method and the carbonized slag feeding equipment structure. , to achieve effective separation between the chlorination furnace and the main silo, and accurate measurement of carbonized slag. In a closed system, by controlling the amount of transported gas, the carbonized slag can be continuously, stably and accurately added to the chlorination furnace to effectively match the chlorine gas, thereby effectively increasing the titanium element in the carbonized slag. comprehensive chlorination effect. The feeding system 100 of the present invention also has the advantages of simplicity, reliability, good continuous stability, high efficiency, small floor space, low energy consumption, and large processing capacity.
下面根据具体的实施例进行说明。The following description is based on specific embodiments.
实施例1Example 1
本实施例为工业应用,在攀钢建成碳化渣低温氯化制备TiCl4生产线上实施,加料系统主要包括:400吨大原料仓1台,仓式输送泵1台,两套密闭称重装置(每套装置含120t称重料仓1台,10吨缓存料仓1台及配套截断阀和气动密封阀,两套装置分别编号为A、B),流态化U型阀1台。两套密闭称重装置交替使用实现碳化连续稳定加料,加料量为12~20t/h。This example is an industrial application and was implemented on the TiCl 4 production line built by Panzhihua Iron and Steel Co., Ltd. for the low-temperature chlorination of carbonized slag. The feeding system mainly includes: 1 large 400-ton raw material warehouse, 1 warehouse-type transfer pump, and two sets of closed weighing devices ( Each set of equipment contains a 120t weighing silo, a 10t buffer silo and supporting cut-off valves and pneumatic sealing valves. The two sets of equipment are numbered A and B respectively, and a fluidized U-shaped valve. Two sets of closed weighing devices are used alternately to achieve continuous and stable carbonization feeding, with a feeding capacity of 12 to 20t/h.
碳化渣原料为攀钢集团公司炼铁厂1#高炉高炉渣,经碳化电炉高温还原并破碎磨细成60~1000目碳化渣。其典型粒度分布见表1。The raw material of carbonized slag is blast furnace slag from the #1 blast furnace of Panzhihua Iron and Steel Group Corporation, which is reduced and ground into 60 to 1000 mesh carbonized slag by high-temperature carbonization electric furnace. Its typical particle size distribution is shown in Table 1.
表1碳化渣典型粒度分布/%Table 1 Typical particle size distribution of carbonized slag/%
碳化渣沸腾氯化连续稳定密闭加料具体的过程包括以下步骤:The specific process of continuous and stable closed feeding of carbonized slag boiling chlorination includes the following steps:
1、将经过高温碳化还原并破碎磨细成60~1000目碳化渣(碳化渣成品)通过罐式汽车运送至低沸腾氯化生产现场,由汽车泵送至大原料仓备用。1. After high-temperature carbonization reduction and crushing and grinding, the carbonized slag (finished carbonized slag) of 60 to 1000 mesh will be transported to the low boiling chlorination production site by tanker truck, and then pumped by the truck to the large raw material warehouse for later use.
2、通过仓式泵将碳化渣送入A高位称重料仓,打开A仓顶切断阀开始向A高位称重料仓进碳化渣,同时为碳化渣称重,当A高位称重料仓重量达到80吨后关闭A仓顶切断阀,开启B仓项切断阀向B高位称重料仓进碳化渣;A高位称重料仓备用。当B高位称重料仓重量达到80吨后停止仓式泵,B高位称重料仓备用。当A高位称重料仓、B高位称重料仓中碳化渣小于30吨时重新启动仓式泵向高位称重料仓补加碳化渣,补加碳化渣时确保该称重料仓未向对应缓存料仓加料。运行期间始终保持A、B称重料仓碳化渣重量在30~80t。2. Send the carbonized slag into the A high-level weighing silo through the warehouse pump, open the cut-off valve on the top of the A silo, and start feeding the carbonized slag into the A high-level weighing silo. At the same time, the carbonized slag is weighed. When the A high-level weighing silo After the weight reaches 80 tons, close the cut-off valve on the top of warehouse A, open the cut-off valve on the top of warehouse B, and feed carbonized slag into high-level weighing silo B; high-level weighing silo A is on standby. When the weight of B high-level weighing silo reaches 80 tons, the warehouse pump is stopped and B high-level weighing silo is reserved. When the carbonized slag in high-level weighing silo A and high-level weighing silo B is less than 30 tons, restart the warehouse pump to replenish carbonized slag to the high-level weighing silo. When adding carbonized slag, make sure that the weighing silo does not add carbonized slag to the high-level weighing silo. Add materials to the corresponding cache silo. During operation, the weight of carbonized slag in A and B weighing silos is always kept at 30 to 80t.
3、A高位称重料仓不再进碳化渣后准确读取碳化渣重量85.647t。依次打开A进料切断阀、A1气动密封阀向A缓存料仓进料,根据A缓存料仓料位计确定A缓存料仓装满后关闭A进料切断阀、A1气动密封阀。根据称重料仓重量减轻量准确计算出缓存料仓碳化渣重量9.752t,A缓存料仓加碳化渣3~5min完成。3. After the carbonized slag is no longer fed into the A high-position weighing silo, the weight of the carbonized slag is accurately read as 85.647t. Open the A feed cut-off valve and A1 pneumatic sealing valve in sequence to feed the A cache silo. According to the A cache silo level gauge, determine that the A cache silo is full and then close the A feed cut-off valve and A1 pneumatic sealing valve. According to the weight reduction of the weighing silo, the weight of carbonized slag in the cache silo was accurately calculated to be 9.752t. The carbonized slag in the cache silo A was added in 3 to 5 minutes.
4、打开A2气动密封阀将碳化渣加入流态化U型阀中,开启流态化U型阀松动气和输送气,开始向氯化炉进碳化渣。根据缓存料仓料位计读数判定碳化渣加料的稳定性,调整流态化U型阀松动气和输送气量,保持缓存料仓每批次加料时间在35min,松动气量控制在10~15m3/h,输送气量在20~30m3/h,根据调整好气量确定流态化U型阀松动气和输送气阀门开度并固定其阀门开度。4. Open the A2 pneumatic sealing valve and add the carbonized slag into the fluidized U-shaped valve, open the fluidized U-shaped valve to loosen the air and transport the gas, and start feeding the carbonized slag into the chlorination furnace. Determine the stability of carbonized slag feeding based on the reading of the cache silo material level meter, adjust the loosening air and conveying air volume of the fluidized U-shaped valve, keep the feeding time of each batch of the cache silo at 35 minutes, and control the loosening air volume at 10 ~ 15m 3 / h, the conveying air volume is 20~30m 3 /h. According to the adjusted air volume, determine the loosening air and conveying air valve openings of the fluidized U-shaped valve and fix the valve openings.
5、加料后期,开启A缓存料仓振打器,并适当加入少量吹扫气,保持碳化渣加入量稳定。当A缓存料仓加完碳化渣后关闭A2气动密封阀,确保氯化炉和A称重系统完全断开,A称重系统碳化渣加料完成,进入下一轮次称重即重复操作步骤3、4。A称重系统加碳化渣期间B称重系统B2气动密封阀关闭,氯化炉和B称重系统完成断开。5. In the later stage of feeding, turn on the vibrator of the A cache silo, and add a small amount of purge gas appropriately to keep the amount of carbonized slag added stable. When the carbonized slag is added to the cache silo A, close the A2 pneumatic sealing valve to ensure that the chlorination furnace and the weighing system A are completely disconnected. The carbonized slag filling of the weighing system A is completed. Enter the next round of weighing and repeat step 3. ,4. While A weighing system is adding carbonized slag, B weighing system B2 pneumatic sealing valve is closed, and the chlorination furnace and B weighing system are completely disconnected.
6、在A称重系统向氯化炉加碳化渣期间,B称重系统开始向B缓存料仓加碳化渣,操作如下:B高位称重料仓不再进碳化渣,准确读取碳化渣重量83.129t。依次打开B进料切断阀,B1气动密封阀向B缓存料仓进碳化渣,根据B缓存料仓料位计确定B缓存料仓装满后关闭B进料切断阀,B1气动密封阀。根据称重料仓重量减轻量准确计算出缓存料仓碳化渣重量9.773t备用,B缓存料仓加碳化渣3~5min完成。6. While the A weighing system is adding carbonized slag to the chlorination furnace, the B weighing system begins to add carbonized slag to the B cache silo. The operation is as follows: B high-level weighing silo no longer feeds carbonized slag, and the carbonized slag is accurately read. Weight 83.129t. Open the B feed cut-off valve and the B1 pneumatic sealing valve in turn to feed carbonized slag into the B cache silo. According to the B cache silo level gauge, determine that the B cache silo is full and then close the B feed cut-off valve and the B1 pneumatic sealing valve. According to the weight reduction of the weighing silo, the weight of carbonized slag in the cache silo is accurately calculated to be 9.773t, and the carbonized slag in the cache silo B is added for 3 to 5 minutes.
7、当A称重缓存料仓碳化渣加完后,及时开启B2气动密封阀将B缓存料仓中碳化渣加入流态化U型阀中,持续稳定向氯化炉进碳化渣。根据缓存料仓料位计读数判定碳化渣加料的稳定性,保持流态化U型阀松动气量控制在10~15m3/h,输送气量在20~30m3/h,加料后期,开启B缓存料仓振打器,并适当加入少量吹扫气,保持碳化渣加入量稳定。当B缓存料仓加完碳化渣后关闭B2气动密封阀,确保氯化炉和B称重系统完全断开。当B缓存料仓碳化渣加完时A缓存料仓也完成碳化渣加料,及时打开A2气动密封阀将碳化渣加入流态化U型阀中持续向氯化炉进碳化渣。7. When the carbonized slag in the weighing cache silo A is completely added, promptly open the B2 pneumatic sealing valve to add the carbonized slag in the cache silo B into the fluidized U-shaped valve, and continuously and steadily feed the carbonized slag into the chlorination furnace. Determine the stability of carbonized slag feeding based on the reading of the cache silo material level gauge. Keep the loose air volume of the fluidized U-shaped valve at 10~ 15m3 /h, and the conveying air volume at 20~ 30m3 /h. At the end of the feeding period, turn on B cache Vibrator of the silo, and add a small amount of purge gas appropriately to keep the amount of carbonized slag added stable. When the carbonized slag is added to the B cache silo, close the B2 pneumatic sealing valve to ensure that the chlorination furnace and B weighing system are completely disconnected. When the carbonized slag is added to the cache silo B, the carbonized slag is also added to the cache silo A. The A2 pneumatic sealing valve is opened in time to add the carbonized slag to the fluidized U-shaped valve and continue to feed the carbonized slag into the chlorination furnace.
此时碳化渣沸腾氯化加料系统已经完成一轮次碳化渣连续稳定密封加料。At this time, the carbonized slag boiling chlorination feeding system has completed one round of continuous and stable sealed feeding of carbonized slag.
所属领域的普通技术人员应当理解:以上任何实施例的讨论仅为示例性的,并非旨在暗示本发明实施例公开的范围(包括权利要求)被限于这些例子;在本发明实施例的思路下,以上实施例或者不同实施例中的技术特征之间也可以进行组合,并存在如上所述的本发明实施例的不同方面的许多其它变化,为了简明它们没有在细节中提供。因此,凡在本发明实施例的精神和原则之内,所做的任何省略、修改、等同替换、改进等,均应包括在本发明实施例的保护范围之内。Those of ordinary skill in the art should understand that the above discussion of any embodiments is only illustrative, and is not intended to imply that the scope of the disclosure of the embodiments of the present invention (including the claims) is limited to these examples; under the thinking of the embodiments of the present invention , the above embodiments or technical features in different embodiments can also be combined, and there are many other changes in different aspects of the embodiments of the present invention as described above, which are not provided in details for the sake of simplicity. Therefore, any omissions, modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of the embodiments of the present invention shall be included in the protection scope of the embodiments of the present invention.
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