CN115386425B - Daily chemical essence for hair dye and preparation method thereof - Google Patents

Daily chemical essence for hair dye and preparation method thereof Download PDF

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CN115386425B
CN115386425B CN202211146571.7A CN202211146571A CN115386425B CN 115386425 B CN115386425 B CN 115386425B CN 202211146571 A CN202211146571 A CN 202211146571A CN 115386425 B CN115386425 B CN 115386425B
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oil
leaf oil
fragrance
hair dye
daily chemical
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CN115386425A (en
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林金华
王志辉
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Guangzhou Fenhao Flavor Co ltd
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Guangzhou Fenhao Flavor Co ltd
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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    • A61K8/35Ketones, e.g. benzophenone
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4973Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/10Preparations for permanently dyeing the hair
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40Mixing liquids with liquids; Emulsifying
    • B01F23/405Methods of mixing liquids with liquids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40Mixing liquids with liquids; Emulsifying
    • B01F23/43Mixing liquids with liquids; Emulsifying using driven stirrers
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    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
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    • C11B9/0007Aliphatic compounds
    • C11B9/0015Aliphatic compounds containing oxygen as the only heteroatom
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    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
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    • C11B9/00Essential oils; Perfumes
    • C11B9/0026Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
    • C11B9/0034Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing six carbon atoms
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    • C11B9/00Essential oils; Perfumes
    • C11B9/0061Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/21Mixing of ingredients for cosmetic or perfume compositions

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Abstract

The application relates to the field of daily chemical essence, and in particular discloses daily chemical essence for hair dye, which comprises the following components in percentage by mass: 0.3-0.4% of white orchid leaf oil; cis-6-nonenol 0.3-0.4%; 0.18-0.25% of 2, 6-nonadienol; 0.1-0.3% of passion flower thioether; 0.1-0.3% of yerba mate leaf oil; 0.1-0.14% of motor gas ylang-ylang oil; 0.1-0.2% of bitter orange leaf oil; 0.13 to 0.33 percent of perfume fixing agent; 33.81 to 39.58 percent of a fragrance composition; 7.84 to 9.11 percent of modifier; the balance being solvent. The application has the effect of better covering the pungent odor of ammonia in the hair dye.

Description

Daily chemical essence for hair dye and preparation method thereof
Technical Field
The application relates to the field of daily chemical essence, in particular to daily chemical essence for hair dye and a preparation method thereof.
Background
In recent years, hair dyeing has become a fashion choice for people. In a survey of the condition of dyeing hair in modern residents, it was found that more than 90% of people had dyed hair and that about half of people had started dyeing hair by the age of 30 years. Undoubtedly, hair dyes have been incorporated into people's lives and become an integral part.
The hair dye generally contains ammonia and other components, and the ammonia has the functions of expanding and softening the hair cuticle so as to facilitate the permeation and absorption of the main agent mercapto compound, but because the ammonia content in the hair dye is high, the hair dye has a pungent peculiar smell, so that daily chemical essence is required to be added to cover the peculiar smell, a certain fragrance is given to the hair dye, and the irritation of the ammonia to people in the hair dyeing process is reduced.
However, when the existing daily chemical essence is applied to a hair dye product, the odor of ammonia in the hair dye cannot be well covered by the aroma of the daily chemical essence, so that the comfort of people in the hair dyeing process is affected. Thus, there is still room for improvement.
Disclosure of Invention
In order to better cover the pungent peculiar smell of ammonia in the hair dye, the application provides daily chemical essence for the hair dye and a preparation method thereof.
In a first aspect, the application provides a daily chemical essence for hair dye, which adopts the following technical scheme:
a daily chemical essence for hair dye comprises the following components in percentage by mass:
0.3-0.4% of white orchid leaf oil;
cis-6-nonenol 0.3-0.4%;
0.18-0.25% of 2, 6-nonadienol;
0.1-0.3% of passion flower thioether;
0.1-0.3% of yerba mate leaf oil;
0.1-0.14% of motor gas ylang-ylang oil;
0.1-0.2% of bitter orange leaf oil;
0.13 to 0.33 percent of perfume fixing agent;
33.81 to 39.58 percent of a fragrance composition;
7.84 to 9.11 percent of modifier;
the balance being solvent.
By adopting the technical scheme, the white orchid leaf oil has linalool fragrance, is more elegant than linalool, slightly has white orchid fragrance, and is transparent without long lasting fragrance; cis-6-nonenol has melon fragrance and faint scent; 2, 6-nonadienol has green fragrance, wax fragrance, cucumber fragrance, watermelon fragrance and vegetable fragrance; the passion flower thioether is accompanied with fruit fragrance and grape-like acid fragrance of tropical green passion flower fruits, so that the fragrance of the daily chemical essence can cover the peculiar smell of ammonia through the mutual matching of the brandy leaf oil, cis-6-nonenol, 2, 6-nonenol and passion flower thioether; meanwhile, because the Paraguay orange leaf oil has orange fragrance and flower fragrance, the fragrance of the daily chemical essence is more prominent, and the pungent peculiar smell of ammonia is better covered, so that the influence of the ammonia on people is reduced. In addition, the motor gas ylang oil contains acid components such as valeric acid, benzoic acid, salicylic acid and the like, so that the acid-base reaction between the motor gas ylang oil and ammonia is increased, the odor of the ammonia and the acid components react and then are enclosed in new molecules, the ammonia content is further obviously reduced, the stimulation of the ammonia to people in the hair dyeing process is reduced, and the experience of people is improved. The bitter orange leaf oil is fragrant in green and fragrant, is sweet, has coarse orange flower fragrance, is stronger than the yerba mate leaf oil, is similar to the bitter orange leaf oil, has slightly less green fragrance, has strong fragrance, is strongly transparent, is matched with the yerba mate leaf oil and the motor gas ylang oil, and is matched with the brandy leaf oil, cis-6-nonenol, 2, 6-nonenol and passion flower thioether, so that the daily chemical essence can stay fragrance for a long time, and the fragrance stay time of the daily chemical essence in the hair dye is prolonged. Therefore, the brandy leaf oil, the cis-6-nonenol, the 2, 6-nonenol, the passion flower thioether, the yerba mate leaf oil, the motor gas oil and the hawksbill leaf oil are adopted as the main perfume, which is beneficial to better covering up the pungent peculiar smell of ammonia, reducing the ammonia content, reducing the stimulation of ammonia to people, relieving the human nerves and leading people to feel relaxed.
Preferably, the mass ratio of the yerba mate leaf oil to the motor gas ylang-ylang oil to the hawk-orange leaf oil is 1.5 (1-1.2): 1.
through adopting above-mentioned technical scheme, adopt the paraguay orange leaf oil of specific proportion, motor gas ganlan oil and hawk orange leaf oil to cooperate each other, be favorable to further reducing the ammonia content, reduce ammonia to people's stimulation for people possess better comfort and light in the hair-dyeing process.
Preferably, the perfume fixing agent comprises the following components in percentage by mass:
0.01-0.03% of geranium oil;
0.12-0.3% of undecalactone at the propylene position.
By adopting the technical scheme, the propinqualide has strong peach fragrance, and the fragrance of the main flavoring agent is stronger by the mutual matching of the propinqualide and the geranium oil, so that the pungent peculiar smell of ammonia is better covered; in addition, the content of ammonia is also beneficial to reducing, because the geranium oil contains aldehydes such as neral, geranial and the like, the oxidation-reduction reaction between the geranium oil and ammonia is enhanced, the content of ammonia is further reduced, and the propionoundecalactone is beneficial to promoting the oxidation-reduction reaction between the aldehydes in the geranium oil and the ammonia, and the content of ammonia is further reduced, so that the stimulation of ammonia to people is reduced.
Preferably, the aromatic compound comprises one or more of benzyl acetate, phenethyl alcohol, chamomile, ethyl 2-methylbutyrate, allyl cyclohexylpropionate and methyl heptenone.
By adopting the technical scheme, the fragrance of the main fragrance agent is stronger and more outstanding by adopting one or more fragrance combining agents in the substances, so that the method is favorable for better covering the pungent peculiar smell of ammonia, reduces the influence of ammonia on people, and ensures that people have better and comfortable experience in the hair dyeing process.
Preferably, the aromatic compound comprises the following components in percentage by mass:
benzyl acetate 8.6-10.2%;
phenyl ethyl alcohol 8.9-9.8%;
6.1 to 7.5 percent of chamomile;
3.9-4.8% of ethyl 2-methylbutyrate;
6.3 to 7.2 percent of cyclohexyl allyl propionate;
0.01-0.08% of methyl heptenone.
By adopting the technical scheme, benzyl acetate, phenethyl alcohol, chamomile, ethyl 2-methylbutyrate, allyl cyclohexyl propionate and methyl heptenone are mutually matched, so that the fragrance of the main fragrance agent is further enhanced; in addition, the components in the daily chemical essence are not easy to oxidize, so that the stability of the daily chemical essence in the hair dye is improved, the fragrance of the daily chemical essence can be kept lasting after being folded, and the influence of ammonia on people is reduced.
Preferably, the modifier comprises one or more of linalool, elemene, phyllitol and methyl decenol.
By adopting the technical scheme, the fragrance of the daily chemical essence is softer and more refreshing by adopting one or more modifier in the substances, and the daily chemical essence has better blending effect, so that the pungent peculiar smell of ammonia is better covered, thereby reducing the influence of the ammonia on people.
Preferably, the modifier comprises the following components in percentage by mass:
7.6-8.5% of linalool;
0.1-0.15% of elemene;
0.01-0.03% of leaf alcohol;
0.13 to 0.16 percent of methyl decenol.
Through adopting above-mentioned technical scheme, adopt linalool, elemene, leaf alcohol, methyl decyl enol to cooperate mutually, not only be favorable to reducing daily chemical essence to the stimulation of skin, still make daily chemical essence's fragrance softer and comfortable, be difficult to appear because too sharp and make people intolerable, be favorable to releiving people's mood for people's experience in the hair dyeing process improves.
Preferably, the solvent is dipropylene glycol.
Through adopting above-mentioned technical scheme, because dipropylene glycol has fine moisture, oil content and hydrocarbon co-solubility ability, consequently adopt dipropylene glycol as the solvent of daily use chemical essence, be favorable to improving the solubility between each component of daily use chemical essence for daily use chemical essence improves in the hair dye, so the time of remaining fragrance of daily use chemical essence is prolonged, thereby make the pungent peculiar smell of ammonia can be better covered, be favorable to reducing the influence of ammonia to people, make people possess more comfortable and fine experience.
In a second aspect, the application provides a preparation method of daily chemical essence for hair dye, which adopts the following technical scheme:
a preparation method of daily chemical essence for hair dye comprises the following steps:
adding the brandy leaf oil, the cis-6-nonenol, the 2, 6-nonenol, the passion flower thioether, the yerba mate leaf oil, the motor gas-ganlan oil, the hawksbill orange leaf oil, the fragrance fixative, the modifier, the fragrance blending agent and the solvent into a stirring kettle according to the formula, and uniformly mixing at normal temperature to obtain the daily use chemical essence for the hair dye.
Through adopting above-mentioned technical scheme, the daily chemical essence for hair dye that adopts the preparation of above-mentioned method not only easy operation, still be favorable to improving daily chemical essence's stability in the hair dye, and then make daily chemical essence cover the pungent peculiar smell of ammonia better, reduce the influence of ammonia to people to make people possess the experience of preferred in the hair dyeing process.
In summary, the present application includes at least one of the following beneficial technical effects:
1. by adopting the brandy leaf oil, the cis-6-nonenol, the 2, 6-nonenol, the passion flower thioether, the yerba mate leaf oil, the motor gas oil and the hawk orange leaf oil as the main perfume, the method is beneficial to better covering up the pungent peculiar smell of ammonia, reducing the ammonia content, reducing the stimulation of ammonia to people, relieving the human nerves and leading people to feel relaxed.
2. By adopting the mutual matching of the propinundecalactone and the geranium oil, the fragrance of the main perfume is stronger, and the pungent peculiar smell of ammonia is better covered; in addition, the content of ammonia is also beneficial to reducing, because the geranium oil contains aldehydes such as neral, geranial and the like, the oxidation-reduction reaction between the geranium oil and ammonia is enhanced, the content of ammonia is further reduced, and the propionoundecalactone is beneficial to promoting the oxidation-reduction reaction between the aldehydes in the geranium oil and the ammonia, and the content of ammonia is further reduced, so that the stimulation of ammonia to people is reduced.
3. The benzyl acetate, the phenethyl alcohol, the matrimony vine, the ethyl 2-methylbutyrate, the cyclohexyl allyl propionate and the methyl heptenone are matched with each other, so that the fragrance of the main fragrance agent is further enhanced; in addition, the components in the daily chemical essence are not easy to oxidize, so that the stability of the daily chemical essence in the hair dye is improved, the fragrance of the daily chemical essence can be kept lasting after being folded, and the influence of ammonia on people is reduced.
Detailed Description
The present application will be described in further detail with reference to examples.
Example 1
The embodiment discloses a daily chemical essence for hair dye, which comprises the following components:
white orchid leaf oil; cis-6-nonenol; 2, 6-nonylene alcohol; passion flower thioether; yerba mate leaf oil; motor gas ylang-ylang oil; bitter orange leaf oil; a fragrance fixative; a fragrance composition; a modifier; a solvent;
wherein the aroma fixing agent is geranium oil, the aroma synthesizing agent is benzyl acetate and phenethyl alcohol, the modifier is linalool and elemene, and the solvent is dipropylene glycol.
The embodiment also discloses a preparation method of the daily chemical essence for the hair dye, which comprises the following steps:
adding the white orchid leaf oil, cis-6-nonenol, 2, 6-nonenol, passion flower thioether, yerba mate leaf oil, motor gas ylang oil, hawksbill orange leaf oil, perfume fixing agent, perfume mixing agent, modifier and solvent into a stirring kettle according to a formula (specific dosage is shown in table 1), mixing at normal temperature, stirring uniformly at the rotating speed of 80r/min, and standing at the room temperature for 24 hours to obtain the daily chemical essence for the hair dye.
Examples 2 to 3
The difference from example 1 is that: the amounts of the components are different.
The amounts of the components in examples 1 to 3 are shown in Table 1, and the unit of the amounts is kg.
TABLE 1
Example 4
The difference from example 3 is that: the mass ratio of the yerba mate leaf oil to the motor gas ylang-ylang oil to the hawk orange leaf oil is 1.5:1:1, the perfume fixative also comprises propinundecalactone, and the amounts of the components are shown in table 2.
Example 5
The difference from example 3 is that: the mass ratio of the yerba mate leaf oil to the motor gas ylang-ylang oil to the hawk orange leaf oil is 1.5:1.4:1, the perfume fixative also comprises propinundecalactone, and the amounts of the components are shown in table 2.
Examples 6 to 7
The difference from example 5 is that: the flavoring agent also comprises chamomile, ethyl 2-methylbutyrate, allyl cyclohexylpropionate and methyl heptenone, and the modifier also comprises phyllitol and methyl decenol, wherein the dosage of each component is shown in Table 2.
TABLE 2
Comparative example 1
The difference from example 3 is that: the yerba mate leaf oil was replaced with an equal amount of dipropylene glycol.
Comparative example 2
The difference from example 3 is that: the equivalent dipropylene glycol is used for replacing the bitter orange leaf oil.
Comparative example 3
The difference from example 3 is that: equal amounts of dipropylene glycol were used instead of motor gas ylang oil.
Comparative example 4
The difference from example 3 is that: equivalent dipropylene glycol is used for replacing yerba mate leaf oil, hawksbill orange leaf oil and motor gas ylang-ylang oil.
Comparative example 5
The difference from example 3 is that: equal amounts of dipropylene glycol were used instead of 2, 6-nonylene alcohol.
Comparative example 6
The difference from example 3 is that:
a daily chemical essence for hair dye comprises the following components in mass:
0.1kg of brandy leaf oil; 0.2kg of cis-6-nonenol; 0.12kg of 2, 6-nonadienol; 0.08kg of passion flower thioether; 0.05kg of yerba mate leaf oil; 0.06kg of bitter orange leaf oil; 0.07kg of motor gas ylang-ylang oil; 0.1kg of perfume fixing agent; 30.42kg of a fragrance composition; 7.66kg of modifier; 61.14kg of solvent.
Comparative example 7
The difference from example 3 is that:
a daily chemical essence for hair dye comprises the following components in mass:
0.8kg of brandy leaf oil; 0.9kg of cis-6-nonenol; 0.5kg of 2, 6-nonadienol; 0.6kg of passion flower thioether; 0.5kg of yerba mate leaf oil; 0.4kg of bitter orange leaf oil; 0.3kg of motor gas ylang-ylang oil; 0.4kg of perfume fixing agent; 42.15kg of a fragrance composition; 10.79kg of modifier; 42.66kg of solvent.
Experiment 1
The experiment refers to QB/T2761-2006 "effect of indoor air purification product", and the ammonia removal rate (%) of the daily chemical essence prepared in the above examples and comparative examples is detected respectively, and the action time is 24 hours. The experimental results are shown in Table 3.
Experiment 2 allergy test experiment
The skin-sensitive 70 volunteers are selected, the average of the skin-sensitive 70 volunteers is divided into 14 groups, each group of 5 people, daily chemical essence of the corresponding example and the comparative example is equally sprayed on three places at the inner side of the wrist, the neck and the back of the ear, after spraying, the allergic conditions at the inner side of the wrist, the neck and the back of the ear of each group of subjects are observed and recorded within 30 minutes, and the experimental results are shown in table 3.
TABLE 3 Table 3
According to the comparison of the data of comparative examples 1-5 in Table 3 with the data of example 3, the addition of Paraguay orange leaf oil, motor Gaussian ylang oil and hawk-orange leaf oil in example 3 is performed at the same time, the ammonia removal rate is obviously improved, and the description that Paraguay orange leaf oil, motor Gaussian ylang oil and hawk-orange leaf oil are simultaneously performed with the white-blue leaf oil, cis-6-nonenol, 2, 6-nonenol and passion flower thioether are performed at the same time, so that the ammonia content is reduced, the stimulation of ammonia to people is reduced, the human nerves are relaxed, and the human feel relaxed is facilitated.
According to the comparison of the data of the comparative examples 6-7 with the data of the example 3, the amounts of the components of the daily use essence in the comparative examples 6-7 are not within the protection range of the application, and the ammonia removal rate in the comparative examples 6-7 is not as good as that in the example 3, which means that the amounts of the components of the daily use essence are only within the protection range of the application, so that the ammonia removal rate is greatly improved, the influence of the ammonia on people is reduced, and people have more comfortable experience in the hair dyeing process.
The data according to examples 4-5 are respectively compared with the data of example 3, the mass ratio of yerba mate leaf oil, motor gas ylang-ylang oil and bitter orange leaf oil is defined in examples 4-5, and the perfume fixative comprises geranium oil and propiolactone, compared with example 3, the removal rate of ammonia of the daily essence in examples 4-5 is improved to a certain extent, which means that the yerba mate leaf oil, motor gas ylang-ylang oil and bitter orange leaf oil are mutually matched in a specific ratio, and the perfume fixative consists of geranium oil and propiolactone in a specific ratio, which is beneficial to improving the removal rate of ammonia, reducing the influence of ammonia on people, and is beneficial to relieving human nerves and allowing people to feel relaxed.
Application example 1
A hair dye comprises the following components in mass:
6kg of cetostearyl alcohol; carbomer 1kg; 0.5kg of glycerol stearate; cetostearyl alcohol polyether-25 kg; resorcinol 0.3kg; 3kg of ascorbic acid; 0.2kg of ethanolamine; 1kg of 20% ammonia water; 0.3kg of daily chemical essence and 15kg of lonicera caerulea fruit extract; 5kg of polygonum multiflorum root extract; 0.2kg of disodium ethylenediamine tetraacetate; 1kg of water-soluble lanolin; 64.5kg of deionized water.
The daily chemical essence prepared in the example 1 is adopted.
The preparation method of the hair dye comprises the following steps:
6kg of cetostearyl alcohol, 1kg of carbomer, 0.5kg of glyceryl stearate, 25 kg of cetostearyl ether, 0.3kg of resorcinol, 3kg of ascorbic acid, 0.2kg of ethanolamine, 1kg of 20% ammonia water, 0.3kg of daily chemical essence, 15kg of lonicera caerulea extract, 5kg of polygonum multiflorum root extract, 0.2kg of disodium ethylenediamine tetraacetate, 1kg of water-soluble lanolin and 64.5kg of deionized water are respectively added into a stirring kettle, the stirring speed is 100r/min, and the hair dye is obtained after uniform mixing.
Application example 2
The difference from application example 1 is that: the daily chemical essence prepared in the example 2 is adopted.
Application example 3
The difference from application example 1 is that: the daily chemical essence prepared in the example 3 is adopted.
Application example 4
The difference from application example 3 is that: the daily chemical essence prepared in example 4 is adopted.
Application example 5
The difference from application example 3 is that: the daily chemical essence prepared in example 5 is adopted.
Application example 6
The difference from application example 5 is that: the daily chemical essence prepared in example 6 is adopted.
Application example 7
The difference from application example 5 is that: the daily chemical essence prepared in example 7 is adopted.
Comparative application example 1
The difference from application example 3 is that: the daily chemical essence prepared in comparative example 1 is adopted.
Comparative application example 2
The difference from application example 3 is that: the daily chemical essence prepared in comparative example 2 is adopted.
Comparative application example 3
The difference from application example 3 is that: the daily chemical essence prepared in the comparative example 3 is adopted.
Comparative application example 4
The difference from application example 3 is that: the daily chemical essence prepared in comparative example 4 is adopted.
Comparative application example 5
The difference from application example 3 is that: the daily chemical essence prepared in comparative example 5 is adopted.
Comparative application example 6
The difference from application example 3 is that: the daily chemical essence prepared in comparative example 6 is adopted.
Comparative application example 7
The difference from application example 3 is that: the daily chemical essence prepared in comparative example 7 is adopted.
Experiment 3 fragrance stability test
The stability of the fragrance added into the hair dye by the daily chemical essence is detected by the experiment, the stability of the fragrance is evaluated by referring to GB/T14454.2-2008 perfume fragrance evaluation method, fragrance retention detection is carried out by adopting a sensory test method, and an evaluator is a member of a skilled sensory evaluation group.
The testing method comprises the following steps: 70 evaluators are selected and divided into 14 groups, 5 evaluators are used for carrying out sensory recording on the fragrance intensity of the hair dye containing the daily chemical essence prepared in each application example and comparative application example, and the result is obtained as an average value. And then, grading the intensity of the fragrance again after the hair dye is placed in the room for 1 month, taking the average value of the intensity of the fragrance, and finally calculating the reduction rate (%) of the fragrance grading before and after the hair dye is placed.
The rate of decrease = (1-fragrance score after placement/fragrance score before placement) ×100% and the experimental results are shown in table 4.
Fragrance scoring criteria (10 full score): none (0 points), very weak (1-4 points); moderate (5-9), extremely strong (10 minutes).
TABLE 4 Table 4
According to the comparison of the data of comparative application examples 1-5 in Table 4 with the data of application example 3, the data of application example 3 are obtained by respectively adding the white orchid leaf oil, cis-6-nonenol, 2, 6-nonenol, passion flower thioether, yerba mate orange leaf oil, motor gas yland oil and hawksbill leaf oil into each other, the reduction rate is reduced from about 80% to 35.16%, which indicates that the white orchid leaf oil, cis-6-nonenol, 2, 6-nonenol, passion flower thioether, yerba mate orange leaf oil, motor gas yland oil and hawksbill leaf oil are mutually matched, so that the stability of daily chemical essence in hair dye is improved, the daily chemical essence can stay fragrance for a long time, the pungent peculiar smell of ammonia is better covered, and people can experience better in the hair dyeing process.
According to the comparison of the data of the comparative application examples 6-7 with the data of the application example 3, the dosages of the components of the daily use essence in the comparative application examples 6-7 are not in the scope of the protection of the application, and the reduction rate of the fragrance intensity of the comparative application examples 6-7 is higher than that of the application example 3, which indicates that the proportion of the components of the daily use essence can influence the stability of the daily use essence in the hair dye. Therefore, the effect of improving the fragrance stability of the daily chemical essence can be achieved only by adopting the protective range of the application, and the effect of the application can not be achieved in any range.
According to the data of application examples 6-7, the data of application example 5 are respectively compared with the data of application example 5, the synthetic flavoring agent of application examples 6-7 is compounded by benzyl acetate, phenethyl alcohol, matrine, 2-methyl ethyl butyrate, cyclohexyl allyl propionate and methyl heptenone, the modifier is compounded by linalool, elemene, leaf alcohol and methyl decenol, the reduction rate is reduced from 35.48% to about 25%, the description that the synthetic flavoring agent is compounded by benzyl acetate, phenethyl alcohol, matrine, 2-methyl ethyl butyrate, cyclohexyl allyl propionate and methyl heptenone, the modifier is compounded by linalool, elemene, leaf alcohol and methyl decenol, the stability of daily chemical essence in the hair dye is improved, the fragrance retention time of daily chemical essence is improved, the irritation peculiar smell of ammonia is better covered, and the influence of ammonia on people is reduced.
The above embodiments are not intended to limit the scope of the present application, so: all equivalent changes in structure, shape and principle of the application should be covered in the scope of protection of the application.

Claims (2)

1. A daily chemical essence for hair dye is characterized in that: the composite material consists of the following components in percentage by mass:
0.3-0.4% of white orchid leaf oil;
cis-6-nonenol 0.3-0.4%;
0.18-0.25% of 2, 6-nonadienol;
0.1-0.3% of passion flower thioether;
0.1-0.3% of yerba mate leaf oil;
0.1-0.14% of motor gas ylang-ylang oil;
0.1-0.2% of bitter orange leaf oil;
0.13 to 0.33 percent of perfume fixing agent;
33.81 to 39.58 percent of a fragrance composition;
7.84 to 9.11 percent of modifier;
the balance of solvent, wherein the solvent is dipropylene glycol;
the mass ratio of the yerba mate leaf oil to the motor gas ganlan oil to the hawk orange leaf oil is 1.5 (1-1.2): 1, a step of;
the perfume fixing agent comprises the following components in percentage by mass:
0.01-0.03% of geranium oil;
0.12-0.3% of propinquity undecalactone;
the aromatic compound agent comprises the following components in percentage by mass:
benzyl acetate 8.6-10.2%;
phenyl ethyl alcohol 8.9-9.8%;
6.1 to 7.5 percent of chamomile;
3.9-4.8% of ethyl 2-methylbutyrate;
6.3 to 7.2 percent of cyclohexyl allyl propionate;
0.01-0.08% of methyl heptenone;
the modifier consists of the following components in percentage by mass:
7.6-8.5% of linalool;
0.1-0.15% of elemene;
0.01-0.03% of leaf alcohol;
0.13 to 0.16 percent of methyl decenol.
2. The method for preparing the daily chemical essence for the hair dye according to claim 1, wherein the method comprises the following steps: the method comprises the following steps:
adding the brandy leaf oil, the cis-6-nonenol, the 2, 6-nonenol, the passion flower thioether, the yerba mate leaf oil, the motor gas-ganlan oil, the hawksbill orange leaf oil, the fragrance fixative, the modifier, the fragrance blending agent and the solvent into a stirring kettle according to the formula, and uniformly mixing at normal temperature to obtain the daily use chemical essence for the hair dye.
CN202211146571.7A 2022-09-20 2022-09-20 Daily chemical essence for hair dye and preparation method thereof Active CN115386425B (en)

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Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101115493A (en) * 2005-08-12 2008-01-30 河乃建仁 Agent for hair growth
CN101193950A (en) * 2005-06-09 2008-06-04 赢创德固赛有限责任公司 Fragrance alcohol-releasing polysiloxane
CN103013659A (en) * 2011-09-21 2013-04-03 张兆雷 Essence
CN106281689A (en) * 2016-09-05 2017-01-04 上海应用技术大学 A kind of Flos Gardeniae essence and preparation method thereof
CN112210438A (en) * 2020-10-19 2021-01-12 广东芬豪生物科技有限公司 Daily chemical essence with flower fragrance and preparation method thereof
CN112745984A (en) * 2020-12-15 2021-05-04 广州芬豪香精有限公司 Lasting fragrance type essence
CN112760168A (en) * 2020-12-15 2021-05-07 广州芬豪香精有限公司 Citrus flavor and preparation method and application thereof
CN113150864A (en) * 2021-03-02 2021-07-23 广州芬豪香精有限公司 Natural and fresh flower and fruit flavor essence and preparation method and application thereof

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101193950A (en) * 2005-06-09 2008-06-04 赢创德固赛有限责任公司 Fragrance alcohol-releasing polysiloxane
CN101115493A (en) * 2005-08-12 2008-01-30 河乃建仁 Agent for hair growth
CN103013659A (en) * 2011-09-21 2013-04-03 张兆雷 Essence
CN106281689A (en) * 2016-09-05 2017-01-04 上海应用技术大学 A kind of Flos Gardeniae essence and preparation method thereof
CN112210438A (en) * 2020-10-19 2021-01-12 广东芬豪生物科技有限公司 Daily chemical essence with flower fragrance and preparation method thereof
CN112745984A (en) * 2020-12-15 2021-05-04 广州芬豪香精有限公司 Lasting fragrance type essence
CN112760168A (en) * 2020-12-15 2021-05-07 广州芬豪香精有限公司 Citrus flavor and preparation method and application thereof
CN113150864A (en) * 2021-03-02 2021-07-23 广州芬豪香精有限公司 Natural and fresh flower and fruit flavor essence and preparation method and application thereof

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